A kind of preparation method of the moisturizing cream containing dendrobium candidum
Technical field
The present invention relates to cosmetic field is and in particular to a kind of preparation method of the moisturizing cream containing dendrobium candidum.
Background technology
In recent years, with the raising of people's standard of living, the spending amount proportion of washing product constantly increases, and people are to flesh
The nursing of skin is increasingly paid attention to, and natural cosmetics are extremely pursued.But the environmental pollution in process of industrialization, the daily four seasons are more
Replace, temperature change that air conditioner eructation brings and pressure, and the metabolism of human normal, skin senescence etc. causes skin moisture
Run off, any season, age, skin quality are all to carry out intensive care on the basis of skin replenishing water and preserving moisture.
The basic reason that the aging phenomenons such as water shortage is that skin is dim, be dried, jaundice, lax and wrinkle produce.Conventional guarantor
Humectant has glycerine, sorbierite, propane diols, can absorb water from environment;Sodium hyaluronate is naturally occurring in tissue skin corium
Material, there is surprising water absorbing capacity, powerful moisture-keeping function;And dendrobium candidum chemical composition is various, mainly have alkaloid,
Polysaccharide, amino acid, luxuriant and rich with fragrance class Compound Compound etc..Have enhancing human body immune function, antitumor, anti-aging, antifatigue, fall blood
Sugared the effects such as, by bioactivation moisturizing compound prescription, the potent skin that compacts, Chinese patent CN 104127341 A just illustrates
Dendrobium candidum adjusts the application in skin collagen metabolism or cosmetics in preparation, maintains enough collagenous fibres and elasticity fine
Dimension, delays the aging of purple skin.
The vine of multiflower knotweed is also called red Pueraria lobota, nine true rattans, chess rattan, is that the fleece-flower root belongs to;External application can treat pruitus, equally has sterilization
Disinfective action;And tea oil equally have moisturizing, moisturizing, anti-inflammation, sun-proof the effects such as.
Content of the invention
It is an object of the invention to provide a kind of moisturiser, specifically a kind of moisturizing cream containing dendrobium candidum, this kind of cream
Frost has good moisturizing antibacterial action.
Technical scheme for realizing purpose of the present invention employing is as follows:
1)Formula
Dendrobium candidum extract 10~20 weight portion;
Caulis Polygoni Multiflori extract 7~15 weight portion;
Stearic acid 1~7 weight portion;
Isopropyl myristate 2~8 weight portion;
Hexadecanol 2~6 weight portion;
Tea oil 1~5 weight portion;
Glycerin monostearate 0.5~5 weight portion;
Beeswax 2~6 weight portion;
Triethanolamine 0.1~2 weight portion;
Tween-80 0.1~3 weight portion;
Arlacel-80 0.1~1.5 weight portion;
Sodium hyaluronate 0.1~1.0 weight portion;
Amino acid humectant 1~10 weight portion;
Glycerine 1~5 weight portion;
Sorbierite 15 weight portion;
Vitamin E 0.5~3 weight portion;
Essential oil 0.05~1 weight portion;
Deionized water 10~70 weight portion.
Wherein said essential oil is one of rose hip oil, lavender oil, lilac oil.
Described dendrobium candidum extract, prepares in accordance with the following methods:
(1)By 65 weight portion dendrobium candidums clean, pulverize, be dispersed in water and stir be thoroughly mixed to form dendrobium candidum suspend
Liquid, dendrobium candidum: the weight part ratio of water is 1:8;
(2)Add 1.1 part by weight of cellulose enzymes under the conditions of 45 DEG C in dendrobium candidum suspension, stirring, react 2.5h;
(3)Continuously add 0.75 weight portion hemicellulase, stirring, react 2.5h;
(4)Continuously add 0.75 weight portion pectase, stirring, react 1.5h;
(5)Control temperature to be 45 DEG C, adjust pH to 4.5, stir after adding 1 weight portion mannase, react 2.5h;
(6)Continuously add 1.2 weight portion neutral proteinase stirrings, 2h after reaction fully, filter, remove filter residue;
(7)Concentrate the filtrate to 2~2.5 times of dendrobium candidum weight portion, obtain final product dendrobium candidum extract.
Described Caulis Polygoni Multiflori extract, prepares in accordance with the following methods:
20~40 weight portion vines of multiflower knotweed will be weighed, be immersed in 12 hours in 2~2.5 times of weight portion water, then at 80~85 DEG C
Soak 5 hours under water-bath, cooled and filtered removes filter residue and obtains Caulis Polygoni Multiflori extract.
2) prepare
First dendrobium candidum extract, Caulis Polygoni Multiflori extract ratio by weight is added in deionized water, puts into 40 DEG C of water
Heat in bath;Then magnetic agitation effect under add successively triethanolamine, Tween-80, sodium hyaluronate, amino acid humectant,
Glycerine, sorbierite, vitamin E formed mixture A, by mixture A be warmed up to 70~80 DEG C standby;By joining in another reactor
Weight portion in side sequentially adds stearic acid, isopropyl myristate, hexadecanol, tea oil, glycerin monostearate, beeswax, department
Disk -80, are positioned over heating for dissolving in 70~80 DEG C of water-baths, form mixture B;Mixture B is equal under quick stirring action
Even being poured in mixture A forms product, adjusts the pH of product between 6.5~7 with citric acid after 2min;Afterwards will
Product is placed under refiner, is homogenized 4min under 1.8w/min power;To be cooled to 38~44 DEG C when, plus essential oil blending, cold
But stand 3d to room temperature, obtain a kind of moisturizing cream containing dendrobium candidum.
Other reagent used in technical solution of the present invention, purchase and common drug company.
Advantages of the present invention is:Product property safety of the present invention, emulsification system is stable, simple production process, smear after no
Thick and heavy greasy feeling;Except adding glycerine, the sorbierite NMF on basis, also amino acid humectant and NMF glass urine
Acid, moistening effect is good, as patent CN104323953A " a kind of natural active hydrating cream containing Effects of Extracts of Grifola frondosa on Active " is only added
Without interworkings such as dendrobium candidum, sorbierite, sodium hyaluronate, amino acid humectants, performance of keeping humidity has much room for improvement glycerine;Add iron
Skin stem of noble dendrobium fleece-flower root rattan increases certain antibiotic skin-care effect, can increase the development and application of both species, and patent
CN104546588A only has simple moisture-keeping function, and no other effects such as anti-inflammation;Adding tea oil can moisturizing, moisturizing, anti-
Bacterium anti-inflammatory, sun-proof the effects such as;The organoleptic indicator of finished product of the present invention and physical and chemical index all meet regulation and require.
Specific embodiment
In order to deepen the understanding of the present invention and understanding, specific embodiment is described below, and the invention will be further described
And introduction.
Embodiment 1
1)Formula
Dendrobium candidum extract 10g, Caulis Polygoni Multiflori extract 7g, stearic acid 1g, isopropyl myristate 2g, hexadecanol 2g, tea oil
2g, glycerin monostearate 1g, beeswax 1g, triethanolamine 0.5g, Tween-80 0.5g, Arlacel-80 0.2g, sodium hyaluronate 0.1g,
Amino acid humectant 1g, glycerine 1g, sorbierite 1g, vitamin E 0.5g, citric acid 0.3g, essential oil 0.5g, deionized water 70g.
Described dendrobium candidum extract, prepares in accordance with the following methods:
(1)65g dendrobium candidum is cleaned, pulverizes, be scattered in 520g water and stir and be thoroughly mixed to form dendrobium candidum suspension;
(2)Add 1.1g cellulase, stirring in dendrobium candidum suspension, fully react 2.5h under the conditions of 45 DEG C;
(3)Add 0.75g hemicellulase, stirring, fully react 2.5h;
(4)Add 0.75g pectase, stirring, fully react 1.5h;
(5)Reduce temperature to 45 DEG C, adjust pH to 4.5, stir after adding 1g mannase, fully react 2.5h;
(6)Add the stirring of 1.2g neutral proteinase, 2h after reaction fully in suspension, filter, remove filter residue;
(7)Concentrate the filtrate to 130g, obtain final product dendrobium candidum extract.
Described Caulis Polygoni Multiflori extract, prepares in accordance with the following methods:
The 25g vine of multiflower knotweed will be weighed, be immersed in 50g and go 12 hours in water, then in 85 DEG C of water-baths 5 hours, cooled and filtered obtained
To Caulis Polygoni Multiflori extract.
2) prepare
First dendrobium candidum extract, Caulis Polygoni Multiflori extract are added in deionized water by formula, put in 40 DEG C of water-baths
Heating;Then triethanolamine, Tween-80, sodium hyaluronate, amino acid humectant, glycerine, mountain are added successively under magnetic agitation effect
Pears alcohol, vitamin E form mixture A, and mixture A is warmed up to 75 DEG C;Tristearin is sequentially added by formula in another reactor
Acid, isopropyl myristate, hexadecanol, tea oil, glycerin monostearate, beeswax, Arlacel-80, are positioned in 75 DEG C of water-baths
Heating for dissolving forms mixture B;Mixture B is uniformly poured under quick stirring action formation product in mixture A,
The pH of product is adjusted 6.5 with citric acid after 2min;Afterwards product is placed under refiner, even under 1.8w/min power
Slurry 4min;To be cooled to 40 DEG C when, plus essential oil blending, stand 3d after being cooled to room temperature, obtain containing prepared by the present embodiment
The moisturizing cream of dendrobium candidum.
Embodiment 2
1)Formula
Dendrobium candidum extract 15g, Caulis Polygoni Multiflori extract 10g, stearic acid 3g, isopropyl myristate 4g, hexadecanol 2g, tea oil
4g, glycerin monostearate 2g, beeswax 1g, triethanolamine 0.5g, Tween-80 2g, Arlacel-80 0.6g, sodium hyaluronate 0.3g, ammonia
Base acid NMF 2g, glycerine 1g, sorbierite 1g, vitamin E 0.5g, essential oil 0.75g, deionized water 50g.Described iron sheet stone
Dry measure used in former times extract, prepares in accordance with the following methods:
(1)65g dendrobium candidum is cleaned, pulverizes, be scattered in 520g water and stir and be thoroughly mixed to form dendrobium candidum suspension;
(2)Add 1.1g cellulase, stirring in dendrobium candidum suspension, fully react 2.5h under the conditions of 45 DEG C;
(3)Add 0.75g hemicellulase, stirring, fully react 2.5h;
(4)Add 0.75g pectase, stirring, fully react 1.5h;
(5)Reduce temperature to 45 DEG C, adjust pH to 4.5, stir after adding 1g mannase, fully react 2.5h;
(6)Add the stirring of 1.2g neutral proteinase, 2h after reaction fully in suspension, filter, remove filter residue;
(7)Concentrate the filtrate to 130g, obtain final product dendrobium candidum extract.
Described Caulis Polygoni Multiflori extract, prepares in accordance with the following methods:
The 25g vine of multiflower knotweed will be weighed, be immersed in 12 hours in 60g water, then in 85 DEG C of water-baths 5 hours, cooled and filtered will obtain
Caulis Polygoni Multiflori extract.
2) prepare
First dendrobium candidum extract, Caulis Polygoni Multiflori extract are added in deionized water by weight, put into 40 DEG C of water-baths
Middle heating;Then magnetic agitation effect under add successively triethanolamine, Tween-80, sodium hyaluronate, amino acid humectant, glycerine,
Sorbierite, vitamin E form mixture A, and mixture A is warmed up to 70 DEG C;The weight portion in formula is pressed in another reactor
Sequentially add stearic acid, isopropyl myristate, hexadecanol, tea oil, glycerin monostearate, beeswax, Arlacel-80, be positioned over
Heat in 80 DEG C of water-baths and be completely dissolved, form mixture B;Mixture B is uniformly poured under quick stirring action mixing
Form product in thing A, after 2min, adjust the pH of product between 6.5~7 with citric acid;Afterwards product is placed on homogenate
Under machine, it is homogenized 4min under 1.8w/min power;To be cooled to 44 DEG C when, plus essential oil blending, stand 3d after being cooled to room temperature, obtain
The moisturizing cream containing dendrobium candidum prepared by the present embodiment.
Embodiment 3
1)Formula
Dendrobium candidum extract 15g, Caulis Polygoni Multiflori extract 7g, stearic acid 1g, isopropyl myristate 2g, hexadecanol 2g, tea oil
5g, glycerin monostearate 2g, beeswax 1.5g, triethanolamine 1.2g, Tween-80 0.8g, Arlacel-80 0.2g, sodium hyaluronate
0.1g, amino acid humectant 2g, glycerine 3g, sorbierite 2g, vitamin E 1g, citric acid 0.7g, essential oil 0.085g, deionized water
15g.
Described dendrobium candidum extract, prepares in accordance with the following methods:
(1)By 65g dendrobium candidum clean, pulverize, be scattered in 520g water, and stir be thoroughly mixed to form dendrobium candidum suspend
Liquid;
(2)Add 1.1g cellulase, stirring in dendrobium candidum suspension, fully react 2.5h under the conditions of 45 DEG C;
(3)Add 0.75g hemicellulase, stirring, fully react 2.5h;
(4)Add 0.75g pectase, stirring, fully react 1.5h;
(5)Reduce temperature to 45 DEG C, adjust pH to 4.5, stir after adding 1g mannase, fully react 2.5h;
(6)Add the stirring of 1.2g neutral proteinase, 2h after reaction fully in suspension, filter, remove filter residue;
(7)Concentrate the filtrate to 130g, obtain final product dendrobium candidum extract.
Described Caulis Polygoni Multiflori extract, prepares in accordance with the following methods:
The 30g vine of multiflower knotweed will be weighed, be immersed in 12 hours in 70g water, then in 80 DEG C of water-baths 5 hours, cooled and filtered will obtain
Caulis Polygoni Multiflori extract.
2) prepare
First dendrobium candidum extract, Caulis Polygoni Multiflori extract are added in deionized water by weight, put into 40 DEG C of water-baths
Middle heating;Then magnetic agitation effect under add successively triethanolamine, Tween-80, sodium hyaluronate, amino acid humectant, glycerine,
Sorbierite, vitamin E form mixture A, and mixture A is warmed up to 80 DEG C;The weight portion in formula is pressed in another reactor
Sequentially add stearic acid, isopropyl myristate, hexadecanol, tea oil, glycerin monostearate, Arlacel-80, be positioned over 75 DEG C of water
In bath, heating is completely dissolved, and forms mixture B;Mixture B is uniformly poured into shape in mixture A under quick stirring action
Become product, use the pH value of lemon acidity test product after 2min between 6.5~7;Afterwards product is placed on refiner
Under, it is homogenized 4min under 1.8w/min power;To be cooled to 44 DEG C when, plus essential oil blending, stand 3d after being cooled to room temperature, obtain
The moisturizing cream containing dendrobium candidum prepared by the present embodiment.
Embodiment 4
1)Formula
Dendrobium candidum extract 20g, Caulis Polygoni Multiflori extract 14g, stearic acid 5g, isopropyl myristate 4g, hexadecanol 3g, tea oil
5g, glycerin monostearate 1g, beeswax 0.5g, triethanolamine 1.5g, Tween-80 1.3g, Arlacel-80 0.6g, sodium hyaluronate
0.2g, amino acid humectant 1.5g, glycerine 1g, sorbierite 2g, vitamin E 1.5g, citric acid 1g, essential oil 0.15g, deionization
Water 70g.
Described dendrobium candidum extract, prepares in accordance with the following methods:
(1)65g dendrobium candidum is cleaned, pulverizes, be scattered in 520g water and stir and be thoroughly mixed to form dendrobium candidum suspension;
(2)Add 1.1 parts of cellulases, stirring in dendrobium candidum suspension, fully react 2.5h under the conditions of 45 DEG C;
(3)Add 0.75g hemicellulase, stirring, fully react 2.5h;
(4)Add 0.75g pectase, stirring, fully react 1.5h;
(5)Reduce temperature to 45 DEG C, adjust pH to 4.5, stir after adding 1g mannase, fully react 2.5h;
(6)Add the stirring of 1.2g neutral proteinase, 2h after reaction fully in suspension, filter, remove filter residue;
(7)Concentrate the filtrate to 130g, obtain final product dendrobium candidum extract.
Described Caulis Polygoni Multiflori extract, prepares in accordance with the following methods:
The 30g vine of multiflower knotweed will be weighed, be immersed in 12 hours in 60g deionized water, then in 85 DEG C of water-baths 5 hours, mistake after cooling
Filter obtains Caulis Polygoni Multiflori extract.
2) prepare
First dendrobium candidum extract, Caulis Polygoni Multiflori extract are added in deionized water by weight, put into 40 DEG C of water-baths
Middle heating;Then magnetic agitation effect under add successively triethanolamine, Tween-80, sodium hyaluronate, amino acid humectant, glycerine,
Sorbierite, vitamin E form mixture A, and mixture A is warmed up to 70 DEG C;Reaction weight portion is pressed successively in another reactor
Add stearic acid, isopropyl myristate, hexadecanol, tea oil, glycerin monostearate, Arlacel-80, be positioned over 70 DEG C of water-baths
Middle heating is completely dissolved, and forms mixture B;Mixture B is uniformly poured under quick stirring action in mixture A and forms life
Become thing, use the pH value of lemon acidity test product after 2min between 6.5~7;Afterwards product is placed under refiner,
It is homogenized 4min under 1.8w/min power;To be cooled to 44 DEG C when, plus essential oil blending, stand 3d after being cooled to room temperature, obtain this reality
Apply the moisturizing cream containing dendrobium candidum prepared by example.
The foregoing is only embodiments of the invention, not thereby limit the protection domain of the patent application of the present invention, all
It is the equivalent structure or equivalent flow conversion made using present specification content, or be directly or indirectly used in other related skills
Art field, is all included in the same manner in the protection domain of the patent application of the present invention.