CN107737069A - Plant shampoo water without emulsifying agent and oil phase - Google Patents
Plant shampoo water without emulsifying agent and oil phase Download PDFInfo
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- CN107737069A CN107737069A CN201711139855.2A CN201711139855A CN107737069A CN 107737069 A CN107737069 A CN 107737069A CN 201711139855 A CN201711139855 A CN 201711139855A CN 107737069 A CN107737069 A CN 107737069A
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- shampoo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/13—Coniferophyta (gymnosperms)
- A61K36/14—Cupressaceae (Cypress family), e.g. juniper or cypress
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/19—Acanthaceae (Acanthus family)
- A61K36/195—Strobilanthes
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/282—Artemisia, e.g. wormwood or sagebrush
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/286—Carthamus (distaff thistle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/31—Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
- A61K36/315—Isatis, e.g. Dyer's woad
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/489—Sophora, e.g. necklacepod or mamani
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
- A61K36/634—Forsythia
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
- A61K36/638—Ligustrum, e.g. Chinese privet
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/85—Verbenaceae (Verbena family)
- A61K36/855—Clerodendrum, e.g. glorybower
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Abstract
The present invention relates to the plant shampoo water without emulsifying agent and oil phase.Specifically, the invention discloses by natural plants surfactant and plant extracts as main component, shampoo without emulsifying agent and oil phase, wherein reduce the use of synthetic surfactant and preservative, and white hair caused by with young person with greying hair, overstrain one's nerves or aging is alleviated, or suppress dandruff generation, alleviate the effect of scalp allergy and itch, it is adapted to wash shield daily.
Description
Technical field
The present invention relates to shampoo, more particularly, to the plant shampoo water without emulsifying agent and oil phase.
Background technology
Shampoo, also known as shampoo, shampoo, hair washing gel, major function is cleaning hair and scalp, that is, dispels hair
With the dust and secretion on scalp, also there are the functions such as some Ju You treatment oil, dyeing, hair cares.Common shampoo on the market
Composition includes surfactant, emulsifying agent and oil compounds.Add the main function of oil compounds (such as silicone oil)
It is to protect hair scale piece, plays moisturizing and the effect such as submissive, and in order to ensure that the stabilization of shampoo physical property needs to add
Emulsifying agent.However, common shampoo generally has the following disadvantages on the market:1) emulsifying agent and oil compounds are usually
It can be attached on scalp, block hair follicle, gently then cause alopecia, it is heavy then hair follicle inflammation may be caused;2) table of some industrial chemicals
It is difficult to be degraded that face activating agent, emulsifying agent etc., which are discharged into environment, pollutes environment.
The content of the invention
It is an object of the invention to provide emulsifying agent and oil phase is not contained, using natural plants surfactant, and with the addition of
The shampoo of plant extracts.The shampoo of the present invention can alleviate alopecia.In addition, according to selected plant extracts not
White hair caused by with that can also have improvement young person with greying hair, overstrain one's nerves and aging or the effect for reducing dandruff.
The invention provides a kind of shampoo consisted of the following composition:
(1) the natural plants surfactant of 50-80 parts is accounted for by weight;
(2) conventional (both sexes) surfactant of 0-6 parts is accounted for by weight;
(3) plant extracts of 1-20 parts by weight;
(4) coagulator of 0.1-4 parts by weight;And
(5) preservative of 0.05-0.1 parts by weight.
Natural surfactant mixes by a certain percentage with amphoteric surfactant, with the dust on scalp and hair, oil
Fat and secretion are combined, and are removed afterwards by washing, and play a part of cleaning scalp and hair.
Natural plants surfactant can extract from gleditsia sinensis, soapberry and/or camellia seed or plant phosphatide.
Preferably, natural plants surfactant can account for 50-60 parts of shampoo by weight.
Preferably, natural plants surfactant is with mass volume ratio 1:Gleditsia sinensis, the soapberry distilled water of 10-30 preparations
Extract.Wherein, the weight of gleditsia sinensis and soapberry ratio is 1:0.3-3.Especially, it is oiliness, mixing according to be applicable hair quality
Property, neutrality or dryness, when preparing natural plants surfactant, the ratio of gleditsia sinensis and soapberry is from 0.3-0.5:1、1:1
To 1:0.3-0.5 changes.
Amphoteric surfactant is selected from betaines and amino acid surfactant, generally selects the beet of 30% concentration
Bases and amino acid surfactant, and betaines can be mixed with amino acid surfactant with arbitrary proportion,
The stabilization of product physical property can be ensured.Preferably, betaines and the ratio of amino acid surfactant are 1:0.5-3's
In the range of.The conventional surfactant of amino acids can be only selected for special sensitive group.For example, amophoteric surface active
Agent can be selected from Cocoamidopropyl betaine, lauroylamidopropyl betaine, sodium cocoyl glycinate, lauroyl glutamate
Sodium and/or coco-nut oil fatty acid Sodium L-alaninate.
The shampoo that is obtained from above-mentioned natural and amphoteric surfactant is soft, does not stimulate, suitable for various hair qualitys,
Alopecia can be significantly reduced, hair and scalp can reach preferable cleaning effect, be adapted to wash shield daily.
Plant extracts can be the distillation water extract of a Chinese medicine compound prescription, and conditioning head is played during hair washing
Skin, the effect for protecting hair scale piece.Preferably, plant extracts can account for 1-3 parts of shampoo by weight.Plant extracts can
To be the extract of following plant:Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, greatly
Leafiness, balsamine, cacumen biotae, kuh-seng, green tea, oriental wormwood and the capsule of weeping forsythia.
For example, Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, phoenix
Celestial flower, the extract of cacumen biotae have protection cell and oxidation resistant effect.In addition, kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, smalt
Leaf, the extract of cacumen biotae are reduced the effect of dandruff.Those skilled in the art can also select other to have as needed
The extract of the medicinal plant of black hair effect, for example, the Radix Astragali, Radix Angelicae Sinensis, the fruit of Chinese wolfberry, Semen sesami nigrum, Ligusticum wallichii, the fruit of Chinese magnoliavine and the red sage root.This
Art personnel can also select the extract of other medicinal plants that there is anti-dandruff to act on as needed, for example, mulberry
White skin, chrysanthemum leaf, lopseed, ramulus mori.
Plant extracts a can be that proportioning is 4-36 by weight:4-36:3-27:2-12:2-20:2-20:2-20:1-
5:1-5:1-5:1-5 Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis,
Balsamine, cacumen biotae mass volume ratio 1:5-15 distilled water extracts obtained extract.Can be by Eclipta prostrata, glossy privet
Son, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae in mass ratio 36:36:
27:12:20:20:20:5:5:5:5 (height), 18:18:12:8:15:15:15:5:5:5:5 (in) and 4:4:3:2:2:2:2:1:
1:1:The formula mass volume ratio 1 of 1 (low):5-15 distilled water extraction obtains plant extracts a.
Preferably, plant extracts a can be that proportioning is 12 by weight:12:9:6:10:10:10:3:3:3:3 drought
Lotus grass, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae matter
Measure volume ratio 1:5-15 distilled water extracts obtained extract.This plant extract composition formula is rich in oxidation-resistant active ingredient
It can alleviate white hair caused by young person with greying hair, overstrain one's nerves or aging with nutritional ingredient, long-term uses such as plant polyoses.Especially,
Alleviated using shampoo made of this plant extracts a using more than one month white hair, had after three months in various degree
Dark hair is newborn, white hair turns black at root of hair.Long-term use of white hair can gradually turn black, and hair amount is increased slightly.
Plant extracts b can be that proportioning is 10 by weight:10:10:3:3:It is 3 kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, big
Leafiness, cacumen biotae mass volume ratio 1:5-15 70% ethanol extracts obtained extract.This plant extract composition formula
In oriental wormwood, kuh-seng, green tea containing suppress bacterium, fungi propagation composition;And the extract of this formula is also with anti-
Scorching, antipruritic bioactive ingredients, dandruff generation can be suppressed, alleviate scalp allergy and itch.Especially, using this plant
Itching of the scalp improves immediately after shampoo made of extract b, and scalp allergy, which has, to be taken a turn for the better, bright using dandruff after a period of time
It is aobvious to reduce.
Coagulator can use the coagulator that food service industry is commonly used, it is for instance possible to use food-grade agar, starch, water-soluble
Property cellulose etc..The usage amount of coagulator can determine according to the physical behavior to be reached.Coagulator can be only from edible
Starch, the time that food starch can keep the physical behavior of shampoo is longer, and more preferably, scalp feels more clear to cleaning effect
Refreshing, hair is more soft.Coagulator can also select weight than 1:1 agar and starch or agar and water-soluble cellulose, so
Coagulator shampoo can be made to be kept for sticky physical behavior long period.
Preservative selects food-grade sorbic acid or sodium benzoate.Because natural plant extracts, anti-corrosion are rich in shampoo
The addition of agent is to prevent the pollution of microorganism.
Present invention also offers the preparation method of the shampoo comprising plant extracts a, methods described includes:
(1) preparation of natural plants surfactant, including by gleditsia sinensis and/or soapberry and distilled water with 1:10-30's
Mass volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution,
By gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges two
Secondary extract solution;And
(2) plant extracts a preparation, 4-36 is compared with weight:4-36:3-27:2-12:2-20:2-20:2-20:1-5:
1-5:1-5:1-5 weigh Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis,
Balsamine and cacumen biotae;Add 70% ethanol, after immersion 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, by than
Example adds 70% ethanol and repeats backflow extraction step, merges extract solution twice.
Preferably, with weight than 12:12:9:6:10:10:10:3:3:3:3 weigh Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, system
Sealwort, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae prepared plant extracts a.
With weight than 36:36:27:12:20:20:20:5:5:5:5 (height), 18:18:12:8:15:15:15:5:5:5:5
(in) or 4:4:3:2:2:2:2:1:1:1:1 (low) weigh Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries,
Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae prepared plant extracts a.
Present invention also offers the preparation method of the shampoo comprising plant extracts b, methods described includes:
(1) preparation of natural plants surfactant, including by gleditsia sinensis and/or soapberry and distilled water with 1:10-30's
Mass volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution,
By gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges two
Secondary extract solution;And
(2) plant extracts b preparation, with weight than 10:10:10:3:3:3 weigh kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, big
Leafiness and cacumen biotae;70% ethanol is added, after soaking 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, in proportion
Add 70% ethanol and repeat backflow extraction step, merge extract solution twice.
The invention further relates to the shampoo comprising plant extracts a caused by young person with greying hair, overstrain one's nerves or aging is alleviated
Application in white hair.
The invention further relates to the shampoo comprising plant extracts b to suppress dandruff generation, alleviate scalp allergy and itch
In application.
The shampoo of the present invention does not contain the grease-like composition for causing scalp hair follicles to block even inflammation, does not contain to ring yet
The industrial chemicals that border be able to can pollute:The composition such as surfactant and emulsifying agent, thus it is safe to the human body;The present invention's washes
Hair will not produce electrostatic, alopecia significantly reduces after shampoo hair washing, have fluffy sense, hair amount to be increased slightly.Long-term use includes
Plant extracts a shampoo, young person with greying hair, gray hair of the middle aged can be improved.Long-term use includes plant extracts b shampoo
There is the effect of anti-dandruff and itching-relieving.The shampoo of the present invention is adapted to the daily of hair to wash shield.
Brief description of the drawings
Fig. 1 shows the effect of plant extracts a protection NCTC cell anti-peroxidation hydroxides.
Fig. 2 shows the preparation flow figure of shampoo, wherein each composition shown is mass parts.
Fig. 3 shows the Color to mouse fur using shampoo prepared by the plant extracts a of different ratio.
Embodiment
Raw material used herein meets international cosmetic raw material standard, therefore single component is unreceipted in this application
Source.Specific embodiment in the application is only explanation of the invention, is not limitation of the present invention.The technology of this area
The modification that personnel carry out no creative contribution to embodiment as needed after specification is read both falls within application claims
The scope of protection.
Embodiment 1-3:The extraction of natural plants surfactant
Gleditsia sinensis and soapberry through screening, cleaning, sterilizing are weighed according to table 1 below, adds distilled water immersion after 30 minutes, it is micro-
Boil refluxing extraction 30 minutes.After pouring out extract solution, it is proportionally added into distilled water and repeats backflow extraction step, merging is extracted twice
Liquid.
Table 1:Natural surfactant extracts embodiment
Embodiment | Gleditsia sinensis (g) | Soapberry (g) | Distilled water (kg) |
1 | 150 | 250 | 3 |
2 | 200 | 200 | 3 |
3 | 250 | 150 | 3 |
Embodiment 4:Plant extracts a preparation
The proportioning by weight through screening, cleaning, sterilizing is weighed as 12:12:9:6:10:10:10:3:3:3:3 non-irrigated lotus
Grass, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae, altogether
121.5g, soaked 30 minutes in 1.5L 70% ethanol, micro-boiling refluxing extraction 90 minutes.After pouring out extract solution, add in proportion
Enter 70% ethanol and repeat backflow extraction step, merge extract solution twice.Revolving is dried to obtain 15.68g extracts.Used during use
1.5L distilled water dissolves again.
Embodiment 5:Plant extracts b preparation
The proportioning by weight through screening, cleaning, sterilizing is weighed as 10:10:10:3:3:3 kuh-seng, green tea, oriental wormwood, company
Stick up, folium isatidis, cacumen biotae, common 117g, after being soaked 30 minutes in 1.5L 70% ethanol, micro-boiling refluxing extraction 90 minutes.Incline
After going out extract solution, it is proportionally added into 70% ethanol and repeats backflow extraction step, merge extract solution twice.Revolving is dried to obtain
13.57g extracts.Dissolved again with 1.5L distilled water during use.
Embodiment 6-11:The preparation of shampoo
By the flow in accompanying drawing 2, natural plants surfactant prepared by embodiment 1-3 is prepared with embodiment 4 and 5
Plant extracts prepares corresponding shampoo respectively.
6kg natural plants surfactant and 200g plant extracts are mixed according to the proportioning of table 2, are heated to 80
DEG C, the amphoteric surfactant for adding 0.5kg 30% concentration stirs, and is added immediately edible agar and Soluble Fiber
Each 12g of element, stops heating while stirring.Treat that temperature is down to 40 DEG C or so addition 6g potassium sorbates.
Table 2:The proportioning of natural plants surfactant and plant extracts
Embodiment | Natural plants surfactant | Plant extracts |
6 | Embodiment 1 | Embodiment 4 |
7 | Embodiment 1 | Embodiment 5 |
8 | Embodiment 2 | Embodiment 4 |
9 | Embodiment 2 | Embodiment 5 |
10 | Embodiment 3 | Embodiment 4 |
11 | Embodiment 3 | Embodiment 5 |
Embodiment 12:The using effect evaluation of embodiment 6-11 shampoo
Experiment content:The people of subject 20 and the 35-75 year people of age subject 20 for collecting 14-24 year age respectively test in fact
Apply the shampoo of a 6-11.Application method is daily or every two days use tested shampoo.Each dosage regard tested human hair amount and
Calmly, first combing hair during use takes a small amount of shampoo gently to rub hair and scalp, and appropriate amount is reused after cleaning up
Shampoo continues gently to rub 2-5 minutes, rinses well.Avoid rubbing of firmly looping.Tune is paid a return visit using using effect is carried out after 1 month
Look into.
Use evaluation of result:
(1) user of embodiment 6:Mr. Jiang, 49 years old age, usage time:6 months
Using hair has been cut after 2 months, the root of hair of black exposes.Just there is young person with greying hair almost not have after 40 years old at an early age
Dark hair, see dark hair again finally;
(2) user of embodiment 7:Mrs Pan, 20 years old age, usage time:2 months
After use, hair greasy feeling substantially mitigates, and alopecia significantly reduces.Back have one's hair wash from right fluffy, fuel-displaced reduction;
(3) user of embodiment 8:Ms Zhang, 52 years old age, usage time:2 weeks
It is also very submissive without hair conditioner hair after use, easily comb, it is short-tempered to be not easy.There is improvement using alopecia at second
Trend;
(4) user of embodiment 8:Mrs Song, 48 years old age, usage time:1 year
Originally easy alopecia, after use, alopecia significantly reduces;
(5) user of embodiment 8:Mrs Song, 74 years old age, usage time:2 years
Primary amount is sparse, turns white.Start to become brown after more than the moon, at root of hair.After one-year age, hair amount has increased
Add;
(6) user of embodiment 9:Mrs Ma, 24 years old age, usage time:Half a year
Primary amount is sparse, easy alopecia.It is obviously improved using rear alopecia, after three months, head hair amount showed increased, head
Skin exposed part is reduced;
(7) user of embodiment 9:Mrs Liang, 24 years old age, usage time:Half a year
Primary amount is sparse, hair cream, and scalp pruritus, it is necessary to have one's hair wash daily.It is obviously improved daily using alopecia, hair is very dry
Only, scalp is also no longer itched, and head hair amount increases;
(8) user of embodiment 10:Mr. Guo, 43 years old age, usage time:Half a year
It is young person with greying hair from the teen age, begins to use shampoo after having shaved shaven head, there is dark hair generation January.Use half a year
Afterwards, white hair disappears substantially;
(9) user of embodiment 10:Mrs Ding, 42 years old age, usage time:1 year
Originally hair amount is less, alopecia is serious, withered and yellowish hairs.Significantly reduced using rear alopecia, after half a year, hair amount substantially increases
Add, hair quality improves, and hair is pitch-black shinny;
(10) user of embodiment 11:Mrs Wang, 25 years old age, usage time:1 month
Originally daily hair washing needs to use hair conditioner, and alopecia is serious.Just it is obviously improved using to third time alopecia, still now
Daily hair washing no longer needs hair conditioner.
Embodiment 13:Use the effect assessment of the plant extracts a of the different ratio shampoos prepared
Prepared plant extracts a:By the Eclipta prostrata, fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, red
Flower, folium isatidis, balsamine, cacumen biotae in mass ratio 36:36:27:12:20:20:20:5:5:5:5 (height), 18:18:12:8:
15:15:15:5:5:5:5 (in) and 4:4:3:2:2:2:2:1:1:1:1 three kinds of (low) ratio prepares Chinese medicine Haircare composition.Take
Small white mouse fur is test sample, tests the hair dyeing effect of three kinds of Chinese medicine Haircare compositions, it is found that prepared by high, medium and low three kinds of ratios
Chinese medicine Haircare composition there is no notable difference to the Color of mouse fur (referring to Fig. 3).
Then, the Chinese medicine Haircare composition of high, medium and low three kinds of ratios is raw material according to above-described embodiment 6 more than respectively
Be prepared into shampoo, look for respectively three groups of ages 55-75 year subject totally 15 people test effect.Subject makes in three groups
Fed back afterwards with 2 times, alopecia significantly reduces, and 5 organized at high proportion people is using 1 (2 people) and 2 (3 people) after individual month respectively
Feedback white hair substantially turns black, and 5 people of middle ratio group are using 1 (3 people) and 2 (2 people) to feed back white hair after individual month respectively
Substantially turn black, 5 people of low ratio group are using 1 (3 people) and 2 (2 people) to feed back white hair after individual month and substantially turn black respectively.
Embodiment 14:Plant extracts a protects the effect of NCTC cell anti-peroxidation hydroxides
It is 1 × 10 to take concentration4Cfu/ml NCTC cells are inoculated in 96 orifice plates, are trained with the MEM containing 10% hyclone
After supporting base culture 16 hours, 100 μ g/mL plant extracts a processing cell is added 2 hours.Original culture medium is suctioned out, is rejoined
H containing 0.5mM2O2After fresh culture continues culture 12 hours, cell is dyed with Hoechst and in fluorescence microscopy Microscopic observation.
The cell that A, B, C and D are respectively normally cultivated in Fig. 1;Only add 0.5mM H2O2The cell of culture;Only add 100
The cell of μ g/mL plant extracts a cultures;In H containing 0.5mM after being handled 2 hours with 100 μ g/mL plant extracts a of addition2O2
Culture medium in the cell cultivated.
Hoechst dyestuffs can colour living cells nucleus, under microscope it has been observed that with regular culture conditions
Cell (A) is contrasted through 0.5mM H2O2Cell (B) quantity of processing significantly reduces.Adding 100 μ g/mL plant extracts a will not shadow
Ring cell quantity.And add after 100 μ g/mL plant extracts a are handled 2 hours and use H containing 0.5mM again2O2Culture medium in cultivate
Cell quantity (D) more untreated cell quantity substantially increase.
Claims (10)
1. the shampoo consisted of the following composition:
(1) the natural plants surfactant of 50-80 parts is accounted for by weight;
(2) amphoteric surfactant of 0-6 parts is accounted for by weight;
(3) plant extracts of 1-20 parts by weight;
(4) coagulator of 0.1-0.5 parts by weight;And
(5) preservative of 0.05-0.1 parts by weight.
2. shampoo according to claim 1, wherein the plant extracts is the extract of following one or more kinds of plants:
Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae are bitter
Ginseng, green tea, oriental wormwood, the capsule of weeping forsythia, the Radix Astragali, Radix Angelicae Sinensis, the fruit of Chinese wolfberry, Semen sesami nigrum, Ligusticum wallichii, the fruit of Chinese magnoliavine, the red sage root, the root bark of white mulberry, chrysanthemum leaf, thoroughly
Bone grass and ramulus mori;Preferably, plant extracts is the extract of following plant:Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, crow
Meal leaf, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae;Preferably, plant extracts carrying for following plant
Take the mixture of thing:Kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, folium isatidis and cacumen biotae;Preferably, wherein plant extracts is by weight
Account for 1-3 parts of shampoo.
3. according to the shampoo of claim 1 or 2, wherein the natural plants surfactant is to extract from gleditsia sinensis, soapberry
And/or the natural plants surfactant of camellia seed, or plant phosphatide;The amphoteric surfactant be selected from betaines and
Amino acid surfactant, it preferably is selected from Cocoamidopropyl betaine, lauroylamidopropyl betaine, cocounut oil acyl glycine
Sodium, sodium lauroyl glutamate and/or coco-nut oil fatty acid Sodium L-alaninate, it is preferable that betaines are lived with amino acids surface
The ratio of property agent is 1:In the range of 0.5-3;Preferably, natural plants surfactant accounts for the 50-60 of shampoo by weight
Part;And the coagulator is food-grade agar, starch or water-soluble cellulose;The preservative is food-grade sorbic acid or benzene
Sodium formate.
4. according to the shampoo of any one of claims 1 to 3, wherein natural plants surfactant is with mass volume ratio 1:
Gleditsia sinensis, the soapberry distillation water extract of 10-30 preparations, wherein, the weight ratio of gleditsia sinensis and soapberry is 1:0.3-3;Preferably,
It is oiliness, Combination, neutrality or dryness according to be applicable hair quality, the ratio of gleditsia sinensis and soapberry is from 0.3-0.5:1、1:1
To 1:0.3-0.5 changes.
5. according to any one of claim 1-4 shampoo, wherein plant extracts is by weight 4-36:4-36:3-27:2-
12:2-20:2-20:2-20:1-5:1-5:1-5:1-5 Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries,
Testa sojae atricolor, safflower, folium isatidis, balsamine, cacumen biotae are using mass volume ratio as 1:The extract that 5-15 distilled water extraction obtains;
Preferably, Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine, side
The weight ratio of CedarLeaves is 36:36:27:12:20:20:20:5:5:5:5,18:18:12:8:15:15:15:5:5:5:5,12:12:
9:6:10:10:10:3:3:3:3 or 4:4:3:2:2:2:2:1:1:1:1.
6. according to any one of claim 1-4 shampoo, wherein plant extracts is by weight 10:10:10:3:3:3
Kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, folium isatidis, cacumen biotae are with mass volume ratio 1:The extraction that 5-15 70% ethanol extraction obtains
Thing.
7. the preparation method of shampoo, methods described include:
(1) preparation of natural plants surfactant, it is included gleditsia sinensis and/or soapberry with distilled water with 1:10-30 matter
Volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes are measured, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution, is pressed
Gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges twice
Extract solution;And
(2) 4-36 is compared with weight:4-36:3-27:2-12:2-20:2-20:2-20:1-5:1-5:1-5:1-5 weigh Eclipta prostrata,
The fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, balsamine and cacumen biotae;Add 70%
Ethanol, after soaking 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, it is proportionally added into 70% ethanol and repeats to flow back
Extraction step, merge extract solution twice;
Preferably, Eclipta prostrata, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA, RHIZOMA POLYGONATI PREPARATA, Smilax, mulberries, Testa sojae atricolor, safflower, folium isatidis, phoenix are celestial
Flower, the weight ratio of cacumen biotae are 36:36:27:12:20:20:20:5:5:5:5,18:18:12:8:15:15:15:5:5:5:5,
12:12:9:6:10:10:10:3:3:3:3 or 4:4:3:2:2:2:2:1:1:1:1.
8. the preparation method of shampoo, methods described include:
(1) preparation of natural plants surfactant, it is included gleditsia sinensis and/or soapberry with distilled water with 1:10-30 matter
Volume ratio distilled water immersion gleditsia sinensis and/or soapberry 30 minutes are measured, micro-boiling refluxing extraction 30 minutes, after pouring out extract solution, is pressed
Gleditsia sinensis and/or soapberry and distilled water 1:10-30 mass volume ratio adds distilled water and repeats backflow extraction step, merges twice
Extract solution;And
(2) with weight than 10:10:10:3:3:3 weigh kuh-seng, green tea, oriental wormwood, the capsule of weeping forsythia, folium isatidis and cacumen biotae;Add 70%
Ethanol, after soaking 30 minutes, micro-boiling refluxing extraction 90 minutes, after pouring out extract solution, it is proportionally added into 70% ethanol and repeats to flow back
Extraction step, merge extract solution twice.
9. shampoo prepared by the shampoo of any one of claim 1 to 5 and the preparation method of claim 7 is few white in alleviation
Application in white hair caused by head, overstrain one's nerves or aging.
10. shampoo prepared by the shampoo of any one of Claims 1-4 and 6 and the preparation method of claim 8 is suppressing head
Application in bits generation, alleviation scalp allergy and itch.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109199977A (en) * | 2018-09-18 | 2019-01-15 | 林文冰 | A kind of shampoo and preparation method thereof |
CN115247103A (en) * | 2021-01-28 | 2022-10-28 | 张伟 | Benzene-free heavy stain removal and sterilization soft and bright laundry detergent |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104042528A (en) * | 2014-07-09 | 2014-09-17 | 重庆蒙丽朱日化品有限公司 | Herbal hair-nourishing hair-loss-preventing dandruff-removing stock shampoo and preparation method thereof |
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2017
- 2017-11-16 CN CN201711139855.2A patent/CN107737069A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104042528A (en) * | 2014-07-09 | 2014-09-17 | 重庆蒙丽朱日化品有限公司 | Herbal hair-nourishing hair-loss-preventing dandruff-removing stock shampoo and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109199977A (en) * | 2018-09-18 | 2019-01-15 | 林文冰 | A kind of shampoo and preparation method thereof |
CN115247103A (en) * | 2021-01-28 | 2022-10-28 | 张伟 | Benzene-free heavy stain removal and sterilization soft and bright laundry detergent |
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