CN113350240A - Planting extract hair dyeing cream and preparation method thereof - Google Patents

Abstract

The invention discloses a plant extract hair-dyeing paste and a preparation method thereof, belonging to the technical field of hair-dyeing pastes and comprising a hair dye and an oxidant; the hair dye comprises the following components in percentage by weight: cetearyl alcohol, ceteareth, stearyltrimethyl ammonium chloride solution, polydimethylsiloxane, liquid paraffin, amodimethicone, chamomile extract, hydrolyzed keratin, p-phenylenediamine, resorcinol, phenylmethylpyrazolone, m-aminophenol, 2, 4-diaminophenoxyethanol HCl, an antioxidant, a chelating agent, a PH adjuster, a humectant, a fragrance; the oxidant comprises the following components in percentage by weight: hydrogen peroxide water solution, cetostearyl alcohol, sodium lauryl sulfate, cetostearyl polyether-25, chelating agent, stabilizing agent, pH regulator, aromatic and other solvents. The plant extract hair dye cream and the preparation method thereof solve the problems that some existing hair dye creams are poor in hair dyeing effect and cause damage to human bodies after being used.

Description

Planting extract hair dyeing cream and preparation method thereof

Technical Field

The invention relates to the technical field of hair dye cream, in particular to planting extract hair dye cream and a preparation method thereof.

Background

The market for hair dyes is growing, and not only young people need hair dyes to change the color of hair, but more and more older people start using hair dyes. The existing hair treatment oil hair-dyeing cream has poor hair-dyeing effect, and can cause great damage to human bodies after being used, such as causing skin allergy and damaging hair.

Disclosure of Invention

In order to solve the defects in the prior art, the invention aims to provide a planting hair-washing and hair-dyeing paste and a preparation method thereof, and solves the problems that some existing hair-dyeing pastes are poor in hair-dyeing effect, and harm is caused to human bodies after the existing hair-dyeing pastes are used.

The technical scheme adopted by the invention for solving the technical problems is as follows:

provides a plant extract hair dye cream and a preparation method thereof, comprising a hair dye and an oxidant;

the hair dye comprises the following components in percentage by weight:

cetearyl alcohol 8.5-9.5%, ceteareth-252.3-3.7%, stearyltrimethyl ammonium chloride solution 1.4-1.6%, dimethicone 0.8-1%, liquid paraffin 0.8-1%, amodimethicone 0.08-0.12%, chamomile extract 0.005-0.015%, hydrolyzed keratin 0.005-0.015%, p-phenylenediamine 2.7-2.9%, resorcinol 0.6-0.75%, phenylmethylpyrazolone 0.34-0.44%, m-aminophenol 0.26-0.35%, 2, 4-diaminophenoxy ethanol HCl 0.1-0.15%, antioxidant 0.7-1.2%, chelating agent 0.2-0.35%, pH regulator 7-10%, humectant 2.5-5%, fragrance 0.5-0.8%, and water as the remaining solvent;

the oxidant comprises the following components in percentage by weight:

11-13% of aqueous hydrogen peroxide solution, 3-4% of cetearyl alcohol, 0.3-0.5% of sodium lauryl sulfate, 0.2-0.4% of ceteareth-250.15, 0.2-0.4% of chelating agent, 0.1-0.2% of stabilizing agent, 0.1-0.2% of pH regulator, 0.6-0.9% of aromatic and the balance of solvent water.

Specifically, the extract of flos Chrysanthemi (Chrysanthemum INDICUM) is powder of flos Chrysanthemi; the liquid paraffin is CAS number 8012-95-1.

Further, in the hair dye component, the antioxidant is sodium sulfite and ascorbic acid; the chelating agent is EDTA disodium water solution; the pH regulator is ammonium hydroxide aqueous solution and ethanolamine; the humectant is urea and propylene glycol; the aromatic is essence;

in the oxidant component, the chelating agent is hydroxyethyldiphosphonic acid; the stabilizer is salicylic acid; the pH regulator is disodium hydrogen phosphate; the aromatic is essence.

Further, in the hair dye component, the antioxidant comprises the following components in percentage by weight of the total weight of the hair dye component: 0.5 to 0.7 percent of sodium sulfite; 0.2-0.4% of ascorbic acid.

Further, in the hair dye components, the PH regulator comprises the following components in percentage by weight of the total weight of the hair dye components: 5-7% of ammonium hydroxide aqueous solution; 2 to 3.5 percent of ethanolamine.

Further, in the hair dye component, the humectant comprises the following components in percentage by weight based on the total weight of the hair dye component: 2 to 3.5 percent of urea; 0.5 to 1.5 percent of propylene glycol.

Further, the stearyl trimethyl ammonium chloride solution is prepared from 70% of stearyl trimethyl ammonium chloride and 30% of ethanol;

the ammonium hydroxide aqueous solution is prepared from 72% of ammonium hydroxide and 28% of water;

the EDTA disodium water solution is prepared from 89.5 percent of EDTA disodium and 10.5 percent of water;

the aqueous hydrogen peroxide solution is prepared from 50% of hydrogen peroxide and 50% of water.

A method for preparing plant extract hair dye cream comprises a hair dye preparation method and an oxidant preparation method,

the preparation method of the hair dye comprises the following steps:

s1: preparation of component A: weighing cetearyl alcohol, ceteareth-25, liquid paraffin, glyceryl stearate, amino-terminated polydimethylsiloxane and polydimethylsiloxane which are raw materials of the component A according to a proportion, heating the mixture in an oil phase pot to 85-90 ℃, and fully and uniformly stirring the mixture;

s2: preparation of the component B: weighing the raw material of the component B, namely the stearyl trimethyl ammonium chloride solution according to a proportion, adding a proper amount of water, heating to 85-90 ℃ in a water phase pot, and fully and uniformly stirring;

s3: firstly, adding the material in the water phase pot into a vacuum emulsifying pot, then adding the raw materials in the oil phase pot into the vacuum emulsifying pot, and homogenizing and emulsifying for 5-20 minutes;

s4: cooling to 58-62 deg.C, adding C phase raw materials completely dissolved in appropriate amount of hot water, EDTA disodium water solution, propylene glycol, ascorbic acid, sodium sulfite, resorcinol, 2, 4-diaminophenoxyethanol HCl, m-aminophenol, p-phenylenediamine and phenyl methyl pyrazolone, and stirring thoroughly;

s5: cooling to 40-45 deg.C, adding D phase urea, E phase ammonium hydroxide aqueous solution, ethanolamine, essence, hydrolyzed keratin, and flos Chrysanthemi extract, stirring, discharging, standing, inspecting, and packaging to obtain hair dye;

the preparation method of the oxidant comprises the following steps:

s1: preparation of component A: weighing cetearyl alcohol and ceteareth-25 as raw materials of the component A in proportion, heating to 85-90 ℃ in an oil phase pot, and fully and uniformly stirring;

s2: preparation of the component B: weighing the B component raw materials of sodium lauryl sulfate and salicylic acid in proportion, adding a proper amount of water, heating to 85-90 ℃ in a water phase pot, and fully and uniformly stirring;

s3: firstly, adding the material in the water phase pot into a vacuum emulsifying pot, then adding the raw materials in the oil phase pot into the vacuum emulsifying pot, homogenizing and emulsifying for 1-10 minutes, preserving heat for 30 minutes, and then stirring and cooling;

s4: cooling to 40-45 deg.C, adding C phase hydrogen peroxide aqueous solution and appropriate amount of water-soluble disodium hydrogen phosphate and hydroxyethyl diphosphate into vacuum emulsifying pot, and stirring;

s5: adding D-phase raw material essence, fully stirring uniformly, discharging, standing, checking and filling to obtain the oxidant.

Compared with the prior art, the invention has the beneficial effects that:

1. the plant extract hair dyeing cream has good hair dyeing effect, and the hair dyed by the hair dyeing cream is soft and smooth and has good luster;

2. according to the plant extract hair dyeing paste disclosed by the invention, the golden chamomile extract is added to be used as a hair conditioner, so that the hair dyeing effect can be increased, the effects of resisting allergy, relieving itching, reducing the damage of the hair dyeing paste to the scalp and maintaining the moisture of the hair are achieved, and the double effects of dyeing the hair and protecting the scalp are achieved.

Drawings

Other features, objects and advantages of the present application will become more apparent upon reading of the following detailed description of non-limiting embodiments thereof, made with reference to the accompanying drawings in which:

FIG. 1 is a flow chart of a process for preparing a hair dye according to the present invention;

FIG. 2 is a flow chart of the oxidant preparation process of the present invention.

Detailed Description

The present application will be described in further detail with reference to the following drawings and examples. It is to be understood that the specific embodiments described herein are merely illustrative of the relevant invention and not restrictive of the invention. It should be noted that, for convenience of description, only the portions related to the present invention are shown in the drawings.

It should be noted that the embodiments and features of the embodiments in the present application may be combined with each other without conflict. The present application will be described in detail below with reference to the embodiments with reference to the attached drawings.

The first embodiment is as follows:

the invention discloses a plant extract hair dye cream, which comprises a hair dye and an oxidant:

the hair dye comprises the following components in percentage by weight:

cetostearyl alcohol 9%; 6% aqueous ammonium hydroxide (28% ammonium hydroxide + 72% water); 3% of urea; 3% of ethanolamine; 2.8 percent of p-phenylenediamine; ceteareth-252%; stearyl trimethyl ammonium chloride solution (70% stearyl trimethyl ammonium chloride + 30% ethanol) 1.5%; 1% of propylene glycol; 1% of glycerol stearate; 1% of polydimethylsiloxane; 1% of liquid paraffin; 0.8% of essence; 0.7% of resorcinol; 0.6 percent of sodium sulfite; 0.4% of phenyl methyl pyrazolone; disodium EDTA aqueous solution (89.5% disodium EDTA + 10.5% water) 0.3%; m-aminophenol 0.3%; ascorbic acid (vitamin C) 0.3%; 2, 4-diaminophenoxyethanol HCl 0.11%; 0.1 percent of amino-terminated polydimethylsiloxane; 0.01% of golden yellow chamomile (Chrysanthellum INDICUM) extract; 0.01% of hydrolyzed keratin; the rest water is filled.

The oxidant comprises the following components in percentage by weight:

12% aqueous hydrogen peroxide (50% hydrogen peroxide + 50% water); cetostearyl alcohol 3.3%; 0.8% of essence; 0.4 percent of sodium lauryl sulfate; 0.3 percent of hydroxyethyldiphosphonic acid; ceteareth-250.2%; 0.1% of disodium hydrogen phosphate; 0.1 percent of salicylic acid; the rest water is filled.

The preparation method of the plant extract hair dye cream exemplified in this example includes a hair dye preparation method and an oxidizer preparation method,

the preparation method of the hair dye comprises the following steps:

s1: preparation of component A: weighing cetearyl alcohol, ceteareth-25, liquid paraffin, glyceryl stearate, amino-terminated polydimethylsiloxane and polydimethylsiloxane serving as phase A raw materials in proportion, heating to 87 ℃ in an oil phase pot, and fully and uniformly stirring;

s2: preparation of the component B: weighing the raw material of the B phase, namely the stearyl trimethyl ammonium chloride solution according to a proportion, adding a proper amount of water, heating to 90 ℃ in a water phase pot, and fully and uniformly stirring;

s3: firstly, adding the material in the water phase pot into a vacuum emulsifying pot, then adding the raw materials in the oil phase pot into the vacuum emulsifying pot, and homogenizing and emulsifying for 10 minutes;

s4: cooling to 60 deg.C, adding C phase raw materials completely dissolved in appropriate amount of hot water, EDTA disodium water solution, propylene glycol, ascorbic acid, sodium sulfite, resorcinol, 2, 4-diaminophenoxyethanol HCl, m-aminophenol, p-phenylenediamine and phenyl methyl pyrazolone, and stirring thoroughly;

s5: cooling to 45 deg.C, adding D-phase urea, E-phase ammonium hydroxide aqueous solution, ethanolamine, essence, hydrolyzed keratin, and flos Chrysanthemi extract, stirring, discharging, standing, checking, and packaging to obtain hair dye;

the preparation method of the oxidant comprises the following steps:

s1: preparation of component A: weighing cetearyl alcohol and ceteareth-25 in proportion, heating to 88 ℃ in an oil phase pot, and fully and uniformly stirring;

s2: preparation of the component B: weighing sodium lauryl sulfate and salicylic acid in proportion, adding appropriate amount of water, heating to 87 deg.C in water phase pot, and stirring thoroughly;

s3: firstly, adding the material in the water phase pot into a vacuum emulsifying pot, then adding the raw materials in the oil phase pot into the vacuum emulsifying pot, homogenizing and emulsifying for 3 minutes, preserving the temperature for 30 minutes, and then stirring and cooling;

s4: cooling to 45 deg.C, adding C phase hydrogen peroxide aqueous solution and appropriate amount of water-soluble disodium hydrogen phosphate and hydroxyethyl diphosphate into vacuum emulsifying pot, and stirring;

s5: adding D-phase raw material essence, fully stirring uniformly, discharging, standing, checking and filling to obtain the oxidant.

The hair dye adopts ceteareth-25 and glyceryl stearate as emulsifiers; cetearyl alcohol as an emulsion stabilizer; stearyl trimethyl ammonium chloride and ethanol, polydimethylsiloxane, liquid paraffin, ammonia-terminated polydimethylsiloxane, flos Chrysanthemi (CHRYSANTHELLUM INDICAUM) extract, hydrolyzed keratin as hair conditioner, p-phenylenediamine, resorcinol, phenylmethylpyrazolone, m-aminophenol, 2, 4-diaminophenoxyethanol HCl as hair colorant, urea, propylene glycol as humectant, ammonium hydroxide, and ethanolamine as pH regulator; disodium EDTA acts as a chelating agent. By adding the golden chamomile extract, the hair dyeing effect can be improved, and the effects of resisting allergy, relieving itching, reducing the damage of the hair dyeing cream to the scalp and maintaining the moisture of the hair are achieved, so that the double effects of dyeing the hair and protecting the scalp are achieved; the glyceryl stearate has better hydrolysis resistance and emulsification effect; the stearyl trimethyl ammonium chloride and the amino-terminated polydimethylsiloxane have cationic groups and can play a role in neutralizing an anionic surfactant, so that a neutral film is formed and covers the surface of hair, the hair is smooth and easy to comb, and the frizziness of the hair is avoided.

Example two:

the invention discloses a plant extract hair dye cream, which comprises a hair dye and an oxidant:

the hair dye comprises the following components in percentage by weight:

cetostearyl alcohol 8.5%; 5.2% aqueous ammonium hydroxide (28% ammonium hydroxide + 72% water); 3.4 percent of urea; 2.1% of ethanolamine; 2.9 percent of p-phenylenediamine; ceteareth-251.7%; stearyl trimethyl ammonium chloride solution (70% stearyl trimethyl ammonium chloride + 30% ethanol) 1.6%; 0.6 percent of propylene glycol; 0.8% of glycerol stearate; 0.9% of polydimethylsiloxane; 0.9 percent of liquid paraffin; 0.8% of essence; resorcinol 0.73%; 0.52 percent of sodium sulfite; 0.35% of phenyl methyl pyrazolone; disodium EDTA aqueous solution (89.5% disodium EDTA + 10.5% water) 0.2%; m-aminophenol 0.28%; ascorbic acid (vitamin C) 0.37%; 2, 4-diamino phenoxy ethanol HCl 0.12%; 0.08 percent of amino-terminated polydimethylsiloxane; 0.008% of golden yellow chamomile (Chrysanthellum INDICUM) extract; 0.015% of hydrolyzed keratin; the rest water is filled.

The oxidant comprises the following components in percentage by weight:

12% aqueous hydrogen peroxide (50% hydrogen peroxide + 50% water); cetostearyl alcohol 3%; 0.7 percent of essence; 0.33 percent of sodium lauryl sulfate; 0.4 percent of hydroxyethyldiphosphonic acid; ceteareth-250.28%; 0.15 percent of disodium hydrogen phosphate; 0.15 percent of salicylic acid; the rest water is filled.

The preparation method of the plant extract hair dye paste of the embodiment comprises a hair dye preparation method and an oxidant preparation method, and the preparation methods of the hair dye and the oxidant are the same as the first embodiment.

Example three:

the invention discloses a plant extract hair dye cream, which comprises a hair dye and an oxidant:

the hair dye comprises the following components in percentage by weight:

cetostearyl alcohol 9.3%; 6.8% aqueous ammonium hydroxide (28% ammonium hydroxide + 72% water); 2.2 percent of urea; 3.5 percent of ethanolamine; 2.7 percent of p-phenylenediamine; ceteareth-252.2%; stearyl trimethyl ammonium chloride solution (70% stearyl trimethyl ammonium chloride + 30% ethanol) 1.4%; 1.5% of propylene glycol; 1.5% of glycerol stearate; 0.8% of polydimethylsiloxane; 0.8% of liquid paraffin; 0.5 percent of essence; 0.6 percent of resorcinol; 0.7 percent of sodium sulfite; 0.44% of phenyl methyl pyrazolone; disodium EDTA aqueous solution (89.5% disodium EDTA + 10.5% water) 0.35%; m-aminophenol 0.35%; ascorbic acid (vitamin C) 0.2%; 2, 4-diamino phenoxy ethanol HCl 0.15%; 0.12 percent of amino-terminated polydimethylsiloxane; 0.015% of golden yellow chamomile (Chrysanthellum INDICUM) extract; 0.005% of hydrolyzed keratin; the rest water is filled.

The oxidant comprises the following components in percentage by weight:

13% aqueous hydrogen peroxide (50% hydrogen peroxide + 50% water); cetostearyl alcohol 4%; 0.9 percent of essence; 0.5 percent of sodium lauryl sulfate; 0.4 percent of hydroxyethyldiphosphonic acid; ceteareth-250.15%; 0.12 percent of disodium hydrogen phosphate; 0.2 percent of salicylic acid; the rest water is filled.

The preparation method of the plant extract hair dye paste of the embodiment comprises a hair dye preparation method and an oxidant preparation method, and the preparation methods of the hair dye and the oxidant are the same as the first embodiment.

It will be appreciated by a person skilled in the art that the scope of the invention as referred to in the present application is not limited to the embodiments with a specific combination of the above-mentioned features, but also covers other embodiments with any combination of the above-mentioned features or their equivalents without departing from the inventive concept. For example, the above features may be replaced with (but not limited to) features having similar functions disclosed in the present application.

Claims (7)

1. A plant extract hair dye cream is characterized by comprising a hair dye and an oxidant;

the hair dye comprises the following components in percentage by weight:

cetearyl alcohol 8.5-9.5%, ceteareth-252.3-3.7%, stearyltrimethyl ammonium chloride solution 1.4-1.6%, dimethicone 0.8-1%, liquid paraffin 0.8-1%, amodimethicone 0.08-0.12%, chamomile extract 0.005-0.015%, hydrolyzed keratin 0.005-0.015%, p-phenylenediamine 2.7-2.9%, resorcinol 0.6-0.75%, phenylmethylpyrazolone 0.34-0.44%, m-aminophenol 0.26-0.35%, 2, 4-diaminophenoxy ethanol HCl 0.1-0.15%, antioxidant 0.7-1.2%, chelating agent 0.2-0.35%, pH regulator 7-10%, humectant 2.5-5%, fragrance 0.5-0.8%, and water as the remaining solvent;

the oxidant comprises the following components in percentage by weight:

11-13% of aqueous hydrogen peroxide solution, 3-4% of cetearyl alcohol, 0.3-0.5% of sodium lauryl sulfate, 0.2-0.4% of ceteareth-250.15, 0.2-0.4% of chelating agent, 0.1-0.2% of stabilizing agent, 0.1-0.2% of pH regulator, 0.6-0.9% of aromatic and the balance of solvent water.

2. The hair dye cream according to claim 1, wherein the antioxidant in the hair dye component is sodium sulfite and ascorbic acid; the chelating agent is EDTA disodium water solution; the pH regulator is ammonium hydroxide aqueous solution and ethanolamine; the humectant is urea and propylene glycol; the aromatic is essence;

in the oxidant component, the chelating agent is hydroxyethyldiphosphonic acid; the stabilizer is salicylic acid; the pH regulator is disodium hydrogen phosphate; the aromatic is essence.

3. The plant extract hair dye cream according to claim 2, wherein the hair dye components comprise the following antioxidant components in percentage by weight of the total weight of the hair dye components: 0.5 to 0.7 percent of sodium sulfite; 0.2-0.4% of ascorbic acid.

4. The plant extract hair dye cream according to claim 2, wherein the hair dye components comprise the following components in percentage by weight based on the total weight of the hair dye components: 5-7% of ammonium hydroxide aqueous solution; 2 to 3.5 percent of ethanolamine.

5. The plant extract hair dye cream according to claim 2, wherein in the hair dye component, the humectant comprises the following components in percentage by weight of the total weight of the hair dye component: 2 to 3.5 percent of urea; 0.5 to 1.5 percent of propylene glycol.

6. The plant hair dye cream of claim 2, wherein the solution of stearyl trimethyl ammonium chloride is prepared from 70% stearyl trimethyl ammonium chloride and 30% ethanol;

the ammonium hydroxide aqueous solution is prepared from 72% of ammonium hydroxide and 28% of water;

the EDTA disodium water solution is prepared from 89.5 percent of EDTA disodium and 10.5 percent of water;

the aqueous hydrogen peroxide solution is prepared from 50% of hydrogen peroxide and 50% of water.

7. A method of preparing a plant extract hair dye paste according to any one of claims 2 to 6, comprising a hair dye preparation method and an oxidizing agent preparation method,

the preparation method of the hair dye comprises the following steps:

s1: preparation of component A: weighing cetearyl alcohol, ceteareth-25, liquid paraffin, glyceryl stearate, amino-terminated polydimethylsiloxane and polydimethylsiloxane which are raw materials of the component A according to a proportion, heating the mixture in an oil phase pot to 85-90 ℃, and fully and uniformly stirring the mixture;

s2: preparation of the component B: weighing the raw material of the component B, namely the stearyl trimethyl ammonium chloride solution according to a proportion, adding a proper amount of water, heating to 85-90 ℃ in a water phase pot, and fully and uniformly stirring;

s3: firstly, adding the material in the water phase pot into a vacuum emulsifying pot, then adding the raw materials in the oil phase pot into the vacuum emulsifying pot, and homogenizing and emulsifying for 5-20 minutes;

s4: cooling to 58-62 deg.C, adding C phase raw materials completely dissolved in appropriate amount of hot water, EDTA disodium water solution, propylene glycol, ascorbic acid, sodium sulfite, resorcinol, 2, 4-diaminophenoxyethanol HCl, m-aminophenol, p-phenylenediamine and phenyl methyl pyrazolone, and stirring thoroughly;

s5: cooling to 40-45 deg.C, adding D phase urea, E phase ammonium hydroxide aqueous solution, ethanolamine, essence, hydrolyzed keratin, and flos Chrysanthemi extract, stirring, discharging, standing, inspecting, and packaging to obtain hair dye;

the preparation method of the oxidant comprises the following steps:

s1: preparation of component A: weighing cetearyl alcohol and ceteareth-25 as raw materials of the component A in proportion, heating to 85-90 ℃ in an oil phase pot, and fully and uniformly stirring;

s2: preparation of the component B: weighing the B component raw materials of sodium lauryl sulfate and salicylic acid in proportion, adding a proper amount of water, heating to 85-90 ℃ in a water phase pot, and fully and uniformly stirring;

s3: firstly, adding the material in the water phase pot into a vacuum emulsifying pot, then adding the raw materials in the oil phase pot into the vacuum emulsifying pot, homogenizing and emulsifying for 1-10 minutes, preserving heat for 30 minutes, and then stirring and cooling;

s4: cooling to 40-45 deg.C, adding C phase hydrogen peroxide aqueous solution and appropriate amount of water-soluble disodium hydrogen phosphate and hydroxyethyl diphosphate into vacuum emulsifying pot, and stirring;

s5: adding D-phase raw material essence, fully stirring uniformly, discharging, standing, checking and filling to obtain the oxidant.

Images