CN107375131A - The anti-dandruff hair care shampoo of plant containing Ba 2672 - Google Patents

The anti-dandruff hair care shampoo of plant containing Ba 2672 Download PDF

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CN107375131A
CN107375131A CN201710580271.2A CN201710580271A CN107375131A CN 107375131 A CN107375131 A CN 107375131A CN 201710580271 A CN201710580271 A CN 201710580271A CN 107375131 A CN107375131 A CN 107375131A
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dandruff
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hair
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CN107375131B (en
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耿鹏飞
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Wuhan Aimin Pharmaceutical Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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    • A61K8/416Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/4913Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/737Galactomannans, e.g. guar; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

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Abstract

The invention belongs to daily chemical product field, specifically disclose a kind of anti-dandruff hair care shampoo of plant containing Ba 2672, the shampoo contains surfactant, cationic conditioning agent, pearling agent, NMF, thickener, siloxanes, plant extraction liquid, pH adjusting agent, foam stabilizer, scalp conditioning agent, thinner, chelating agent and preservative etc., described plant extraction liquid is Ba 2672, and coordinate Chinese honey locust seed extract, gadol extract, lemon grass leaf oil, Radix Platycodonis extract, radix codonpsis tangshen root extract, common cnidium fruit P.E, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, cryptomeria leaf extract, Cacumen Platycladi extract, red sage root root extract, any three kinds in camellia seed extract etc..The present invention improves scalp microcirculation using Ba 2672, promotes the mechanism of scalp metabolism, then coordinates various plants elite, fundamentally improves dandruff, head is itched, hair oil problem, nourishes hair and scalp, reaches the effect of long-term anti-dandruff hair care.

Description

The anti-dandruff hair care shampoo of plant containing Ba 2672
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of anti-dandruff hair care hair washing of the plant containing Ba 2672 Dew.
Background technology
Because environmental pollution aggravates, operating pressure increases, and the factors such as rhythm of life is accelerated, increasing people feels to the end Skin itch, dandruff increase.Long-term use of shampoo is that people solve the problems, such as the main selection of dandruff, but popular big on the market Most shampoos are only mixed by compound, and long-term use can cause hair quality withered and yellow, easily broken, easy to fall off.So people are more next More need it is a kind of effectively it is anti-dandruff, nourish hair shampoo go solve such issues that.
The main active of horse chestnut is Ba 2672, is a kind of triterpene saponin compound.Otoginsenoside can press down System destroys the activity of the enzyme (such as Collagenase, hyaluronidase and elastoser) of vein integrality, can safeguard blood vessel Balance, promote scalp blood circulation, provide various nutrients for scalp, enhance metabolism, also have for dandruff dermatitis Good effect, long-term use can make scalp more healthy, improve the vitality of hair.Soap is coordinated with rare Ba 2672 Pod seed extract, gadol extract, lemon grass leaf oil extract, Radix Platycodonis extract, radix codonpsis tangshen root extract, frutus cnidii carry Take thing, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, cryptomeria leaf extract, Cacumen Platycladi extract, red sage root root extract, camellia seed Extract, sarranine flower extract, ginseng extract, plant essence auxotype shampoo does not appear in the newspapers made of dendrobium candidum extract Road mistake.
The content of the invention
It is an object of the invention to provide a kind of anti-dandruff hair care shampoo of plant containing Ba 2672, containing traditional Chinese medicine ingredients Plant extraction liquid, by effectively match can relieving itching and removing dandruff, scalp is nourished in conditioning, long-term use of, can make scalp health, and hair quality is black It is bright submissive.
To achieve these goals, the present invention adopts the following technical scheme that:
The anti-dandruff hair care shampoo of plant containing Ba 2672, is made up of the raw material of following percentage by weight:
Described surfactant is laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, methyl cocoyl ox sulphur Any 3 kinds or 4 kinds of combination in sour sodium and cocaminopropionic acid sodium, Cocoamidopropyl betaine;
Described cationic conditioning agent is Polyquaternium-10, hydroxypropyl guar hydroxypropyltrimonium chloride and two palm fibres Any a kind in palmitic acid acyloxyethyl alkyl dimethyl ammonium chloride, or 3 kinds of combination;
Described pearling agent is glycol distearate;
Described NMF is the combination of glycine betaine and pyrrolidone sodium carboxylate;
Described thickener is a kind in coconut oleoyl amine MEA and sodium chloride, or 2 kinds of combination;
Described siloxanes is the combination of dimethyl silicone polymer and ammonia end dimethyl silicone polymer;
Described plant extraction liquid is Ba 2672, and coordinates Chinese honey locust seed extract, gadol extract, lemon grass Leaf oil, Radix Platycodonis extract, radix codonpsis tangshen root extract, common cnidium fruit P.E, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, cryptomeria leaf Extract, Cacumen Platycladi extract, red sage root root extract, camellia seed extract, sarranine flower extract, ginseng extract, iron sheet stone Any 3 kinds in dry measure used in former times extract;
Described PH conditioning agents are citric acid;
The foam stabilizer is two (hydrogenated-tallow group) phthalic acid amides;
Described scalp conditioning agent is any a kind or 2 kinds in polyethylene glycol -14M, cetanol, PPG-3 Octyl Ethers;
Described thinner is ammonium xylene sulfonate;
Described chelating agent is EDETATE SODIUM;
Described preservative is hexamidine two (isethionic acid) salt, methylchloroisothiazandnone and methylisothiozoline Any 3 kinds of combination in ketone, piroctone olamine salt;
Described aromatic is essence.
The anti-dandruff hair care shampoo of plant containing Ba 2672 (no silicone oil), by the raw material system of following mass percent Into:
The plant extraction liquid is Ba 2672, sarranine flower extract, ginseng extract, four kinds of dendrobium candidum extract Combination.
Ba 2672 is made by following methods in the above-mentioned anti-dandruff hair care shampoo of the plant containing Ba 2672:
1) buckeye crushes in pulverizer, sieving;
2) according to buckeye and 30-70% ethanol volume ratio 1:10 ratio, buckeye, 30-70% ethanol are added to carrying Take in tank, be warming up to 55-60 DEG C of stirring 1.5-2h, filter, collect filtrate;
3) filter residue extracts again according to the method described above, merges extract solution twice, be concentrated under reduced pressure into 50-60 DEG C alcohol content≤ 7%;Concentrate is diluted to 8-10 times of volume with purified water, is warming up to 40 DEG C -45 DEG C upper macroporous resin adsorptions;
4) respectively with water, 30-50% ethanol elution impurity, then with 50-75% ethanol elution working substances, eluent is collected;
5) eluent is concentrated in clean area, temperature control is concentrated into the 1/10 of original volume at 55-60 DEG C;
6) concentrate is dried under vacuum to dry in clean area.
Above-mentioned raw materials effectively proportioning has rapid flocculation, can significantly improve the functioning efficiency of cationic conditioning agent, subtract The side effects such as gently accumulation seriously produces scalp as caused by conditioning agent, head is itched;Cationic conditioning agent selection Polyquaternium-10, Hydroxypropyl guar hydroxypropyltrimonium chloride and two palm acyloxyethyl alkyl dimethyl ammonium chlorides, can make hair quality soft, smooth, It is heavy, tacky and send out withered etc. and negatively affect to eliminate hair;NMF chooses glycine betaine and Anjidew NL50 (pyrrolidone sodium carboxylate), has Help improve the moist degree of hair;Described plant extraction liquid is Ba 2672, and coordinates Chinese honey locust seed extract, rhodiola root to carry Take thing, lemon grass leaf oil;Radix Platycodonis extract, radix codonpsis tangshen root extract, common cnidium fruit P.E;Radix-polygoni multiflori extract, Semen sesami nigrum Extract, cryptomeria leaf extract, Cacumen Platycladi extract, red sage root root extract, camellia seed extract, sarranine flower extract, ginseng Any 3 kinds of compositions in extract, dendrobium candidum extract, energy deep layer nourish scalp and hair, reach the effect of long-term anti-dandruff hair care Fruit.
Compared with prior art, the present invention has advantages below and beneficial effect:
The present invention coordinates the hair washing of plant extraction liquid to combine using Ba 2672, according to test result indicates that can effectively press down Dandruff generation processed, is combined different from other hair washings only mixed by chemical composition, and plant hair care of the invention combination can deep layer taste Support hair and scalp.
Brief description of the drawings
Fig. 1 is the fungistatic effect of the anti-dandruff hair care shampoo of the plant containing Ba 2672.A is the hair washing group of embodiment 1 The fungistatic effect of conjunction, B are the fungistatic effect of the hair washing combination of comparative example 1.
Embodiment
The source explanation of primary raw material in the embodiment of the present invention:Chinese honey locust seed extract, rhodiola root extraction in plant extraction liquid Thing, Radix Platycodonis extract, radix codonpsis tangshen root extract, common cnidium fruit P.E, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, cryptomeria leaf carry Take thing, Cacumen Platycladi extract, red sage root root extract, camellia seed extract, sarranine flower extract, ginseng extract, dendrobium candidum Extract is purchased from Huzhou Jiamei Biochemical Products Co., Ltd., and lemon grass leaf oil is purchased from Hugezeal Bio- chemical Australia Inc。
Embodiment 1:
The anti-dandruff hair care shampoo of plant containing Ba 2672, is prepared by following raw materials according:
Described surfactant is laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, methyl cocoyl ox sulphur The combination of four kinds of sour sodium, Cocoamidopropyl betaine compositions;
Described cationic conditioning agent is Polyquaternium-10, hydroxypropyl guar hydroxypropyltrimonium chloride, two palms The combination of three kinds of compositions of acyloxyethyl alkyl dimethyl ammonium chloride;
Described pearling agent is glycol distearate;
Described NMF is glycine betaine and pyrrolidone sodium carboxylate (Anjidew NL50);
Described thickener is the combination of two kinds of compositions of coconut oleoyl amine MEA and sodium chloride;
Described siloxanes is the combination of dimethyl silicone polymer and ammonia end dimethyl silicone polymer;
Described plant extraction liquid is Ba 2672, Chinese honey locust seed extract, gadol extract and lemon grass leaf oil The combination of four kinds of compositions;
Described PH conditioning agents are citric acid, and PH is adjusted to 5.5-6.0;
Described foam stabilizer is two (hydrogenated-tallow group) phthalic acid amides;
Described scalp conditioning agent is polyethylene glycol -14M;
Described thinner is ammonium xylene sulfonate;
Described chelating agent is EDETATE SODIUM;
Described preservative is hexamidine two (isethionic acid) salt, methylchloroisothiazandnone and methylisothiazolinone The combination of three kinds of compositions;
Described aromatic is Robert's essence and flavoring agent.
The plant extraction liquid of the present embodiment is Ba 2672, Chinese honey locust seed extract, gadol extract and lemon grass Leaf oil.Ba 2672 can help improve scalp microcirculation, nourish root of hair, play maintenance effect, contribute to hair healthy to grow; Chinese honey locust seed extract, which is used for shampoo, has the function that anti-dandruff and itching-relieving, clean hair hair care;Gadol extract is formed in hair surface Protective layer is moistened, prevents the injury of external environment condition, hair moisture is balanced, repairs impaired hair epidermis, prevent in hair The loss of protein and moisture and hair tip jag and fracture, make the submissive health of healthy hair, and soft non-stimulated;Lemon grass leaf oil Help to improve slim and frahile hair quality, promote scalp circulation.Effective proportioning of these plant essence things has hair care and nourishing, anti-dandruff submissive Effect.
The preparation technology of Ba 2672 is as follows in above-mentioned plant extraction liquid:
1. buckeye crushes in pulverizer, 10 mesh sieves are crossed;
2. according to buckeye and 30%-70% ethanol volume ratio 1:10 ratio, add buckeye, 30-70% ethanol arrives In extractor, 55-60 DEG C of stirring 1.5-2h is warming up to, mixing speed is 50-75 revs/min, filters, collects filtrate;
3. filter residue extracts again according to the method described above, merge extract solution twice, be concentrated under reduced pressure into 50-60 DEG C alcohol content≤ 7%;Concentrate is diluted to 8-10 times of volume with purified water, is warming up to 40 DEG C -45 DEG C upper macroporous resin adsorptions;
4. using water and 30%-50% ethanol elution impurity respectively, with 50%-75% ethanol elution working substances, elution is collected Liquid;
5. eluent is concentrated in clean area, temperature control is concentrated into the 1/10 of original volume at 55-60 DEG C;
6. concentrate is dried under vacuum to dry in clean area;Packaging material sterilizes, filling storage.
Preferably, in step 2, extracted with 70% ethanol solution.
Preferably, the macroreticular resin model HPD100 described in step 3.
Preferably, step 4 uses water and 30% ethanol elution impurity successively, then with 75% ethanol elution working substance.
The preparation method of the above-mentioned anti-dandruff hair care shampoo of the plant containing Ba 2672, its step are:
Raw material and proportioning are as follows:
1. each raw material is weighed according to the above ratio;
2. A phases raw material is added in agitated kettle, 50-60 degree is warming up to, insulated and stirred (speed is 100 revs/min) is extremely molten Solution is complete;
3. again add B phases raw material in above-mentioned agitated kettle one by one, 70-75 degree is warming up to, to dissolving completely, (speed is for stirring 80 revs/min);
4. C phases raw material is added in above-mentioned agitated kettle one by one, 80-85 degree, 40 minutes (speed 80 of insulated and stirred are warming up to Rev/min) complete to dissolving;
5. cooling to 70-75 degree adds D phases, stirring is to being completely dissolved (speed is 80 revs/min);
Stirred 6. cooling to 50-55 degree and adding E phases to being completely dissolved (speed be 60 revs/min);
7. cooling to the mixture of less than 45 degree plus F phases, stirring 30 minutes (speed is 60 revs/min) is stirred to completely molten Solution.
Embodiment 2
The anti-dandruff hair care shampoo of plant containing Ba 2672, is prepared by following raw materials according:
Raw material components Percentage by weight
Deionized water 69.015%
Surfactant 23.5%
Cationic conditioning agent 0.6%
Pearling agent 1.6%
NMF 1.7%
Thickener 1.4%
Siloxanes 1.1%
Plant extraction liquid 0.155%
PH conditioning agents 0.1%
Scalp conditioning agent 0.1%
Thinner 0.1%
Chelating agent 0.1%
Preservative 0.03%
Aromatic 0.5%
Described surfactant is by laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, methyl cocoyl ox sulphur The combination of sour three kinds of compositions of sodium;Described plant extraction liquid is Ba 2672, Radix Platycodonis extract, radix codonpsis tangshen root extract, snake The combination of four kinds of compositions of machine tool extract;Other raw materials are identical with the composition of embodiment 1.
The plant extraction liquid of the present embodiment is Ba 2672, Radix Platycodonis extract, radix codonpsis tangshen root extract, frutus cnidii extraction Thing.Ba 2672 and Radix Platycodonis extract all contain saponins compound, and penetrating power is good, there is the effect of removing grease;Snake Machine tool extract, which is used for shampoo, has the function that anti-dandruff and itching-relieving.Effective proportioning of these plant essence things has hair care and nourishing, The effect of anti-dandruff maintenance.
The preparation method of the above-mentioned anti-dandruff hair care shampoo of the plant containing Ba 2672 is the same as embodiment 1, specific raw material And proportioning is as follows:
Embodiment 3
The anti-dandruff hair care shampoo of plant containing Ba 2672, is prepared by following raw materials according:
Raw material components Percentage by weight
Deionized water 74.265%
Surfactant 18%
Cationic conditioning agent 1.5%
Pearling agent 1.6%
Foam stabilizer 2%
NMF 0.5%
Thickener 0.2%
Siloxanes 1.1%
Plant extraction liquid 0.155%
PH conditioning agents 0.05%
Scalp conditioning agent 0.1%
Thinner 0.2%
Chelating agent 0.1%
Preservative 0.03%
Aromatic 0.2%
Described surfactant is by laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, methyl cocoyl ox sulphur The combination of sour three kinds of compositions of sodium;Described plant extraction liquid is Ba 2672, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, willow The combination of four kinds of compositions of China fir leaf extract.Other raw materials are identical with the composition of embodiment 1.
The plant extraction liquid of the present embodiment is Ba 2672, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, the extraction of cryptomeria leaf Thing.Otoginsenoside can promote scalp blood circulation, grow hair hair care;Radix-polygoni multiflori extract Yin-nourishing and Qi-supplementing, hair can be made shiny black;Black sesame Nettle extract has the effect of help essence and blood, prevention poliosis;Cryptomeria leaf extract play the role of it is clearing heat and detoxicating, for having one's hair wash Water plays a part of having anti-dandruff and itching-relieving.Effective proportioning of these plant essence things has abundant nutritional ingredient, long-term use of energy Make healthy hair pitch-black glossy.
The preparation method of the above-mentioned anti-dandruff hair care shampoo of the plant containing Ba 2672 is the same as embodiment 1, specific raw material And proportioning is as follows:
Embodiment 4
The anti-dandruff hair care shampoo of plant containing Ba 2672, is prepared by following raw materials according:
Raw material components Percentage by weight
Deionized water 73.465%
Surfactant 15%
Cationic conditioning agent 0.65%
Pearling agent 1.5%
Foam stabilizer 3%
NMF 2.5%
Thickener 1.5%
Siloxanes 1.1%
Plant extraction liquid 0.155%
PH conditioning agents 0.15%
Scalp conditioning agent 0.05%
Thinner 0.2%
Chelating agent 0.1%
Preservative 0.03%
Aromatic 0.6%
Described surfactant is by laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, methyl cocoyl ox sulphur The combination of sour three kinds of compositions of sodium;Described plant extraction liquid is Ba 2672, red sage root root extract, Cacumen Platycladi extract, mountain The four kinds of combinations of tea seed extract;Other raw materials are identical with the composition of embodiment 1.
The plant extraction liquid of the present embodiment is Ba 2672 extract, red sage root root extract, Semen Sesami Nigrum extract, camellia Seed extract.Effective proportioning of these plant essence things, which has, grows the foster method of hair, the effect of salubrious oil-control.
The preparation method of the above-mentioned anti-dandruff hair care shampoo of the plant containing Ba 2672 is the same as embodiment 1, specific raw material And proportioning is as follows:
Embodiment 5
The anti-dandruff hair care shampoo of plant containing Ba 2672, is prepared by following raw materials according:
Described surfactant by laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, cocaminopropionic acid sodium, The combination of four kinds of compositions of Cocoamidopropyl betaine, described cationic conditioning agent are hydroxypropyl melon glue Hydroxyproyl Trimethyl Ammonium chloride, described thickener are sodium chloride, and described scalp conditioning agent is the combination of cetanol and PPG-3 Octyl Ethers, described Preservative be methylisothiazolinone, three kinds of methylchloroisothiazandnone, piroctone olamine salt compositions combination, it is described Plant extraction liquid for Ba 2672, sarranine flower extract, ginseng extract, the group of four kinds of compositions of dendrobium candidum extract Close;Other raw materials are identical with the composition of embodiment 1.
The plant extraction liquid of the present embodiment is Ba 2672, sarranine flower extract, ginseng extract, dendrobium candidum extraction Thing.Effective proportioning of these plant essence things has abundant nutritional ingredient, can supplement the nutrient needed for hair.The shampoo Not silicone-containing, pearling agent, foam stabilizer and thinner are characterised by, is to have one's hair wash to be formulated without silicone oil containing various plants elite, Property is gentle, maintenance scalp and impaired hair.
The preparation method of the above-mentioned anti-dandruff hair care shampoo of the plant containing Ba 2672 is the same as embodiment 1, specific raw material And proportioning is as follows:
In other embodiments, the surfactant of the anti-dandruff hair care shampoo of plant of the present invention can be selected from bay Alcohol polyethers sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, sodium methyl cocoyl taurate and cocaminopropionic acid sodium, coconut oleoyl amine Any 3 kinds or 4 kinds in CAB;Described cationic conditioning agent is also selected from Polyquaternium-10, hydroxypropyl melon Any one in glue hydroxypropyl-trimethyl ammonium chloride and two palm acyloxyethyl alkyl dimethyl ammonium chlorides;Described thickener It may be selected from any one in coconut oleoyl amine MEA and sodium chloride;Described scalp conditioning agent may be selected from polyethylene glycol -14M, spermaceti Any one in alcohol, PPG-3 Octyl Ethers or two kinds;Described preservative can be hexamidine two (isethionic acid) salt, first Any three kinds in base chloroisothiazole quinoline ketone, methylisothiazolinone, piroctone olamine salt;Plant extraction liquid, which removes, contains seven Leaf tree saponin(e, also containing Chinese honey locust seed extract, gadol extract, lemon grass leaf oil, Radix Platycodonis extract, the extraction of radix codonpsis tangshen root Thing, common cnidium fruit P.E, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, cryptomeria leaf extract, Cacumen Platycladi extract, red sage root carry Take any three kinds in thing, camellia seed extract, tomato sage extract, ginseng extract, dendrobium candidum extract.
Embodiment 6
The measure of merit of the anti-dandruff hair care shampoo of plant containing Ba 2672
1st, sensory effects are tested
Test material:Shampoo made of embodiment 1-5 and comparative example 1-2, the difference of comparative example 1 and embodiment 1 are Without plant extraction liquid, the difference of comparative example 2 and embodiment 5 is to be free of plant extraction liquid.
Subjects:The people of Subject Population 175, wherein age distribution 18-55 year, the people of male's number 77, the people of women number 98.
Test method:Experiment number is divided into 7 groups, every group of 25 people, respectively to made of embodiment 1-5 and comparative example 1-2 Shampoo carries out sensory evaluation test.Each sampling 1 month, tester feels to be scored according to the experience of oneself.Comment Minute mark standard is ten point system, and 1 point worst, and 10 points best, and fraction more high effect is better.
Test result is as follows:
Found out by test result, shampoo scoring prepared by the present invention is higher, and embodiment 1 and embodiment 2 are at anti-dandruff aspect With remarkable result, embodiment 3 has preferable effect in terms of hair moisture is kept, and embodiment 4 is imitated in terms of salubrious oil-control Fruit is preferable, and embodiment 5 is the significant effect in the fluffy degree for improving hair without silicone oil formula.Test and go according to sensory evaluation Consider measure of merit to be worth doing, embodiment group anti-dandruff, is obviously improved than control group in terms of moistening degree.Test result shows Ba 2672 The shampoo effectively matched with various plants elite has anti-dandruff and itching-relieving, grows the effect of hair hair care.
2nd, fungistatic effect is tested
Test method:45-50 DEG C or so of olive oil solid medium is poured into culture dish, is divided after to be solidified with card punch Do not punched in two plates.Liquid-transfering gun draws the shampoo of embodiment 1 and the shampoo of control group 1 of 100 microlitres of 10 times of dilutions respectively, In adding hole.Chlosma liquid, 37 DEG C of incubated 1h are coated with, then overturn culture 24-48h, observe result.
Olive oil culture medium:Maltose 20g/L, yeast extract 2g/L, glucose 20g/L, olive oil 20g/L plus distillation After water dissolving, 121 DEG C of 15min autoclavings
The judgement of bacteriostasis:Antibacterial circle diameter shows that more greatly bacteriostasis is stronger.Antibacterial circle diameter >=20mm is extremely quick Sense, has been judged to bacteriostasis, the bigger fungistatic effect of inhibition zone is better;15mm≤bacteriostatic diameter < 20mm are Gao Min;10mm≤suppression Bacterium diameter < 15mm are quick in being;Bacteriostatic diameter < 10mm are invalid, are judged to no bacteriostasis.
Shown according to Fig. 1 result, embodiment 1 (Figure 1A) is quick in being to the bacteriostatic level of chlosma, (the figure of control group 1 1B) bacteriostatic level to chlosma is invalid.Test result indicates that the plant extraction liquid containing Ba 2672 is for horse traction This causes the Main Bacteria accessory of dandruff and itching of the scalp to have certain bacteriostasis to color bacterium, and is substantially better than and is not added with plant The shampoo of extract solution.

Claims (3)

1. the anti-dandruff hair care shampoo of the plant containing Ba 2672, it is characterised in that by the raw material system of following percentage by weight Into:
Described surfactant is laureth sulfuric ester ammonium, bay alcohol sulfuric ester ammonium, sodium methyl cocoyl taurate And any 3 kinds or 4 kinds of combination in cocaminopropionic acid sodium, Cocoamidopropyl betaine;
Described cationic conditioning agent is Polyquaternium-10, hydroxypropyl guar hydroxypropyltrimonium chloride and two palmityls Any a kind in oxygen ethyl alkyl dimethyl ammonium chloride, or 3 kinds of combination;
Described pearling agent is glycol distearate;
Described NMF is the combination of glycine betaine and pyrrolidone sodium carboxylate;
Described thickener is a kind in coconut oleoyl amine MEA and sodium chloride, or 2 kinds of combination;
Described siloxanes is the combination of dimethyl silicone polymer and ammonia end dimethyl silicone polymer;
Described plant extraction liquid is Ba 2672, and coordinates Chinese honey locust seed extract, gadol extract, lemon grass leaf Oil, Radix Platycodonis extract, radix codonpsis tangshen root extract, common cnidium fruit P.E, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, cryptomeria leaf carry Take thing, Cacumen Platycladi extract, red sage root root extract, camellia seed extract, sarranine flower extract, ginseng extract, dendrobium candidum Any 3 kinds in extract;
Described PH conditioning agents are citric acid;
The foam stabilizer is two (hydrogenated-tallow group) phthalic acid amides;
Described scalp conditioning agent is any a kind or 2 kinds in polyethylene glycol -14M, cetanol, PPG-3 Octyl Ethers;
Described thinner is ammonium xylene sulfonate;
Described chelating agent is EDETATE SODIUM;
Described preservative is hexamidine two (isethionic acid) salt, methylchloroisothiazandnone and methylisothiazolinone, pyrrole Any 3 kinds of combination in Roc ketone ethanolamine salt;
Described aromatic is essence.
2. the anti-dandruff hair care shampoo of the plant containing Ba 2672 according to claim 1, it is characterised in that by following The raw material of mass percent is made:
The plant extraction liquid is Ba 2672, sarranine flower extract, ginseng extract, the group of four kinds of dendrobium candidum extract Close.
3. the anti-dandruff hair care shampoo of the plant containing Ba 2672 according to claim 1 or 2, it is characterised in that institute Ba 2672 is made by following methods in the plant extraction liquid stated:
1) buckeye crushes in pulverizer, sieving;
2) according to buckeye and 30-70% ethanol volume ratio 1:10 ratio, add buckeye, 30-70% ethanol to extractor In, 55-60 DEG C of stirring 1.5-2h is warming up to, filters, collects filtrate;
3) filter residue extracts again according to the method described above, merges extract solution twice, alcohol content≤7% is concentrated under reduced pressure into 50-60 DEG C; Concentrate is diluted to 8-10 times of volume with purified water, is warming up to 40 DEG C -45 DEG C upper macroporous resin adsorptions;
4) respectively with water, 30-50% ethanol elution impurity, then with 50-75% ethanol elution working substances, eluent is collected;
5) eluent is concentrated in clean area, temperature control is concentrated into the 1/10 of original volume at 55-60 DEG C;
6) concentrate is dried under vacuum to dry in clean area.
CN201710580271.2A 2017-07-17 2017-07-17 Dandruff-removing and hair-nourishing plant shampoo containing aescin Active CN107375131B (en)

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CN110664702A (en) * 2018-07-02 2020-01-10 中山市泛华精细化学品有限公司 Natural plant amino acid anti-dandruff shampoo and preparation method thereof
CN111388364A (en) * 2020-03-02 2020-07-10 深圳苏露中医诊所 Antibacterial shampoo
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CN108567636A (en) * 2018-06-14 2018-09-25 广州植境生物科技有限公司 A kind of draft Haircare composition of the extract containing hamamelis
CN108619053B (en) * 2018-06-20 2021-04-20 广州市惠芳日化有限公司 Anti-dandruff composition, shampoo and preparation method thereof
CN108619053A (en) * 2018-06-20 2018-10-09 广州市惠芳日化有限公司 Desquamation compositions, leaves shampoo and preparation method thereof
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CN111388364A (en) * 2020-03-02 2020-07-10 深圳苏露中医诊所 Antibacterial shampoo
CN112472630A (en) * 2020-12-18 2021-03-12 上海家化联合股份有限公司 Self-thickening composition of amino acid surfactants
CN112472630B (en) * 2020-12-18 2023-10-17 上海家化联合股份有限公司 Self-thickening compositions of amino acid surfactants
CN117442535A (en) * 2023-12-21 2024-01-26 拉芳家化股份有限公司 Anti-dandruff shampoo
CN117442535B (en) * 2023-12-21 2024-03-19 拉芳家化股份有限公司 Anti-dandruff shampoo

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