CN113230184A - Scalp composition for 1+1 scalp hair cleaning and preparation method thereof - Google Patents
Scalp composition for 1+1 scalp hair cleaning and preparation method thereof Download PDFInfo
- Publication number
- CN113230184A CN113230184A CN202110559338.0A CN202110559338A CN113230184A CN 113230184 A CN113230184 A CN 113230184A CN 202110559338 A CN202110559338 A CN 202110559338A CN 113230184 A CN113230184 A CN 113230184A
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- China
- Prior art keywords
- parts
- stirring
- extract
- scalp
- peg
- Prior art date
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Abstract
The invention discloses a scalp composition for 1+1 scalp hair cleaning, which comprises water and the following components in parts by weight: disodium lauryl sulfosuccinate, cocamide MEA, cocamidopropyl betaine, glycerol, glyceryl stearate, propylene glycol, polyquaternium-7, acrylic acid (ester) copolymers, sodium chloride, PEG-120 methylglucdioleate, PEG-7 glyceryl cocoate, PPG-3 octyl ether, guar hydroxypropyltrimonium chloride, polyquaternium-10, essences, plant functional components, preservatives, citric acid, panthenol, sodium hydroxide, DMDM hydantoin, menthol, Hamamelis virginiana extract, aloe vera extract, niacinamide, tocopheryl acetate, pyridoxine HCL, piroctone olamine, allantoin, and EDTA-disodium.
Description
Technical Field
The invention belongs to the technical field of hair washing and caring cosmetics, and particularly relates to a scalp composition for cleaning scalp hair 1+1 and a preparation method thereof.
Background
With environmental pollution caused by the rapid development of society, the factors such as increasing living pressure, irregular diet, perm and hair dyeing of people and the like seriously affect the hair health of people. The problems of greasy hair, dandruff, alopecia and the like bring serious troubles to the daily life of people.
Dandruff is a chronic, recurrent, more common scalp problem, manifested by the loss of keratinocytes aggregated into macroscopic clumps with a diameter greater than 0.2 mm. The pathological examination is manifested by keratinocyte parakeratosis, overgrowth, and misalignment. Except for flaky desquamation, dandruff is mainly clinically manifested by pruritus, dry and tense scalp, stabbing pain, and subclinical inflammation change.
The factors for generating dandruff are many, and relate to various factors such as scalp lipid, scalp microecology, scalp physiology, immunity and antioxidation. In addition, dry weather or seriously polluted environment damages the scalp barrier to cause scalp dryness and pruritus, thereby causing scalp inflammation, further causing abnormal scalp keratosis and generating dandruff; in addition, the problems of various intractable scurf and head itch caused by the over-stressed work and life and irregular living habits of people can even generate the symptoms of scalp hair follicle inflammation, pimple, scalp moss, and the like.
In order to solve these problems, a great variety of hair care products are available on the market. The applicant researches and discovers that most of products in the market have single functions, the adopted raw materials of the products are mostly artificially synthesized substances, the substances inevitably have certain side effects such as irritation and the like, and the long-term use of the substances inevitably causes influence on human bodies. Moreover, the obtained effect is not ideal.
In addition, most of the anti-dandruff agents used in the existing common anti-dandruff shampoo products are antifungal chemotherapeutic drugs, such as zinc pyrithione ZPT, tin sulfide, climbazole, OCT, hexamidine, ketoconazole and the like, which intensively inhibit Malassezia (Malassezia), and although the anti-dandruff agents can remove dandruff, the scalp can be damaged after long-term use. In addition, most of cationic polymers added in the existing shampoo are high-molecular-weight silicone oil silica gel, have high irritation, and can not only nourish scalp but also irritate scalp.
Disclosure of Invention
The present invention is to solve the above technical problems and to provide a method.
In order to solve the problems, the invention is realized according to the following technical scheme:
in a first aspect, the present invention provides a scalp composition for 1+1 scalp hair cleansing, characterized by comprising water and the following components in parts by weight:
35-55 parts of disodium lauryl sulfosuccinate, 1-3 parts of cocamide MEA, 3-10 parts of cocamidopropyl betaine, 3-12 parts of glycerol, 0.5-2.0 parts of glycerol stearate, 0.5-2.0 parts of propylene glycol, 70.5-3.0 parts of polyquaternium, 0.5-5.0 parts of acrylic acid (ester) copolymer, 0.5-2.0 parts of sodium chloride, 0.1-1.0 parts of PEG-120 methyl glucose dioleate, 0.2-1.0 parts of PEG-7 glycerol cocoate, 0.1-1.0 parts of PPG-3 octyl ether, 0.1-0.35 parts of guar hydroxypropyl trimethyl ammonium chloride, 100.1-0.3 parts of polyquaternium, 0.2-0.8 parts of essence, 0.1-3.0 parts of plant functional component, 0.05-0.09 parts of preservative, 0.1-0.5 parts of citric acid, 0.5 parts of hydantoin, 0.1-0.5 parts of panthenol, 0.5 parts of DMM 0.05-0 parts of menthol extract, 0.15 parts of Hamamelis mollis extract, 0.05-0.0.0 parts of DMM-15 parts of DMT 0.05-0 parts of menthol extract, 0.5-2 parts of aloe extract, 0.5-2 parts of nicotinamide, 0.5-2 parts of tocopherol acetate, 0.2-1 part of pyridoxine HCL, 0.1-0.4 part of piroctone olamine, 0.5-2 parts of allantoin and 0.05-0.1 part of EDTA-disodium.
Preferably, the plant functional component is a mixture of butylene glycol, water, an extract of astragalus membranaceus, an extract of saposhnikovia divaricata roots, an extract of calendula officinalis, an extract of albizia julibrissin flowers and an extract of gastrodia elata roots.
Preferably, the plant extract in the scalp composition is prepared by the following plant extraction procedures:
selecting each plant raw material to be extracted, and cleaning and sterilizing the plant raw materials for later use;
various plant materials are extracted by a water extraction process to obtain plant extracts.
Preferably, the preservative is methyl chloro isothiazolinone and a mixture of methyl isothiazolinone and magnesium oxide and magnesium nitrate, and the preservative meets the requirements of national standard GB/T29666-2013 preservative for cosmetics.
Preferably, the scalp composition is prepared by the following method:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is between 80 and 85 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 15 to 20 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 70-75 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the temperature of the stirring pot solution is reduced to 70-75 ℃, stirring uniformly, and continuously reducing the temperature;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 5.5-6.5, and stirring for 20-30 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
In a second aspect, the present invention also provides a method of preparing a scalp composition for 1+1 scalp hair cleansing comprising water and the following components in parts by weight:
35-55 parts of disodium lauryl sulfosuccinate, 1-3 parts of cocamide MEA, 3-10 parts of cocamidopropyl betaine, 3-12 parts of glycerol, 0.5-2.0 parts of glycerol stearate, 0.5-2.0 parts of propylene glycol, 70.5-3.0 parts of polyquaternium, 0.5-5.0 parts of acrylic acid (ester) copolymer, 0.5-2.0 parts of sodium chloride, 0.1-1.0 parts of PEG-120 methyl glucose dioleate, 0.2-1.0 parts of PEG-7 glycerol cocoate, 0.1-1.0 parts of PPG-3 octyl ether, 0.1-0.35 parts of guar hydroxypropyl trimethyl ammonium chloride, 100.1-0.3 parts of polyquaternium, 0.2-0.8 parts of essence, 0.1-3.0 parts of plant functional component, 0.05-0.09 parts of preservative, 0.1-0.5 parts of citric acid, 0.5 parts of hydantoin, 0.1-0.5 parts of panthenol, 0.5 parts of DMM 0.05-0 parts of menthol extract, 0.15 parts of Hamamelis mollis extract, 0.05-0.0.0 parts of DMM-15 parts of DMT 0.05-0 parts of menthol extract, 0.5-2 parts of aloe extract, 0.5-2 parts of nicotinamide, 0.5-2 parts of tocopherol acetate, 0.2-1 part of pyridoxine HCL, 0.1-0.4 part of piroctone olamine, 0.5-2 parts of allantoin and 0.05-0.1 part of EDTA-disodium;
the scalp composition is prepared by the following method:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is between 80 and 85 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 15 to 20 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 70-75 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the temperature of the stirring pot solution is reduced to 70-75 ℃, stirring uniformly, and continuously reducing the temperature;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 5.5-6.5, and stirring for 20-30 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
Preferably, the plant functional component is a mixture of butylene glycol, water, an extract of astragalus membranaceus, an extract of saposhnikovia divaricata roots, an extract of calendula officinalis, an extract of albizia julibrissin flowers and an extract of gastrodia elata roots.
Preferably, the preservative is methyl chloro isothiazolinone and a mixture of methyl isothiazolinone and magnesium oxide and magnesium nitrate, and the preservative meets the requirements of national standard GB/T29666-2013 preservative for cosmetics.
Compared with the prior art, the invention has the beneficial effects that:
according to the scalp composition product, various mild surfactants and various functional active raw materials are compounded to obtain the scalp composition product, and all substances in the scalp composition product are matched with each other to realize synergistic interaction, so that on one hand, dirt of the scalp can be effectively and thoroughly removed, dead skin cells accumulated in hair follicles and residues of grease can be deeply removed, and excessive grease can be removed. On the other hand, the hair conditioner also has the functions of properly supplementing water and oil to the scalp, realizing proper balance of oil and water, providing a clean and comfortable healthy environment for the scalp and promoting the growth of hair follicles. On the other hand, the product is compounded with a plurality of components which can inhibit and kill fungi and nourish the scalp, thereby promoting the blood circulation of the scalp, improving the activity of scalp cells and promoting the metabolism of scalp cells. According to the invention, various mild surfactants are compounded with various functional active raw materials, the micro-environment of scalp cells is improved, the problems of scalp cleanness, excessive hair oil and dandruff are fundamentally solved, the scalp is provided with sufficient nutrients, and the scalp is nourished and moisturized, so that the scalp is healthy and attractive.
Detailed Description
The following description of the preferred embodiments of the present invention is provided for the purpose of illustration and description, and is in no way intended to limit the invention.
Description of scalp compositions
The invention provides a scalp composition for 1+1 scalp hair cleaning, which is characterized by comprising water and the following components in parts by weight:
35-55 parts of disodium lauryl sulfosuccinate, 1-3 parts of cocamide MEA, 3-10 parts of cocamidopropyl betaine, 3-12 parts of glycerol, 0.5-2.0 parts of glycerol stearate, 0.5-2.0 parts of propylene glycol, 70.5-3.0 parts of polyquaternium, 0.5-5.0 parts of acrylic acid (ester) copolymer, 0.5-2.0 parts of sodium chloride, 0.1-1.0 parts of PEG-120 methyl glucose dioleate, 0.2-1.0 parts of PEG-7 glycerol cocoate, 0.1-1.0 parts of PPG-3 octyl ether, 0.1-0.35 parts of guar hydroxypropyl trimethyl ammonium chloride, 100.1-0.3 parts of polyquaternium, 0.2-0.8 parts of essence, 0.1-3.0 parts of plant functional component, 0.05-0.09 parts of preservative, 0.1-0.5 parts of citric acid, 0.5 parts of hydantoin, 0.1-0.5 parts of panthenol, 0.5 parts of DMM 0.05-0 parts of menthol extract, 0.15 parts of Hamamelis mollis extract, 0.05-0.0.0 parts of DMM-15 parts of DMT 0.05-0 parts of menthol extract, 0.5-2 parts of aloe extract, 0.5-2 parts of nicotinamide, 0.5-2 parts of tocopherol acetate, 0.2-1 part of pyridoxine HCL, 0.1-0.4 part of piroctone olamine, 0.5-2 parts of allantoin and 0.05-0.1 part of EDTA-disodium.
Preferably, the plant functional components of the invention are a mixture of butylene glycol, water, an extract of astragalus membranaceus, an extract of saposhnikovia divaricata roots, an extract of calendula officinalis, an extract of albizia julibrissin flowers and an extract of gastrodia elata roots.
The preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate, and meets the requirements of national standard GB/T29666-2013 preservative for cosmetics.
Further, in the present invention, the plant extract in the scalp composition is prepared by the following plant extraction process:
selecting each plant raw material to be extracted, and cleaning and sterilizing the plant raw materials for later use;
various plant materials are extracted by a water extraction process to obtain plant extracts.
As used herein, "synergy" or "synergistic effect" refers to an effect that occurs when chemical substances or biological structures interact and produce a total effect that is greater than the sum of the individual effects of any one of them.
The astragalus membranaceus extract used in the invention, which is an important active ingredient of astragalus saponin, can stimulate the proliferation of cortical cells and has the effect of conditioning scalp. Has antiaging and antioxidant effects;
the radix sileris root extract used in the invention contains a plurality of coumarin compounds and chromone compounds, has the elimination effect on various free radicals, has a certain inhibition effect on melanin, and can shrink pores. Has antioxidant, astringent, antibacterial, and antiinflammatory effects.
The calendula extract used in the invention has the main active ingredient of carotenoid compounds, inhibits the activity of elastase based on the proliferation effect of the calendula extract on epidermal cells and dermal cells, combines the excellent antioxidant property of the calendula extract, and can enhance the activity of skin, and calendula has certain moisturizing effect.
The research of the applicant finds that the astragalus membranaceus extract, the radix sileris extract, the calendula extract and the 3 specific plant extracts are compounded, and the 3 raw materials are mutually cooperated to play a role in stimulating the proliferation, oxidation resistance, inflammation diminishing and bacteria resistance of cortical cells and inhibiting melanin to a certain extent, so that the hair conditioner has the functions of removing dirt of scalp, nourishing and moistening hair and providing sufficient nutrients for scalp compared with the existing products.
Use of scalp compositions
A method of using a scalp composition for 1+1 scalp hair cleansing comprising the steps of:
step A, firstly, warm water (35-45 ℃) is used for showering scalp and hair;
step B, taking a proper amount of the hair conditioner (5-10g), putting the hair conditioner into the palm of the hand, kneading a little foam, and then applying the foam to scalp hair;
wherein, the wet water is smeared with bubbling massage for a moment (5 to 10 minutes) in a rounding mode, and finally, the massage is washed clean by warm water.
Process for preparing scalp composition for 1+1 scalp hair cleansing
The present invention also provides a preparation method of the above scalp composition for scalp hair 1+1 cleansing, comprising the steps of:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is between 80 and 85 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 15 to 20 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 70-75 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the temperature of the stirring pot solution is reduced to 70-75 ℃, stirring uniformly, and continuously reducing the temperature;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 5.5-6.5, and stirring for 20-30 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
Preparation examples
Example 1
The embodiment 1 provides a plant multi-effect anti-hair loss, hair growth and hair nourishing compound composition, which comprises water and the following components in parts by weight:
35 parts of disodium lauryl sulfosuccinate, 1 part of cocamide MEA, 3 parts of cocamidopropyl betaine, 3 parts of glycerol, 0.5 part of glycerol stearate, 0.5 part of propylene glycol, 70.5 parts of polyquaternary ammonium salt, 0.5 part of acrylic acid (ester) copolymer, 0.5 part of sodium chloride, 0.1 part of PEG-120 methyl glucose dioleate, 0.2 part of PEG-7 glycerol cocoate, 0.1 part of PPG-3 octyl ether, 0.1 part of guar gum hydroxypropyl trimethyl ammonium chloride, 100.1 parts of polyquaternary ammonium salt and 0.2 part of essence, 0.1 part of plant functional component, 0.05 part of preservative, 0.1 part of citric acid, 0.1 part of panthenol, 0.1 part of sodium hydroxide, 0.15 part of DMDM hydantoin, 0.05 part of menthol, 0.5 part of Hamamelis virginiana extract, 0.5 part of aloe extract, 0.5 part of nicotinamide, 0.5 part of tocopherol acetate, 0.2 part of pyridoxine HCL, 0.1 part of piroctone olamine salt, 0.5 part of allantoin and 0.05 part of EDTA-disodium.
Wherein the plant functional components are butylene glycol, water, an extract of astragalus membranaceus, an extract of divaricate saposhnikovia root, an extract of calendula, a mixture of an extract of albizia julibrissin and an extract of gastrodia elata root. The preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate.
The scalp composition is prepared by the following method:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is up to 80 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 15 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 70 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the solution in the stirring pot is cooled to 70 ℃, stirring uniformly, and continuously cooling;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 6, and stirring for 20 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
Example 2
The embodiment 2 provides a plant multi-effect anti-hair loss, hair growth and hair nourishing compound composition, which comprises water and the following components in parts by weight:
45 parts of disodium lauryl sulfosuccinate, 2 parts of cocamide MEA (MEA), 7 parts of cocamidopropyl betaine, 6 parts of glycerol, 1 part of glycerol stearate, 1 part of propylene glycol, 71.5 parts of polyquaternium, 2.5 parts of acrylic acid (ester) copolymer, 1 part of sodium chloride, 0.4 part of PEG-120 methyl glucose dioleate, 0.3 part of PEG-7 glycerol cocoate, 0.4 part of PPG-3 octyl ether, 0.15 part of guar hydroxypropyl trimethyl ammonium chloride, 100.2 parts of polyquaternium, 0.4 part of essence, 1.5 parts of plant functional component, 0.06 part of preservative, 0.3 part of citric acid, 0.3 part of panthenol, 0.3 part of sodium hydroxide, DMDM hydantoin and dimethyl sulfoxide
0.2 part, 0.06 part of menthol, 1.5 parts of witch hazel extract, 1 part of aloe extract, 1 part of nicotinamide, 1 part of tocopherol acetate, 0.4 part of pyridoxine HCL, 0.2 part of piroctone olamine salt, 1 part of allantoin and 0.06 part of EDTA-disodium.
Wherein the plant functional components are butylene glycol, water, an extract of astragalus membranaceus, an extract of divaricate saposhnikovia root, an extract of calendula, a mixture of an extract of albizia julibrissin and an extract of gastrodia elata root. The preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate.
The scalp composition is prepared by the following method:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is 85 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 20 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 75 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the solution in the stirring pot is cooled to 75 ℃, stirring uniformly, and continuously cooling;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 6.5, and stirring for 30 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
Example 3
The embodiment 3 provides a plant multi-effect anti-hair loss, hair growth and hair nourishing compound composition, which comprises water and the following components in parts by weight:
55 parts of disodium lauryl sulfosuccinate, 2 parts of cocamide MEA (MEA), 8 parts of cocamidopropyl betaine, 10 parts of glycerol, 1.5 parts of glycerol stearate, 1.5 parts of propylene glycol, 72 parts of polyquaternium, 3.5 parts of acrylic acid (ester) copolymer, 1.5 parts of sodium chloride, 0.7 part of PEG-120 methyl glucose dioleate, 0.7 part of PEG-7 glyceryl cocoate, 0.7 part of PPG-3 octyl ether, 0.25 part of guar hydroxypropyl trimethyl ammonium chloride, 100.2 parts of polyquaternium, 0.6 part of essence, 2.5 parts of plant functional component, 0.7 part of preservative, 0.4 part of citric acid, 0.4 part of panthenol, 0.4 part of sodium hydroxide, DMDM hydantoin
0.25 part, 0.1 part of menthol, 1.5 parts of witch hazel extract, 1.5 parts of aloe extract, 1.5 parts of nicotinamide, 1.5 parts of tocopherol acetate, 0.8 part of pyridoxine HCL, 0.3 part of piroctone olamine salt, 1.5 parts of allantoin and 0.08 part of EDTA-disodium.
Wherein the plant functional components are butylene glycol, water, an extract of astragalus membranaceus, an extract of divaricate saposhnikovia root, an extract of calendula, a mixture of an extract of albizia julibrissin and an extract of gastrodia elata root. The preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate.
The scalp composition of example 3 was prepared by the process of example 2.
Example 4
The embodiment 4 provides a plant multi-effect anti-hair loss, hair growth and hair nourishing compound composition, which comprises water and the following components in parts by weight:
55 parts of disodium lauryl sulfosuccinate, 3 parts of cocamide MEA, 10 parts of cocamidopropyl betaine, 12 parts of glycerol, 2.0 parts of glycerol stearate, 2.0 parts of propylene glycol, 73.0 parts of polyquaternary ammonium salt, 5.0 parts of acrylic acid (ester) copolymer, 2.0 parts of sodium chloride, 1.0 part of PEG-120 methyl glucose dioleate, 1.0 part of PEG-7 glycerol cocoate, 1.0 part of PPG-3 octyl ether, 0.35 part of guar gum hydroxypropyl trimethyl ammonium chloride, 100.3 parts of polyquaternary ammonium salt and 0.8 part of essence, 3.0 parts of plant functional components, 0.09 part of preservative, 0.5 part of citric acid, 0.5 part of panthenol, 0.5 part of sodium hydroxide, 0.3 part of DMDM hydantoin, 0.15 part of menthol, 2 parts of Hamamelis virginiana extract, 2 parts of aloe extract, 2 parts of nicotinamide, 2 parts of tocopheryl acetate, 1 part of pyridoxine HCL, 0.4 part of piroctone olamine salt, 2 parts of allantoin and 0.1 part of EDTA-disodium.
Wherein the plant functional components are butylene glycol, water, an extract of astragalus membranaceus, an extract of divaricate saposhnikovia root, an extract of calendula, a mixture of an extract of albizia julibrissin and an extract of gastrodia elata root. The preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate.
The scalp composition of this example 4 was prepared according to the process of example 2.
Product testing
Comparative example 1
The plant functional components in the example 3 are removed, and the rest components and the mixture ratio are unchanged.
Comparative example 2
The plant functional components, the witch hazel extract and the aloe extract in example 3 were removed, and the remaining components and the mixture ratio were unchanged.
Test example 1
120 volunteers with dandruff are screened by adopting a civil investigation and grading method (the age range is between 20 and 40 years, the ratio of male to female is 1:1), the volunteers are randomly divided into three groups, 30 volunteers are selected, and the shampoo prepared in the example 3 and the shampoo prepared in the comparative examples 1 and 2 and the common dandruff-removing and itching-relieving shampoo on the market are respectively used.
The use effect and use feeling of the anti-dandruff cleaning were used as evaluation criteria: the dandruff removing shampoo is effective in removing dandruff without itching, and the problems of dandruff remaining or itching of the head and the like are ineffective, so that the scalp composition disclosed by the invention is compared with the common dandruff removing and itching relieving shampoo. Shampoo was used 4-6 times a week for one month, and the overall effect was observed after one month. See table 1.
Table 1 evaluation table of the anti-dandruff cleaning effect
The above table shows that the scalp composition for cleaning scalp hair 1+1 prepared by the invention can effectively remove dandruff and relieve itching, effectively and thoroughly remove dirt on the scalp, deeply remove dead skin cells and residues of grease accumulated in hair follicles, remove excessive grease to prevent alopecia, is fresh and comfortable after use, is not itchy and not tight, fundamentally solves the problems of scalp cleaning, excessive hair oil and dandruff occurrence by improving the microenvironment of scalp cells, and enables the scalp to obtain sufficient nutrients, nourish and moisten the hair, so that the scalp is healthy and attractive. Compared with the commercially available dandruff-removing and itching-relieving shampoo, the shampoo has obvious advantages.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (8)
1. A scalp composition for 1+1 scalp hair cleansing, comprising water and the following components in parts by weight:
35-55 parts of disodium lauryl sulfosuccinate, 1-3 parts of cocamide MEA, 3-10 parts of cocamidopropyl betaine, 3-12 parts of glycerol, 0.5-2.0 parts of glycerol stearate, 0.5-2.0 parts of propylene glycol, 70.5-3.0 parts of polyquaternium, 0.5-5.0 parts of acrylic acid (ester) copolymer, 0.5-2.0 parts of sodium chloride, 0.1-1.0 parts of PEG-120 methyl glucose dioleate, 0.2-1.0 parts of PEG-7 glycerol cocoate, 0.1-1.0 parts of PPG-3 octyl ether, 0.1-0.35 parts of guar hydroxypropyl trimethyl ammonium chloride, 100.1-0.3 parts of polyquaternium, 0.2-0.8 parts of essence, 0.1-3.0 parts of plant functional component, 0.05-0.09 parts of preservative, 0.1-0.5 parts of citric acid, 0.5 parts of hydantoin, 0.1-0.5 parts of panthenol, 0.5 parts of DMM 0.05-0 parts of menthol extract, 0.15 parts of Hamamelis mollis extract, 0.05-0.0.0 parts of DMM-15 parts of DMT 0.05-0 parts of menthol extract, 0.5-2 parts of aloe extract, 0.5-2 parts of nicotinamide, 0.5-2 parts of tocopherol acetate, 0.2-1 part of pyridoxine HCL, 0.1-0.4 part of piroctone olamine, 0.5-2 parts of allantoin and 0.05-0.1 part of EDTA-disodium.
2. A scalp composition for 1+1 scalp hair cleansing according to claim 1 wherein:
the plant functional components comprise butanediol, water, an extract of astragalus membranaceus, an extract of radix sileris root, an extract of calendula officinalis, and a mixture of an extract of albizia julibrissin and an extract of rhizoma gastrodiae.
3. A scalp composition for 1+1 scalp hair cleansing according to claim 1, wherein the plant extract in the scalp composition is prepared by the following plant extraction procedure:
selecting each plant raw material to be extracted, and cleaning and sterilizing the plant raw materials for later use;
various plant materials are extracted by a water extraction process to obtain plant extracts.
4. A scalp composition for 1+1 scalp hair cleansing according to claim 1 wherein:
the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate, and meets the requirements of national standard GB/T29666-2013 preservative for cosmetics.
5. A scalp composition for 1+1 scalp hair cleansing according to any of claims 1 to 4 characterized in that it is prepared by the following method:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is between 80 and 85 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 15 to 20 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 70-75 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the temperature of the stirring pot solution is reduced to 70-75 ℃, stirring uniformly, and continuously reducing the temperature;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 5.5-6.5, and stirring for 20-30 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
6. A method of preparing a scalp composition for 1+1 scalp hair cleansing comprising water and the following components in parts by weight:
35-55 parts of disodium lauryl sulfosuccinate, 1-3 parts of cocamide MEA, 3-10 parts of cocamidopropyl betaine, 3-12 parts of glycerol, 0.5-2.0 parts of glycerol stearate, 0.5-2.0 parts of propylene glycol, 70.5-3.0 parts of polyquaternium, 0.5-5.0 parts of acrylic acid (ester) copolymer, 0.5-2.0 parts of sodium chloride, 0.1-1.0 parts of PEG-120 methyl glucose dioleate, 0.2-1.0 parts of PEG-7 glycerol cocoate, 0.1-1.0 parts of PPG-3 octyl ether, 0.1-0.35 parts of guar hydroxypropyl trimethyl ammonium chloride, 100.1-0.3 parts of polyquaternium, 0.2-0.8 parts of essence, 0.1-3.0 parts of plant functional component, 0.05-0.09 parts of preservative, 0.1-0.5 parts of citric acid, 0.5 parts of hydantoin, 0.1-0.5 parts of panthenol, 0.5 parts of DMM 0.05-0 parts of menthol extract, 0.15 parts of Hamamelis mollis extract, 0.05-0.0.0 parts of DMM-15 parts of DMT 0.05-0 parts of menthol extract, 0.5-2 parts of aloe extract, 0.5-2 parts of nicotinamide, 0.5-2 parts of tocopherol acetate, 0.2-1 part of pyridoxine HCL, 0.1-0.4 part of piroctone olamine, 0.5-2 parts of allantoin and 0.05-0.1 part of EDTA-disodium;
the scalp composition is prepared by the following method:
(1) adding appropriate amount of water into a stirring pot, stirring under heating condition, and adding disodium lauryl succinate, cocamide MEA, cocamidopropyl betaine, glyceryl stearate, PEG-120 methyl glucose dioleate, sodium chloride, piroctone olamine, allantoin, propylene glycol, tocopherol acetate, glycerol and EDTA-disodium;
wherein, heating is carried out while stirring, the heating is stopped when the temperature is between 80 and 85 ℃, the stirring is carried out until the materials are completely dissolved, the temperature is kept for 15 to 20 minutes at constant temperature, and the temperature is reduced for standby;
(2) pre-mixing and dissolving polyquaternium-10, polyquaternium-7 and guar gum hydroxypropyl trimethyl ammonium chloride by using a proper amount of water, heating the mixed solution to 70-75 ℃, stirring and dissolving completely, adding the mixed solution into a stirring pot when the temperature of the stirring pot solution is reduced to 70-75 ℃, stirring uniformly, and continuously reducing the temperature;
(3) mixing PEG-7 glyceryl cocoate, panthenol, nicotinamide, pyridoxine HCL, PPG-3 octyl ether, DMDM hydantoin, plant functional components, antiseptic, essence and menthol to obtain transparent liquid, cooling the materials in a stirring pot to below 50 deg.C, adding the transparent liquid, Hamamelis virginiana extract and Aloe extract into the stirring pot, and stirring;
(4) mixing with acrylic acid (ester) copolymer with appropriate amount of water in advance, diluting, adding into a stirring pot, stirring, and cooling to below 40 deg.C;
(5) adding sodium hydroxide solution into a stirring pot, and uniformly stirring;
(6) adding a citric acid solution into a stirring pot, uniformly stirring, adjusting the pH value to 5.5-6.5, and stirring for 20-30 minutes;
(7) stopping stirring, standing, inspecting, and packaging to obtain scalp composition.
7. A method of preparing a scalp composition for 1+1 scalp hair cleansing according to claim 6 wherein:
the plant functional components comprise butanediol, water, an extract of astragalus membranaceus, an extract of radix sileris root, an extract of calendula officinalis, and a mixture of an extract of albizia julibrissin and an extract of rhizoma gastrodiae.
8. A method of preparing a scalp composition for 1+1 scalp hair cleansing according to claim 6 wherein:
the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium oxide and magnesium nitrate, and meets the requirements of national standard GB/T29666-2013 preservative for cosmetics.
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| CN114177115A (en) * | 2022-01-11 | 2022-03-15 | 毕道彬 | Scalp purification spray liquid and preparation method thereof |
| CN114344190A (en) * | 2022-01-21 | 2022-04-15 | 泉后(广州)生物科技研究院有限公司 | Anti-dandruff nourishing composition and application thereof in shampoo |
| FR3132842A1 (en) * | 2022-02-21 | 2023-08-25 | L'oreal | compositions and methods for treating keratinous materials |
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| CN113750009A (en) * | 2021-09-03 | 2021-12-07 | 北京东方淼森生物科技有限公司 | Preparation for improving scalp health state and preparation method thereof |
| CN113750009B (en) * | 2021-09-03 | 2022-08-09 | 北京东方淼森生物科技有限公司 | Preparation for improving scalp health state and preparation method thereof |
| CN114177115A (en) * | 2022-01-11 | 2022-03-15 | 毕道彬 | Scalp purification spray liquid and preparation method thereof |
| CN114344190A (en) * | 2022-01-21 | 2022-04-15 | 泉后(广州)生物科技研究院有限公司 | Anti-dandruff nourishing composition and application thereof in shampoo |
| FR3132842A1 (en) * | 2022-02-21 | 2023-08-25 | L'oreal | compositions and methods for treating keratinous materials |
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