CN109431915A - A kind of natural plant composition, hair dye and its preparation method and application - Google Patents
A kind of natural plant composition, hair dye and its preparation method and application Download PDFInfo
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- CN109431915A CN109431915A CN201811615281.6A CN201811615281A CN109431915A CN 109431915 A CN109431915 A CN 109431915A CN 201811615281 A CN201811615281 A CN 201811615281A CN 109431915 A CN109431915 A CN 109431915A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
- A61K2800/4322—Direct dyes in preparations for temporarily coloring the hair further containing an oxidizing agent
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Abstract
The present invention relates to a kind of natural plant compositions, hair dye and its preparation method and application.Natural plant composition, it is grouped as by the group of following parts by weight: 0.01 ~ 20 part of Gotu Kola P.E, 0.01 ~ 20 part of polygonum cuspidate root extract, 0.01 ~ 20 part of radix scutellariae root extract, 0.01 ~ 30 part of tea extract, 0.01 ~ 20 part of glycyrrhiza glabra root extract, 0.01 ~ 20 part of german chamomile flower extract, 0.01 ~ 20 part of rosemary leaf extract, 0.01 ~ 20 part of rough gentian root extract.Natural plant composition provided by the invention there is preferable compatibility can improve the dyeing property of hair conducive to the infiltration of dyestuff intermediate hair, in the case where less basifier dosage, realize preferable dyeing effect, color durability is good；In addition, the dosage due to basifier reduces, and the releiving effect of natural plant composition, to the stimulation of scalp when can substantially reduce hair dyeing, small to the stimulation of hair and scalp, damage is small.
Description
Technical field
The invention belongs to cosmetic fields, and in particular, to a kind of natural plant composition, hair dye and preparation method thereof
And application.
Background technique
Hair dye is to a kind of cosmetics of hair-dyeing.In recent years, hair dye is as a kind of daily beauty for changing color development
Hold cosmetics and gradually come into common people house, become modern's self-expression and pursue interspersing for individual character, on the one hand, hair dyeing
Agent can make color development back to nature, some inadequate natural endowments or posteriori sorry be made up, as Asians is traditionally with natural dark hair
Beauty, once since heredity, metabolism, nutrition or disease, the year factor of waiting for a long time lead to white hair etc., people need to be subject to by hair dye
Modification, to embody oneself young mental attitude.On the other hand, as individual character and it is fashionable intersperse, many people require to change
Primary colors is altered or modified as other colors using hair dye on the basis of original color development for oneself single hair color, with
Colorful color development is pursued, especially in recent years, hair dyeing has become the wind direction mark of fashion.
Hair dyeing is actually hair dye since the interfacial reactions such as the outermost contact wetting of hair epidermis, absorption, then
Its generation is impregnated with by the complex arrival hair epithelium and hair marrow of cell membrane, diffusion phenomena, occur with situation difference
" polymerization " reaction, acts on hair generation and hair is made to change color.It can be divided by the firmness of dyeing temporary, semipermanent
Property and permanent three classes；Permanent hairdye occupies 70%~80% in entirely hair dyeing cosmetic product, its effective component can
Stable biggish dye molecule is formed in medula inside hair to penetrate into, is closed in hair fiber, is held to play
Long hair dyeing effect, can generally keep 1~3 month.Mechanism can be sketched are as follows: inside small molecule dyes color developing agent → infiltration hair quality →
→ with couplant progress condensation reaction generation macromolecular dyestuff → be locked inside hair quality through oxidizing → form persistence
Hair dyeing.Permanent hair dye is mostly oxidized form hair dyeing cosmetic, generally is double-formulation, the dye constituted based on color developing agent and couplant
It sends out I agent and II agent is constituted with oxidant and form.Progress is separated for two doses when production is prepared, in use, two doses of mixing are coated
Hair is penetrated into be dyed.Research confirms that oxidative hair dyes have certain damage to scalp, and stimulation is big, and skin is easy to cause to produce
The senses of discomfort such as raw redness, shouting pain.
It develops that safety, irritation be low, hair dye without any toxicity and side effects has attracted increasing attention, has important
Meaning.
Summary of the invention
It is an object of the invention to overcome the defect that hair dye irritation is strong in the prior art, a kind of natural plants group is provided
Close object.Natural plant composition provided by the invention has preferable compatibility can conducive to the infiltration of dyestuff intermediate in hair
The dyeing property for improving hair realizes preferable dyeing effect in the case where less basifier dosage, and color durability is good；
In addition, the dosage due to basifier reduces, and the effect of releiving of natural plant composition, to scalp when can substantially reduce hair dyeing
Stimulation, it is small to the stimulation of hair and scalp, it damages small.
Another object of the present invention is to provide the preparation methods of above-mentioned natural plant composition.
Another object of the present invention is to provide above-mentioned natural plant compositions to prepare the application in hair dyeing product.
Another object of the present invention is to provide a kind of hair dyes.
For achieving the above object, the present invention adopts the following technical scheme:
A kind of natural plant composition is grouped as by the group of following parts by weight:
0.01~20 part of Gotu Kola P.E,
0.01~20 part of polygonum cuspidate root extract,
0.01~20 part of radix scutellariae root extract,
0.01~20 part of tea extract,
0.01~20 part of glycyrrhiza glabra root extract,
0.01~20 part of german chamomile flower extract,
0.01~20 part of rosemary leaf extract,
0.01~20 part of rough gentian root extract.
The hair dyeing effect of hair dye and be to consider the principal element of hair dye superiority and inferiority to the irritation of scalp.Dyestuff intermediate
Oxidation, coupling and condensation reaction can occur under the action of oxidant with coupling agent, generate dyestuff macromolecular to be dyed.
The color that the dyestuff intermediate and coupling agent for only infiltrating through hair core generate after reacting permanent can be just maintained in hair,
Obtain preferable hair dyeing firmness；The dye molecule meeting that chemical reaction generates occurs in hair surface without infiltrating through hair core
Cracking to be rinsed out by shampoo, hair dyeing effect is poor.Hair dye in the prior art mainly passes through a large amount of basifier of addition
Core is sent out to promote dyestuff former to infiltrate through hair before chemically reacting, to realize preferable hair dyeing effect.But it is big
The basifier of amount is stronger to the stimulation of scalp, influences the usage experience of consumer；And the few basifier of dosage can not reach
To preferable hair dyeing effect.
Containing there are many triterpenes in Gotu Kola P.E, main component is Asiaticoside and asiatic acid etc., has heat-clearing
Removing toxic substances, the effect that inducing diuresis and reducing edema, antibacterial anti-inflammatory, antiallergic are protected；And play the role of promoting natural on-off cycles of hair growth.
Polygonum cuspidate root extract is mainly made of resveratrol and rheum emodin etc., has extensive anti-oxidation characteristics, and there are also anti-
The anti-inflammatory effect of bacterium.
Scutellariae,radix extract main component is astragalus polyose and Astragaloside IV etc., can be used for anti-inflammatory agent, allergy inhibitor and
Moisturizer.
The nutriments such as tea extract phytoprotein rich in, Tea Saponin and a variety of amino acid, these substances
There is good nursing role to hair and scalp, hair and scalp can be moistened, keeps hair more compliant；In addition in tealeaves also
Containing tea polyphenols and theanine, tea polyphenols have good antioxidation, and the catechin in tea polyphenols is to a variety of harmful organisms
Have the function of sterilization and antibacterial, theanine has relaxation nerve, the good action relieved fatigue.
Glycyrrhiza glabra root extract is the stem of certain species or glycyrrhiza glabra.Glycyrrhiza glabra root extract can go deep into hair
Inside and keep high activity, effectively inhibit melanin production during a variety of enzymes activity, main function is with antibacterial
Anti-inflammatory, anti-oxidant, anti-aging, antiultraviolet and other effects.
German chamomile flower extract is containing Multiple components such as volatile oil, flavone compound, amino acid, chlorogenic acid and microelements.
With the bioactivity such as antibacterial, anti-oxidant, anti-inflammatory, antiallergic of releiving.
The effective component of rosemary leaf extract mainly has the ingredients such as Rosmarinic acid, carnosic acid, rosmanol, has and kills
Bacterium anti-inflammatory, it is anti-oxidant the effects of.
Rough gentian root extract, which has, inhibits stimulation, antiallergy, and antibacterial anti-inflammatory and the effect for promoting hair tonic, there are also moisturizings
Effect.
Inventor by find after numerous trials will by Gotu Kola P.E, polygonum cuspidate root extract, radix scutellariae root extract,
The day that tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, rosemary leaf extract and rough gentian root extract form
After right plant composition is added in conventional hair dye, obtained product is in the case where lesser basifier dosage, Neng Gouda
To better hair dyeing effect and hair dyeing firmness, and effectively mitigate the stimulation to scalp.This may be because of the natural plant
Object effective component and hair have better affinity, and dyestuff intermediate and coupling agent can be promoted to seep before chemically reacting
Hair hair core is penetrated, while delaying the speed reacted after dyestuff intermediate and coupling agent and the oxidant mixing in second dose, is made
More times can be had to infiltrate through hair core by obtaining dyestuff intermediate and coupling agent, and generate effective chemical staining reaction, be generated
Dyestuff macromolecular is to be dyed.
Natural plant composition provided by the invention has preferable compatibility to hair, conducive to the infiltration of dyestuff intermediate
Thoroughly, the dyeing property that can improve hair realizes that preferable dyeing effect, color are lasting in the case where less basifier dosage
Property is good；In addition, the dosage due to basifier reduces, and the effect of releiving of natural plant composition, when can substantially reduce hair dyeing pair
The stimulation of scalp, it is small to the stimulation of hair and scalp, it damages small.
Preferably, the natural plant composition is grouped as by the group of following parts by weight:
0.1~15 part of Gotu Kola P.E,
0.1~15 part of cane root extract,
0.1~15 part of radix scutellariae root extract,
0.1~15 part of tea extract,
0.1~15 part of glycyrrhiza glabra root extract,
0.1~15 part of german chamomile flower extract,
0.1~15 part of rosemary leaf extract,
0.1~15 part of rough gentian root extract.
Preferably, the natural plant composition is grouped as by the group of following parts by weight:
10 parts of Gotu Kola P.E,
4 parts of polygonum cuspidate root extract,
4 parts of radix scutellariae root extract,
2 parts of tea extract,
2 parts of glycyrrhiza glabra root extract,
1 part of german chamomile flower extract,
1 part of rosemary leaf extract,
6 parts of rough gentian root extract.
Each extract in the present invention can extract to obtain by conventional extracting method.
The preparation method of above-mentioned natural plant composition, includes the following steps:
S1: by dry centella, polygoni cuspidati,radix, scutellariae,radix, tealeaves, glycyrrhiza glabra root, Flos Chrysanthemi, rosemary leave and rough gentian
Root grinds respectively, is sieved, and obtains powder；
S2: powder is dissolved in alcoholic solution, and stirring obtains Gotu Kola P.E, polygoni cuspidati,radix respectively after microwave abstracting
Extract, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, rosemary leaf extract and
Rough gentian root extract；
S3: extract is mixed up to the natural plant composition.
The final state of natural plant composition obtained in above-mentioned preparation method, which can according to need, to be adjusted, can be with
It is the either gel gel type of solid, liquid.
Preferably, the alcoholic solution is one or more of propylene glycol, glycerol, butanediol, methyl propanediol or ethyl alcohol.
Above-mentioned natural plant composition prepare in hair dyeing product application it is also within the scope of the present invention.
A kind of hair dye is made of first dose and second dose, described first dose include dyestuff intermediate, it is coupling agent, above-mentioned
Natural plant composition, basifier and adjuvant；Described second dose includes oxidant；Natural plant composition in described first dose
Mass fraction is 1.0%~50%.
Preferably, the mass fraction of natural plant composition is 2.0~40% in described first dose.
It is further preferable that the mass fraction of natural plant composition is 30% in described first dose.
The type of basifier is the type of this field routine, and dosage in the present invention is less than conventional dosage, about
It is the 50~70% of conventional amount used.
Preferably, the basifier is ammonium hydroxide, basic carbonate, alkanolamine and its derivative, sodium hydroxide or hydroxide
One or more of potassium.
Preferably, the alkanolamine is monoethanolamine, diethanol amine or triethanolamine.
It is further preferable that the basifier is ammonium hydroxide, the mass fraction of ammonium hydroxide is 3~5% in first dose.
Ammonium hydroxide is common and effect preferably basifier in permanent hairdye, but the use of ammonium hydroxide is being brought more preferably
Hair dyeing effect and hair dyeing firmness while, side effect also becomes apparent, as ammonium hydroxide enemy's leatherware has stronger stimulation work
With, and biggish penetrating odor can be generated.Hair dye provided by the invention is being guaranteed by adding natural plant composition
Ammonia volume (mass fraction of ammonium hydroxide is 6~9% in lower first dose of normal condition) is reduced while same hair dyeing effect, is reduced
Ammonium hydroxide stimulation.
Dyestuff intermediate, coupling agent and adjuvant are the type and dosage of this field routine in the present invention.
Preferably, the adjuvant includes thickener, antioxidant, oxidation delayed-action activator, bleeding agent, chelating agent, fragrance, caching
One of agent, dispersing agent, regulator, silicone oil, film forming agent, ceramide, preservative, conditioner or opacifier are a variety of.
Preferably, the oxidant is one of hydrogen peroxide, urea peroxide, alkali metal bromate or peroxy salt or several
Kind.
It is further preferable that the oxidant is hydrogen peroxide.
Preferably, the dyestuff intermediate is p-phenylenediamine, 2- chlorine p-phenylenediamine, 4- amino -3- methylphenol, 1- hydroxyl second
Base -4,5- diamino-pyrazole, para-aminophenol, 2- dimethyl-p-phenylenediamine, p-methylaminophenol, 2,5- diaminotoluene, N,
One or more of bis- (2- ethoxy) p-phenylenediamine of N-.
Preferably, the coupling agent is dimethyl phenylene diamine, -4 oxyethylamine methyl phenyl ethers anisole of 2- amino, 2,4- diamino phenoxy second
Alcohol, 2- amino -3- pyridone, resorcinol, 4- chloro resorcinol, 2- methyl resorcinol, m-aminophenol, 1- naphthols,
1,5- dihydroxy naphthlene, -5 pyrazolone of 1- phenyl -3- methyl, 5- amino -6- chlorine o-cresol, 2- methyl -5- amino-phenol or hydrogen
One or more of quinone.
Preferably, first dose of the pH is 3~12.
It is further preferable that first dose of the pH is 7~12；
Most preferably, first dose of the pH is 9~11.
The present invention can using commonly used in dyeing keratin fibres acid, alkali, or using standard buffer system come
PH value is adjusted, to reach the pH value of needs.
Hair dye provided by the invention is suitable for keratin fiber and is dyed, especially human hair.
Compared with prior art, the invention has the following beneficial effects:
Natural plant composition provided by the invention has preferable compatibility to hair, conducive to the infiltration of dyestuff intermediate
Thoroughly, the dyeing property that can improve hair realizes that preferable dyeing effect, color are lasting in the case where less basifier dosage
Property is good；In addition, the dosage due to basifier reduces, and the effect of releiving of natural plant composition, when can substantially reduce hair dyeing pair
The stimulation of scalp, it is small to the stimulation of hair and scalp, it damages small.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.These embodiments are retouched to typical case of the invention
It states, however, the present invention is not limited thereto.Test method as used in the following examples unless otherwise specified, is conventional method, is made
Raw material, reagent etc. are unless otherwise specified the raw materials and reagents that can be obtained from commercial sources such as conventional markets.
Embodiment 1
The present embodiment provides a kind of natural plant compositions, by Gotu Kola P.E 10g, polygonum cuspidate root extract 4g, radix scutellariae
Root extract 4g, tea extract 2g, glycyrrhiza glabra root extract 2g, german chamomile flower extract 1g, rosemary leaf extract 1g, dragon
Gallbladder root extract 6g composition.
The natural plant composition is prepared via a method which to obtain:
(1) each extract is prepared
Gotu Kola P.E: dry centella being ground, is sieved, by the powder of preparation (d50=100~100 μm,
It 10kg) is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stirs at room temperature；Pass through microwave extracting apparatus in batches,
Under the conditions of microwave frequency 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
Polygonum cuspidate root extract: by dry polygonum cuspidate with grinding, being sieved, by the powder of preparation (d50=100~100 μm,
It 10kg) is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stirs at room temperature；Pass through microwave extracting apparatus in batches,
Under the conditions of microwave frequency 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
Radix scutellariae root extract: dry scutellariae,radix being ground, is sieved, by the powder of preparation (d50=100~100 μm,
It 10kg) is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stirs at room temperature；Pass through microwave extracting apparatus in batches,
Under the conditions of microwave frequency 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
Tea extract: dry tealeaves being ground, is sieved, and the powder (d50=100~100 μm, 10kg) of preparation is molten
Solution stirs at room temperature in 50% (v/v) butanediol aqueous solution 150L；In batches by microwave extracting apparatus, in Microwave Frequency
Under the conditions of rate 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
Glycyrrhiza glabra root extract: dry glycyrrhiza glabra root being ground, is sieved, by the powder of preparation (d50=100~
100 μm, 10kg) it is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stir at room temperature；Pass through microwave abstracting in batches
Device extracts 3 hours under the conditions of microwave frequency 5000MHz, obtains extract liquor, spare；
German chamomile flower extract: dry Flos Chrysanthemi being ground, is sieved, by the powder of preparation (d50=100~100 μm,
It 10kg) is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stirs at room temperature；Pass through microwave extracting apparatus in batches,
Under the conditions of microwave frequency 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
Rosemary leaf extract: dry rosemary leave being ground, is sieved, by the powder (μ of d50=100~100 of preparation
M, 10kg) it is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stir at room temperature；Pass through microwave extracting apparatus in batches,
Under the conditions of microwave frequency 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
Rough gentian root extract: dry gentian being ground, is sieved, by the powder of preparation (d50=100~100 μm,
It 10kg) is dissolved in 50% (v/v) butanediol aqueous solution 150L, and stirs at room temperature；Pass through microwave extracting apparatus in batches,
Under the conditions of microwave frequency 5000MHz, extracts 3 hours, obtain extract liquor, it is spare；
By Gotu Kola P.E, polygonum cuspidate root extract, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract,
German chamomile flower extract, rosemary leaf extract and rough gentian root extract mix up to natural plant composition.
Embodiment 2
The present embodiment provides a kind of natural plant compositions, by Gotu Kola P.E 20g, polygonum cuspidate root extract 20g, radix scutellariae
Root extract 20g, tea extract 20g, glycyrrhiza glabra root extract 0.01g, german chamomile flower extract 0.01g, rosemary leave mention
Take object 0.01g, rough gentian root extract 0.01g composition.
Preparation method and embodiment 1 are consistent.
Embodiment 3
The present embodiment provides a kind of natural plant composition, by Gotu Kola P.E 0.01g, polygonum cuspidate root extract 0.01g,
Radix scutellariae root extract 0.01g, tea extract 0.01g, glycyrrhiza glabra root extract 20g, german chamomile flower extract 20g, rosemary
Leaf extract 20g, rough gentian root extract 20g composition.
Preparation method and embodiment 1 are consistent.
Embodiment 4
The present embodiment provides a kind of natural plant compositions, by Gotu Kola P.E 15g, polygonum cuspidate root extract 15g, radix scutellariae
Root extract 15g, tea extract 15g, glycyrrhiza glabra root extract 0.1g, german chamomile flower extract 0.1g, rosemary leave are extracted
Object 0.1g, rough gentian root extract 0.1g composition.
Preparation method and embodiment 1 are consistent.
Embodiment 5
The present embodiment provides a kind of natural plant compositions, yellow by Gotu Kola P.E 0.1g, polygonum cuspidate root extract 0.1g
A kind of reed mentioned in ancient books root extract 0.1g, tea extract 0.1g, glycyrrhiza glabra root extract 15g, german chamomile flower extract 15g, rosemary leave mention
Take object 15g, rough gentian root extract 15g composition.
Preparation method and embodiment 1 are consistent.
Embodiment 6~14 and reference examples 1~10
Tables 1 and 2 is respectively the formula (unit: wt%) of the hair dye of embodiment 6~14 and reference examples 1~10, is
Coloured silk dye claret effect.
Wherein the natural plant composition in Examples 1 to 5 is denoted as 1~5* of composition respectively.
In addition, preparation 1~8# of reference composition, wherein removed in reference composition 1# and replace with Gotu Kola P.E
Outside the water of amount, remaining composition is consistent with embodiment 1.Except the water that polygonum cuspidate root extract is replaced with to equivalent in reference composition 2#
Outside, remaining composition is consistent with embodiment 1.In reference composition 3# in addition to radix scutellariae root extract is replaced with the water of equivalent,
Remaining composition is consistent with embodiment 1.In reference composition 4# in addition to the water that tea extract is replaced with to equivalent, remaining composition is equal
It is consistent with embodiment 1.In reference composition 5# in addition to glycyrrhiza glabra root extract is replaced with the water of equivalent, remaining composition with
Embodiment 1 is consistent.In reference composition 6# in addition to german chamomile flower extract is replaced with the water of equivalent, remaining composition is and embodiment
1 is consistent.In reference composition 7# in addition to the water that rosemary leaf extract is replaced with to equivalent, remaining composition with embodiment 1 one
It causes.In reference composition 8# in addition to rough gentian root extract is replaced with the water of equivalent, remaining composition is consistent with embodiment 1.
The formula for the hair dye that 1 embodiment 6~14 of table provides
The formula for the hair dye that 2 reference examples 1~10 of table provide
The formula of adjuvant in first dose is as follows:
Cetostearyl alcohol 5g, hexadecyltrimethylammonium chloride 1g, isopropyl palmitate 1.5g, stearic acid list glycerolipid
1.5g, propylene glycol 3g, oleyl alcohol 1g, ceteareth -202g, hydroxyethyl cellulose 0.3g, antioxidant 0.2g, chelating agent
0.3g, surplus are water, and prescription quality summation is 100g.
In upper table 1, the pH of hydrogenperoxide steam generator is 3.1, mixes and adjust pH with second dose by first dose as 9.8 up to institute
State the hair dye in each embodiment and reference examples.
Performance measurement
Hair dyeing experiment
(1) dyeing effect is assessed
The absorbing state of the hair dye of embodiment 6~14 and reference examples 1~10.By embodiment 6~14 and reference examples in table 1
First dose of 1~10 hair dye and second dose (color developing agent) ratio with 1:1 mixes, which is pressed twice hair weight
The dosage of amount smears level dyeing to the human hair of 12cm long.After 30 minutes, flowing water is carried out to hair dyeing with shampoo and rinses 1 point
Clock, then electricity consumption blowing drying.With the color of colorimeter (Hunterlab Labscan XE) measurement drying hair.By colorimeter measurement
Brightness value L * result is compared.Higher L* value refers to light color, and lower L* value then refers to dark color.Therefore, lesser L* value table
Bright preferable hair dyeing effect.
The dyeing effect for the hair dye that 3 embodiment 6~14 of table provides
The dyeing effect for the hair dye that 4 reference examples 1~10 of table provide
As shown in Tables 3 and 4, it is added with natural plant composition in embodiment 6~14, is not added with day to show to be better than
The hair dyeing effect of the reference examples 1 of right plant composition；Embodiment 10 is than the less ammonium hydroxide of reference examples 2, but dyeing effect is more
It is good, show that adding natural plant composition can be reduced the dosage of ammonium hydroxide, to reduce the irritation of hair dye, more mildly.It is right
Dyeing effect also slightly improves in 3~10 as usual, but the synergistic effect due to lacking a Plant Extracts, between extract
Cannot play a role well, so as to cause under less ammonium hydroxide additive amount hair dyeing effect not as good as embodiment 10 it is good.
(2) washable firmness test
It is water-soluble that hair after the hair dye provided using experimental example 6~14 and reference examples 1~10 dyeing is immersed in hair washing
In liquid, with oscillator with 200rpm speed oscillation 30 minutes, flowing water is rinsed 1 minute, then electricity consumption blowing drying.Then, colorimetric is used
Meter measurement L* value.According to the firmness of the Numerical evaluation dyeing in the difference △ L* of brightness value and table 5,6.Lesser △ L* value is
Refer to preferable color fast degree.The results are shown in Table 3
The dyeing firmness for the hair dye that 5 embodiment 6~14 of table provides
The dyeing firmness for the hair dye that 6 reference examples 1~10 of table provide
As shown in Table 5 and 6, natural plant composition is added in embodiment 6~14, it is therefore prevented that the colour fading of colored hair is simultaneously
Fabulous dyeing firmness is reached.The fastness to washing of embodiment 10 is substantially better than the fastness to washing of reference examples 1 and 2.Embodiment 6
Also there is good fastness to washing with embodiment 8, but for embodiment 10, can increased in terms of cost.Reference examples 3
Fastness to washing in~10 is more better with the fastness to washing of ammonium hydroxide additive amount than reference examples 1, but mentions due to lacking a kind of plant
Object is taken, the synergistic effect between them cannot play well, good not as good as embodiment 10 so as to cause fastness to washing.
(3) true man, which have hair dyed, tests
The volunteer that 126 skins are responsive type is divided into 19 groups, every group of 4 people use embodiment 6~14 and reference examples respectively
1~10 hair dye provided carries out trial dyeing.Concrete operations are that the hair dye of embodiment 6~14 is respectively adopted to carry out every group of 4 people
Hair dyeing, every group of 4 people use identical hair dye, and difference group uses different hair dyes；Then, to they inquired with
Assessment stimulates improveds degree, and gives a mark, and indicates the improved degree of stimulation with the height of the average mark of 4 people；Using reference examples 1
~10 hair dye has hair dyed to every group of 4 people, and every group of 4 people use identical hair dye, and difference group uses different
Hair dye；Then, they are inquired to assess and stimulate improved degree, and is given a mark, table is come with the height of the average mark of 4 people
Showing stimulates improved degree.
Inquire that each group improves situation with 1~5 point and 0.05 point for interval assessment stimulation after hair dyeing.When their sensory stimulis change
1 point is given when kind degree very little, when feeling that scalp irritation has clear improvement to 5 points.Finally integrate score and the averaging of 4 people
Value, calculated result are shown in Table 4.
The true man's hair dyeing test experiments data for the hair dye that 7 embodiment 6~14 of table provides
The true man's hair dyeing test experiments data for the hair dye that 8 reference examples 1~10 of table provide
By table 7 and 8 it is found that being added with natural plant composition in embodiment 6~14, the thorn to scalp can be obviously improved
Swash, without the hair dyeing added natural plant composition and a large amount of ammonium hydroxide has been used to provide as basifier (reference examples 1 and control 2)
Agent has very strong irritation to the skin of responsive type user, and effect is poor；Reference examples 3~10 are due to lacking one of plant
Object extract, the synergistic effect between them cannot play well, larger so as to cause the irritation of product.
(4) hair hand valuation
Hair sense of touch: gently clamping hair with index finger and thumb, and hair tail portion position, sense are gently slided to from the root of hair position of topknot
Feel smooth feeling, the moisture feeling of hair, and score: 5 is excellent, and 4 is good, and 3 is general, and 2 is poor, and 1 is very poor；Test result is shown in Table 9 and table
10。
Hair lesion assessment after the hair dyeing for the hair dye that 9 embodiment 6~14 of table provides
By upper table 9 and table 10 it is found that the hair dye of the offer of embodiment 6~14 is smaller to the degree of hair damage, hair ratio
Compared with lubrication and moisture feeling it is good, show as it is excellent, and the hair dyeing product that the composition in reference examples 1~10 is prepared to hair damage
The degree of wound is larger, and wherein the injury of reference examples 2 is maximum.
Claims (10)
1. a kind of natural plant composition, which is characterized in that be grouped as by the group of following parts by weight:
0.01 ~ 20 part of Gotu Kola P.E,
0.01 ~ 20 part of polygonum cuspidate root extract,
0.01 ~ 20 part of radix scutellariae root extract,
0.01 ~ 20 part of tea extract,
0.01 ~ 20 part of glycyrrhiza glabra root extract,
0.01 ~ 20 part of german chamomile flower extract,
0.01 ~ 20 part of rosemary leaf extract,
0.01 ~ 20 part of rough gentian root extract.
2. natural plant composition according to claim 1, which is characterized in that the natural plant composition is by following weight
The group of number is grouped as:
0.1 ~ 15 part of Gotu Kola P.E,
0.1 ~ 15 part of polygonum cuspidate root extract,
0.1 ~ 15 part of radix scutellariae root extract,
0.1 ~ 15 part of tea extract,
0.1 ~ 15 part of glycyrrhiza glabra root extract,
0.1 ~ 15 part of german chamomile flower extract,
0.1 ~ 15 part of rosemary leaf extract,
0.1 ~ 15 part of rough gentian root extract.
3. natural plant composition according to claim 2, which is characterized in that the natural plant composition is by following weight
The group of number is grouped as:
10 parts of Gotu Kola P.E,
4 parts of polygonum cuspidate root extract,
4 parts of radix scutellariae root extract,
2 parts of tea extract,
2 parts of glycyrrhiza glabra root extract,
1 part of german chamomile flower extract,
1 part of rosemary leaf extract,
6 parts of rough gentian root extract.
4. the preparation method of any natural plant composition of claim 1 ~ 3, which comprises the steps of:
S1: by dry centella, polygoni cuspidati,radix, scutellariae,radix, tealeaves, glycyrrhiza glabra root, Flos Chrysanthemi, rosemary leave and gentian point
It does not grind, be sieved, obtain powder；
S2: powder is dissolved in alcoholic solution, and stirring obtains Gotu Kola P.E, polygoni cuspidati,radix extraction respectively after microwave abstracting
Object, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, rosemary leaf extract and rough gentian
Root extract；
S3: extract is mixed up to the natural plant composition.
5. any natural plant composition of claim 1 ~ 4 is preparing the application in hair dyeing product.
6. a kind of hair dye, which is characterized in that be made of first dose and second dose, described first dose includes dyestuff intermediate, idol
Any natural plant composition of mixture, claim 1 ~ 4, basifier and adjuvant；Described second dose includes oxidant；It is described
The mass fraction of natural plant composition is 1.0% ~ 50% in first dose.
7. hair dye according to claim 6, which is characterized in that the mass fraction of natural plant composition in described first dose
It is 2.0 ~ 40%.
8. hair dye according to claim 6, which is characterized in that the basifier be ammonium hydroxide, basic carbonate, alkanolamine and
One or more of its derivative, sodium hydroxide or potassium hydroxide.
9. hair dye according to claim 8, which is characterized in that the basifier is ammonium hydroxide, the quality of ammonium hydroxide in first dose
Score is 3 ~ 5%.
10. hair dye according to claim 6, which is characterized in that the adjuvant includes that thickener, antioxidant, oxidation are prolonged
Slow agent, bleeding agent, chelating agent, fragrance, caching agent, dispersing agent, regulator, silicone oil, film forming agent, ceramide, preservative, conditioning
One of agent or opacifier are a variety of；Oxidant is one in hydrogen peroxide, urea peroxide, alkali metal bromate or peroxy salt
Kind is several.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112426387A (en) * | 2020-12-09 | 2021-03-02 | 泉后(广州)生物科技研究院有限公司 | Composition for delaying color change of hair dye cream and application thereof |
| CN112641662A (en) * | 2020-12-31 | 2021-04-13 | 泉后(广州)生物科技研究院有限公司 | Soothing and anti-allergy composition and application thereof |
| CN113350240A (en) * | 2021-06-25 | 2021-09-07 | 张勇 | Planting extract hair dyeing cream and preparation method thereof |
| CN113712880A (en) * | 2021-07-26 | 2021-11-30 | 广东卡迪娜实业有限公司 | Dyeing and protecting two-in-one hair dyeing conditioning composition |
-
2018
- 2018-12-27 CN CN201811615281.6A patent/CN109431915A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112426387A (en) * | 2020-12-09 | 2021-03-02 | 泉后(广州)生物科技研究院有限公司 | Composition for delaying color change of hair dye cream and application thereof |
| CN112641662A (en) * | 2020-12-31 | 2021-04-13 | 泉后(广州)生物科技研究院有限公司 | Soothing and anti-allergy composition and application thereof |
| CN113350240A (en) * | 2021-06-25 | 2021-09-07 | 张勇 | Planting extract hair dyeing cream and preparation method thereof |
| CN113712880A (en) * | 2021-07-26 | 2021-11-30 | 广东卡迪娜实业有限公司 | Dyeing and protecting two-in-one hair dyeing conditioning composition |
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