CN101744735A - Ecological treatment oil cream rinse and preparing method thereof - Google Patents
Ecological treatment oil cream rinse and preparing method thereof Download PDFInfo
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- CN101744735A CN101744735A CN201010039618A CN201010039618A CN101744735A CN 101744735 A CN101744735 A CN 101744735A CN 201010039618 A CN201010039618 A CN 201010039618A CN 201010039618 A CN201010039618 A CN 201010039618A CN 101744735 A CN101744735 A CN 101744735A
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Abstract
Ecological treatment oil cream rinse of the present invention is a composite agent comprising hair dye and an oxidizer, wherein the hair dye has the components of stearyl alcohol, glycerol stearate, propanediol, ammonia water, levelling agents, dye intermediates, emulsifiers, antioxidant and solvent water; and the oxidizer has the components of stearyl alcohol, glycerol stearate, propanediol, peroxide, propanediol, emulsifiers, stabilizing agents, PH value modifying agents and solvent water. A preparing method of the ecological treatment oil cream rinse comprises a hair dye preparing method and an oxidizer preparing method. The present invention has the advantages of good hair-dyeing effect, no harm for human bodies and convenient use.
Description
Technical field
The invention belongs to the household chemicals field, specifically a kind of ecological treatment oil cream rinse and preparation method thereof.
Background technology
Existing Yi Xie treatment oil cream rinse, not only hair dyeing effect is poor, and owing to contain the harmful substance of more amount in the prescription, as heavy metal, phenols etc., also can cause bigger injury after the use, as cause skin allergy, damage hair (hair become fragile, come off etc.) human body.
Summary of the invention
The objective of the invention is to work out a kind of ecological treatment oil cream rinse and preparation method thereof.
The present invention will solve is existing Yi Xie treatment oil cream rinse, and hair dyeing effect is poor, the problem of using the back that human body is damaged etc.
Ecological treatment oil cream rinse of the present invention is a kind of combination agent, comprises hair dye and oxidant;
The percentage by weight of each component is in the hair dye: stearyl alcohol is 6-10%, and glyceryl stearate is 3-5%, and propylene glycol is 3-5%, ammonia is 2-4%, and levelling agent is 1-4%, and dyestuff intermediate is 1-3%, emulsifying agent is 0.5-2%, and antioxidant is 0.1-1%, and all the other are aqueous solvent;
The percentage by weight of each component is in the oxidant: stearyl alcohol is 4-8%, and glyceryl stearate is 3-7%, and hydrogen peroxide is 3-7%, propylene glycol is 3-5%, and emulsifying agent is 0.5-2%, and stabilizing agent is 0.05-0.5%, pH value regulator 0.05-0.5%, all the other are aqueous solvent;
Hair dye and oxidant be remix in use, and the consumption of hair dye is by weight percentage during mixing: 40-60%, the consumption of oxidant are 60-40% by weight percentage.
The preparation method of ecological treatment oil cream rinse of the present invention comprises hair dye preparation method and oxidant preparation method,
Described hair dye preparation method comprises the steps: at least
1) preparation of A component: take by weighing stearyl alcohol and glyceryl stearate in proportion, mix post-heating to 94 ℃-96 ℃, stir, and be cooled to 90 ℃-92 ℃, the A component;
2) preparation of B component liquid: take by weighing propylene glycol in proportion, levelling agent, dyestuff intermediate, emulsifying agent, antioxidant and water mix post-heating to 94 ℃-96 ℃, stir, and be cooled to 90 ℃-92 ℃, the B component;
3) emulsified body and half-finished preparation: the B component is joined the A component, and holding temperature stirred 5-15 minute down at 90 ℃-92 ℃, got emulsified body; After emulsified body is cooled to 43 ℃-47 ℃ with water-bath, after adding ammonia again and being cooled to 33-37 ℃ with water-bath semi-finished product, the qualified back fill of the inspection of semifinished product, hair dye;
Described oxidant preparation method comprises the steps: at least
1) preparation of C component: take by weighing stearyl alcohol and glyceryl stearate in proportion, mix post-heating to 94 ℃-96 ℃, stir, and be cooled to 90 ℃-92 ℃, the C component;
2) preparation of D component liquid: take by weighing hydrogen peroxide in proportion, propylene glycol, emulsifying agent, stabilizing agent, the pH value regulator, water mixes post-heating to 94 ℃-96 ℃, stirs, and is cooled to 90 ℃-92 ℃, the D component;
3) emulsified body and half-finished preparation: the D component is joined the C component, and holding temperature stirred 5-15 minute down at 90 ℃-92 ℃, got emulsified body; After emulsified body is cooled to 33-37 ℃ with water-bath, add phosphoric acid when adding hydrogen peroxide again and being cooled to 28-30 ℃, regulate pH value with water-bath, semi-finished product, fill again after the inspection of semifinished product is qualified, oxidant.
The advantage that ecological treatment oil cream rinse of the present invention has: the one, hair dyeing effect is good, and the hair soft after the hair dyeing is smooth, good luster; The 2nd, human body there is not injury, three are to use conveniently.
Description of drawings
Fig. 1 is a hair dye preparation technology flow chart of the present invention.
Fig. 2 is an oxidant preparation technology flow chart of the present invention.
The specific embodiment
Now the present invention is further illustrated in conjunction with the accompanying drawings and embodiments.
Embodiment one
A kind of ecological treatment oil cream rinse of the present invention is a kind of combination agent, comprises hair dye and oxidant;
The percentage by weight of each component is in the hair dye: stearyl alcohol is 8%, glyceryl stearate is 4%, propylene glycol is 4%, ammonia is that ammonium hydroxide is 3%, the concentration expressed in percentage by weight of NH3 in this ammonia is 20%, levelling agent laureth-20 is 3%, the dyestuff intermediate Toluene-2,4-diisocyanate, 5-diamidogen sulfate 1%, dyestuff intermediate 2,4-diamino phenoxy ethanol sulfate is 0.1%, the emulsifying agent cetrimonium chloride is 0.9%, oxidation preventive isoascorbic acid sodium is 0.3%, and solvent deionized water is 75.7%;
The percentage by weight of each component is in the oxidant: stearyl alcohol is 6%, glyceryl stearate is 5%, hydrogen peroxide is 5%, the concentration expressed in percentage by weight of this hydrogen peroxide is 27.5%, propylene glycol is 3%, and the emulsifying agent sodium lauryl sulfate is 1%, and the stabilizing agent acetanilide is 0.1%, pH value regulator phosphoric acid 0.1%, solvent deionized water are 79.8%;
Hair dye and oxidant be remix in use, and the consumption of hair dye is by weight percentage during mixing: 50%, and the consumption of oxidant is 50% by weight percentage.
The preparation method of ecological treatment oil cream rinse of the present invention comprises hair dye preparation method and oxidant preparation method,
Described hair dye preparation method comprises the steps: at least
1) preparation of A component: take by weighing stearyl alcohol and glyceryl stearate in proportion, join in the oil phase jar of 200 liters of tilting-type mulsers and mix,, stir, and be cooled to 90 ℃ with Steam Heating to 95 ℃, the A component;
2) preparation of B component liquid: take by weighing propylene glycol in proportion, levelling agent, dyestuff intermediate, emulsifying agent, antioxidant and water join in the water jar of 200 liters of tilting-type mulsers and mix, with Steam Heating to 95 ℃, stir, and be cooled to 90 ℃, the B component;
3) emulsified body and half-finished preparation: the homogenizing jar 200 liters of tilting-type mulsers of A component filtration back injection, add the B component after filtering again, under 90 ℃, stirred 10 minutes, carry out the vacuum emulsifying, get emulsified body; The stirring and emulsifying body and be cooled to 45 ℃ with water-bath after, add again stir behind the ammonia and be cooled to 35 ℃ with water-bath after semi-finished product, the qualified back fill of the inspection of semifinished product, hair dye;
Described oxidant preparation method comprises the steps: at least
1) preparation of C component: take by weighing stearyl alcohol and glyceryl stearate in proportion, join in the oil phase jar of 300 liters of tilting-type mulsers and mix,, stir, and be cooled to 90 ℃ with Steam Heating to 95 ℃, the C component;
2) preparation of D component liquid: take by weighing hydrogen peroxide in proportion, propylene glycol, emulsifying agent, stabilizing agent, the pH value regulator, water joins in the water jar of 300 liters of tilting-type mulsers and mixes, and with Steam Heating to 95 ℃, stirs, and is cooled to 90 ℃, the D component;
3) emulsified body and half-finished preparation: the homogenizing jar 300 liters of tilting-type mulsers of C component filtration back injection, add the D component after filtering again, under 90 ℃, stirred 10 minutes, carry out the vacuum emulsifying, get emulsified body; The stirring and emulsifying body and be cooled to 35 ℃ with water-bath after, add again and stir behind the hydrogen peroxide and, add phosphoric acid when being cooled to 30 ℃ with the water-bath cooling, regulate pH value, semi-finished product, fill again after the inspection of semifinished product is qualified, oxidant.
Embodiment two
A kind of ecological treatment oil cream rinse of the present invention is a kind of combination agent, comprises hair dye and oxidant;
The percentage by weight of each component is in the hair dye: stearyl alcohol is 9%, glyceryl stearate is 3%, propylene glycol is 5%, ammonia is that ammonium hydroxide is 3%, the concentration expressed in percentage by weight of NH3 in this ammonia is 20%, levelling agent laureth-20 is 4%, the dyestuff intermediate Toluene-2,4-diisocyanate, 5-diamidogen sulfate 2%, dyestuff intermediate 2,4-diamino phenoxy ethanol sulfate is 0.08%, the emulsifying agent cetrimonium chloride is 0.8%, oxidation preventive isoascorbic acid sodium is 0.3%, and solvent deionized water is 74.82%;
The percentage by weight of each component is in the oxidant: stearyl alcohol is 7%, glyceryl stearate is 4%, hydrogen peroxide is 5%, the concentration expressed in percentage by weight of this hydrogen peroxide is 27.5%, propylene glycol is 4%, and the emulsifying agent sodium lauryl sulfate is 1%, and the stabilizing agent acetanilide is 0.1%, pH value regulator phosphoric acid 0.1%, solvent deionized water are 78.8%;
Hair dye and oxidant be remix in use, and the consumption of hair dye is by weight percentage during mixing: 51%, and the consumption of oxidant is 49% by weight percentage.
The preparation method of ecological treatment oil cream rinse of the present invention comprises hair dye preparation method and oxidant preparation method, and the preparation method of described hair dye and oxidant is with embodiment one.
Claims (10)
1. an ecological treatment oil cream rinse is characterized in that it is a kind of combination agent, comprises hair dye and oxidant;
The percentage by weight of each component is in the hair dye: stearyl alcohol is 6-10%, and glyceryl stearate is 3-5%, and propylene glycol is 3-5%, ammonia is 2-4%, and levelling agent is 1-4%, and dyestuff intermediate is 1-3%, emulsifying agent is 0.5-2%, and antioxidant is 0.1-1%, and all the other are aqueous solvent;
The percentage by weight of each component is in the oxidant: stearyl alcohol is 4-8%, and glyceryl stearate is 3-7%, and hydrogen peroxide is 3-7%, propylene glycol is 3-5%, and emulsifying agent is 0.5-2%, and stabilizing agent is 0.05-0.5%, pH value regulator 0.05-0.5%, all the other are aqueous solvent;
Hair dye and oxidant be remix in use, and the consumption of hair dye is by weight percentage during mixing: 40-60%, the consumption of oxidant are 60-40% by weight percentage.
2. ecological treatment oil cream rinse according to claim 1, it is characterized in that levelling agent selects laureth-20 for use, dyestuff intermediate select Toluene-2,4-diisocyanate for use, 5-diamidogen sulfate and 2,4-diamino phenoxy ethanol sulfate, Toluene-2,4-diisocyanate wherein, the percentage by weight that 5-diamidogen sulfate accounts for the component total amount is 1-2.5%, 2, the percentage by weight that 4-diamino phenoxy ethanol sulfate accounts for the component total amount is 0.05-0.5%, emulsifying agent in the hair dye is selected cetrimonium chloride for use, and antioxidant is selected sodium erythorbate for use.
3. ecological treatment oil cream rinse according to claim 1 is characterized in that the emulsifying agent in the oxidant is selected sodium lauryl sulfate for use, and stabilizing agent is selected acetanilide for use, and the pH value regulator is selected phosphoric acid for use.
4. ecological treatment oil cream rinse according to claim 1 is characterized in that ammonia is ammonium hydroxide, and the concentration expressed in percentage by weight of the NH3 of ammonia is 20%; The concentration expressed in percentage by weight of used hydrogen peroxide is 27.5%.
5. ecological treatment oil cream rinse according to claim 1 is characterized in that aqueous solvent is a deionized water.
6. the preparation method of ecological treatment oil cream rinse according to claim 1 is characterized in that this method comprises hair dye preparation method and oxidant preparation method,
Described hair dye preparation method comprises the steps: at least
1) preparation of A component: take by weighing stearyl alcohol and glyceryl stearate in proportion, mix post-heating to 94 ℃-96 ℃, stir, and be cooled to 90 ℃-92 ℃, the A component;
2) preparation of B component liquid: take by weighing propylene glycol in proportion, levelling agent, dyestuff intermediate, emulsifying agent, antioxidant and water mix post-heating to 94 ℃-96 ℃, stir, and be cooled to 90 ℃-92 ℃, the B component;
3) emulsified body and half-finished preparation: the B component is joined the A component, and holding temperature stirred 5-15 minute down at 90 ℃-92 ℃, got emulsified body; After emulsified body is cooled to 43 ℃-47 ℃ with water-bath, after adding ammonia again and being cooled to 33-37 ℃ with water-bath semi-finished product, the qualified back fill of the inspection of semifinished product, hair dye;
Described oxidant preparation method comprises the steps: at least
1) preparation of C component: take by weighing stearyl alcohol and glyceryl stearate in proportion, mix post-heating to 94 ℃-96 ℃, stir, and be cooled to 90 ℃-92 ℃, the C component;
2) preparation of D component liquid: take by weighing hydrogen peroxide in proportion, propylene glycol, emulsifying agent, stabilizing agent, the pH value regulator, water mixes post-heating to 94 ℃-96 ℃, stirs, and is cooled to 90 ℃-92 ℃, the D component;
3) emulsified body and half-finished preparation: the D component is joined the C component, and holding temperature stirred 5-15 minute down at 90 ℃-92 ℃, got emulsified body; After emulsified body is cooled to 33-37 ℃ with water-bath, add phosphoric acid when adding hydrogen peroxide again and being cooled to 28-30 ℃, regulate pH value with water-bath, semi-finished product, fill again after the inspection of semifinished product is qualified, oxidant.
7. the preparation method of ecological treatment oil cream rinse according to claim 6, it is characterized in that carrying out in the oil phase jar that is blended in 200 liters of tilting-type mulsers of stearyl alcohol in the A component and glyceryl stearate, adopt Steam Heating to 94 ℃-96 ℃, propylene glycol in the B component, levelling agent, dyestuff intermediate, emulsifying agent, carry out in the water jar that is blended in 200 liters of tilting-type mulsers of antioxidant and water, adopt Steam Heating to 94 ℃-96 ℃; When emulsified body prepares, should filter the homogenizing jar that 200 liters of tilting-type mulsers are injected in the back to the A component, add the B component after filtering again, under 90 ℃-92 ℃, carry out the vacuum emulsifying.
8. the preparation method of ecological treatment oil cream rinse according to claim 6, it is characterized in that carrying out in the oil phase jar that stearyl alcohol in the C component and glyceryl stearate be blended in 300 liters of tilting-type mulsers, adopt Steam Heating to 94 ℃-96 ℃, hydrogen peroxide in the D component, propylene glycol, emulsifying agent, stabilizing agent, pH value regulator and water are blended in the water jar of 300 liters of tilting-type mulsers and carry out, adopt Steam Heating to 94 ℃-96 ℃, when emulsified body prepares, the C component is filtered the homogenizing jar that 300 liters of tilting-type mulsers are injected in the back, add the D component after filtering again, under 90 ℃-92 ℃, carry out the vacuum emulsifying.
9. the preparation method of ecological treatment oil cream rinse according to claim 6, the emulsified body that it is characterized in that hair dye will stir in be cooled to 43 ℃ of-47 ℃ of processes with water-bath simultaneously; Then add ammonia and be cooled to stir simultaneously in the 33-37 ℃ of process with water-bath.
10. the preparation method of ecological treatment oil cream rinse according to claim 6, the emulsified body that it is characterized in that oxidant will stir in be cooled to 43 ℃ of-47 ℃ of processes with water-bath simultaneously; Then add hydrogen peroxide and be cooled to stir simultaneously in the 33-37 ℃ of process with water-bath.
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| CN2010100396180A CN101744735B (en) | 2010-01-12 | 2010-01-12 | Ecological treatment hair-oiling and dyeing cream and preparing method thereof |
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| CN2010100396180A CN101744735B (en) | 2010-01-12 | 2010-01-12 | Ecological treatment hair-oiling and dyeing cream and preparing method thereof |
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| CN101744735A true CN101744735A (en) | 2010-06-23 |
| CN101744735B CN101744735B (en) | 2012-02-22 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103751042A (en) * | 2013-12-31 | 2014-04-30 | 广州市白云区大荣精细化工有限公司 | Hair dye with low stimulation and preparation method thereof |
| CN104127336A (en) * | 2014-07-07 | 2014-11-05 | 曲传一 | Anti-allergic hair oiling and dyeing cream, and manufacturing method thereof |
| CN105411938A (en) * | 2015-12-18 | 2016-03-23 | 岳双辰 | Novel plant water-cleaning hair-blackening hair dye |
| CN106727052A (en) * | 2017-03-01 | 2017-05-31 | 广州无与伦比企业集团有限公司 | Draft hair care dying cream and its preparation technology containing matrimony vine berry extract |
| CN113350240A (en) * | 2021-06-25 | 2021-09-07 | 张勇 | Planting extract hair dyeing cream and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101152130A (en) * | 2007-08-31 | 2008-04-02 | 叶芳 | Hair dyes agent |
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2010
- 2010-01-12 CN CN2010100396180A patent/CN101744735B/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103751042A (en) * | 2013-12-31 | 2014-04-30 | 广州市白云区大荣精细化工有限公司 | Hair dye with low stimulation and preparation method thereof |
| CN103751042B (en) * | 2013-12-31 | 2015-09-16 | 广州市白云区大荣精细化工有限公司 | Cream rinse of a kind of low irritant and preparation method thereof |
| CN104127336A (en) * | 2014-07-07 | 2014-11-05 | 曲传一 | Anti-allergic hair oiling and dyeing cream, and manufacturing method thereof |
| CN105411938A (en) * | 2015-12-18 | 2016-03-23 | 岳双辰 | Novel plant water-cleaning hair-blackening hair dye |
| CN106727052A (en) * | 2017-03-01 | 2017-05-31 | 广州无与伦比企业集团有限公司 | Draft hair care dying cream and its preparation technology containing matrimony vine berry extract |
| CN113350240A (en) * | 2021-06-25 | 2021-09-07 | 张勇 | Planting extract hair dyeing cream and preparation method thereof |
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| CN101744735B (en) | 2012-02-22 |
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