CN108567636A - A kind of draft Haircare composition of the extract containing hamamelis - Google Patents
A kind of draft Haircare composition of the extract containing hamamelis Download PDFInfo
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- CN108567636A CN108567636A CN201810615176.6A CN201810615176A CN108567636A CN 108567636 A CN108567636 A CN 108567636A CN 201810615176 A CN201810615176 A CN 201810615176A CN 108567636 A CN108567636 A CN 108567636A
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- hamamelis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/004—Preparations used to protect coloured hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses a kind of draft Haircare compositions of extract containing hamamelis.The composition contains hamamelis extract, nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extract, and mass ratio is 6~12：4~8：3~5：2~4：3~6.The draft Haircare composition is compounded by reasonably optimizing, and each component produces apparent synergistic effect, has the function of nourishing strengthen the hair, performance is mild, product can effectively be reduced to the stimulation anaphylaxis of scalp, scalp allergy is effectively prevent, can be applied to various hair care products；The hair dyeing product of preparation significantly reduces the stimulation of scalp, and hair dyeing effect and persistence are good, good color fastness of having hair dyed, while can also repair hair quality；The hair conditioner of preparation, it is non-stimulated to scalp, it is strong to the repair of hair quality；The shampoo of preparation, anti-dandruff and itching-relieving effect is good, and without side-effects.And the draft hair care compositions raw material is easy to get, and preparation process is simple, has good application prospect.
Description
Technical field
The invention belongs to technical field of daily necessities, are protected more particularly, to a kind of draft of extract containing hamamelis
Send out composition.
Background technology
Currently, hairdressing is liked by people seeking beauty very much, including some different forms such as cuts, washes, blowing, scalding, contaminating, drawing.Than
If hair dyeing is favored by young people and fashion personage very much, the hair dyeing products such as cream rinse can change head as a kind of cosmetics
The color of hair meets modern consumer for beautiful and fashion pursuit.
But the product reagent majority used during the hairdressings such as boiling hot, dye, drawing, which has hair and scalp, stimulates damage work
With severe patient generates allergic reaction；How much the even hair care products such as shampoo, hair jelly, gel also have stimulation damage and make
With.
For example hair dyeing product, oxidative hair dyes are generally popular currently on the market a kind of hair dyes, have user
Just, the features such as dyeing range is wide.However, research shows that using with compared with strong and stimulating in hair dyeing product, it is more likely that cause people
Body skin sensitivity reacts, although firmness is relatively good after oxidative hair dyes hair dyeing, should not wash away, with hair care and nourishing tune
Manage the addition of agent, it is bad that dyeing often occur in many cream rinses, or easily washes off, it is unstable phenomena such as dye after hair, through more
After secondary washing, poor color fastness.
Therefore, there is an urgent need for seek a kind of small to the human body irritation and preferable hair dyeing cosmetic of color fastness.
Invention content
The technical problem to be solved by the present invention is to overcome the deficiencies of the prior art and provide a kind of low irritant, at the same it is simultaneous
The draft Haircare composition cream rinse of tool hair care function and the color fastness preferably extract containing hamamelis.
The first purpose of the invention is to provide a kind of draft Haircare compositions of extract containing hamamelis.
Second object of the present invention is to provide application of the draft Haircare composition in preparing hair care product.
Third object of the present invention is to provide a kind of draft cream rinses and preparation method thereof.
Fourth object of the present invention is to provide a kind of draft shampoo and preparation method thereof.
Fifth object of the present invention is to provide a kind of draft hair conditioner and preparation method thereof.
To achieve the goals above, the present invention is achieved by the following technical programs：
A kind of draft Haircare composition of the extract containing hamamelis is extracted containing hamamelis extract, nettle
Object, peony extract, Rosmarinus officinalis extract and horse chestnut extract.
Preferably, in the draft Haircare composition, hamamelis extract, nettle extract, peony extract, fan
Repeatedly the mass ratio of fragrant extract and horse chestnut extract is 6~12：4~8：3~5：2~4：3~6.
It is highly preferred that in the draft Haircare composition, hamamelis extract, nettle extract, peony extract,
The mass ratio of Rosmarinus officinalis extract and horse chestnut extract is 10：5：3：3：3.
Application of the draft Haircare composition in hair care product also belongs to protection scope of the present invention.
A kind of hair care product containing the draft Haircare composition also belongs to protection scope of the present invention.
Preferably, the hair care product is hair dyeing product, hair washing product, hair products or hair jelly.
The hair dyeing product such as cream rinse.The hair washing product such as shampoo.The hair products such as hair conditioner.
The present invention also provides a kind of cream rinses containing the draft Haircare composition, with weight ratio meter, draft hair care
Composition accounts for the 20~35% of cream rinse total amount.
Preferably, with weight ratio meter, the draft Haircare composition accounts for the 24% of cream rinse total amount.
It is highly preferred that with weight ratio meter, the cream rinse also contains thickener 8~10%, pH adjusting agent 2~2.50%,
Antioxidant 0.50~0.80%, emulsifier 3~4%, conditioner for hair 0.5~1%, hair colorant 2~3%, moisturizer 1
~2%, chelating agent 0.1~0.5%, remaining is deionized water.
In the cream rinse, thickener, which has, inhibits greasy feeling, reduces wax class raw material stickiness, stable cosmetic gel etc.
Effect.
Preferably, thickener is cetostearyl alcohol.
In the cream rinse, pH adjusting agent is capable of providing colorant and aoxidizes had alkaline condition, and aminomethyl propanol
Good security will not cause to damage to skin, and the combination of the pH adjusting agent in addition can also promote colorant oxidation more to add
Entirely so that the hair of dyeing is vivider.
Preferably, pH adjusting agent is monoethanolamine and aminomethyl propanol.
Preferably, pH adjusting agent is monoethanolamine and aminomethyl propanol, mass ratio 2~3:1~2.
It is highly preferred that pH adjusting agent is monoethanolamine and aminomethyl propanol, mass ratio 1:1.
In the cream rinse, antioxidant is avoided that in traditional cream rinse product that colorant oxidation rate is too fast and causes
Non-uniform phenomenon is dyed, ensures that colorant penetrates into hair core by the sufficient time so that dyeing is more uniform, and color is more
It is vivid.
Preferably, antioxidant is the mixture of sodium sulfite and sodium isoascorbate, and mass ratio is 4~6：2~4.
It is highly preferred that antioxidant is the mixture of sodium sulfite and sodium isoascorbate, mass ratio 2:1.
In the cream rinse, conditioner for hair has good lubricity；There is permeability to skin, has preferably with skin
Compatibility is easily absorbed by skin histology, makes skin emolliency.
Preferably, conditioner for hair is one kind in Trivent OCG, Triglyceride DDD or tristerin
Or several ground mixture.
It is highly preferred that conditioner for hair is Triglyceride DDD.
Preferably, emulsifier is the mixture of ceteareth -20 and stearine.
Preferably, emulsifier is ceteareth -20 and stearine, and mass ratio is 2~3:1~2.
It is highly preferred that emulsifier is ceteareth -20 and stearine, mass ratio 2：1.
Preferably, colorant is ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2-
The mixture of amino -3- pyridones.
It is highly preferred that colorant be ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and
The mixture of 2- amino -3- pyridones, mass ratio 20:6:3:1.
Preferably, chelating agent is EDETATE SODIUM in the cream rinse.
Preferably, moisturizer is propylene glycol.
Most preferably, by weight, the cream rinse contains：Hamamelis extract, nettle extract, Chinese herbaceous peony extraction
The mixing draft Haircare composition of object, Rosmarinus officinalis extract and horse chestnut extract, thickener 8~10%, pH adjusting agent 2~
2.50%, antioxidant 0.50~0.80%, emulsifier 3~4%, conditioner for hair 0.5~1%, hair colorant 2~3%,
Moisturizer 1~2%, chelating agent 0.1~0.5%, remaining is deionized water；
Wherein, thickener is cetostearyl alcohol；
PH adjusting agent is monoethanolamine and aminomethyl propanol, mass ratio 1:1；
Antioxidant is the mixture of sodium sulfite and sodium isoascorbate, mass ratio 2:1；
Emulsifier is ceteareth -20 and stearine, mass ratio 2:1；
Conditioner for hair is Triglyceride DDD；
Colorant is ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino -3-
The mixture of pyridone, mass ratio 20:6:3:1；
Chelating agent is EDETATE SODIUM；
Moisturizer is propylene glycol；
With weight ratio meter, draft Haircare composition accounts for the 20~35% of cream rinse total amount；
In the draft Haircare composition, hamamelis extract, nettle extract, peony extract, rosemary carry
It is 6~12 to take the mass ratio of object and horse chestnut extract：4~8：3~5：2~4：3~6.
It is highly preferred that by weight, the cream rinse contains：Hamamelis extract 10%, nettle extract 5%,
Peony extract 3%, Rosmarinus officinalis extract 3%, horse chestnut extract 3%, thickener cetostearyl alcohol 10%, pH adjusting agent list
Ethanol amine and aminomethyl propanol mass ratio 1：1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are
2：1 mixture 0.50%, emulsifier ceteareth -20 and stearine mass ratio are 2：1 mixture
3%, conditioner for hair Triglyceride DDD 0.50%, hair colorant ethoxy-p-PDA sulfate, resorcinol, 2,
4- diaminophenoxy ethanols and 2- amino -3- pyridone mass ratioes are 20：6：3：1 mixture 2%, moisturizer propylene glycol,
Chelating agent EDTA- disodiums 0.3%, remaining is deionized water.
In addition, the preparation method of the cream rinse, includes the following steps：
S1. moisturizer and chelating agent, heating stirring are added in deionized water, until the temperature of the mixture is to 80~85 DEG C
Component stops after all melting afterwards, obtains mixture A；
S2. thickener, emulsifier and conditioner for hair are mixed, component all melts after heating and being stirred to 80~85 DEG C
After stop, obtaining mixture B；
S3. hair colorant and antioxidant are uniformly mixing to obtain mixture C；
S4. mixture B and mixture C are added into mixture A, stirs evenly so that mixture A, B, C are fully emulsified to be obtained
To mixture D；
S5. any draft Haircare composition of claims 1 to 3 and PH conditioning agents are added into mixture D, stirring is equal
It is even.
In addition, the present invention also provides a kind of shampoo of the draft Haircare composition of hamamelis extract, each group
Point quality be：Hamamelis extract, nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extract
Mixing draft Haircare composition, laureth sodium sulfovinate 9~11%, Cocoamidopropyl betaine 4.5~5.5%,
Trivent OCG 4~6%, moisturizer sorbierite 1.8~2.2%, citric acid 0.9~1.1%, chelating agent EDETATE SODIUM 0.25
~0.35%, vitamin C 0.25~0.35%, remaining is deionized water；
With weight ratio meter, draft Haircare composition accounts for the 20~35% of shampoo total amount；
In the draft Haircare composition, hamamelis extract, nettle extract, peony extract, rosemary carry
It is 6~12 to take the mass ratio of object and horse chestnut extract：4~8：3~5：2~4：3~6.
Preferably, the quality of the shampoo, each component is：Hamamelis extract 10%, nettle extract 5%,
Peony extract 3%, Rosmarinus officinalis extract 3%, horse chestnut extract 3%, laureth sodium sulfovinate 10%, coconut oleoyl amine
Propyl betaine 5%, Trivent OCG 5%, moisturizer sorbierite 2%, citric acid 1%, chelating agent EDETATE SODIUM 0.3%,
Vitamin C 0.3%, remaining is deionized water.
Preparation method includes the following steps：
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) laureth sodium sulfovinate, Cocoamidopropyl betaine and Trivent OCG are mixed, is added
Heat and be stirred to 70~75 DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) hamamelis extract, nettle extract, peony extract, rosemary are finally added into mixture C to carry
Object, horse chestnut extract, citric acid, vitamin C is taken to stir evenly.
In addition, the present invention also provides a kind of hair conditioner of the draft Haircare composition of extract containing hamamelis, respectively
The quality of component is：Hamamelis extract, nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extraction
The mixing draft Haircare composition of object, cetostearyl alcohol 9~11%, fatty alcohol polyoxyethylene ether 7.5~8.5%, sorbierite 1.8
~2.2%, citric acid 0.9~1.1%, chelating agent EDETATE SODIUM 0.25~0.35%, vitamin C 0.25~0.35%, remaining
For deionized water；
With weight ratio meter, draft Haircare composition accounts for the 20~35% of hair conditioner total amount；
In the draft Haircare composition, hamamelis extract, nettle extract, peony extract, rosemary carry
It is 6~12 to take the mass ratio of object and horse chestnut extract：4~8：3~5：2~4：3~6.
Furthermore, it is preferred that the hair conditioner, the quality of each component are：Hamamelis extract 10%, nettle extract
5%, peony extract 3%, Rosmarinus officinalis extract 3%, horse chestnut extract 3%, cetostearyl alcohol 10%, fatty alcohol polyoxy second
Alkene ether 8%, sorbierite 2%, citric acid 0.9~1.1%, chelating agent EDETATE SODIUM 0.3%, vitamin C 0.3%, remaining is to go
Ionized water.
2, preparation method
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) by cetostearyl alcohol, fatty alcohol polyoxyethylene ether, sorbierite mixes, heats and be stirred to 70~75
DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) hamamelis extract, nettle extract, peony extract, rosemary are finally added into mixture C to carry
Object, horse chestnut extract, citric acid, vitamin C is taken to stir evenly.
Compared with prior art, the present invention has the advantages that：
Draft Haircare composition provided by the invention include hamamelis extract, nettle extract, peony extract,
Rosmarinus officinalis extract and horse chestnut extract, are compounded by reasonably optimizing, and apparent synergistic effect can be generated, can be with
Applied in various hair care products, having the function of nourishing strengthen the hair, performance is mild, and raw material is easy to get, and preparation process is simple, tool
There is good application prospect.
The draft Haircare composition is applied to hair dyeing product, gained hair dyeing product can reduce the stimulation in hair dye
Quick property effectively prevent scalp allergy, and hair dyeing effect and persistence are good, and hair dyeing while can also repair hair quality；Applied to hair care
Product, products obtained therefrom such as hair conditioner is non-stimulated to scalp, strong to the repair of hair quality；Applied to hair washing product, products obtained therefrom
Such as shampoo, anti-dandruff and itching-relieving effect is good, and without side-effects.
Description of the drawings
Fig. 1 is that hair dyeing is preceding to be compared with aberration after hair dyeing.
Fig. 2 is each group project hair cross section color fastness disparity map after processing.
Fig. 3 is to add the processed hair of cream rinse (embodiment 1) of herbaceous plant extract and be not added with herbaceous plant
The processed hair of cream rinse (reference examples) SEM of extract schemes.
Fig. 4 cream rinses process the cystine analysis in topknot.
Specific implementation mode
The present invention is made with specific embodiment with reference to the accompanying drawings of the specification and further being elaborated, the embodiment
It is served only for explaining the present invention, be not intended to limit the scope of the present invention.Test method used in following embodiments is such as without spy
Different explanation, is conventional method；Used material, reagent etc., unless otherwise specified, for the reagent commercially obtained
And material.
The cream rinse of the draft Haircare composition of 1 extract containing hamamelis of embodiment
1, the cream rinse of the draft Haircare composition of a kind of extract containing hamamelis
The mass ratio of each component is：Hamamelis extract 10%, nettle extract 5%, peony extract 3%, fan
Repeatedly fragrant extract 3%, horse chestnut extract 3%, thickener cetostearyl alcohol 10%, pH adjusting agent monoethanolamine and aminomethyl third
Alcohol mass ratio 1:1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2:1 mixture
0.50%, emulsifier ceteareth -20 and stearine mass ratio are 2:1 mixture 3%, conditioner for hair
Triglyceride DDD 0.50%, hair colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminobenzene oxygen second
Alcohol and 2- amino -3- pyridone mass ratioes are 20:6:3:1 mixture 2%, moisturizer propylene glycol, chelating agent EDTA- disodiums
0.3%, remaining is deionized water.
2, preparation method
(1) moisturizing reagent propylene glycol and chelating agent EDTA- disodiums are added in ionized water, heats while stirring, until this
After the temperature of mixture is to 80~85 DEG C to component all fusing, stop heating and stirring, the mixture A stirred evenly；
(2) it is 2 by thickener cetostearyl alcohol, emulsifier ceteareth -20 and stearine mass ratio：
1 mixture and conditioner Triglyceride DDD mixes, heat and be stirred to 80~85 DEG C to component all fusing after
Stop heating and stirring, the mixture B stirred evenly；
(3) by colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino-
3- pyridone mass ratioes are 20:6:3:1 mixture and antioxidant sodium sulfite and sodium isoascorbate mass ratio is 2：1
Mixture be uniformly mixing to obtain mixture C；
(4) mixture B and mixture C are added into mixture A, stirs evenly so that mixture A, B, C is fully emulsified to be obtained
To mixture D；
(5) hamamelis extract, nettle extract, peony extract, rosemary are finally added into mixture D to carry
Take object, horse chestnut extract, pH adjusting agent monoethanolamine and aminomethyl propanol mass ratio 1:1 mixture, stirs evenly.
The cream rinse of the draft Haircare composition of 2 extract containing hamamelis of embodiment
1, the cream rinse of the draft Haircare composition of a kind of extract containing hamamelis
The quality of each component is：Hamamelis extract 6%, nettle extract 4%, peony extract 5%, rosemary
Extract 4%, horse chestnut extract 4%, thickener cetostearyl alcohol 10%, pH adjusting agent monoethanolamine and aminomethyl propanol matter
Measure ratio 1:1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2:1 mixture 0.50%, breast
Agent ceteareth -20 and stearine mass ratio are 2:1 mixture 3%, conditioner for hair capric acid glycerine
Three esters 0.50%, hair colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- ammonia
Base -3- pyridone mass ratioes are 20:6:3:1 mixture 2%, moisturizer propylene glycol, chelating agent EDTA- disodiums 0.3%,
Remaining is deionized water.
2, preparation method
With embodiment 1.
The cream rinse of the draft Haircare composition of 3 extract containing hamamelis of embodiment
1, a kind of cream rinse of the draft Haircare composition of hamamelis extract
The quality of each component is：Hamamelis extract 12%, nettle extract 8%, peony extract 2%, fan change
Fragrant extract 2%, horse chestnut extract 6%, thickener cetostearyl alcohol 10%, pH adjusting agent monoethanolamine and aminomethyl propanol
Mass ratio 1:1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2:1 mixture 0.50%,
Emulsifier ceteareth -20 and stearine mass ratio are 2:1 mixture 3%, conditioner for hair capric acid are sweet
Oily three esters 0.50%, hair colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2-
Amino -3- pyridone mass ratioes are 20:6:3:1 mixture 2%, moisturizer propylene glycol, chelating agent EDTA- disodiums 0.3%,
Remaining is deionized water.
2, preparation method
With embodiment 1.
Comparative example
1, a kind of cream rinse
The quality of each component is：Thickener cetostearyl alcohol 10%, pH adjusting agent monoethanolamine and aminomethyl propanol quality
Than 1:1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2:1 mixture 0.50%, emulsification
Agent ceteareth -20 and stearine mass ratio are 2:1 mixture 3%, conditioner for hair capric acid glycerine three
Ester 0.50%, hair colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino-
3- pyridone mass ratioes are 20:6:3:1 mixture 2%, moisturizer propylene glycol, chelating agent EDTA- disodiums 0.3%, remaining
For deionized water.
2, preparation method
With 1 preparation method of embodiment (1)~(4).
The hair dyeing effect of the cream rinse of the draft Haircare composition of 4 extract containing hamamelis of embodiment is tested
1, experiment packet
It is first group, second group, third group that cream rinse made from Examples 1 to 3 is compiled respectively, while not add draft
Extract as a control group, chooses 120 volunteers, it is a group to compile for every 30, corresponds to this 4 groups respectively.
2, it operates
The cream rinse prepared respectively using said program to these volunteers is tested, and test method is sensory testing,
Respectively to the bright-coloured degree of the hair-dyeing of volunteer (being divided into very bright-coloured, more bright-coloured, common three indexs), dye uniformity
Whether (being divided into highly uniform, relatively uniform, common three indexs), scalp have sensation, (are divided into very using rear compliance
Submissive, submissiveer, common three indexs) it votes as index.
3 results
Voting results are as shown in table 1.
Table 1：
Show that hair dyeing effect, the irritation of the cream rinse of addition herbal essences are better than un-added by table 1；Embodiment 1 contaminates
The coloring of hair cream, irritation are better than what other ratios combined, and especially dye uniformity is best.
The color fastness of the cream rinse of the draft Haircare composition of 5 extract containing hamamelis of embodiment measures
1, it operates
By natural hair sample, it is divided into 4 beams by identical quality, complete wetting is in 60ml 5% (w/v) embodiment 1 respectively
~3 and comparative example cream rinse solution in, be placed in water-bath constant temperature oscillator and wash 3min and take out, rinsed to dry with tap water
Only, hair is dried up with hair-dryer.Each group of sample passes through the test of 60 shampoo washes and color fastness.
Evaluation method：The test of color fastness after being had hair dyed with color difference meter.By test and calculate hair dyeing before and hair dyeing after
Aberration (Δ E values average value), the color fastness after evaluation hair dyeing, Δ E numerical value is smaller, shows that the aberration for cleaning front and back hair dyeing is smaller,
Color fastness after hair dyeing is better.
2, result
It is shown according to Fig. 1, the cream rinse aberration for not adding draft combination is maximum, and color fastness is worst；With 1 North America of embodiment gold
The mass ratio of thread prunus mume extract/nettle extract/peony extract/Rosmarinus officinalis extract/horse chestnut extract is 10：5：3：3：
The dyeing cream aberration of 3 combinations is minimum, and color fastness is best.
The hair quality of the cream rinse of the draft Haircare composition of 6 extract containing hamamelis of embodiment measures
As Fig. 2 and Fig. 3 are shown by the way that with the processed topknot surface of electron microscope observation, observation hair surface is damaged face
Reparation degree, addition the processed hair surface hair scale piece of herbaceous plant extractant it is smooth, and be not added with herbaceous plant extraction
The processed hair surface of agent does not have protection effect, the damage of hair scale piece to tilt, and damage is more serious.
The irritant experiment of the cream rinse of the draft Haircare composition of 7 extract containing hamamelis of embodiment
It has chosen 400 rabbit and carries out irritant experiment, rabbit is before experiment for 24 hours in the cropping of back both sides, unhairing range
In 3cm*6cm, divides 4 groups, every group 100, take cream rinse 0.1ml, be coated on the skin of the area of 2.5cm*2.5cm, then use
One layer of oilpaper covering, immobilization with adhesive tape, the other side is smeared with control group.Cream rinse is being removed for 24 hours, observes skin irritatin situation.
Evaluation criterion refers to version in 2015《Cosmetics safety technical specification》, skin allergic reaction experiment, skin irritatin is anti-
Standard is answered specifically to be shown in Table 2, skin irritatin intensity evaluation standard is shown in Table 3.
Table 2：
Table 3：
| Stimulus intensity | Score value |
| It is nonirritant | 0-0.4 |
| Subexcite | 0.5-1.9 |
| Medium irritation | 2-5.9 |
| Strong and stimulating | 6-8 |
As a result it shows：Cream rinse prepared by the present invention is due to being added to herb extract, and each component produces in extract
Apparent synergistic effect, effectively reduces the stimulation degree to scalp, and safe to use, and health effectively, makes hair healthier, together
When have the function of hair care.Wherein hamamelis extract/nettle extract/peony extract/Rosmarinus officinalis extract/horse chestnut
The mass ratio of extract is 10：5：3：3：3 combination it is best.
Table 4：
| Test event | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example |
| Erythema forms (total score) | 0 | 21 | 37 | 251 |
| Oedema forms (total score) | 0 | 9 | 15 | 199 |
| Average total mark | 0 | 0.30 | 0.52 | 4.50 |
| Stimulus intensity | Nothing | Nothing | Gently | It is medium |
The stability of the cream rinse of the draft Haircare composition of 8 extract containing hamamelis of embodiment
By test, hair care dying cream of the present invention is kept for 72 hours at a temperature of 40 ± 2 DEG C, without grease after recovery room temperature
Segregation phenomenon；It is kept for 72 hours at a temperature of -10 ± 2 DEG C, without water-oil separating phenomenon after recovery room temperature.
Therefore, it in hair dye, is easy to be applied to hair, it is not easy to generate dropping liquid, will not trickle, skin will not be infected with
And clothes.
The optimization of 9 herb composition of embodiment
1, experiment packet
It is compounded as variable (as shown in table 5) with the different component of herb composition, remaining reference implementation example 1 prepares a series of
Cream rinse.
That is the draft hair care component total amount of cream rinse is identical, and specific compounded combination and mass content are shown in Table 5.And cream rinse
Non- draft hair care component is identical, is thickener cetostearyl alcohol 10%, pH adjusting agent monoethanolamine and aminomethyl propanol quality
Than 1:1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2:1 mixture 0.50%, emulsification
Agent ceteareth -20 and stearine mass ratio are 2:1 mixture 3%, conditioner for hair capric acid glycerine three
Ester 0.50%, hair colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino-
3- pyridone mass ratioes are 20:6:3:1 mixture 2%, moisturizer propylene glycol, chelating agent EDTA- disodiums 0.3%, remaining
For deionized water.
Table 5：
2, experimental method
(Jia Zebao, Xu Debiao, Wu Shuiping wait the research [J] of the impaired method of amino acid systems evaluation hair days to reference papers
With chemicals science, 2013,36 (5):Method 30-33.), the hair dyeing taken care of hair containing draft to difference with high performance liquid chromatograph
The cystine that cream processes in topknot is analyzed, normally as a contrast without the hair of cream rinse processing.
Concrete operations：It by natural hair sample, is grouped by identical quality, complete wetting is in 60ml5% (w/v) table respectively
In the cream rinse solution of 5 combinations, it is placed in water-bath constant temperature oscillator and washs 3min taking-ups, rinsed to clean with tap water；It will be every
Hair after group dyeing is washed by 60 clear water, after natural drying for use.
3, result
It is shown (Fig. 4) according to result, the Guang in the processed topknot of cream rinse of the 21st group of the Haircare composition containing draft
Histidine content highest, i.e. hamamelis extract/nettle extract/peony extract/Rosmarinus officinalis extract/horse chestnut extraction
The mass ratio of object is 10：5：3：3：The cystine highest of 3 combinations, matches the cream rinse being prepared, repairs the effect of hair quality
Fruit is best.Illustrate that the draft combination of the extract containing hamamelis has and nourishes scalp, hair care effect.
A kind of shampoo of the draft Haircare composition of 10 extract containing hamamelis of embodiment
1, a kind of shampoo of the draft Haircare composition of hamamelis extract
The quality of each component is：Hamamelis extract 10%, nettle extract 5%, peony extract 3%, fan change
Fragrant extract 3%, horse chestnut extract 3%, laureth sodium sulfovinate 10%, Cocoamidopropyl betaine 5%, octanoic acid
Triglycerides 5%, moisturizer sorbierite 2%, citric acid 1%, chelating agent EDETATE SODIUM 0.3%, vitamin C 0.3%, remaining
For deionized water.
2, preparation method
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) laureth sodium sulfovinate, Cocoamidopropyl betaine and Trivent OCG are mixed, is added
Heat and be stirred to 70~75 DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) hamamelis extract, nettle extract, peony extract, rosemary are finally added into mixture C to carry
Object, horse chestnut extract, citric acid, vitamin C is taken to stir evenly.
A kind of shampoo of the draft Haircare composition of 11 extract containing hamamelis of embodiment uses sensory evaluation
60 volunteers, unlimited gender are chosen, the age between 16~65 years old, divides 2 groups, every group of 30 people.It uses respectively real
Apply the shampoo of example 10 and control group (not adding any draft combination).
1, it operates
Two groups are recorded respectively using the impressions after shampoo, with hair washing process whether have eye irritation, scalp whether spinosity
Excitation feels that the moist degree using rear compliance (being divided into very submissive, submissiveer, common three degree) and hair (is divided
Moistened, commonly to moisten very much, comparing), sensory experience is basis for estimation.
2, result
Statistical result is shown in Table 6.
Table 6：
It can be obtained by table 6, the shampoo of the draft combination of the extract containing hamamelis has low stimulation, can make hair
It easily combs, moistens the effect of hair care.
A kind of hair conditioner of the draft Haircare composition of 12 extract containing hamamelis of embodiment
1, the hair conditioner of the draft Haircare composition of a kind of extract containing hamamelis
The quality of each component is：Hamamelis extract 10%, nettle extract 5%, peony extract 3%, fan change
Fragrant extract 3%, horse chestnut extract 3%, cetostearyl alcohol 10%, fatty alcohol polyoxyethylene ether 8%, sorbierite 2%, lemon
Acid 1%, chelating agent EDETATE SODIUM 0.3%, vitamin C 0.3%, remaining is deionized water.
2, preparation method
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) by cetostearyl alcohol, fatty alcohol polyoxyethylene ether, sorbierite mixes, heats and be stirred to 70~75
DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) hamamelis extract, nettle extract, peony extract, rosemary are finally added into mixture C to carry
Object, horse chestnut extract, citric acid, vitamin C is taken to stir evenly.
A kind of hair conditioner skin allergic reaction of the draft Haircare composition of 13 extract containing hamamelis of embodiment is surveyed
Examination
According to Ministry of Health of the People's Republic of China《The 6th chapter of cosmetics health specification second part：Skin allergic reaction tries
It tests》.
1, operating method
80 Albino guinea pigs are taken, are randomly divided into 2 groups, every group 40, one group is embodiment 12, and one group is control group.It will be every
Unhairing on the left of guinea pig back, area are 4~6cm2, to going gross area to use 95% alcohol disinfecting, cover 5 layers of about 8cm2Drop
The lens wiping paper for adding appropriate amount of sample leaching liquor makes it stick on shoulder blade inside skin, then covers the plastics of 3*3cm sizes successively
Film, gauze, then being fixed with medical non-stimulated adhesive tape makes it not fall off closing fixation for 24 hours.
Control group is the hair conditioner for not adding draft combination.
Evaluation method carries out integral statistics by the experiment dermoreaction grading of 7 allergy of table, when tested material group animal occurs
When dermoreaction integral >=2, it is judged to the animal and the skin allergic reaction positive occurs, the sensitization intensity of tested material is judged by table 8.
Table 7：
Table 8：
| Sensitization intensity | Sensitization rate % |
| It is weak | 0~8 |
| Gently | 9~28 |
| In | 29~64 |
| By force | 65~80 |
| It is extremely strong | 81~100 |
2, result
It can show that the hair conditioner that the draft of addition extract containing hamamelis combines can reduce scalp sensitization by table 9,
The effect that anti-anaphylaxis is releived.
Table 9：Test result
| Test event | Embodiment 12 | Control group |
| Dermoreaction integral >=2 | 0 | 33 |
| Sensitization rate % | 0 | 82.5% |
| Sensitization intensity | Nothing | It is extremely strong |
In conclusion the herb composition of extract containing hamamelis is applied in various hair products, can generate
Synergistic effect has and moistens well, protection scalp, repairs damaged hair, and without side-effects；It especially applies in hair dyeing product
In, there is good color fastness.
Claims (10)
1. a kind of draft Haircare composition of extract containing hamamelis, which is characterized in that containing hamamelis extract,
Nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extract.
2. draft Haircare composition according to claim 1, which is characterized in that hamamelis extract, nettle extract,
Peony extract, Rosmarinus officinalis extract and horse chestnut extract quality ratio are 6~12：4~8：3~5：2~4：3~6.
3. draft Haircare composition according to claim 2, which is characterized in that hamamelis extract, nettle extract,
The mass ratio of peony extract, Rosmarinus officinalis extract and horse chestnut extract is 10：5：3：3：3.
4. application of any draft Haircare composition of claims 1 to 3 in preparing hair care product.
5. a kind of hair care product containing any draft Haircare composition of claims 1 to 3.
6. hair care product according to claim 5, which is characterized in that the hair care product is hair dyeing product, shield
Send out product, hair washing product or hair jelly.
7. a kind of cream rinse containing any draft Haircare composition of claims 1 to 3, which is characterized in that with weight ratio
Meter, any draft Haircare composition of claims 1 to 3 account for the 20~35% of cream rinse total amount.
8. cream rinse according to claim 7, which is characterized in that with weight ratio meter, the cream rinse also contain thickener 8~
10%, pH adjusting agent 2~2.50%, antioxidant 0.50~0.80%, emulsifier 3~4%, conditioner for hair 0.5~1%, hair
Toner 2~3%, moisturizer 1~2%, chelating agent 0.1~0.5%, remaining is deionized water.
9. a kind of shampoo containing any draft Haircare composition of claims 1 to 3, which is characterized in that with weight ratio
Meter, each group are divided into：Hamamelis extract, nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extract
Mixing draft Haircare composition, laureth sodium sulfovinate 9~11%, Cocoamidopropyl betaine 4.5~5.5% is pungent
Acid glycerol three ester 4~6%, moisturizer sorbierite 1.8~2.2%, citric acid 0.9~1.1%, chelating agent EDETATE SODIUM 0.25~
0.35%, vitamin C 0.25~0.35%, remaining is deionized water；Wherein, draft Haircare composition accounts for shampoo gross mass
20~30%；In the draft Haircare composition, hamamelis extract, nettle extract, peony extract, rosemary carry
It is 6~12 to take the mass ratio of object and horse chestnut extract：4~8：3~5：2~4：3~6.
10. a kind of hair conditioner containing any draft Haircare composition of claims 1 to 3, which is characterized in that with weight
Than meter, each group is divided into：Hamamelis extract, nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extraction
The mixing draft Haircare composition of object, cetostearyl alcohol 9~11%, fatty alcohol polyoxyethylene ether 7.5~8.5%, sorbierite 1.8~
2.2%, citric acid 0.9~1.1%, chelating agent EDETATE SODIUM 0.25~0.35%, vitamin C 0.25~0.35%, remaining for go from
Sub- water；Wherein, draft Haircare composition accounts for the 20~35% of hair conditioner gross mass；In the draft Haircare composition, North America gold thread
Prunus mume extract, nettle extract, peony extract, Rosmarinus officinalis extract and horse chestnut extract mass ratio be 6~12：4~
8：3~5：2~4：3~6.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114732768A (en) * | 2022-04-21 | 2022-07-12 | 广州帝臣生物科技股份有限公司 | Anti-dandruff shampoo |
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| CN107375131A (en) * | 2017-07-17 | 2017-11-24 | 武汉爱民制药股份有限公司 | The anti-dandruff hair care shampoo of plant containing Ba 2672 |
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| CN1452477A (en) * | 2000-05-30 | 2003-10-29 | 宝洁公司 | Hair conditioning composition comprising frizz control agent |
| CN102908272A (en) * | 2012-09-27 | 2013-02-06 | 张小文 | Scurf-removal and anti-hair loss shampoo |
| CN105434220A (en) * | 2015-11-26 | 2016-03-30 | 澳宝化妆品（惠州）有限公司 | Hair washing composition containing peony extract |
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