CN104739717A - Shampoo with linseed extract and preparation method of shampoo with linseed extract - Google Patents
Shampoo with linseed extract and preparation method of shampoo with linseed extract Download PDFInfo
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- CN104739717A CN104739717A CN201510097017.8A CN201510097017A CN104739717A CN 104739717 A CN104739717 A CN 104739717A CN 201510097017 A CN201510097017 A CN 201510097017A CN 104739717 A CN104739717 A CN 104739717A
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- Prior art keywords
- extract
- mixture
- flaxseed
- surfactant
- calculated
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- 235000004426 flaxseed Nutrition 0.000 title claims abstract description 80
- 239000002453 shampoo Substances 0.000 title claims abstract description 64
- 235000004431 Linum usitatissimum Nutrition 0.000 title claims abstract description 51
- 240000006240 Linum usitatissimum Species 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000000605 extraction Methods 0.000 title description 2
- 239000000203 mixture Substances 0.000 claims abstract description 64
- 229940107657 flaxseed extract Drugs 0.000 claims abstract description 50
- 235000020704 flaxseed extract Nutrition 0.000 claims abstract description 50
- 239000004094 surface-active agent Substances 0.000 claims abstract description 46
- 239000002562 thickening agent Substances 0.000 claims abstract description 35
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 31
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- 239000003755 preservative agent Substances 0.000 claims abstract description 27
- 238000002156 mixing Methods 0.000 claims abstract description 13
- 230000002335 preservative effect Effects 0.000 claims abstract description 13
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 8
- 239000003002 pH adjusting agent Substances 0.000 claims abstract 9
- 230000003750 conditioning effect Effects 0.000 claims abstract 2
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 45
- MJYQFWSXKFLTAY-OVEQLNGDSA-N (2r,3r)-2,3-bis[(4-hydroxy-3-methoxyphenyl)methyl]butane-1,4-diol;(2r,3r,4s,5s,6r)-6-(hydroxymethyl)oxane-2,3,4,5-tetrol Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O.C1=C(O)C(OC)=CC(C[C@@H](CO)[C@H](CO)CC=2C=C(OC)C(O)=CC=2)=C1 MJYQFWSXKFLTAY-OVEQLNGDSA-N 0.000 claims description 32
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 27
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 26
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- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 23
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- 125000002091 cationic group Chemical group 0.000 claims description 15
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- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical group CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 7
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- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Abstract
本发明公开一种含亚麻籽提取液的洗发水及制备方法,所述含有亚麻籽提取液的洗发水,制备所用原料由亚麻籽提取液、主表面活性剂、辅助表面活性剂、调理剂、增稠剂、pH调节剂和防腐剂组成。制备方法即首先将增稠剂中的卡波姆组分分散于2/3总重量的亚麻籽提取液中,升温至65-75℃后依次加入主表面活性剂和辅助表面活性剂,混匀降温至55-60℃后再加入调理剂,混匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的亚麻籽提取液,混匀后即得含有亚麻籽提取液的洗发水,该含有亚麻籽提取液的洗发水具有良好的护发效果,还具有对头发保湿和抗静电的功效,使头发持久柔顺亮泽。The invention discloses a shampoo containing linseed extract and a preparation method thereof. The shampoo containing linseed extract is prepared from linseed extract, a main surfactant, an auxiliary surfactant, a conditioning agent, Thickener, pH adjuster and preservative composition. The preparation method is to first disperse the carbomer component in the thickener in 2/3 of the total weight of the flaxseed extract, heat up to 65-75°C, add the main surfactant and auxiliary surfactant in turn, and mix well Cool down to 55-60°C and then add conditioner, mix well and continue to cool down to 38-42°C, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total weight of flax flaxseed extract, after mixing, the shampoo containing flaxseed extract has a good hair care effect, and also has the effect of moisturizing and antistatic on the hair, making the hair soft and shiny for a long time Ze.
Description
技术领域technical field
本发明涉及一种亚麻籽提取液洗发水及其制备方法,属于日用化妆品领域。The invention relates to a linseed extract shampoo and a preparation method thereof, belonging to the field of daily cosmetics.
背景技术Background technique
亚麻籽(flaxseed或linseed)又称胡麻籽,是亚麻科、亚麻属的一年生或多年生草本植物亚麻的种子,呈扁卵形,前端稍尖,具光泽,有褐、棕褐、深褐、白色等颜色。中国最早在《图经本草》中就有亚麻籽可治肠燥便秘、眩晕、病后虚弱、皮肤痒疹、皮肤干燥起屑、脱发和痈疮肿毒的记载。亚麻籽的成分如表1,其中的活性成分包括α-亚麻酸、亚油酸、油酸、硬脂酸甘油三酯、棕榈酸甘油三酯、木酚素、谷甾醇、多糖、维生素E、维生素A、维生素F和钙、铁、钾、镁、铜、锌等多种矿物质。油脂和碳水化合物共同对头发起到护理作用,其中的α-亚麻酸及亚油酸还具有消炎的作用,木酚素能够清除过半数的过氧化氢自由基,表现出抗氧化的性能,对机体的氧化损伤起到一定的保护作用。亚麻籽中还含有的丰富的维生素和矿物质,有延缓衰老和抗氧化的作用。亚麻籽中包含的各种活性成分扩大了其在食品、保健品、日用化工和制药领域的应用。Flaxseed (flaxseed or linseed), also known as flaxseed, is the seed of flax, an annual or perennial herb of the family Linaceae and the genus Flax. Wait for the color. In China's "Picture Classics of Materia Medica", there are records that flaxseed can treat intestinal dryness, constipation, dizziness, weakness after illness, skin prurigo, dry skin and scaling, hair loss and carbuncle sores. The ingredients of flaxseed are shown in Table 1, and the active ingredients include α-linolenic acid, linoleic acid, oleic acid, triglyceride stearate, triglyceride palmitate, lignans, sitosterol, polysaccharides, vitamin E, Vitamin A, vitamin F and calcium, iron, potassium, magnesium, copper, zinc and other minerals. Fat and carbohydrates work together to care for the hair. The α-linolenic acid and linoleic acid also have anti-inflammatory effects. protection against oxidative damage. Flaxseed is also rich in vitamins and minerals, which have anti-aging and anti-oxidation effects. The various active ingredients contained in flaxseed expand its application in the fields of food, health care products, daily chemicals and pharmaceuticals.
表1 亚麻籽的成分表Table 1 Composition list of flaxseed
现有的洗发水中多有添加植物成分达到植物洗护发效果,但是目前市场上未见有与本发明添加植物成分及制作工艺相同或者相仿的产品或工艺。Most of the existing shampoos add plant components to achieve the effect of plant shampoo and hair care, but there is no product or process that is the same or similar to the addition of plant components and the production process of the present invention in the market.
发明内容Contents of the invention
本发明的目的之一是为了提供一种含有亚麻籽提取液的洗发水,该含有亚麻籽提取液的洗发水具有洗发、天然活性成分护理头发、保湿和抗静电等特点。One of the objectives of the present invention is to provide a shampoo containing flaxseed extract, which has the characteristics of shampooing, hair care with natural active ingredients, moisturizing and antistatic.
本发明的目的之二是提供上述的一种含有亚麻籽提取液的洗发水的制备方法,该制备方法具有能将多种不易分散的原料合理分散,同时其制备过程具有操作简单等特点。The second object of the present invention is to provide the above-mentioned preparation method of a shampoo containing linseed extract, the preparation method can reasonably disperse a variety of difficult-to-disperse raw materials, and the preparation process has the characteristics of simple operation and the like.
本发明的技术原理Technical principle of the present invention
由于亚麻籽经过人工提取后,其中的活性成分如多糖类、油脂、木脂素、维生素和矿物质等溶出,且以可溶性形式存在于提取液中。将亚麻籽提取液加入到洗发水中后,其中的活性成分如多糖类、油脂、木脂素、维生素和矿物质等作用于头发及头皮,对头发的养护效果有着重要的现实和商业意义。After the flaxseed is artificially extracted, the active ingredients such as polysaccharides, oils, lignans, vitamins and minerals are dissolved out and exist in the extract in soluble form. After the flaxseed extract is added to the shampoo, the active ingredients in it, such as polysaccharides, oils, lignans, vitamins and minerals, act on the hair and scalp, which has important practical and commercial significance for the hair maintenance effect .
本发明的技术方案Technical scheme of the present invention
一种含有亚麻籽提取液的洗发水,按重量百分比计算,其原料组成及含量如下:A shampoo containing linseed extract, calculated by weight percentage, its raw material composition and content are as follows:
所述的亚麻籽提取液,按重量比计算,即天然亚麻籽:水为1:30的比例,将天然亚麻籽加入到60-65℃水中,搅拌条件下进行混合,同时控制转速300r/min,水浴恒温65℃进行提取30min,然后过滤,所得的上清液以300r/min转速搅拌降到室温,即得亚麻籽提取液;The flaxseed extract is calculated by weight ratio, that is, the ratio of natural flaxseed: water is 1:30, the natural flaxseed is added to 60-65°C water, mixed under stirring conditions, and the speed is controlled at 300r/min at the same time , extract in a water bath at a constant temperature of 65°C for 30 minutes, then filter, and stir the obtained supernatant at a speed of 300 r/min to room temperature to obtain the linseed extract;
所述天然亚麻籽为油纤两用亚麻种子;The natural flaxseed is dual-purpose flaxseed for oil and fiber;
所述主表面活性剂为脂肪醇聚氧乙烯醚硫酸铵盐、脂肪醇聚氧乙烯醚硫酸钠盐、十二烷基硫酸铵、十二烷基硫酸钠及月桂醇硫磺酸钠中的一种或两种以上组成的混合物;The main surfactant is one of fatty alcohol polyoxyethylene ether sulfate ammonium salt, fatty alcohol polyoxyethylene ether sulfate sodium salt, ammonium lauryl sulfate, sodium lauryl sulfate and sodium lauryl sulfuric acid or a mixture of two or more;
所述辅助表面活性剂为椰油酰胺丙基甜菜碱、椰子油脂肪酸单乙醇酰胺、椰子油酸二乙醇胺、十二烷基甜菜碱、咪唑啉甜菜碱、烷基糖苷、椰油致酰基谷氨酸三乙醇胺盐、甲基椰油酰基牛磺酸钠及月桂基二甲基氨基醋酸甜菜碱中的一种或两种以上组成的混合物;The cosurfactant is cocamidopropyl betaine, coconut oil fatty acid monoethanolamide, coconut oil diethanolamine, lauryl betaine, imidazoline betaine, alkyl glucoside, coconut oil-induced acyl glutamine Acid triethanolamine salt, sodium methyl cocoyl taurate and lauryl dimethylaminoacetate betaine or a mixture of two or more;
所述增稠剂为卡波姆与氯化钠、氯化铵、羟乙基纤维素、羟丙基纤维素中的一种或两种以上组成的混合物;The thickener is a mixture of carbomer and one or more of sodium chloride, ammonium chloride, hydroxyethyl cellulose, and hydroxypropyl cellulose;
所述调理剂为聚季铵盐-7、聚季铵盐-10、阳离子瓜尔胶、汉生胶、季铵化蛋白、十六烷基三甲基氯化铵、乳化硅油、二甲基硅油、十六十八醇、羊毛脂中的一种或两种以上组成的混合物;The conditioner is polyquaternium-7, polyquaternium-10, cationic guar gum, xanthan gum, quaternized protein, cetyltrimethylammonium chloride, emulsified silicone oil, dimethyl One or a mixture of two or more of silicone oil, cetostearyl alcohol, and lanolin;
所述pH调节剂为氢氧化钠、三乙醇胺及柠檬酸中的一种或两种以上组成的混合物;The pH regulator is one or a mixture of two or more of sodium hydroxide, triethanolamine and citric acid;
所述防腐剂为1,3—二羟甲基—5,5—二甲基乙内酰脲、尼泊金丙酯或卡松。The preservative is 1,3-dimethylol-5,5-dimethylhydantoin, propylparaben or kason.
上述的一种含有亚麻籽提取液的洗发水的制备方法,步骤如下:A kind of preparation method of above-mentioned shampoo containing linseed extract, the steps are as follows:
首先将增稠剂中的卡波姆组分均匀分散于2/3总重量的亚麻籽提取液中,分散均匀后升温至65-75℃,然后依次加入主表面活性剂和辅助表面活性剂,混合均匀后降温至55-60℃,再加入调理剂,混合均匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的的亚麻籽提取液,混合均匀后即得含有亚麻籽提取液的洗发水。First, the carbomer component in the thickener is evenly dispersed in 2/3 of the total weight of the flaxseed extract, and after the dispersion is uniform, the temperature is raised to 65-75°C, and then the main surfactant and the auxiliary surfactant are added in sequence, After mixing evenly, cool down to 55-60°C, then add conditioner, continue to cool down to 38-42°C after mixing evenly, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total The flaxseed extract of 50 wt.% is mixed evenly to obtain the shampoo containing the flaxseed extract.
本发明的结果表明,含有亚麻籽提取液的洗发水具有滋养头发、护发、保湿、防止静电、抗氧化、消炎的功效。此外含有亚麻籽提取液的洗发水还可有效防止紫外线辐射对头发造成的损伤、修复受损毛囊、改善头皮微环境、使头发乌黑浓密、有效改善发质、定型、控油、可改善染发、烫发后产生的头发毛糙、干枯、分叉问题。The result of the present invention shows that the shampoo containing the linseed extract has the effects of nourishing hair, hair care, moisturizing, preventing static electricity, anti-oxidation and anti-inflammation. In addition, the shampoo containing linseed extract can also effectively prevent the damage caused by ultraviolet radiation to the hair, repair damaged hair follicles, improve the microenvironment of the scalp, make the hair black and thick, effectively improve hair quality, shape, oil control, and improve hair dyeing and perm The resulting hair is rough, dry, and split ends.
本发明的有益效果Beneficial effects of the present invention
本发明的一种含亚麻籽提取液的洗发水,由于将天然植物亚麻籽提取液加入到配方中,使亚麻籽中的活性成分如多糖类碳水化合物、木酚素、和少量的油脂、维生素及矿物质等作用于头发,是一种集洁发、护发于一体的多功能洗发水;亚麻籽提取液中多糖类化合物具有增稠的效果,可以进一步提高洗发水的稳定性。A kind of shampoo containing linseed extract of the present invention, because the natural plant linseed extract is added in formula, make the active ingredient in linseed such as polysaccharide carbohydrate, lignan, and a small amount of oil, Vitamins and minerals act on the hair. It is a multifunctional shampoo that integrates hair cleansing and hair care; the polysaccharides in the flaxseed extract have a thickening effect, which can further improve the stability of the shampoo.
本发明的含有亚麻籽提取液的洗发水,提取工艺简单,可操作性强。由于亚麻籽经过人工提取后,其中的活性成分溶出,且以可溶性形式存在于提取液中。配方中使用亚麻籽提取液替代余量水,提高了洗发水中亚麻籽活性成分的用量,增加头发与亚麻籽中活性成分接触率,对头发的护理效果有着重要的现实意义。The shampoo containing the linseed extract of the present invention has simple extraction process and strong operability. After the flaxseed is artificially extracted, the active ingredients are dissolved out and exist in the extract in a soluble form. The flaxseed extract is used in the formula to replace the remaining water, which increases the amount of active ingredients in the flaxseed in the shampoo and increases the contact rate between the hair and the active ingredients in the flaxseed, which has important practical significance for the hair care effect.
本发明的含有亚麻籽提取液的洗发水,其制备方法简单,容易实现。The shampoo containing the linseed extract of the present invention has a simple preparation method and is easy to realize.
具体实施方式Detailed ways
下面结合具体实施例对本发明做进一步描述,但本发明的保护范围并不仅限于此。The present invention will be further described below in conjunction with specific embodiments, but the protection scope of the present invention is not limited thereto.
本发明各实施例中所用的原料规格及生产厂家如表2Raw material specification and manufacturer used in each embodiment of the present invention are as table 2
实施例1Example 1
一种含有亚麻籽提取液的洗发水,按重量百分比计算,其原料组成及含量如下:A shampoo containing linseed extract, calculated by weight percentage, its raw material composition and content are as follows:
所述的亚麻籽提取液,按重量比计算,即亚麻籽:水为1:30的比例,将100g亚麻籽加入到60-65℃的3000g水中,搅拌条件下进行混合,同时控制转速300r/min,水浴恒温65℃进行提取30min,然后过滤,所得的上清液以300r/min转速搅拌降到室温,即得亚麻籽提取液;The flaxseed extract is calculated by weight ratio, that is, the ratio of flaxseed: water is 1:30, 100g of flaxseed is added to 3000g of water at 60-65°C, and mixed under stirring conditions, while controlling the speed of 300r/ min, extract in a water bath at a constant temperature of 65°C for 30 min, then filter, and stir the obtained supernatant at a speed of 300 r/min to room temperature to obtain the linseed extract;
所述天然亚麻籽为油纤两用亚麻种子。The natural linseed is a dual-purpose linseed for oil and fiber.
所述主表面活性剂为脂肪醇聚氧乙烯醚硫酸铵盐;The main surfactant is fatty alcohol polyoxyethylene ether ammonium sulfate;
所述辅助表面活性剂为椰油酰胺丙基甜菜碱和十二烷基甜菜碱按重量比计算,即椰油酰胺丙基甜菜碱:十二烷基甜菜碱为2:1组成的混合物;The cosurfactant is cocamidopropyl betaine and dodecyl betaine calculated by weight ratio, i.e. cocamidopropyl betaine: lauryl betaine is a mixture of 2:1 composition;
所述增稠剂为卡波姆与氯化钠按重量比计算,即卡波姆:氯化钠为1:0.4组成的混合物;The thickener is calculated by weight ratio between carbomer and sodium chloride, that is, carbomer: sodium chloride is a mixture of 1:0.4;
所述调理剂为聚季铵盐-10、乳化硅油与十六十八醇按重量比计算,即聚季铵盐-10:乳化硅油:十六十八醇为1:2:0.5组成的混合物;The conditioner is polyquaternium-10, emulsified silicone oil and cetostearyl alcohol by weight ratio, that is, a mixture of polyquaternium-10: emulsified silicone oil: cetostearyl alcohol at a ratio of 1:2:0.5 ;
所述pH调节剂为氢氧化钠;The pH regulator is sodium hydroxide;
所述防腐剂为1,3—二羟甲基—5,5—二甲基乙内酰脲。The preservative is 1,3-dimethylol-5,5-dimethylhydantoin.
上述的一种含有亚麻籽提取液的洗发水的制备方法,步骤如下:A kind of preparation method of above-mentioned shampoo containing linseed extract, the steps are as follows:
首先将增稠剂中的卡波姆均匀分散于2/3总重量的亚麻籽提取液中,分散均匀后升温至65-75℃,然后依次加入主表面活性剂和辅助表面活性剂,混合均匀后降温至55-60℃,再加入调理剂,混合均匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的的亚麻籽提取液,混合均匀后即得含有亚麻籽提取液的洗发水。First, evenly disperse the carbomer in the thickener in 2/3 of the total weight of the flaxseed extract, heat up to 65-75°C after dispersing evenly, then add the main surfactant and auxiliary surfactant in turn, and mix well Then cool down to 55-60°C, then add conditioner, mix evenly and continue to cool down to 38-42°C, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total weight The flaxseed extract is mixed evenly to obtain the shampoo containing the flaxseed extract.
实施例2Example 2
一种含有亚麻籽提取液的洗发水,按重量百分比计算,其原料组成及含量如下:A shampoo containing linseed extract, calculated by weight percentage, its raw material composition and content are as follows:
所述的亚麻籽提取液,按重量比计算,即亚麻籽:水为1:30的比例,将100g亚麻籽加入到60-65℃的3000g水中,搅拌条件下进行混合,同时控制转速300r/min,水浴恒温65℃进行提取30min,然后过滤,所得的上清液以300r/min转速搅拌降到室温,即得亚麻籽提取液;The flaxseed extract is calculated by weight ratio, that is, the ratio of flaxseed: water is 1:30, 100g of flaxseed is added to 3000g of water at 60-65°C, and mixed under stirring conditions, while controlling the speed of 300r/ min, extract in a water bath at a constant temperature of 65°C for 30 min, then filter, and stir the obtained supernatant at a speed of 300 r/min to room temperature to obtain the linseed extract;
所述天然亚麻籽油纤两用亚麻种子。The natural flaxseed oil fiber dual purpose flaxseed.
所述主表面活性剂为脂肪醇聚氧乙烯醚硫酸钠盐;The main surfactant is fatty alcohol polyoxyethylene ether sulfate sodium salt;
所述辅助表面活性剂为椰子油脂肪酸单乙醇酰胺、椰子油酸二乙醇胺按重量比计算,即椰子油脂肪酸单乙醇酰胺:椰子油酸二乙醇胺为1:0.5组成的混合物;The auxiliary surfactant is coconut oil fatty acid monoethanolamide and coconut oleic acid diethanolamine calculated by weight ratio, that is, coconut oil fatty acid monoethanolamide: coconut oleic acid diethanolamine is a mixture of 1:0.5;
所述增稠剂为卡波姆与氯化铵按重量比计算,即卡波姆:氯化铵为1:0.3组成的混合物;The thickener is calculated by weight ratio between carbomer and ammonium chloride, that is, carbomer: ammonium chloride is a mixture of 1:0.3;
所述调理剂为聚季铵盐-7、汉生胶、乳化硅油、十六十八醇按重量比计算,即聚季铵盐-7:汉生胶:乳化硅油:十六十八醇为1:0.2:2:0.4组成的混合物;The conditioner is polyquaternium-7, xanthan gum, emulsified silicone oil, and cetostearyl alcohol by weight ratio, that is, polyquaternium-7: xanthan gum: emulsified silicone oil: cetostearyl alcohol is 1:0.2:2:0.4 mixture;
所述pH调节剂为三乙醇胺;The pH regulator is triethanolamine;
所述防腐剂为尼泊金丙酯。Described preservative is propylparaben.
上述的一种含有亚麻籽提取液的洗发水的制备方法,步骤如下:A kind of preparation method of above-mentioned shampoo containing linseed extract, the steps are as follows:
首先将增稠剂中的卡波姆组分均匀分散于2/3总重量的亚麻籽提取液中,分散均匀后升温至65-75℃,然后依次加入主表面活性剂和辅助表面活性剂,混合均匀后降温至55-60℃,再加入调理剂,混合均匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的的亚麻籽提取液,混合均匀后即得含有亚麻籽提取液的洗发水。First, the carbomer component in the thickener is evenly dispersed in 2/3 of the total weight of the flaxseed extract, and after the dispersion is uniform, the temperature is raised to 65-75°C, and then the main surfactant and the auxiliary surfactant are added in sequence, After mixing evenly, cool down to 55-60°C, then add conditioner, continue to cool down to 38-42°C after mixing evenly, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total The flaxseed extract of 50 wt.% is mixed evenly to obtain the shampoo containing the flaxseed extract.
实施例3Example 3
一种含有亚麻籽提取液的洗发水,按重量百分比计算,其原料组成及含量如下:A shampoo containing linseed extract, calculated by weight percentage, its raw material composition and content are as follows:
所述的亚麻籽提取液,按重量比计算,即亚麻籽:水为1:30的比例,将100g亚麻籽加入到60-65℃的3000g水中,搅拌条件下进行混合,同时控制转速300r/min,水浴恒温65℃进行提取30min,然后过滤,所得的上清液以300r/min转速搅拌降到室温,即得亚麻籽提取液;The flaxseed extract is calculated by weight ratio, that is, the ratio of flaxseed: water is 1:30, 100g of flaxseed is added to 3000g of water at 60-65°C, and mixed under stirring conditions, while controlling the speed of 300r/ min, extract in a water bath at a constant temperature of 65°C for 30 min, then filter, and stir the obtained supernatant at a speed of 300 r/min to room temperature to obtain the linseed extract;
所述天然亚麻籽为油纤两用亚麻种子。The natural linseed is a dual-purpose linseed for oil and fiber.
所述主表面活性剂为十二烷基硫酸铵;The main surfactant is ammonium lauryl sulfate;
所述辅助表面活性剂为咪唑啉甜菜碱与烷基糖苷按重量百分比计算,即咪唑啉甜菜碱:烷基糖苷为1:1组成的混合物;The auxiliary surfactant is imidazoline betaine and alkyl glucoside calculated by weight percentage, that is, imidazoline betaine: alkyl glycoside is a mixture composed of 1:1;
所述增稠剂为卡波姆与羟乙基纤维素按重量百分比计算,即卡波姆:羟乙基纤维素为1:0.6组成的混合物;The thickener is calculated by weight percentage of carbomer and hydroxyethyl cellulose, that is, carbomer: hydroxyethyl cellulose is a mixture of 1:0.6;
所述调理剂为聚季铵盐-7、阳离子瓜尔胶、乳化硅油和十六十八醇按重量比计算,即聚季铵盐-7:阳离子瓜尔胶:乳化硅油:十六十八醇为1:0.3:2:0.4组成的混合物;The conditioner is polyquaternium-7, cationic guar gum, emulsified silicone oil and cetostearyl alcohol by weight ratio, that is, polyquaternium-7: cationic guar gum: emulsified silicone oil: cetearyl Alcohol is a mixture of 1:0.3:2:0.4;
所述pH调节剂为三乙醇胺和柠檬酸按重量百分比计算,即三乙醇胺:柠檬酸为1:0.001-0.2组成的混合物;The pH regulator is calculated by weight percentage of triethanolamine and citric acid, that is, a mixture of triethanolamine: citric acid at a ratio of 1:0.001-0.2;
所述防腐剂为尼泊金丙酯。Described preservative is propylparaben.
上述的一种含有亚麻籽提取液的洗发水的制备方法,步骤如下:A kind of preparation method of above-mentioned shampoo containing linseed extract, the steps are as follows:
首先将增稠剂中的卡波姆组分均匀分散于2/3总重量的亚麻籽提取液中,分散均匀后升温至65-75℃,然后依次加入主表面活性剂和辅助表面活性剂,混合均匀后降温至55-60℃,再加入调理剂,混合均匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的的亚麻籽提取液,混合均匀后即得含有亚麻籽提取液的洗发水。First, the carbomer component in the thickener is evenly dispersed in 2/3 of the total weight of the flaxseed extract, and after the dispersion is uniform, the temperature is raised to 65-75°C, and then the main surfactant and the auxiliary surfactant are added in sequence, After mixing evenly, cool down to 55-60°C, then add conditioner, continue to cool down to 38-42°C after mixing evenly, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total The flaxseed extract of 50 wt.% is mixed evenly to obtain the shampoo containing the flaxseed extract.
实施例4Example 4
一种含有亚麻籽提取液的洗发水,按重量百分比计算,其原料组成及含量如下:A shampoo containing linseed extract, calculated by weight percentage, its raw material composition and content are as follows:
所述的亚麻籽提取液,按重量比计算,即亚麻籽:水为1:30的比例,将100g亚麻籽加入到60-65℃的3000g水中,搅拌条件下进行混合,同时控制转速300r/min,水浴恒温65℃进行提取30min,然后过滤,所得的上清液以300r/min转速搅拌降到室温,即得亚麻籽提取液;The flaxseed extract is calculated by weight ratio, that is, the ratio of flaxseed: water is 1:30, 100g of flaxseed is added to 3000g of water at 60-65°C, and mixed under stirring conditions, while controlling the speed of 300r/ min, extract in a water bath at a constant temperature of 65°C for 30 min, then filter, and stir the obtained supernatant at a speed of 300 r/min to room temperature to obtain the linseed extract;
所述天然亚麻籽为油纤两用亚麻种子。The natural linseed is a dual-purpose linseed for oil and fiber.
所述主表面活性剂为十二烷基硫酸钠;The main surfactant is sodium lauryl sulfate;
所述辅助表面活性剂为椰油酰基谷氨酸三乙醇胺盐;Described cosurfactant is cocoyl glutamic acid triethanolamine salt;
所述增稠剂为卡波姆与羟丙基纤维素按重量比计算,即卡波姆:羟丙基纤维素为1:0.5组成的混合物;The thickener is calculated by weight ratio of carbomer and hydroxypropyl cellulose, that is, carbomer: hydroxypropyl cellulose is a mixture composed of 1:0.5;
所述调理剂为十六烷基三甲基氯化铵、阳离子瓜尔胶、乳化硅油和十六十八醇按重量比计算,即十六烷基三甲基氯化铵:阳离子瓜尔胶:乳化硅油:十六十八醇为1:0.3:2:0.4组成的混合物;The conditioner is cetyltrimethylammonium chloride, cationic guar gum, emulsified silicone oil and cetostearyl alcohol calculated by weight ratio, i.e. cetyltrimethylammonium chloride: cationic guar gum : Emulsified silicone oil: Cetostearyl alcohol is a mixture of 1:0.3:2:0.4;
所述pH调节剂为三乙醇胺和柠檬酸按重量百分比计算,即三乙醇胺:柠檬酸为1:0.001-0.2组成的混合物;The pH regulator is calculated by weight percentage of triethanolamine and citric acid, that is, a mixture of triethanolamine: citric acid at a ratio of 1:0.001-0.2;
所述防腐剂为尼泊金丙酯。Described preservative is propylparaben.
上述的一种含有亚麻籽提取液的洗发水的制备方法,步骤如下:A kind of preparation method of above-mentioned shampoo containing linseed extract, the steps are as follows:
首先将增稠剂中的卡波姆组分均匀分散于2/3总重量的亚麻籽提取液中,分散均匀后升温至65-75℃,然后依次加入主表面活性剂和辅助表面活性剂,混合均匀后降温至55-60℃,再加入调理剂,混合均匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的的亚麻籽提取液,混合均匀后即得含有亚麻籽提取液的洗发水。First, the carbomer component in the thickener is evenly dispersed in 2/3 of the total weight of the flaxseed extract, and after the dispersion is uniform, the temperature is raised to 65-75°C, and then the main surfactant and the auxiliary surfactant are added in sequence, After mixing evenly, cool down to 55-60°C, then add conditioner, continue to cool down to 38-42°C after mixing evenly, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total The flaxseed extract of 50 wt.% is mixed evenly to obtain the shampoo containing the flaxseed extract.
实施例5Example 5
一种含有亚麻籽提取液的洗发水,按重量百分比计算,其原料组成及含量如下:A shampoo containing linseed extract, calculated by weight percentage, its raw material composition and content are as follows:
所述的亚麻籽提取液,按重量比计算,即亚麻籽:水为1:30的比例,将100g亚麻籽加入到60-65℃的3000g水中,搅拌条件下进行混合,同时控制转速300r/min,水浴恒温65℃进行提取30min,然后过滤,所得的上清液以300r/min转速搅拌降到室温,即得亚麻籽提取液;The flaxseed extract is calculated by weight ratio, that is, the ratio of flaxseed: water is 1:30, 100g of flaxseed is added to 3000g of water at 60-65°C, and mixed under stirring conditions, while controlling the speed of 300r/ min, extract in a water bath at a constant temperature of 65°C for 30 min, then filter, and stir the obtained supernatant at a speed of 300 r/min to room temperature to obtain the linseed extract;
所述天然亚麻籽为油纤两用亚麻种子。The natural linseed is a dual-purpose linseed for oil and fiber.
所述主表面活性剂为月桂醇硫磺酸钠;Described primary surfactant is sodium lauryl sulfur sulfate;
所述辅助表面活性剂为甲基椰油酰基牛磺酸钠与月桂基二甲基氨基醋酸甜菜碱按重量比计算,即甲基椰油酰基牛磺酸钠:月桂基二甲基氨基醋酸甜菜碱为2:1组成的混合物;The cosurfactant is sodium methyl cocoyl taurate and lauryl dimethyl aminoacetate betaine calculated by weight ratio, i.e. sodium methyl cocoyl taurate: lauryl dimethyl aminoacetate betaine The base is a mixture composed of 2:1;
所述增稠剂为卡波姆、羟丙基纤维素,按重量比计算,即卡波姆:羟丙基纤维素为1:4组成的混合物;The thickener is carbomer and hydroxypropyl cellulose, calculated by weight ratio, that is, carbomer: hydroxypropyl cellulose is a mixture of 1:4;
所述调理剂为十六烷基三甲基氯化铵、阳离子瓜尔胶、乳化硅油、十六十八醇和植物油脂按重量比计算,即十六烷基三甲基氯化铵:阳离子瓜尔胶:乳化硅油:十六十八醇为1:0.3:2:0.4组成的混合物;The conditioner is cetyltrimethylammonium chloride, cationic guar gum, emulsified silicone oil, cetostearyl alcohol and vegetable oil by weight ratio, namely cetyltrimethylammonium chloride: cationic guar gum Er gum: emulsified silicone oil: cetostearyl alcohol is a mixture of 1:0.3:2:0.4;
所述pH调节剂为氢氧化钠与柠檬酸按重量百分比计算,即氢氧化钠:柠檬酸为1:0.001-0.2组成的混合物;The pH regulator is calculated by weight percentage of sodium hydroxide and citric acid, namely sodium hydroxide: citric acid is a mixture of 1:0.001-0.2;
所述防腐剂为卡松。The preservative is Kathon.
上述的一种含有亚麻籽提取液的洗发水的制备方法,步骤如下:A kind of preparation method of above-mentioned shampoo containing linseed extract, the steps are as follows:
首先将增稠剂中的卡波姆组分均匀分散于2/3总重量的亚麻籽提取液中,分散均匀后升温至65-75℃,然后依次加入主表面活性剂和辅助表面活性剂,混合均匀后降温至55-60℃,再加入调理剂,混合均匀后继续降温至38-42℃,然后加入余下的增稠剂组分、pH调节剂、防腐剂,最后加入剩余1/3总重量的的亚麻籽提取液,混合均匀后即得含有亚麻籽提取液的洗发水。First, the carbomer component in the thickener is evenly dispersed in 2/3 of the total weight of the flaxseed extract, and after the dispersion is uniform, the temperature is raised to 65-75°C, and then the main surfactant and the auxiliary surfactant are added in sequence, After mixing evenly, cool down to 55-60°C, then add conditioner, continue to cool down to 38-42°C after mixing evenly, then add the remaining thickener components, pH regulators, preservatives, and finally add the remaining 1/3 of the total The flaxseed extract of 50 wt.% is mixed evenly to obtain the shampoo containing the flaxseed extract.
根据国标QB/T1974-2004对上述实施例1-5所得的5种含有亚麻籽提取液的洗发水的理化指标进行测试,结果见下表:According to the national standard QB/T1974-2004, the physical and chemical indicators of 5 kinds of shampoos containing the linseed extract obtained in the above-mentioned embodiments 1-5 are tested, and the results are shown in the following table:
从上表中可以看出实施例1-5所得的5种含有亚麻籽提取液的洗发水的各项理化指标均符合国标QB/T1974-2004洗发水要求中的各项理化指标。It can be seen from the above table that the physical and chemical indexes of the five shampoos containing flaxseed extract obtained in Examples 1-5 all meet the physical and chemical indexes in the national standard QB/T1974-2004 shampoo requirements.
应用实施例Application example
将上述实施例1-5所得的含亚麻籽提取液的洗发水,以市场上洗护兼具的洗发水为对照,进行洗发水人群半头测试。The shampoo containing the linseed extract obtained in the above-mentioned Examples 1-5 was compared with the shampoo on the market that has both washing and care, and the half-head test of the shampoo crowd was carried out.
洗发水人群半头测试,先把测试人的头发从中间分成左右两部分,两部分各使用ー款测试洗发水样品,分别轻揉左右两部分头发,至洗发水完全涂抹到所有头发上,并评估洗发水的稠度和铺展性,泡沫的大小和细腻度,大约揉60秒,然后冲水,在冲水时感觉头发的柔顺度,洗发水的冲洗性。冲洗后,感觉左右两边头发的顺滑度、柔软性,并用两把相同的梳子同时梳理两边头发,评估易梳理性。用电吹风把头发吹至八成干,再次评估两边头发的顺滑度、柔软性、光泽度、梳理性和抗静电性能。调查30名受试者使用本发明所得的含有亚麻籽提取液的洗发水与对照所用的洗护兼具的洗发水的情況。对各方面性能进行打分,5分为效果显著(最高分),1分为不明显(最低分),2-4分为有效,综合数据取平均值,最后将数据汇集统计,进行分析,结果见下表:For the half-head test of the shampoo crowd, first divide the tester's hair from the middle into left and right parts, use a test shampoo sample for each of the two parts, gently rub the left and right parts of hair, until the shampoo is completely applied to all hair, and Evaluate the consistency and spreadability of the shampoo, the size and fineness of the foam, knead for about 60 seconds, then flush, feel the softness of the hair when flushing, and the rinseability of the shampoo. After rinsing, feel the smoothness and softness of the hair on the left and right sides, and use two identical combs to comb the hair on both sides at the same time to evaluate the combability. Blow the hair to 80% dry with a hair dryer, and evaluate the smoothness, softness, gloss, combability and antistatic properties of the hair on both sides again. Investigate 30 test subjects using the shampoo containing the linseed extract obtained by the present invention and the condition of both washing and care shampoos used in the control. Score all aspects of performance, 5 points for significant effect (highest score), 1 point for insignificant effect (lowest score), 2-4 points for effective, comprehensive data is averaged, and finally the data is collected and analyzed for analysis. See the table below:
从上表的结果中可以看出,实施例1-5所得的含亚麻籽提取液的洗发水,相较于对照即市场上洗护兼具的洗发水,稠度和在头发上的铺展性及冲洗效果相同的条件下,用于头发形成泡沫细腻度、头发柔顺度、冲洗后湿发的柔顺度、柔软性和易梳理性,及干发的各项评价指标都有提升效果。由此表明了本发明所得的含有亚麻籽提取液的洗发水,由于含有的亚麻籽提取液能够与洗发水中的其他成分协同增效,在达到清洁头发基础上滋养调理头发,使头发莹润黑亮。As can be seen from the results in the table above, the shampoo containing flaxseed extract obtained in Examples 1-5, compared with the shampoo that has both washing and care on the market, has a better consistency and spreadability on the hair. Under the same condition of rinsing effect, the fineness of foam formed by hair, hair suppleness, softness, softness and combability of wet hair after rinsing, and various evaluation indicators of dry hair all have improved effects. This shows that the shampoo containing flaxseed extract obtained in the present invention, because the contained flaxseed extract can be synergistic with other ingredients in the shampoo, nourishes and regulates the hair on the basis of cleaning the hair, making the hair shiny and moist Black and bright.
综上所述,本发明的一种含亚麻籽提取液的洗发水,具有清洁与保湿、护发的功效,修护受损发质,保持头发柔顺亮泽。In summary, the shampoo containing linseed extract of the present invention has the functions of cleaning, moisturizing and hair care, repairs damaged hair, and keeps hair soft and shiny.
以上所述仅是本发明的实施方式的举例,应当指出,对于本技术领域的普通技术人员来说,在不脱离本发明技术原理的前提下,还可以做出若干改进和变型,这些改进和变型也应视为本发明的保护范围。The foregoing is only an example of the embodiment of the present invention. It should be pointed out that for those of ordinary skill in the art, some improvements and modifications can be made without departing from the technical principles of the present invention. These improvements and Modifications should also be regarded as the scope of protection of the present invention.
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CN105176691A (en) * | 2015-08-26 | 2015-12-23 | 湖州旭龙生物化学有限公司 | Orange-peel-oil liquid shampoo and preparation method thereof |
CN105267100A (en) * | 2015-11-18 | 2016-01-27 | 华文蔚 | Hair conditioner with ginger and angelica sinensis ingredients |
CN107982082A (en) * | 2016-10-26 | 2018-05-04 | 日油株式会社 | Transparent class shampoo Compositions |
CN109512755A (en) * | 2017-11-24 | 2019-03-26 | 北京东方淼森生物科技有限公司 | With exterior-applied plant extract, the head nursing product and preparation method thereof for nourishing the submissive brighten the hair effect of maintenance |
CN112933012A (en) * | 2021-03-04 | 2021-06-11 | 西双版纳傣密药业有限公司 | Formula of hair growing and blackening shampoo and preparation method thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN105176691A (en) * | 2015-08-26 | 2015-12-23 | 湖州旭龙生物化学有限公司 | Orange-peel-oil liquid shampoo and preparation method thereof |
CN105267100A (en) * | 2015-11-18 | 2016-01-27 | 华文蔚 | Hair conditioner with ginger and angelica sinensis ingredients |
CN107982082A (en) * | 2016-10-26 | 2018-05-04 | 日油株式会社 | Transparent class shampoo Compositions |
CN107982082B (en) * | 2016-10-26 | 2021-12-31 | 日油株式会社 | Transparent shampoo composition |
CN109512755A (en) * | 2017-11-24 | 2019-03-26 | 北京东方淼森生物科技有限公司 | With exterior-applied plant extract, the head nursing product and preparation method thereof for nourishing the submissive brighten the hair effect of maintenance |
CN112933012A (en) * | 2021-03-04 | 2021-06-11 | 西双版纳傣密药业有限公司 | Formula of hair growing and blackening shampoo and preparation method thereof |
CN112933012B (en) * | 2021-03-04 | 2022-06-10 | 西双版纳傣密药业有限公司 | Formula of hair growing and blackening shampoo and preparation method thereof |
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