CN109679788A - The preparation method and applications of tea seed cake detergent - Google Patents
The preparation method and applications of tea seed cake detergent Download PDFInfo
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- CN109679788A CN109679788A CN201910092485.4A CN201910092485A CN109679788A CN 109679788 A CN109679788 A CN 109679788A CN 201910092485 A CN201910092485 A CN 201910092485A CN 109679788 A CN109679788 A CN 109679788A
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- tea seed
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
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- Epidemiology (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
A kind of preparation method and applications of tea seed cake detergent, the following steps are included: milling step, decoct step, decolorization and purification step, filter extraction step and detergent preparation steps, tea seed cake is crushed, tea seed cake powder is made, 20 to 40 mesh of smashing fineness, moisture content is retained in 10% to 20%, wild crow Chinese toon seed with the tea seed cake equivalent weight is fried into rear grinds, it mixes the tea seed cake powder and the open country crow Chinese toon seed meal is tea seed cake open country crow Chinese toon seed meal, the water of 100 times of parts by weight is added in the tea seed cake open country crow Chinese toon seed meal, it is boiled between 150 to 160 DEG C of temperature 3 to 5 hours, tea seed meal liquid is cooled to after the completion of decocting, the tea seed meal liquid is decolourized and purified using active carbon, by tea seed cake liquid precipitate 3 hours after decolorization and purification, coarse filtration is primary, then reprecipitation 3 hours, fine filtering is primary, discard filter residue, Tea seed meal liquid after filtering is extracted is diluted with water and prepares the detergent that tea seed cake liquid hold-up is 1% to 10%.
Description
Technical field
The invention belongs to field of daily chemicals, relates in particular to a kind of preparation method of tea seed cake detergent and its answer
With.
Background technique
Detergents and cosmetic detergent is becoming the daily necessities that today's society people be unable to do without step by step.Either in public affairs
Place, deluxe hotel altogether, or in each family, public refreshment stand, we it can be seen that chemical detergent trace.Daily
News media such as broadcast, TV, on newpapers and periodicals also in the advertisement for doing chemical detergent in large quantities.It is colorfully packaged at these
In the use process of colourful chemical detergent, people are unawares increasingly dependent on it.At the same time, chemical contamination
Harm is carried out to the health of the mankind through various channels.People are widely using chemical detergent wash my hair, chopsticks of washing the dishes, are washing
While clothes, bathing, chemical toxicant is easy for penetrating into from the pore of human body, and chemical contamination is penetrated into from mouth, penetrates into from skin,
It accumulates over a long period, hides and assemble.Since the harm of this pollution in a short time can not be often ignored it is obvious that therefore.
But micropollution continues into vivo, serious consequence can be caused by taking care of the pence, and lead to the various lesions of human body.
Tea seed cake is also tea seed cake, and it is a blob of slag of the tea seed after extracting oil, effective component is saponin that particle, which is in puce,
Element and a kind of important source material of plant source ecology articles for washing, can be used for the important source material of various detergent, it can also be used to change
Work, machine derusting etc., the saponin in tea seed cake is known as poison, cannot act as consumable products, but may be used as hair washing bathing soap and wash
Wash the raw material of the life articless for washing such as powder.And tea seed meal liquid hair washing, which is used for a long time, is beneficial to hair and scalp health is effectively prevented
Hair has the function such as hair washing, hair care, black hair and anti-dandruff, Anti-hair loss, but cannot function as medical supplies.In addition, by refinement
Also there are the nutriments such as crude protein abundant and a variety of amino acid in tea seed meal liquid, have very well to scalp, hair, skin
Maintenance effect: the smooth Anti-hair loss of black hair brighten the hair, can also anti-dandruff and itching-relieving.Because tea seed cake is rich in natural tea saponin powder, can remove rapidly
Greasy dirt, bowls and chopsticks capable of washing, plate, bowl, veterinary antibiotics ... etc., deoil, dirt-removing power it is very strong, good punching is washed well again, is not hurt
Hand does not hurt top grade tableware cup very, can decompose the remaining pesticide in vegetables and fruits.
Wild crow Chinese toon is Staphyleaceae defoliation small arbor or shrub, is a kind of ornamental plant of great Exploitative potential, wild crow Chinese toon
For seed oil content in 25%-38%, seed oil can soapmaking.
Chinese patent CN104263541A discloses a kind of tea seed cake powder detergent and preparation method thereof, Chinese patent
CN104146900A discloses a kind of natural washing lotion of tea seed cake, Chinese patent CN107468599A disclose a kind of tea seed cake hand cleanser and
Preparation method.In the preparation of these existing tea seed cake detergent, it is required to be equipped with other a large amount of Chinese herbs, such as reed
Luxuriant growth extract liquor, cactus extract liquor etc. are unfavorable for general production and some equipment first because the material described in it is more
Factory even middle-size and small-size workshop development and progress.Still not mainly using tea seed cake and wild crow Chinese toon seed having for raw material preparation
The tea seed cake special purpose detergent of effect.
Summary of the invention
To solve the above-mentioned problems, the present invention provides a kind of preparation method of tea seed cake detergent, and its technical solution is as follows:
A kind of preparation method of tea seed cake detergent comprising following steps:
Milling step: tea seed cake being crushed, tea seed cake powder, 20 to 40 mesh of smashing fineness be made, and moisture content is retained in 10% to 20%,
Wild crow Chinese toon seed with the tea seed cake equivalent weight is fried into rear grinds, the tea seed cake powder is mixed and the open country crow Chinese toon seed meal is tea
Dregs of rice open country crow Chinese toon seed meal；
It decocts step: the water of 100 times of parts by weight being added in the tea seed cake open country crow Chinese toon seed meal, in 150 to 160 DEG C of temperature
It is boiled between degree 2 to 5 hours, tea seed meal liquid is cooled to after the completion of decocting；
Decolorization and purification step: the tea seed meal liquid is decolourized and is purified using active carbon；
Filter extraction step: by tea seed cake liquid precipitate 3 hours after decolorization and purification, coarse filtration was primary, then reprecipitation 3 hours,
Fine filtering is primary；
Detergent preparation steps: the tea seed meal liquid after filtering is extracted is diluted with water and is configured to 1% to 10% weight ratio
Detergent.
Preferably, the detergent preparation steps further include steps of
The tea seed meal liquid temperature less than 90 DEG C and pH adjust in 3-6, be added 0.1%~0.5% parts by weight miaow
Oxazolidinyl urea.
Preferably, the detergent preparation steps further include steps of
0.5% parts by weight lauryl sodium sulfate is added in the tea seed meal liquid.
Preferably, the detergent preparation steps further include steps of
The guar gum of 0.5% parts by weight is added in the tea seed meal liquid.
Preferably, the detergent preparation steps further include steps of
The natural rose pollen end of 10% parts by weight is added in the tea seed meal liquid.
Preferably, the detergent preparation steps further include steps of
The natural Jasmine powder of 10% parts by weight is added in the tea seed meal liquid.
Another technical solution of the present invention is to provide a kind of shampoo or bath essence, is using preparation above-mentioned
Before the rose shampoo and/or bath essence and use that natural rose pollen end is prepared into is added in the tea seed meal liquid of method preparation
The Jasmine shampoo and/or bath essence that natural Jasmine powder is prepared into is added in the tea seed meal liquid for the preparation method preparation stated.
Advantageous effect of the invention:
The raw material that the present invention uses are single, are easy to obtain, easy to operation, convenient to tea seed cake and wild crow Chinese toon seed
Processing, turns waste into wealth.Using tea seed meal liquid as cleaning, skincare product, the health of people is not only protected, but also solve
The utilization again of tea seed cake after tea grower's oil squeezes, even small-sized workshop even tea grower oneself can also make, to also increase
The income of tea grower.
Specific embodiment
Cooperate presently preferred embodiments of the present invention below, the present invention is further explained reaches predetermined goal of the invention and taken
Technological means.
A kind of preparation method and applications of tea seed cake detergent, specifically includes the following steps:
Milling step: tea seed cake being crushed, tea seed cake powder, 20 to 40 mesh of smashing fineness be made, and moisture content is retained in 10% to 20%,
Wild crow Chinese toon seed with the tea seed cake equivalent weight is fried into rear grinds, the tea seed cake powder is mixed and the open country crow Chinese toon seed meal is tea
Dregs of rice open country crow Chinese toon seed meal；
It decocts step: the water of 100 times of parts by weight being added in the tea seed cake open country crow Chinese toon seed meal, in 150 to 160 DEG C of temperature
It is boiled between degree, 2 to 5 hours, tea seed meal liquid is cooled to after the completion of decocting；
Decolorization and purification step: the tea seed meal liquid is decolourized and is purified using active carbon；
Filter extraction step: by tea seed cake liquid precipitate 3 hours after decolorization and purification, coarse filtration was primary, then reprecipitation 3 hours,
Fine filtering is primary；
Detergent preparation steps: the tea seed meal liquid after filtering is extracted is diluted with water and is configured to 1% to 10% weight ratio
Detergent.
Preferably, the rose that natural rose pollen end is prepared into is added in the tea seed meal liquid prepared using preparation method above-mentioned
Flower shampoo and/or bath essence, or Jasmine shampoo and/or bath essence that natural Jasmine powder is prepared into is added.
Embodiment one
1 kilogram of wild crow Chinese toon seed after using 1 kilogram of tea seed cake and frying obtains tea seed cake open country crow as raw material after being crushed
Chinese toon seed meal, smashing fineness 20-40 mesh, moisture content are retained in 10-20%.Then 20 kilograms of aqueous fusion solution is added into liquid, high temperature
It decocts, decocts maximum boiling point between 150-160 DEG C, decocting time is 3 hours, after the completion of decoction, obtains 200 kilograms of tea seed cake
Liquid.By the decoction process, effectively toxicant can be got rid of.After the tea seed meal liquid is cooling, mentioned with active carbon decoloring
Pure, such active carbon can fall toxicant and the absorption of pigment composition.Active carbon decolorization and purification can be using the general of industry
Method.After active carbon decolorization and purification, tea seed meal liquid filtering is extracted 2 times, the slag recycling of filtering is used for bio-feritlizer.It is aforementioned
Filtering to extract include: for 2 times that coarse filtration will be primary, then fine filtering will be primary after reprecipitation 3 hours after extracting liquid precipitate 3 hours, remove
Part impurity.Finally plus water is configured to the detergent system example that content is 1-10%.
Embodiment two
Step 1: wild 1 kilogram of grinds of crow Chinese toon seed that tea seed cake is mass number and is fried with 1 kilogram, add 200 kilograms of water
With being boiled at a temperature of 150-160 2 hours.Cooled and filtered, which removes residue water is added to be prepared into 200 kilograms of concentrated liquid, separately deposits.
Step 2: conditioner imidazolidinyl urea is added in 200 kilograms of tea seed meal liquids, dosage is 0.1%~0.5%, enhancing
Its anti-corrosion effect, (90 DEG C of <) is added in camellia dregs of rice liquid cooling temperature range, checks that PH should be in 3-6, because in meta-alkalescence
Easily catch Pseudomonas aeruginosa.And then 0.5% lauryl sodium sulfate is added, effect is cleaning function, while can be increased
Add foam sense.
Step 3: 0.5% guar gum is added in tea seed meal liquid after the cooling period.Guar gum is macromolecule glue liquid solution, can be changed
The wet cardability and antistatic property of kind shampoo, can increase washing fluid viscosity, stable foam.Due in tea seed cake oil content >
5%, thus without adding lubricant, thus ensure that articles for washing made of the camellia dregs of rice is pure natural, it is nuisanceless.
Step 4: the smashed natural rose flower that 10% is added in the tea seed meal liquid modulated carries out flavouring as camellia
Rose shampoo, bath essence；10% smashed natural non-jasmine progress flavouring, which is added, to be become the non-jasmine shampoo of camellia, washes
Bath liquid.Certainly, the smashed flower of addition is not restricted to above-mentioned two kinds, is also possible to the other kinds of flowers with fragrance.
From the above embodiments as can be seen that the present invention with tea seed cake and wild crow Chinese toon seed for main raw material, operating procedure
It is simple and easy, specifically when production, it can according to need and carry out flexile adjustment, to meet the demand of different groups.
The above is only the preferred embodiment of the present invention, not does limitation in any form to the present invention, though
So the present invention is disclosed above with preferred embodiment, and however, it is not intended to limit the invention, any technology people for being familiar with this profession
Member, in the range of not departing from technical solution of the present invention, when the technology contents using the disclosure above make a little change or repair
Decorations are the equivalent embodiment of equivalent variations, but anything that does not depart from the technical scheme of the invention content, technology according to the present invention are real
Matter any simple modification, equivalent change and modification to the above embodiments, still fall within the range of technical solution of the present invention
It is interior.
Claims (8)
1. a kind of preparation method of tea seed cake detergent, which comprises the following steps:
Milling step: tea seed cake being crushed, tea seed cake powder be made, and 20 to 40 mesh of smashing fineness, moisture content is retained in 10% to 20%, will be with
The wild crow Chinese toon seed of the tea seed cake equivalent weight fries rear grinds, mixes the tea seed cake powder and the open country crow Chinese toon seed meal is that tea seed cake is wild
Crow Chinese toon seed meal；
Decoct step: in the tea seed cake open country crow Chinese toon seed meal be added 100 times of parts by weight water, 150 to 160 DEG C of temperature it
Between boil 2 to 5 hours, be cooled to tea seed meal liquid after the completion of decocting；
Decolorization and purification step: the tea seed meal liquid is decolourized and is purified using active carbon；
Filter extraction step: by tea seed cake liquid precipitate 3 hours after decolorization and purification, coarse filtration was primary, then reprecipitation 3 hours, fine filtering
Once, filter residue is discarded；
Detergent preparation steps: it is 1% to 10% that the tea seed meal liquid after filtering is extracted, which is diluted with water and prepares tea seed cake liquid hold-up,
Detergent.
2. the preparation method of tea seed cake detergent according to claim 1, which is characterized in that the detergent preparation steps
It further includes steps of
When the tea seed meal liquid temperature is less than 90 DEG C and pH is adjusted 3 to 6, the imidazolidine of 0.1% to 0.5% parts by weight is added
Base urea.
3. the preparation method of tea seed cake detergent according to claim 2, which is characterized in that the detergent preparation steps
It further includes steps of
The lauryl sodium sulfate of 0.5% parts by weight is added in the tea seed meal liquid.
4. the preparation method of tea seed cake detergent according to claim 2, which is characterized in that the detergent preparation steps
It further includes steps of
The guar gum of 0.5% parts by weight is added in the tea seed meal liquid.
5. the preparation method of tea seed cake detergent according to any one of claims 1 to 4, which is characterized in that described washes
Agent preparation steps are washed to further include steps of
The natural rose pollen end of 10% parts by weight is added in the tea seed meal liquid.
6. the preparation method of tea seed cake detergent according to any one of claims 1 to 4, which is characterized in that described washes
Agent preparation steps are washed to further include steps of
The natural Jasmine powder of 10% parts by weight is added in the tea seed meal liquid.
7. a kind of the rose shampoo and/or bath essence of preparation method preparation according to claim 5.
8. a kind of the Jasmine shampoo and/or bath essence of preparation method preparation according to claim 6.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910092485.4A CN109679788A (en) | 2019-01-30 | 2019-01-30 | The preparation method and applications of tea seed cake detergent |
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| CN201910092485.4A CN109679788A (en) | 2019-01-30 | 2019-01-30 | The preparation method and applications of tea seed cake detergent |
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| CN201910092485.4A Pending CN109679788A (en) | 2019-01-30 | 2019-01-30 | The preparation method and applications of tea seed cake detergent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112126533A (en) * | 2020-09-28 | 2020-12-25 | 湖南雪峰源山茶油科技有限公司 | Preparation method of tea seed cake cleaning agent |
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2019
- 2019-01-30 CN CN201910092485.4A patent/CN109679788A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1754883A (en) * | 2004-10-01 | 2006-04-05 | 南华大学 | Production process for extracting tea saponin from tea-oil tree cake by using water as dissoluent |
| CN101497642A (en) * | 2009-03-19 | 2009-08-05 | 韶关学院 | Method for directly extracting tea saponin from tea seeds |
| CN103666793A (en) * | 2013-09-27 | 2014-03-26 | 红河五里冲生态茶业有限公司 | Tea soap powder and use thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112126533A (en) * | 2020-09-28 | 2020-12-25 | 湖南雪峰源山茶油科技有限公司 | Preparation method of tea seed cake cleaning agent |
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Application publication date: 20190426 |