CN106727052A - Draft hair care dying cream and its preparation technology containing matrimony vine berry extract - Google Patents
Draft hair care dying cream and its preparation technology containing matrimony vine berry extract Download PDFInfo
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- CN106727052A CN106727052A CN201710117776.5A CN201710117776A CN106727052A CN 106727052 A CN106727052 A CN 106727052A CN 201710117776 A CN201710117776 A CN 201710117776A CN 106727052 A CN106727052 A CN 106727052A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
- A61K2800/4324—Direct dyes in preparations for permanently dyeing the hair
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Abstract
The present invention provides a kind of draft hair care dying cream containing matrimony vine berry extract and its preparation technology, first to NMF and chelating agent is added in deionized water, heats while stirring, and temperature obtains mixture A after reaching 80 85 DEG C；Thickener, emulsifying agent and conditioner for hair are mixed again, is heated while stirring, temperature obtains mixture B after reaching 80 85 DEG C；Then hair colouring agent and antioxidant are uniformly mixing to obtain mixture C；Again to mixture B and mixture C is added in mixture A, stirring makes to obtain mixture D；Matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush bark extract, pH adjusting agent and aromatic are added in most backward mixture D, draft hair care dying cream is uniformly mixing to obtain.Cream rinse of the present invention contains herbaceous plant, and moderate performance will not produce injury after hair dyeing to hair and scalp, and enemy returns good maintenance effect, moreover it is possible to alleviate itching of the scalp.
Description
Technical field
The invention belongs to hair dyeing and care product technical field, and in particular to be a kind of draft containing matrimony vine berry extract
Hair care dying cream and its preparation technology.
Background technology
Hair dye is that in recent years, hair dyeing has just like turned into the selection of people's fashion, root to a kind of cosmetics of hair-dyeing
Show according to investigations, receive investigation number in, contaminated hair people accounted for it is more than half.Existing hair dye is divided into：Plant
Hair dye, metallic hairdye and oxidative coloration of hair agent.Botanical hair dye is contaminated using the material extracted from the scape leaf of plant
Color, it is smaller to human injury, but colorability is not strong, and color comes off comparatively fast after hair dyeing.Metallic hairdye, the mechanism of action is main
Be during metal ion in hair dye penetrates into hair, with hair protein in cysteine in sulphur effect, generate black sulphur
Change lead etc., hair is contaminated black；The heavy metal ion contained in metallic hairdye, in addition to damaging hair healthy and easily causing allergy, very
Easily cause and accumulate poisoning, the harm to human body is very big.It is used in the various hair dyes or cream rinse sold in the market
The dyestuff of dyestuff generally oxidisability, oxidative dyestuff is made up of intermediate, coupling agent and oxidant, in the dyestuff of small molecule
Mesosome and coupling agent first penetrate into cortical layer and the medullary substance layer of hair, and oxidant occurs by intermediate oxidation, then with coupling agent
Reaction forms larger dye molecule, is penetrated into hair fiber, so as to play lasting hair dyeing effect.In the middle of dyestuff
Body is different with the species of coupling agent, content ratio difference, therefore produces the different product of tone, various tone product compositions
Into different tones, hair is set to catch different colors.Because dyestuff macromolecular is to pass through dyestuff intermediate in hair fiber
Reacted with coupling agent small molecule and generated, therefore in washing, the dyestuff macromolecular of formation is to be easily detected by the hole of hair fiber
Footpath is rinsed.Such hair dye possesses the condition of persistence hair dyeing, but the chemical substance for containing is more, to the excitant of scalp compared with
Greatly, allergic phenomena can be caused to some skin sensitivities person, long-term use can be damaged to human body.
The content of the invention
It is small to scalp irritation it is an object of the invention to provide a kind of draft hair care dying cream containing matrimony vine berry extract,
Colorability is strong, and can not only have hair dyed to take care of hair.
It is a further object to provide the preparation technology of above-mentioned draft hair care dying cream.
The technical solution adopted in the present invention is,
Draft hair care dying cream containing matrimony vine berry extract, it is by mass percentage, raw materials used to be made up of following component：
20~28% base-material, 3~5% matrimony vine berry extract, 3~5% ginkgo biloba p.e, 3~5% Rhizoma Chuanxiong extract, 3
~5% Angelica roots, 3~5% bush bark extract, remaining is deionized water, the quality hundred of above each component
It is 100% to divide than summation.
The base-material by mass percentage, is made up of following component：38~45% thickener, 8~12% pH regulations
Agent, 8~12% NMF, 14~17.5% emulsifying agent, 3~5% conditioner for hair, 10~15% hair coloring
Agent, 2~4% antioxidant, 1~3% aromatic, 0.5~2% chelating agent；The mass percent of above each component is total
Be 100%.
The above-mentioned preparation technology containing matrimony vine berry extract draft hair care dying cream, its concrete operation step is as follows：
Step 1,
By mass percentage, 20~28% base-material is weighed, 3~5% matrimony vine berry extract, 3~5% ginkgo leaf is carried
Take thing, 3~5% Rhizoma Chuanxiong extract, 3~5% Angelica roots, 3~5% bush bark extract, remaining is to go
Ionized water, the mass percent summation of above each component is 100%；
Wherein, base-material by mass percentage, is made up of following component：38~45% thickener, 8~12% pH regulations
Agent, 8~12% NMF, 14~17.5% emulsifying agent, 3~5% conditioner for hair, 10~15% hair coloring
Agent, 2~4% antioxidant, 1~3% aromatic, 0.5~2% chelating agent；The mass percent of above each component is total
Be 100%；
Step 2,
To NMF and chelating agent is added in deionized water, heat while stirring, until the temperature of the mixture reaches 80-
After 85 DEG C, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Thickener, emulsifying agent and conditioner for hair are mixed, is heated while stirring, until the temperature of the mixture
After reaching 80-85 DEG C, stop heating and stir, the mixture B for being stirred is standby；
Step 4,
Hair colouring agent and antioxidant are uniformly mixing to obtain mixture C, it is standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C
It is fully emulsified to obtain mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush in mixture D
Bark extract, pH adjusting agent and aromatic, stir, and obtain draft hair care dying cream.
Wherein,
The thickener is cetostearyl alcohol；
The pH adjusting agent is ammonium hydroxide；
The NMF is propane diols；
The emulsifying agent be ceteareth -20 and stearine, wherein, ceteareth -20 and
The mass ratio of stearine is 2~3：1~2；
The conditioner for hair is the one kind in Trivent OCG, Triglyceride DDD or the ester of glycerol stearate three；
The hair colouring agent be ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and
2- amino -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and
The mass ratio of 2- amino -3- pyridones is 20:6:3:1；
The antioxidant is sodium sulfite and sodium isoascorbate, and the mass ratio of sodium sulfite and sodium isoascorbate is
4~6：2~4；
The aromatic is essence；
The chelating agent is EDETATE SODIUM.
The beneficial effects of the invention are as follows：
1. herbaceous plant is contained, and moderate performance will not produce injury, and enemy to return in hair and scalp after hair dyeing
Good maintenance effect, moreover it is possible to alleviate itching of the scalp；
2. colorability is strong, and hair is dried without heating, hair can be made to paint at normal temperatures；Dye fastness is good, dyeing effect
Persistently, smell is friendly for fruit；
3. hair dyeing back luminance is submissive smooth, it is easy to which combing, hair is more rich in gloss；In hair dye and after hair dyeing,
Scalp is not tight without scratchiness, stingless excitation, without redness.
Specific embodiment
The present invention provides a kind of draft hair care dying cream containing matrimony vine berry extract, by mass percentage, by with the following group
Part composition：20~28% base-material, 3~5% matrimony vine berry extract, 3~5% ginkgo biloba p.e, 3~5% Ligusticum wallichii
Extract, 3~5% Angelica roots, 3~5% bush bark extract, remaining is deionized water, above each component
Mass percent summation be 100%.
Wherein, base-material by mass percentage, is made up of following component：38~45% thickener, 8~12% pH regulations
Agent, 8~12% NMF, 14~17.5% emulsifying agent, 3~5% conditioner for hair, 10~15% hair coloring
Agent, 2~4% antioxidant, 1~3% aromatic, 0.5~2% chelating agent；The mass percent of above each component is total
Be 100%.
Matrimony vine (LYCIUM CHINENSE) berry extract：The capillary of scalp can be expanded, is stimulated circulation, from
And nourished hair；And abundant nutrition can be provided to hair, the hair tip, improvement hair quality is nourished, can have hair
Good compliance and toughness, can also improve the tensile strength of hair, keep hair lubrication gloss, hair is easy to combing.
Ginkgo (GINKGO BILOBA) leaf extract：The capillary of scalp can be expanded, is stimulated circulation, so that
Nourished hair, nourishing hair promotes natural on-off cycles of hair growth, strengthens the metabolism of scalp.
Ligusticum wallichii (LIGUSTICUM CHUANXIONG) extract：With wind-dispelling, promoting blood circulation, moisturizing, it is antipruritic the effect of；Can expand
Scalp capillary is opened, is stimulated circulation, increase hair nutrition, promote natural on-off cycles of hair growth.
Radix Angelicae Sinensis (ANGELICA POLYMORPHA SINENSIS) root extract：With promoting blood circulation, promote scalp blood
Effect of circulation；And vitamin E can be provided for hair, anti-alopecia-stopping moistens hair of scalp, makes hair submissive glossy,
And scalp water and oil balance, unobstructed hair follicle can be adjusted.
Bush bark extract：With stronger anti-inflammation and sterilization, antiallergy, anti-corrosion, deodorant function, scalp can be alleviated and disturbed
Itch.
In addition, bush bark and Ligusticum wallichii, the two all can promoting blood circulation analgesic, bush promoting blood circulation and dissolving stasis are hot, in Ligusticum wallichii promoting circulation of blood
The stagnation of the circulation of vital energy, with application, its promoting blood circulation, dispersing blood stasis, analgesic effect strengthens two medicine phases.
Thickener：Hair care dying cream system viscosity is become big, improve the viscosity of whole system, the thickening that the present invention is provided
Agent content can make the viscosity of hair care dying cream between 1000mPas~100000mPas, the hair care dying in the range of this
Cream is preferable with the adsorptivity of hair, is easily applied to hair, it is not easy to produce dropping liquid, will not trickle, and prevents from being infected with skin.
PH adjusting agent：The pH value of regulation hair care dying lotion system is 7.0~11.0, because only in the basic conditions
Hair can be just set to expand and soften, hair scale piece is opened makes dyestuff preferably diffuse and penetrate into cortical layer.
NMF：Enemy is initiated to lubrication and moisture-keeping function, prevents hair short-tempered.
Emulsifying agent：Oil phase and water in hair care dying cream is mutually mutually mixed, form fully decentralized emulsion.
Conditioner for hair：Because hair care dying cream of the present invention is alkalescence, there can be certain damage to hair in hair dye
Wound, so addition conditioner for hair has certain protection and moisten effect to hair.
Ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- in hair colouring agent
Amino -3- pyridones are all hair dye intermediate；Wherein, " ethoxy-p-PDA sulfate " is used as the centre of hair dye
Body, its oxidizing process is exactly the fixation process of color when having hair dyed, and its advantage is：1st, its oxidation resistance is strong, and 2, to hair damages
It is small, 3, small is destroyed to hair structure, 4, strong (above advantage is obtained anti-ultraviolet property for another similar intermediate p-phenylenediamine of contrast
Come)；" resorcinol " is all hair dye intermediate, as complex dye, with sterilizing function.Ethoxy-p-PDA sulfuric acid
The mass ratio of salt, resorcinol, 2,4- diamino phenoxies ethanol and 2- amino -3- pyridones is 20:6:3:1, so match somebody with somebody
, used as hair dye intermediate, its toxicity is more much smaller than the p-phenylenediamine commonly used on existing market, to scalp and head for the mixture of ratio
The stimulation of hair is small, and the structure of hair will not be damaged, and sense of discomfort will not be also caused to scalp, and wound will not be more caused to human body
Evil, and oxidation resistance is strong.
Antioxidant：Hair colouring agent oxidation rate can be avoided too fast and cause the uneven phenomenon of dyeing, it is anti-oxidant
Agent enables to hair colouring agent oxidation rate slack-off, it is ensured that hair colouring agent has the sufficient time to infiltrate through hair core so that dye
Color is more uniform, dyes vivider.
Aromatic：So that the smell of hair care dying cream becomes delicate fragrance, it is not pungent.
Chelating agent：Can chelated metal ions, metal ion is difficult to occur normal valence state and react, so as to safeguard hair care
The stability of cream rinse, reduces injury of the metal ion to hair and scalp.The chelating agent of hair care dying cream of the present invention is selected
EDETATE SODIUM, EDETATE SODIUM has preferable bacteriostasis to Gram-negative bacteria except having chelation, also antisepsis.
Embodiment 1
A kind of preparation technology containing matrimony vine berry extract draft hair care dying cream, its concrete operation step is as follows：
Step 1,
By mass percentage, 24.3% base-material, 3% matrimony vine berry extract, 3% ginkgo biloba p.e, 3% are weighed
Rhizoma Chuanxiong extract, 3% Angelica roots, 3% bush bark extract, 60.7% deionized water；
Matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots employed in the present embodiment and
The purchase information of bush bark extract is：
FRUCTUS LYCII (LYCIUM CHINENSE) extract-manufacturer：Changsha Naturalin Bio-resources Co., Ltd.；Product
Title：Matrimony vine berry extract；Product batch number：NAT-115178 20171028；
Ginkgo (GINKGO BILOBA) leaf extract-manufacturer：Ganzhou Hua Han bio tech ltd；ProductName
Claim：Ginkgo biloba p.e；Product batch number：HH143867 20170811；
Ligusticum wallichii (LIGUSTICUM CHUANXIONG) extract-manufacturer：The former day domain biological products in Shaanxi three are limited
Company；Name of product：Rhizoma Chuanxiong extract；Product batch number：TY146284-C 20170405；
Radix Angelicae Sinensis (ANGELICA POLYMORPHA SINENSIS) root extract-manufacturer：Ganzhou Hua Han biotechnologies
Co., Ltd；Name of product：Angelica roots；Product batch number：HH164235 20170914；
Bush bark extract-manufacturer：Nanjing draft source bio tech ltd；Name of product：Bush bark
Extract；Product batch number：SM26487 20170913；
Wherein, base-material by mass percentage, is made up of following component：41.2% thickener, 10.3% pH adjusting agent,
10.3% NMF, 16.5% emulsifying agent, 4.1% conditioner for hair, 12.3% hair colouring agent, 3.3% it is anti-
Oxidant, 1.2% aromatic, 0.8% chelating agent；
Thickener is cetostearyl alcohol；
PH adjusting agent is ammonium hydroxide；
NMF is propane diols；
Emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 2.5：1.5；
Conditioner for hair is Trivent OCG；
Hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
Antioxidant is sodium sulfite and sodium isoascorbate, and the mass ratio of sodium sulfite and sodium isoascorbate is 5：3；
Aromatic is essence；
Chelating agent is EDETATE SODIUM；
Step 2,
To propane diols and EDETATE SODIUM is added in deionized water, heat while stirring, until the temperature of the mixture reaches
After 85 DEG C, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Cetostearyl alcohol, ceteareth -20, stearine and Trivent OCG are mixed,
Heat while stirring, after the temperature of the mixture reaches 85 DEG C, stop heating and stir, the mixture for being stirred
B, it is standby；
Step 4,
By ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol, 2- amino -3- hydroxyl pyrroles
Pyridine, sodium sulfite and sodium isoascorbate are uniformly mixing to obtain mixture C, standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C
It is fully emulsified to obtain mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush in mixture D
Bark extract, ammonium hydroxide and essence, stir, and obtain draft hair care dying cream A.
Embodiment 2
A kind of preparation technology containing matrimony vine berry extract draft hair care dying cream, its concrete operation step is as follows：
Step 1,
By mass percentage, 24.3% base-material, 4% matrimony vine berry extract, 4% ginkgo biloba p.e, 4% are weighed
Rhizoma Chuanxiong extract, 4% Angelica roots, 4% bush bark extract, 55.7% deionized water；
Matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots employed in the present embodiment and
The purchase information of bush bark extract is consistent with embodiment 1；
Wherein, base-material by mass percentage, is made up of following component：41.2% thickener, 10.3% pH adjusting agent,
10.3% NMF, 16.5% emulsifying agent, 4.1% conditioner for hair, 12.3% hair colouring agent, 3.3% it is anti-
Oxidant, 1.2% aromatic, 0.8% chelating agent；
Thickener is cetostearyl alcohol；
PH adjusting agent is ammonium hydroxide；
NMF is propane diols；
Emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 2.5：1.5；
Conditioner for hair is Trivent OCG；
Hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
Antioxidant is sodium sulfite and sodium isoascorbate, and the mass ratio of sodium sulfite and sodium isoascorbate is 5：3；
Aromatic is essence；
Chelating agent is EDETATE SODIUM；
Step 2,
To propane diols and EDETATE SODIUM is added in deionized water, heat while stirring, until the temperature of the mixture reaches
After 85 DEG C, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Cetostearyl alcohol, ceteareth -20, stearine and Trivent OCG are mixed,
Heat while stirring, after the temperature of the mixture reaches 85 DEG C, stop heating and stir, the mixture for being stirred
B, it is standby；
Step 4,
By ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol, 2- amino -3- hydroxyl pyrroles
Pyridine, sodium sulfite and sodium isoascorbate are uniformly mixing to obtain mixture C, standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C
It is fully emulsified to obtain mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush in mixture D
Bark extract, ammonium hydroxide and essence, stir, and obtain draft hair care dying cream B.
Embodiment 3
A kind of preparation technology containing matrimony vine berry extract draft hair care dying cream, its concrete operation step is as follows：
Step 1,
By mass percentage, 24.3% base-material, 5% matrimony vine berry extract, 5% ginkgo biloba p.e, 5% are weighed
Rhizoma Chuanxiong extract, 5% Angelica roots, 5% bush bark extract, 50.7% deionized water；
Matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots employed in the present embodiment and
The purchase information of bush bark extract is consistent with embodiment 1；
Wherein, base-material by mass percentage, is made up of following component：41.2% thickener, 10.3% pH adjusting agent,
10.3% NMF, 16.5% emulsifying agent, 4.1% conditioner for hair, 12.3% hair colouring agent, 3.3% it is anti-
Oxidant, 1.2% aromatic, 0.8% chelating agent；
Thickener is cetostearyl alcohol；
PH adjusting agent is ammonium hydroxide；
NMF is propane diols；
Emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 2.5：1.5；
Conditioner for hair is Trivent OCG；
Hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
Antioxidant is sodium sulfite and sodium isoascorbate, and the mass ratio of sodium sulfite and sodium isoascorbate is 5：3；
Aromatic is essence；
Chelating agent is EDETATE SODIUM；
Step 2,
To propane diols and EDETATE SODIUM is added in deionized water, heat while stirring, until the temperature of the mixture reaches
After 85 DEG C, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Cetostearyl alcohol, ceteareth -20, stearine and Trivent OCG are mixed,
Heat while stirring, after the temperature of the mixture reaches 85 DEG C, stop heating and stir, the mixture for being stirred
B, it is standby；
Step 4,
By ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol, 2- amino -3- hydroxyl pyrroles
Pyridine, sodium sulfite and sodium isoascorbate are uniformly mixing to obtain mixture C, standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C
It is fully emulsified to obtain mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush in mixture D
Bark extract, ammonium hydroxide and essence, stir, and obtain draft hair care dying cream C.
The hair dyeing and care effect of the hair care dying cream prepared by verification experimental verification above three embodiment：
Under the indoor environment that temperature is 25 DEG C, on the hair of same experimenter, draft hair care dying cream A is uniformly smeared
On No. 1 region white hair of the experimenter, draft hair care dying cream B is uniformly put on No. 2 region white hairs of the experimenter, will
Draft hair care dying cream C is uniformly put on No. 3 region white hairs of the experimenter；After standing 20 minutes, lotion is washed off with clear water, treated
Experimenter's hair is air-dried, and is visually observed：No. 1 white hair in region is contaminated black, and color is uniform, and hair quality is pitch-black, there is slight light
Pool；No. 2 white hairs in region are contaminated black, and color is uniform, and hair quality is pitch-black, more glossy than No. 1 region, and hair is more smooth；No. 3
The white hair in region is contaminated black, and color is uniform, and hair quality is naturally pitch-black, and color is full, and glossiness is full and hair is merrily and lightheartedly submissive.
The herbaceous plant extract contained in draft hair care dying cream C is can be seen that from above-mentioned experiment at most, after hair dyeing, 3
The hair in number region most has glossy, and most submissive, most smooth, hair dyeing effect is best；In illustrating draft hair care dying cream of the present invention
Herbaceous plant has hair care to act on.
Embodiment 4
A kind of preparation technology containing matrimony vine berry extract draft hair care dying cream, its concrete operation step is as follows：
Step 1,
By mass percentage, 20% base-material is weighed, 5% matrimony vine berry extract, 5% ginkgo biloba p.e, 5%
Rhizoma Chuanxiong extract, 5% Angelica roots, 5% bush bark extract, 55% deionized water；
Matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots employed in the present embodiment and
The purchase information of bush bark extract is consistent with embodiment 1；
Wherein, base-material by mass percentage, is made up of following component：38% thickener, 12% pH adjusting agent, 12%
NMF, 17.5% emulsifying agent, 5% conditioner for hair, 10% hair colouring agent, 4% antioxidant, 1%
Aromatic, 0.5% chelating agent；
Thickener is cetostearyl alcohol；
PH adjusting agent is ammonium hydroxide；
NMF is propane diols；
Emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 2：1；
Conditioner for hair is Triglyceride DDD；
Hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
Antioxidant is sodium sulfite and sodium isoascorbate, and the mass ratio of sodium sulfite and sodium isoascorbate is 4：2；
Aromatic is essence；
Chelating agent is EDETATE SODIUM；
Step 2,
To propane diols and EDETATE SODIUM is added in deionized water, heat while stirring, until the temperature of the mixture reaches
After 82 DEG C, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Cetostearyl alcohol, ceteareth -20, stearine and Triglyceride DDD are mixed,
Heat while stirring, after the temperature of the mixture reaches 82 DEG C, stop heating and stir, the mixture for being stirred
B, it is standby；
Step 4,
By ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol, 2- amino -3- hydroxyl pyrroles
Pyridine, sodium sulfite and sodium isoascorbate are uniformly mixing to obtain mixture C, standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C
It is fully emulsified to obtain mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush in mixture D
Bark extract, ammonium hydroxide and essence, stir, and obtain draft hair care dying cream D.
Embodiment 5
A kind of preparation technology containing matrimony vine berry extract draft hair care dying cream, its concrete operation step is as follows：
Step 1,
By mass percentage, 28% base-material is weighed, 5% matrimony vine berry extract, 5% ginkgo biloba p.e, 5%
Rhizoma Chuanxiong extract, 5% Angelica roots, 5% bush bark extract, 47% deionized water；
Matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots employed in the present embodiment and
The purchase information of bush bark extract is consistent with embodiment 1；
Wherein, base-material by mass percentage, is made up of following component：45% thickener, 8% pH adjusting agent, 8%
NMF, 14% emulsifying agent, 3% conditioner for hair, 15% hair colouring agent, 2% antioxidant, 3% fragrance
Agent, 2% chelating agent；
Thickener is cetostearyl alcohol；
PH adjusting agent is ammonium hydroxide；
NMF is propane diols；
Emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 3：2；
Conditioner for hair is the ester of glycerol stearate three；
Hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
Antioxidant is sodium sulfite and sodium isoascorbate, and the mass ratio of sodium sulfite and sodium isoascorbate is 6：4；
Aromatic is essence；
Chelating agent is EDETATE SODIUM；
Step 2,
To propane diols and EDETATE SODIUM is added in deionized water, heat while stirring, until the temperature of the mixture reaches
After 80 DEG C, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Cetostearyl alcohol, ceteareth -20, stearine and the ester of glycerol stearate three are blended in one
Rise, heat while stirring, after the temperature of the mixture reaches 80 DEG C, stop heating and stir, what is stirred is mixed
Compound B, it is standby；
Step 4,
By ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol, 2- amino -3- hydroxyl pyrroles
Pyridine, sodium sulfite and sodium isoascorbate are uniformly mixing to obtain mixture C, standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C
It is fully emulsified to obtain mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush in mixture D
Bark extract, ammonium hydroxide and essence, stir, and obtain draft hair care dying cream E.
Hair care dying cream of the present invention is kept for 6 hours at a temperature of 40 ± 2 DEG C, without water-oil separating phenomenon after recovery room temperature,
Kept for 24 hours at a temperature of -10 ± 2 DEG C, without water-oil separating phenomenon after recovery room temperature.In hair dye, easily it is applied to
Hair, it is not easy to produce dropping liquid, will not trickle, and will not be infected with skin and clothes.Colorability is strong, hair is dried without heating, normal
Temperature is lower can to make hair paint；Dye fastness is good, and persistently, after being had one's hair wash through 50 times, hair color and glossiness are not for Color
Generation significant change；Hair dyeing back luminance is submissive smooth, it is easy to which combing, hair is more rich in gloss.Hair dye performance of the present invention
Gently, in hair dye and after hair dyeing, scalp is not tight without scratchiness, stingless excitation, without redness.
Claims (5)
1. the draft hair care dying cream containing matrimony vine berry extract, it is characterised in that by mass percentage, raw materials used by following
Component is constituted：20~28% base-material, 3~5% matrimony vine berry extract, 3~5% ginkgo biloba p.e, 3~5% river
Rhizome of chuanxiong extract, 3~5% Angelica roots, 3~5% bush bark extract, remaining is deionized water, above each group
The mass percent summation of part is 100%.
2. the draft hair care dying cream containing matrimony vine berry extract according to claim 1, it is characterised in that the base-material is pressed
Mass percent, is made up of following component：38~45% thickener, 8~12% pH adjusting agent, 8~12% NMF,
14~17.5% emulsifying agent, 3~5% conditioner for hair, 10~15% hair colouring agent, 2~4% antioxidant, 1
~3% aromatic, 0.5~2% chelating agent；The mass percent summation of above each component is 100%.
3. the draft hair care dying cream containing matrimony vine berry extract according to claim 2, it is characterised in that：
The thickener is cetostearyl alcohol；
The pH adjusting agent is ammonium hydroxide；
The NMF is propane diols；
The emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 2~3：1~2；
The conditioner for hair is the one kind in Trivent OCG, Triglyceride DDD or the ester of glycerol stearate three；
The hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
The antioxidant is sodium sulfite and sodium isoascorbate, the mass ratio of sodium sulfite and sodium isoascorbate for 4~
6：2~4；
The aromatic is essence；
The chelating agent is EDETATE SODIUM.
4. the preparation technology of matrimony vine berry extract draft hair care dying cream is contained described in a kind of claim 2, it is characterised in that its
Concrete operation step is as follows：
Step 1,
By mass percentage, 20~28% base-material is weighed, 3~5% matrimony vine berry extract, 3~5% ginkgo leaf is extracted
Thing, 3~5% Rhizoma Chuanxiong extract, 3~5% Angelica roots, 3~5% bush bark extract, remaining for go from
Sub- water, the mass percent summation of above each component is 100%；
Wherein, base-material by mass percentage, is made up of following component：38~45% thickener, 8~12% pH adjusting agent, 8
~12% NMF, 14~17.5% emulsifying agent, 3~5% conditioner for hair, 10~15% hair colouring agent, 2~
4% antioxidant, 1~3% aromatic, 0.5~2% chelating agent；The mass percent summation of above each component is
100%；
Step 2,
To NMF and chelating agent is added in deionized water, heat while stirring, until the temperature of the mixture reaches 80-85 DEG C
Afterwards, stop heating and stir, the mixture A for being stirred is standby；
Step 3,
Thickener, emulsifying agent and conditioner for hair are mixed, is heated while stirring, until the temperature of the mixture reaches
After 80-85 DEG C, stop heating and stir, the mixture B for being stirred is standby；
Step 4,
Hair colouring agent and antioxidant are uniformly mixing to obtain mixture C, it is standby；
Step 5,
To mixture B and mixture C is added in mixture A, stir so that mixture A, mixture B and mixture C are abundant
Emulsification obtains mixture D；
Step 6,
To addition matrimony vine berry extract, ginkgo biloba p.e, Rhizoma Chuanxiong extract, Angelica roots, bush bark in mixture D
Extract, pH adjusting agent and aromatic, stir, and obtain draft hair care dying cream.
5. the preparation technology of matrimony vine berry extract draft hair care dying cream is contained according to claim 4, it is characterised in that：
The thickener is cetostearyl alcohol；
The pH adjusting agent is ammonium hydroxide；
The NMF is propane diols；
The emulsifying agent is ceteareth -20 and stearine, wherein, ceteareth -20 and glycerine
The mass ratio of stearate is 2~3：1~2；
The conditioner for hair is the one kind in Trivent OCG, Triglyceride DDD or the ester of glycerol stearate three；
The hair colouring agent is ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
Base -3- pyridones；Wherein, ethoxy-p-PDA sulfate, resorcinol, 2,4- diamino phenoxies ethanol and 2- ammonia
The mass ratio of base -3- pyridones is 20:6:3:1；
The antioxidant is sodium sulfite and sodium isoascorbate, the mass ratio of sodium sulfite and sodium isoascorbate for 4~
6：2~4；
The aromatic is essence；
The chelating agent is EDETATE SODIUM.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111150693A (en) * | 2019-12-18 | 2020-05-15 | 广州市妆妍生物技术有限公司 | Eyelash nourishing liquid and preparation method thereof |
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| CN111150693A (en) * | 2019-12-18 | 2020-05-15 | 广州市妆妍生物技术有限公司 | Eyelash nourishing liquid and preparation method thereof |
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