CN107737069A - Plant shampoo water without emulsifying agent and oil phase - Google Patents

Plant shampoo water without emulsifying agent and oil phase Download PDF

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Publication number
CN107737069A
CN107737069A CN201711139855.2A CN201711139855A CN107737069A CN 107737069 A CN107737069 A CN 107737069A CN 201711139855 A CN201711139855 A CN 201711139855A CN 107737069 A CN107737069 A CN 107737069A
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Prior art keywords
shampoo
weight
soapberry
surfactant
plant extracts
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Inventor
丁滨
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Hangzhou Zhimo Biotechnology Co.,Ltd.
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Yan Fazhan
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Priority to CN201711139855.2A priority Critical patent/CN107737069A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/13Coniferophyta (gymnosperms)
    • A61K36/14Cupressaceae (Cypress family), e.g. juniper or cypress
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/19Acanthaceae (Acanthus family)
    • A61K36/195Strobilanthes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/282Artemisia, e.g. wormwood or sagebrush
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/286Carthamus (distaff thistle)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/31Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
    • A61K36/315Isatis, e.g. Dyer's woad
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/45Ericaceae or Vacciniaceae (Heath or Blueberry family), e.g. blueberry, cranberry or bilberry
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/489Sophora, e.g. necklacepod or mamani
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/60Moraceae (Mulberry family), e.g. breadfruit or fig
    • A61K36/605Morus (mulberry)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/63Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
    • A61K36/634Forsythia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/63Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
    • A61K36/638Ligustrum, e.g. Chinese privet
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/70Polygonaceae (Buckwheat family), e.g. spineflower or dock
    • A61K36/704Polygonum, e.g. knotweed
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/85Verbenaceae (Verbena family)
    • A61K36/855Clerodendrum, e.g. glorybower
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/896Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8969Polygonatum (Solomon's seal)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

Abstract

The present invention relates to the plant shampoo water without emulsifying agent and oil phase.Specifically, the invention discloses by natural plants surfactant and plant extracts as main component, shampoo without emulsifying agent and oil phase, wherein reduce the use of synthetic surfactant and preservative, and white hair caused by with young person with greying hair, overstrain one's nerves or aging is alleviated, or suppress dandruff generation, alleviate the effect of scalp allergy and itch, it is adapted to wash shield daily.

Description

Plant shampoo water without emulsifying agent and oil phase
Technical field
The present invention relates to shampoo, more particularly, to the plant shampoo water without emulsifying agent and oil phase.
Background technology
Shampoo, also known as shampoo, shampoo, hair washing gel, major function is cleaning hair and scalp, that is, dispels hair With the dust and secretion on scalp, also there are the functions such as some Ju You treatment oil, dyeing, hair cares.Common shampoo on the market Composition includes surfactant, emulsifying agent and oil compounds.Add the main function of oil compounds (such as silicone oil) It is to protect hair scale piece, plays moisturizing and the effect such as submissive, and in order to ensure that the stabilization of shampoo physical property needs to add Emulsifying agent.However, common shampoo generally has the following disadvantages on the market:1) emulsifying agent and oil compounds are usually It can be attached on scalp, block hair follicle, gently then cause alopecia, it is heavy then hair follicle inflammation may be caused;2) table of some industrial chemicals It is difficult to be degraded that face activating agent, emulsifying agent etc., which are discharged into environment, pollutes environment.
The content of the invention
It is an object of the invention to provide emulsifying agent and oil phase is not contained, using natural plants surfactant, and with the addition of The shampoo of plant extracts.The shampoo of the present invention can alleviate alopecia.In addition, according to selected plant extracts not White hair caused by with that can also have improvement young person with greying hair, overstrain one's nerves and aging or the effect for reducing dandruff.
The invention provides a kind of shampoo consisted of the following composition:
(1) the natural plants surfactant of 50-80 parts is accounted for by weight;
(2) conventional (both sexes) surfactant of 0-6 parts is accounted for by weight;
(3) plant extracts of 1-20 parts by weight;
(4) coagulator of 0.1-4 parts by weight;And
(5) preservative of 0.05-0.1 parts by weight.
Natural surfactant mixes by a certain percentage with amphoteric surfactant, with the dust on scalp and hair, oil Fat and secretion are combined, and are removed afterwards by washing, and play a part of cleaning scalp and hair.
Natural plants surfactant can extract from gleditsia sinensis, soapberry and/or camellia seed or plant phosphatide. Preferably, natural plants surfactant can account for 50-60 parts of shampoo by weight.
Preferably, natural plants surfactant is with mass volume ratio 1:Gleditsia sinensis, the soapberry distilled water of 10-30 preparations Extract.Wherein, the weight of gleditsia sinensis and soapberry ratio is 1:0.3-3.Especially, it is oiliness, mixing according to be applicable hair quality Property, neutrality or dryness, when preparing natural plants surfactant, the ratio of gleditsia sinensis and soapberry is from 0.3-0.5:1、1:1 To 1:0.3-0.5 changes.
Amphoteric surfactant is selected from betaines and amino acid surfactant, generally selects the beet of 30% concentration Bases and amino acid surfactant, and betaines can be mixed with amino acid surfactant with arbitrary proportion, The stabilization of product physical property can be ensured.Preferably, betaines and the ratio of amino acid surfactant are 1:0.5-3's In the range of.The conventional surfactant of amino acids can be only selected for special sensitive group.For example, amophoteric surface active Agent can be selected from Cocoamidopropyl betaine, lauroylamidopropyl betaine, sodium cocoyl glycinate, lauroyl glutamate Sodium and/or coco-nut oil fatty acid Sodium L-alaninate.
The shampoo that is obtained from above-mentioned natural and amphoteric surfactant is soft, does not stimulate, suitable for various hair qualitys, Alopecia can be significantly reduced, hair and scalp can reach preferable cleaning effect, be adapted to wash shield daily.
Plant extracts can be the distillation water extract of a Chinese medicine compound prescription, and conditioning head is played during hair washing Skin, the effect for protecting hair scale piece.Preferably, plant extracts can account for 1-3 parts of shampoo by weight.Plant extracts can To be the extract of following plant:Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, greatly Leafiness, balsamine, cacumen biotae, kuh-seng, green tea, oriental wormwood and the capsule of weeping forsythia.
For example, Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, phoenix Celestial flower, the extract of cacumen biotae have protection cell and oxidation resistant effect.In addition, kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, smalt Leaf, the extract of cacumen biotae are reduced the effect of dandruff.Those skilled in the art can also select other to have as needed The extract of the medicinal plant of black hair effect, for example, the Radix Astragali, Radix Angelicae Sinensis, the fruit of Chinese wolfberry, Semen sesami nigrum, Ligusticum wallichii, the fruit of Chinese magnoliavine and the red sage root.This Art personnel can also select the extract of other medicinal plants that there is anti-dandruff to act on as needed, for example, mulberry White skin, chrysanthemum leaf, lopseed, ramulus mori.
Plant extracts a can be that proportioning is 4-36 by weight:4-36:3-27:2-12:2-20:2-20:2-20:1- 5:1-5:1-5:1-5 Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, Balsamine, cacumen biotae mass volume ratio 1:5-15 distilled water extracts obtained extract.Can be by Eclipta prostrata, glossy privet Son, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae in mass ratio 36:36: 27:12:20:20:20:5:5:5:5 (height), 18:18:12:8:15:15:15:5:5:5:5 (in) and 4:4:3:2:2:2:2:1: 1:1:The formula mass volume ratio 1 of 1 (low):5-15 distilled water extraction obtains plant extracts a.
Preferably, plant extracts a can be that proportioning is 12 by weight:12:9:6:10:10:10:3:3:3:3 drought Lotus grass, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae matter Measure volume ratio 1:5-15 distilled water extracts obtained extract.This plant extract composition formula is rich in oxidation-resistant active ingredient It can alleviate white hair caused by young person with greying hair, overstrain one's nerves or aging with nutritional ingredient, long-term uses such as plant polyoses.Especially, Alleviated using shampoo made of this plant extracts a using more than one month white hair, had after three months in various degree Dark hair is newborn, white hair turns black at root of hair.Long-term use of white hair can gradually turn black, and hair amount is increased slightly.
Plant extracts b can be that proportioning is 10 by weight:10:10:3:3:It is 3 kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, big Leafiness, cacumen biotae mass volume ratio 1:5-15 70% ethanol extracts obtained extract.This plant extract composition formula In oriental wormwood, kuh-seng, green tea containing suppress bacterium, fungi propagation composition;And the extract of this formula is also with anti- Scorching, antipruritic bioactive ingredients, dandruff generation can be suppressed, alleviate scalp allergy and itch.Especially, using this plant Itching of the scalp improves immediately after shampoo made of extract b, and scalp allergy, which has, to be taken a turn for the better, bright using dandruff after a period of time It is aobvious to reduce.
Coagulator can use the coagulator that food service industry is commonly used, it is for instance possible to use food-grade agar, starch, water-soluble Property cellulose etc..The usage amount of coagulator can determine according to the physical behavior to be reached.Coagulator can be only from edible Starch, the time that food starch can keep the physical behavior of shampoo is longer, and more preferably, scalp feels more clear to cleaning effect Refreshing, hair is more soft.Coagulator can also select weight than 1:1 agar and starch or agar and water-soluble cellulose, so Coagulator shampoo can be made to be kept for sticky physical behavior long period.
Preservative selects food-grade sorbic acid or sodium benzoate.Because natural plant extracts, anti-corrosion are rich in shampoo The addition of agent is to prevent the pollution of microorganism.
Present invention also offers the preparation method of the shampoo comprising plant extracts a, methods described includes:
(1) preparation of natural plants surfactant, including by gleditsia sinensis and/or soapberry and distilled water with 1:10-30's Mass volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution, By gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges two Secondary extract solution;And
(2) plant extracts a preparation, 4-36 is compared with weight:4-36:3-27:2-12:2-20:2-20:2-20:1-5: 1-5:1-5:1-5 weigh Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, Balsamine and cacumen biotae;Add 70% ethanol, after immersion 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, by than Example adds 70% ethanol and repeats backflow extraction step, merges extract solution twice.
Preferably, with weight than 12:12:9:6:10:10:10:3:3:3:3 weigh Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, system Sealwort, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae prepared plant extracts a.
With weight than 36:36:27:12:20:20:20:5:5:5:5 (height), 18:18:12:8:15:15:15:5:5:5:5 (in) or 4:4:3:2:2:2:2:1:1:1:1 (low) weigh Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae prepared plant extracts a.
Present invention also offers the preparation method of the shampoo comprising plant extracts b, methods described includes:
(1) preparation of natural plants surfactant, including by gleditsia sinensis and/or soapberry and distilled water with 1:10-30's Mass volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution, By gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges two Secondary extract solution;And
(2) plant extracts b preparation, with weight than 10:10:10:3:3:3 weigh kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, big Leafiness and cacumen biotae;70% ethanol is added, after soaking 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, in proportion Add 70% ethanol and repeat backflow extraction step, merge extract solution twice.
The invention further relates to the shampoo comprising plant extracts a caused by young person with greying hair, overstrain one's nerves or aging is alleviated Application in white hair.
The invention further relates to the shampoo comprising plant extracts b to suppress dandruff generation, alleviate scalp allergy and itch In application.
The shampoo of the present invention does not contain the grease-like composition for causing scalp hair follicles to block even inflammation, does not contain to ring yet The industrial chemicals that border be able to can pollute:The composition such as surfactant and emulsifying agent, thus it is safe to the human body;The present invention's washes Hair will not produce electrostatic, alopecia significantly reduces after shampoo hair washing, have fluffy sense, hair amount to be increased slightly.Long-term use includes Plant extracts a shampoo, young person with greying hair, gray hair of the middle aged can be improved.Long-term use includes plant extracts b shampoo There is the effect of anti-dandruff and itching-relieving.The shampoo of the present invention is adapted to the daily of hair to wash shield.
Brief description of the drawings
Fig. 1 shows the effect of plant extracts a protection NCTC cell anti-peroxidation hydroxides.
Fig. 2 shows the preparation flow figure of shampoo, wherein each composition shown is mass parts.
Fig. 3 shows the Color to mouse fur using shampoo prepared by the plant extracts a of different ratio.
Embodiment
Raw material used herein meets international cosmetic raw material standard, therefore single component is unreceipted in this application Source.Specific embodiment in the application is only explanation of the invention, is not limitation of the present invention.The technology of this area The modification that personnel carry out no creative contribution to embodiment as needed after specification is read both falls within application claims The scope of protection.
Embodiment 1-3:The extraction of natural plants surfactant
Gleditsia sinensis and soapberry through screening, cleaning, sterilizing are weighed according to table 1 below, adds distilled water immersion after 30 minutes, it is micro- Boil refluxing extraction 30 minutes.After pouring out extract solution, it is proportionally added into distilled water and repeats backflow extraction step, merging is extracted twice Liquid.
Table 1:Natural surfactant extracts embodiment
Embodiment Gleditsia sinensis (g) Soapberry (g) Distilled water (kg)
1 150 250 3
2 200 200 3
3 250 150 3
Embodiment 4:Plant extracts a preparation
The proportioning by weight through screening, cleaning, sterilizing is weighed as 12:12:9:6:10:10:10:3:3:3:3 non-irrigated lotus Grass, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae, altogether 121.5g, soaked 30 minutes in 1.5L 70% ethanol, micro-boiling refluxing extraction 90 minutes.After pouring out extract solution, add in proportion Enter 70% ethanol and repeat backflow extraction step, merge extract solution twice.Revolving is dried to obtain 15.68g extracts.Used during use 1.5L distilled water dissolves again.
Embodiment 5:Plant extracts b preparation
The proportioning by weight through screening, cleaning, sterilizing is weighed as 10:10:10:3:3:3 kuh-seng, green tea, oriental wormwood, company Stick up, folium isatidis, cacumen biotae, common 117g, after being soaked 30 minutes in 1.5L 70% ethanol, micro-boiling refluxing extraction 90 minutes.Incline After going out extract solution, it is proportionally added into 70% ethanol and repeats backflow extraction step, merge extract solution twice.Revolving is dried to obtain 13.57g extracts.Dissolved again with 1.5L distilled water during use.
Embodiment 6-11:The preparation of shampoo
By the flow in accompanying drawing 2, natural plants surfactant prepared by embodiment 1-3 is prepared with embodiment 4 and 5 Plant extracts prepares corresponding shampoo respectively.
6kg natural plants surfactant and 200g plant extracts are mixed according to the proportioning of table 2, are heated to 80 DEG C, the amphoteric surfactant for adding 0.5kg 30% concentration stirs, and is added immediately edible agar and Soluble Fiber Each 12g of element, stops heating while stirring.Treat that temperature is down to 40 DEG C or so addition 6g potassium sorbates.
Table 2:The proportioning of natural plants surfactant and plant extracts
Embodiment Natural plants surfactant Plant extracts
6 Embodiment 1 Embodiment 4
7 Embodiment 1 Embodiment 5
8 Embodiment 2 Embodiment 4
9 Embodiment 2 Embodiment 5
10 Embodiment 3 Embodiment 4
11 Embodiment 3 Embodiment 5
Embodiment 12:The using effect evaluation of embodiment 6-11 shampoo
Experiment content:The people of subject 20 and the 35-75 year people of age subject 20 for collecting 14-24 year age respectively test in fact Apply the shampoo of a 6-11.Application method is daily or every two days use tested shampoo.Each dosage regard tested human hair amount and Calmly, first combing hair during use takes a small amount of shampoo gently to rub hair and scalp, and appropriate amount is reused after cleaning up Shampoo continues gently to rub 2-5 minutes, rinses well.Avoid rubbing of firmly looping.Tune is paid a return visit using using effect is carried out after 1 month Look into.
Use evaluation of result:
(1) user of embodiment 6:Mr. Jiang, 49 years old age, usage time:6 months
Using hair has been cut after 2 months, the root of hair of black exposes.Just there is young person with greying hair almost not have after 40 years old at an early age Dark hair, see dark hair again finally;
(2) user of embodiment 7:Mrs Pan, 20 years old age, usage time:2 months
After use, hair greasy feeling substantially mitigates, and alopecia significantly reduces.Back have one's hair wash from right fluffy, fuel-displaced reduction;
(3) user of embodiment 8:Ms Zhang, 52 years old age, usage time:2 weeks
It is also very submissive without hair conditioner hair after use, easily comb, it is short-tempered to be not easy.There is improvement using alopecia at second Trend;
(4) user of embodiment 8:Mrs Song, 48 years old age, usage time:1 year
Originally easy alopecia, after use, alopecia significantly reduces;
(5) user of embodiment 8:Mrs Song, 74 years old age, usage time:2 years
Primary amount is sparse, turns white.Start to become brown after more than the moon, at root of hair.After one-year age, hair amount has increased Add;
(6) user of embodiment 9:Mrs Ma, 24 years old age, usage time:Half a year
Primary amount is sparse, easy alopecia.It is obviously improved using rear alopecia, after three months, head hair amount showed increased, head Skin exposed part is reduced;
(7) user of embodiment 9:Mrs Liang, 24 years old age, usage time:Half a year
Primary amount is sparse, hair cream, and scalp pruritus, it is necessary to have one's hair wash daily.It is obviously improved daily using alopecia, hair is very dry Only, scalp is also no longer itched, and head hair amount increases;
(8) user of embodiment 10:Mr. Guo, 43 years old age, usage time:Half a year
It is young person with greying hair from the teen age, begins to use shampoo after having shaved shaven head, there is dark hair generation January.Use half a year Afterwards, white hair disappears substantially;
(9) user of embodiment 10:Mrs Ding, 42 years old age, usage time:1 year
Originally hair amount is less, alopecia is serious, withered and yellowish hairs.Significantly reduced using rear alopecia, after half a year, hair amount substantially increases Add, hair quality improves, and hair is pitch-black shinny;
(10) user of embodiment 11:Mrs Wang, 25 years old age, usage time:1 month
Originally daily hair washing needs to use hair conditioner, and alopecia is serious.Just it is obviously improved using to third time alopecia, still now Daily hair washing no longer needs hair conditioner.
Embodiment 13:Use the effect assessment of the plant extracts a of the different ratio shampoos prepared
Prepared plant extracts a:By the Eclipta prostrata, fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, red Flower, folium isatidis, balsamine, cacumen biotae in mass ratio 36:36:27:12:20:20:20:5:5:5:5 (height), 18:18:12:8: 15:15:15:5:5:5:5 (in) and 4:4:3:2:2:2:2:1:1:1:1 three kinds of (low) ratio prepares Chinese medicine Haircare composition.Take Small white mouse fur is test sample, tests the hair dyeing effect of three kinds of Chinese medicine Haircare compositions, it is found that prepared by high, medium and low three kinds of ratios Chinese medicine Haircare composition there is no notable difference to the Color of mouse fur (referring to Fig. 3).
Then, the Chinese medicine Haircare composition of high, medium and low three kinds of ratios is raw material according to above-described embodiment 6 more than respectively Be prepared into shampoo, look for respectively three groups of ages 55-75 year subject totally 15 people test effect.Subject makes in three groups Fed back afterwards with 2 times, alopecia significantly reduces, and 5 organized at high proportion people is using 1 (2 people) and 2 (3 people) after individual month respectively Feedback white hair substantially turns black, and 5 people of middle ratio group are using 1 (3 people) and 2 (2 people) to feed back white hair after individual month respectively Substantially turn black, 5 people of low ratio group are using 1 (3 people) and 2 (2 people) to feed back white hair after individual month and substantially turn black respectively.
Embodiment 14:Plant extracts a protects the effect of NCTC cell anti-peroxidation hydroxides
It is 1 × 10 to take concentration4Cfu/ml NCTC cells are inoculated in 96 orifice plates, are trained with the MEM containing 10% hyclone After supporting base culture 16 hours, 100 μ g/mL plant extracts a processing cell is added 2 hours.Original culture medium is suctioned out, is rejoined H containing 0.5mM2O2After fresh culture continues culture 12 hours, cell is dyed with Hoechst and in fluorescence microscopy Microscopic observation.
The cell that A, B, C and D are respectively normally cultivated in Fig. 1;Only add 0.5mM H2O2The cell of culture;Only add 100 The cell of μ g/mL plant extracts a cultures;In H containing 0.5mM after being handled 2 hours with 100 μ g/mL plant extracts a of addition2O2 Culture medium in the cell cultivated.
Hoechst dyestuffs can colour living cells nucleus, under microscope it has been observed that with regular culture conditions Cell (A) is contrasted through 0.5mM H2O2Cell (B) quantity of processing significantly reduces.Adding 100 μ g/mL plant extracts a will not shadow Ring cell quantity.And add after 100 μ g/mL plant extracts a are handled 2 hours and use H containing 0.5mM again2O2Culture medium in cultivate Cell quantity (D) more untreated cell quantity substantially increase.

Claims (10)

1. the shampoo consisted of the following composition:
(1) the natural plants surfactant of 50-80 parts is accounted for by weight;
(2) amphoteric surfactant of 0-6 parts is accounted for by weight;
(3) plant extracts of 1-20 parts by weight;
(4) coagulator of 0.1-0.5 parts by weight;And
(5) preservative of 0.05-0.1 parts by weight.
2. shampoo according to claim 1, wherein the plant extracts is the extract of following one or more kinds of plants: Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae are bitter Ginseng, green tea, oriental wormwood, the capsule of weeping forsythia, the Radix Astragali, Radix Angelicae Sinensis, the fruit of Chinese wolfberry, Semen sesami nigrum, Ligusticum wallichii, the fruit of Chinese magnoliavine, the red sage root, the root bark of white mulberry, chrysanthemum leaf, thoroughly Bone grass and ramulus mori;Preferably, plant extracts is the extract of following plant:Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, crow Meal leaf, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae;Preferably, plant extracts carrying for following plant Take the mixture of thing:Kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, folium isatidis and cacumen biotae;Preferably, wherein plant extracts is by weight Account for 1-3 parts of shampoo.
3. according to the shampoo of claim 1 or 2, wherein the natural plants surfactant is to extract from gleditsia sinensis, soapberry And/or the natural plants surfactant of camellia seed, or plant phosphatide;The amphoteric surfactant be selected from betaines and Amino acid surfactant, it preferably is selected from Cocoamidopropyl betaine, lauroylamidopropyl betaine, cocounut oil acyl glycine Sodium, sodium lauroyl glutamate and/or coco-nut oil fatty acid Sodium L-alaninate, it is preferable that betaines are lived with amino acids surface The ratio of property agent is 1:In the range of 0.5-3;Preferably, natural plants surfactant accounts for the 50-60 of shampoo by weight Part;And the coagulator is food-grade agar, starch or water-soluble cellulose;The preservative is food-grade sorbic acid or benzene Sodium formate.
4. according to the shampoo of any one of claims 1 to 3, wherein natural plants surfactant is with mass volume ratio 1: Gleditsia sinensis, the soapberry distillation water extract of 10-30 preparations, wherein, the weight ratio of gleditsia sinensis and soapberry is 1:0.3-3;Preferably, It is oiliness, Combination, neutrality or dryness according to be applicable hair quality, the ratio of gleditsia sinensis and soapberry is from 0.3-0.5:1、1:1 To 1:0.3-0.5 changes.
5. according to any one of claim 1-4 shampoo, wherein plant extracts is by weight 4-36:4-36:3-27:2- 12:2-20:2-20:2-20:1-5:1-5:1-5:1-5 Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae are using mass volume ratio as 1:The extract that 5-15 distilled water extraction obtains; Preferably, Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, side The weight ratio of CedarLeaves is 36:36:27:12:20:20:20:5:5:5:5,18:18:12:8:15:15:15:5:5:5:5,12:12: 9:6:10:10:10:3:3:3:3 or 4:4:3:2:2:2:2:1:1:1:1.
6. according to any one of claim 1-4 shampoo, wherein plant extracts is by weight 10:10:10:3:3:3 Kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, folium isatidis, cacumen biotae are with mass volume ratio 1:The extraction that 5-15 70% ethanol extraction obtains Thing.
7. the preparation method of shampoo, methods described include:
(1) preparation of natural plants surfactant, it is included gleditsia sinensis and/or soapberry with distilled water with 1:10-30 matter Volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes are measured, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution, is pressed Gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges twice Extract solution;And
(2) 4-36 is compared with weight:4-36:3-27:2-12:2-20:2-20:2-20:1-5:1-5:1-5:1-5 weigh Eclipta prostrata, The fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae;Add 70% Ethanol, after soaking 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, it is proportionally added into 70% ethanol and repeats to flow back Extraction step, merge extract solution twice;
Preferably, Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, phoenix are celestial Flower, the weight ratio of cacumen biotae are 36:36:27:12:20:20:20:5:5:5:5,18:18:12:8:15:15:15:5:5:5:5, 12:12:9:6:10:10:10:3:3:3:3 or 4:4:3:2:2:2:2:1:1:1:1.
8. the preparation method of shampoo, methods described include:
(1) preparation of natural plants surfactant, it is included gleditsia sinensis and/or soapberry with distilled water with 1:10-30 matter Volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes are measured, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution, is pressed Gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges twice Extract solution;And
(2) with weight than 10:10:10:3:3:3 weigh kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, folium isatidis and cacumen biotae;Add 70% Ethanol, after soaking 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, it is proportionally added into 70% ethanol and repeats to flow back Extraction step, merge extract solution twice.
9. shampoo prepared by the shampoo of any one of claim 1 to 5 and the preparation method of claim 7 is few white in alleviation Application in white hair caused by head, overstrain one's nerves or aging.
10. shampoo prepared by the shampoo of any one of Claims 1-4 and 6 and the preparation method of claim 8 is suppressing head Application in bits generation, alleviation scalp allergy and itch.
CN201711139855.2A 2017-11-16 2017-11-16 Plant shampoo water without emulsifying agent and oil phase Pending CN107737069A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109199977A (en) * 2018-09-18 2019-01-15 林文冰 A kind of shampoo and preparation method thereof
CN115247103A (en) * 2021-01-28 2022-10-28 张伟 Benzene-free heavy stain removal and sterilization soft and bright laundry detergent

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104042528A (en) * 2014-07-09 2014-09-17 重庆蒙丽朱日化品有限公司 Herbal hair-nourishing hair-loss-preventing dandruff-removing stock shampoo and preparation method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104042528A (en) * 2014-07-09 2014-09-17 重庆蒙丽朱日化品有限公司 Herbal hair-nourishing hair-loss-preventing dandruff-removing stock shampoo and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109199977A (en) * 2018-09-18 2019-01-15 林文冰 A kind of shampoo and preparation method thereof
CN115247103A (en) * 2021-01-28 2022-10-28 张伟 Benzene-free heavy stain removal and sterilization soft and bright laundry detergent

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