CN106727254A - Draft hair care dying cream and its preparation technology containing nutgall extractive - Google Patents

Abstract

The present invention provides a kind of draft hair care dying cream containing nutgall extractive and its preparation technology, first to NMF and chelating agent is added in deionized water, heats while stirring, and temperature obtains mixture A after reaching 80 85 DEG C；Thickener, emulsifying agent and conditioner for hair are mixed again, is heated while stirring, temperature obtains mixture B after reaching 80 85 DEG C；Then hair colouring agent and antioxidant are uniformly mixing to obtain mixture C；Again to mixture B and mixture C is added in mixture A, stirring makes to obtain mixture D；Nutgall extractive, juglandis folia (seed) extract, Flos Nelumbinis extract, tea extract, ginseng root extract, pH adjusting agent and aromatic are added in most backward mixture D, draft hair care dying cream is uniformly mixing to obtain.Cream rinse of the present invention contains herbaceous plant, and moderate performance will not produce injury after hair dyeing to hair and scalp, and enemy returns good maintenance effect, moreover it is possible to alleviate itching of the scalp.

Description

Herbal hair care and hair dye cream containing gallnut extract and preparation process thereof

Technical Field

The invention belongs to the technical field of hair dyeing and caring products, and particularly relates to a herbal hair care and dyeing cream containing a gallnut extract and a preparation process thereof.

Background

Hair dye is a cosmetic for dyeing hair, and in recent years, dyeing has become a fashionable choice, and according to survey, more than half of people who have dyed hair are on the spot among people who receive the survey. The existing hair dye is divided into: plant hair dyes, metal hair dyes, and oxidative hair dyes. The plant hair dye is used for dyeing by using substances extracted from flower stems and leaves of plants, so that the plant hair dye has small harm to a human body, but has weak coloring capability and quick color falling after hair dyeing. The metal hair dye has the action mechanism that metal ions in the hair dye penetrate into hair and react with sulfur in cysteine in hair protein to generate black lead sulfide and the like, so that the hair is dyed black; the heavy metal ions contained in the metal hair dye are easy to cause accumulation poisoning and great harm to human bodies besides damage to hair health and allergy. The dyes used in various hair dyes or hair dye pastes sold in the market at present are generally oxidative dyes, the oxidative dyes are composed of intermediates, couplers and oxidants, small molecular dye intermediates and couplers firstly permeate into cortex layers and medulla layers of hair, the oxidants oxidize the intermediates, then react with the couplers to form larger dye molecules, and the larger dye molecules permeate into hair fibers, thereby achieving a durable hair dyeing effect. Because of different kinds and content ratios of the dye intermediate and the coupler, reaction products with different hues are generated, and various hue products are combined into different hues, so that the hair is dyed with different colors. Since the dye macromolecules are formed in the hair fibers by the reaction of the dye intermediates and coupler small molecules, the dye macromolecules formed are not easily washed through the pore size of the hair fibers during washing. The hair dye has the condition of permanent hair dyeing, but contains more chemicals, has larger irritation to the scalp, can cause allergic phenomenon to some skin-sensitive people, and can cause harm to human bodies after long-term use.

Disclosure of Invention

The invention aims to provide the herbal hair care and hair dyeing paste containing the gallnut extract, which has small irritation to scalp, strong coloring capability, hair dyeing and hair care.

The invention also aims to provide a preparation method of the herbal hair care and hair dye cream.

The technical scheme adopted by the invention is that,

the herbal hair care and hair dye cream containing the gallnut extract comprises the following raw materials in percentage by mass: 20-28% of base material, 3-5% of nutgall extract, 3-5% of walnut leaf (seed) extract, 3-5% of lotus flower extract, 3-5% of tea extract, 3-5% of ginseng root extract and the balance of deionized water, wherein the sum of the mass percentages of the components is 100%.

The base material comprises the following components in percentage by mass: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent.

The preparation process of the herbal hair care and hair dye cream containing the gallnut extract comprises the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 20-28% of base material, 3-5% of nutgall extract, 3-5% of walnut leaf (seed) extract, 3-5% of lotus flower extract, 3-5% of tea extract, 3-5% of ginseng root extract and the balance of deionized water according to mass percentage, wherein the sum of the mass percentages of the components is 100%;

wherein, the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent;

in the step 2, the step of mixing the raw materials,

adding a humectant and a chelating agent into deionized water, heating while stirring until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing the thickening agent, the emulsifying agent and the hair conditioner together, heating and stirring the mixture at the same time until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;

in the step 4, the step of,

uniformly stirring a hair colorant and an antioxidant to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

adding Galla chinensis extract, folium Juglandis (seed) extract, flos Nelumbinis extract, folium Camelliae sinensis extract, radix Ginseng extract, pH regulator and aromatic into mixture D, and stirring to obtain herbal hair caring and dyeing cream.

Wherein,

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2-3: 1-2;

the hair conditioner is one of caprylic triglyceride, capric triglyceride or stearic triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4-6: 2-4;

the aromatic is essence;

the chelating agent is disodium EDTA.

The invention has the beneficial effects that:

1. the hair conditioner contains herbaceous plants, has mild performance, does not damage hair and scalp after hair dyeing, has good repairing effect on the hair, and can relieve scalp itch;

2. the coloring capability is strong, the hair can be colored at normal temperature without heating and drying the hair; the dyeing fastness is good, the dyeing effect is durable, and the smell is friendly;

3. the hair dyed is bright, smooth and easy to comb, and the hair is rich in luster; during and after hair dyeing, the scalp has no itching, tightness, irritation and red swelling.

Detailed Description

The invention provides a herbal hair care and hair dyeing paste containing a gallnut extract, which comprises the following components in percentage by mass: 20-28% of base material, 3-5% of nutgall extract, 3-5% of walnut leaf (seed) extract, 3-5% of lotus flower extract, 3-5% of tea extract, 3-5% of ginseng root extract and the balance of deionized water, wherein the sum of the mass percentages of the components is 100%.

Wherein, the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent.

Gallnut extract: has obvious bacteriostatic or bactericidal effects on staphylococcus aureus, streptococcus, pneumococcus, typhoid fever, paratyphoid fever, dysentery, anthrax, diphtheria, pseudomonas aeruginosa and the like; the tannic acid in Galla chinensis can form insoluble complex with heavy metal ions in hair dye, and has antidotal effect.

Walnut leaf (seed) extract: the hair conditioner is rich in linoleic acid, linolenic acid, various trace elements, vitamins and mineral substances, and the vitamin E rich in the hair conditioner can moisten scalp and hair, nourish and repair hair, make the hair smooth and glossy, and adjust the water-oil balance of the scalp.

Extract of lotus (NELUMBO NUCIFERA) flower: can supplement water lost from hair and scalp, and recover smoothness and luster of hair; the hair follicle is balanced in water and oil, more oil is prevented from being secreted by the hair follicle, and the occurrence of folliculitis is reduced; in addition, it has antifungal and antibacterial effects, and can be used for preventing tinea capitis and scalp pruritus.

Tea (CAMELLIA SINENSIS) leaf extract: the hair conditioner contains rich nutrient substances such as plant protein, tea saponin, various amino acids and the like, has good nursing effect on hair and scalp, and can moisten the hair and the scalp to make the hair more smooth; in addition, the tea leaves also contain tea polyphenol and theanine, the tea polyphenol has good antioxidation, catechin in the tea polyphenol has the functions of sterilization and antibiosis to various harmful microorganisms, and the theanine has good functions of relaxing nerves and relieving fatigue.

GINSENG (PANAX GINSENG) root extract: the hair conditioner has the advantages that the hair conditioner can expand the capillary vessels of the scalp, enhance the cell activity of the scalp and the hair, increase the nutrition of the hair, improve the toughness of the hair, reduce the hair loss and the hair breakage and has a protection effect on the damaged hair; moreover, the secretion function of the scalp sebaceous glands can be regulated, redundant grease is removed, water-oil balance is achieved, and the breeding of bacteria and fungi is reduced by controlling the water-oil balance of the scalp sebaceous glands.

Thickening agent: the viscosity of the hair care and hair dyeing paste system is increased, the viscosity of the whole system is improved, the content of the thickening agent provided by the invention can ensure that the viscosity of the hair care and hair dyeing paste is between 1000 mPa.s and 100000 mPa.s, the hair care and hair dyeing paste in the range has good adsorbability with hair, is easy to apply to the hair, is not easy to generate dropping liquid, cannot flow, and can prevent the skin from being stained.

pH regulator: the pH value of the hair care and hair dyeing paste system is adjusted to be 7.0-11.0, because the hair can be expanded and softened only under the alkaline condition, and the hair scales are opened, so that the dye can be better diffused and permeated into the cortex.

Humectant: has effects of lubricating and moisturizing hair, and preventing frizziness of hair.

Emulsifier: the oil phase and the water phase in the hair care and hair dyeing cream can be mixed with each other to form a completely dispersed emulsion.

Conditioner for hair: because the hair care and dyeing cream is alkaline and can damage hair to a certain extent in the hair dyeing process, the hair conditioner added has certain protection and moistening effects on the hair.

Hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine in the hair colorant are hair dye intermediates; wherein, the 'hydroxyethyl-p-phenylenediamine sulfate' is used as an intermediate of the hair dye, the oxidation process is the fixation process of the color during the hair dyeing, and the method has the advantages that: 1. the antioxidant capacity is strong, 2, the damage to hair is small, 3, the damage to hair structure is small, 4, the ultraviolet resistance is strong (the advantages are obtained by comparing another similar intermediate p-phenylenediamine); the resorcinol is also a hair dye intermediate and is used as a complex dye, and has a sterilization function. The mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3:1, and the mixture prepared by the ratio is used as a hair dye intermediate, so that the toxicity of the hair dye intermediate is much lower than that of the common p-phenylenediamine in the existing market, the hair dye intermediate has small stimulation to scalp and hair, the hair dye intermediate does not damage the structure of the hair, does not cause discomfort to the scalp, does not cause harm to human bodies, and has strong oxidation resistance.

Antioxidant: can avoid sending out and lead to the inhomogeneous phenomenon of dyeing with colorant oxidation rate at the excessive speed, the antioxidant can make sending out and use colorant oxidation rate to slow down, guarantees to send out and has abundant time infiltration into the hair core with the colorant for it is more even to dye, and the dyeing is more bright.

Aromatic agent: the hair care and dyeing cream has fragrant smell and is not pungent.

Chelating agent: can chelate metal ions, so that the metal ions are difficult to have normal valence state reaction, thereby maintaining the stability of the hair care and hair dyeing cream and reducing the damage of the metal ions to hair and scalp. The chelating agent of the hair care and hair dyeing cream disclosed by the invention selects disodium EDTA, and the disodium EDTA has a chelating effect, a preservative effect and a good bacteriostatic ability on gram-negative bacteria.

Example 1

A preparation process of a herbal hair care and hair dye cream containing a Chinese gall extract comprises the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 24.3% of base material, 3% of nutgall extract, 3% of walnut leaf (seed) extract, 3% of lotus flower extract, 3% of tea extract, 3% of ginseng root extract and 60.7% of deionized water according to mass percentage;

the purchase information of the nutgall extract, the walnut leaf (seed) extract, the lotus flower extract, the tea leaf extract and the ginseng root extract adopted in the embodiment is as follows:

gallnut extract-manufacturer: sienna Tianrui Biotechnology, Inc.; the product name is as follows: galla chinensis extract; production batch number: TR 16974-W20170816;

walnut leaf (seed) extract-manufacturer: shaanxi Sinot Biotechnology, Inc.; the product name is as follows: walnut leaf (seed) extract (extracted from the leaves and seeds of black walnut); production batch number: HT 16274520171109;

lotus (NELUMBO NUCIFERA) flower extract-manufacturer: sienna Tianrui Biotechnology, Inc.; the product name is as follows: lotus flower extract; production batch number: TR 34215-L20171214;

tea (CAMELLIA SINENSIS) leaf extract-manufacturer: ganzhou Huahan Biotech Co., Ltd; the product name is as follows: tea leaf extract (extracted from green tea); production batch number: HH 12934520171104;

GINSENG (PANAX GINSENG) root extract-manufacturer: ganzhou Huahan Biotech Co., Ltd; the product name is as follows: ginseng root extract (ginsenoside); production batch number: HH 12436520171018;

wherein, the base material comprises the following components by mass percent: 41.2% of a thickening agent, 10.3% of a pH regulator, 10.3% of a humectant, 16.5% of an emulsifier, 4.1% of a hair conditioner, 12.3% of a hair colorant, 3.3% of an antioxidant, 1.2% of a fragrance, 0.8% of a chelating agent;

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of ceteareth-20 to glyceryl stearate is 2.5: 1.5;

the hair conditioner is caprylic triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 5: 3;

the aromatic is essence;

the chelating agent is EDTA disodium;

in the step 2, the step of mixing the raw materials,

adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and caprylic triglyceride together, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;

in the step 4, the step of,

uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

adding Galla chinensis extract, folium Juglandis (seed) extract, flos Nelumbinis extract, folium Camelliae sinensis extract, radix Ginseng extract, ammonium hydroxide and essence into mixture D, and stirring to obtain herbal hair caring and dyeing paste A.

Example 2

A preparation process of a herbal hair care and hair dye cream containing a Chinese gall extract comprises the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 24.3% of base material, 4% of nutgall extract, 4% of walnut leaf (seed) extract, 4% of lotus flower extract, 4% of tea extract, 4% of ginseng root extract and 55.7% of deionized water according to mass percentage;

the purchase information of the gallnut extract, the walnut leaf (seed) extract, the lotus flower extract, the tea leaf extract and the ginseng root extract adopted in the present example is the same as that of example 1;

wherein, the base material comprises the following components by mass percent: 41.2% of a thickening agent, 10.3% of a pH regulator, 10.3% of a humectant, 16.5% of an emulsifier, 4.1% of a hair conditioner, 12.3% of a hair colorant, 3.3% of an antioxidant, 1.2% of a fragrance, 0.8% of a chelating agent;

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of ceteareth-20 to glyceryl stearate is 2.5: 1.5;

the hair conditioner is caprylic triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 5: 3;

the aromatic is essence;

the chelating agent is EDTA disodium;

in the step 2, the step of mixing the raw materials,

adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and caprylic triglyceride together, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;

in the step 4, the step of,

uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

and adding a gallnut extract, a walnut leaf (seed) extract, a lotus flower extract, a tea leaf extract, a ginseng root extract, ammonium hydroxide and essence into the mixture D, and uniformly stirring to obtain the herbal hair care and hair dyeing cream B.

Example 3

A preparation process of a herbal hair care and hair dye cream containing a Chinese gall extract comprises the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 24.3% of base material, 5% of nutgall extract, 5% of walnut leaf (seed) extract, 5% of lotus flower extract, 5% of tea extract, 5% of ginseng root extract and 50.7% of deionized water according to mass percentage;

the purchase information of the gallnut extract, the walnut leaf (seed) extract, the lotus flower extract, the tea leaf extract and the ginseng root extract adopted in the present example is the same as that of example 1;

wherein, the base material comprises the following components by mass percent: 41.2% of a thickening agent, 10.3% of a pH regulator, 10.3% of a humectant, 16.5% of an emulsifier, 4.1% of a hair conditioner, 12.3% of a hair colorant, 3.3% of an antioxidant, 1.2% of a fragrance, 0.8% of a chelating agent;

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of ceteareth-20 to glyceryl stearate is 2.5: 1.5;

the hair conditioner is caprylic triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 5: 3;

the aromatic is essence;

the chelating agent is EDTA disodium;

in the step 2, the step of mixing the raw materials,

adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and caprylic triglyceride together, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;

in the step 4, the step of,

uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

and adding a gallnut extract, a walnut leaf (seed) extract, a lotus flower extract, a tea leaf extract, a ginseng root extract, ammonium hydroxide and essence into the mixture D, and uniformly stirring to obtain the herbal hair care and hair dyeing cream C.

Tests prove that the hair care and hair care effects of the hair care and hair dye cream prepared by the three embodiments are as follows:

under an indoor environment with the temperature of 25 ℃, on the hair of the same tester, the herbal hair care and hair dye cream A is uniformly smeared on the No. 1 area white hair of the tester, the herbal hair care and hair dye cream B is uniformly smeared on the No. 2 area white hair of the tester, and the herbal hair care and hair dye cream C is uniformly smeared on the No. 3 area white hair of the tester; after standing for 20 minutes, washing off the paste with clear water, and observing the paste with naked eyes when the hair of a tester is air-dried: the white hair in the area No. 1 is dyed black, the color is uniform, the hair is black, and the hair has slight luster; the white hair in the No. 2 area is dyed black, the color is uniform, the hair quality is black, the white hair is shinier than that in the No. 1 area, and the hair is smoother; the white hair in the No. 3 area is dyed black, the color is uniform, the hair is naturally black, the color is full, the glossiness is full, and the hair is light and smooth.

As can be seen from the above tests, the herbal hair care and dyeing cream C contains the most herbal extracts, and after dyeing, the hair in the area No. 3 is the most glossy, the most smooth and the most smooth, and the hair dyeing effect is the best; the herbaceous plants in the herbaceous hair care and hair dyeing cream have the hair care effect.

Example 4

A preparation process of a herbal hair care and hair dye cream containing a Chinese gall extract comprises the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 20% of base material, 5% of nutgall extract, 5% of walnut leaf (seed) extract, 5% of lotus flower extract, 5% of tea extract, 5% of ginseng root extract and 55% of deionized water according to mass percentage;

the purchase information of the gallnut extract, the walnut leaf (seed) extract, the lotus flower extract, the tea leaf extract and the ginseng root extract adopted in the present example is the same as that of example 1;

wherein, the base material comprises the following components by mass percent: 38% of a thickener, 12% of a pH adjuster, 12% of a humectant, 17.5% of an emulsifier, 5% of a hair conditioner, 10% of a hair colorant, 4% of an antioxidant, 1% of a fragrance, 0.5% of a chelating agent;

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2: 1;

the hair conditioner is capric triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4: 2;

the aromatic is essence;

the chelating agent is EDTA disodium;

in the step 2, the step of mixing the raw materials,

adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 82 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and capric triglyceride together, heating while stirring until the temperature of the mixture reaches 82 deg.C, and stopping heating and stirring to obtain uniformly stirred mixture B;

in the step 4, the step of,

uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

and adding a gallnut extract, a walnut leaf (seed) extract, a lotus flower extract, a tea leaf extract, a ginseng root extract, ammonium hydroxide and essence into the mixture D, and uniformly stirring to obtain the herbal hair care and hair dyeing cream D.

Example 5

A preparation process of a herbal hair care and hair dye cream containing a Chinese gall extract comprises the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 28% of base material, 5% of nutgall extract, 5% of walnut leaf (seed) extract, 5% of lotus flower extract, 5% of tea extract, 5% of ginseng root extract and 47% of deionized water according to mass percentage;

the purchase information of the gallnut extract, the walnut leaf (seed) extract, the lotus flower extract, the tea leaf extract and the ginseng root extract adopted in the present example is the same as that of example 1;

wherein, the base material comprises the following components by mass percent: 45% of a thickener, 8% of a pH adjuster, 8% of a humectant, 14% of an emulsifier, 3% of a hair conditioner, 15% of a hair colorant, 2% of an antioxidant, 3% of a fragrance, 2% of a chelating agent;

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 3: 2;

the hair conditioner is stearic acid triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 6: 4;

the aromatic is essence;

the chelating agent is EDTA disodium;

in the step 2, the step of mixing the raw materials,

adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 80 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and glyceryl tristearate together, heating while stirring until the temperature of the mixture reaches 80 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;

in the step 4, the step of,

uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

and adding a gallnut extract, a walnut leaf (seed) extract, a lotus flower extract, a tea leaf extract, a ginseng root extract, ammonium hydroxide and essence into the mixture D, and uniformly stirring to obtain the herbal hair care and hair dyeing cream E.

The hair care and hair dyeing cream is kept at the temperature of 40 +/-2 ℃ for 6 hours, has no oil-water separation phenomenon after the room temperature is recovered, is kept at the temperature of-10 +/-2 ℃ for 24 hours, and has no oil-water separation phenomenon after the room temperature is recovered. In the process of dyeing hair, the hair dye is easy to apply to hair, does not easily generate dropping liquid, does not flow, and does not stain skin and clothes. The coloring capability is strong, the hair can be colored at normal temperature without heating and drying the hair; the dyeing fastness is good, the dyeing effect is durable, and the hair color and the glossiness are not obviously changed after 50 times of hair washing; after dyeing, the hair is bright, smooth, easy to comb and rich in luster. The hair dye has mild performance, and has no itching, no tension, no irritation and no red swelling of scalp during and after hair dyeing.

Claims (5)

1. The herbal hair care and hair dye cream containing the gallnut extract is characterized by comprising the following raw materials in percentage by mass: 20-28% of base material, 3-5% of nutgall extract, 3-5% of walnut leaf (seed) extract, 3-5% of lotus flower extract, 3-5% of tea extract, 3-5% of ginseng root extract and the balance of deionized water, wherein the sum of the mass percentages of the components is 100%.

2. The herbal hair care and hair dye cream containing the gallnut extract as claimed in claim 1, wherein the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent.

3. The herbal hair care and hair dye cream containing gallnut extract according to claim 2, characterized in that:

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2-3: 1-2;

the hair conditioner is one of caprylic triglyceride, capric triglyceride or stearic triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4-6: 2-4;

the aromatic is essence;

the chelating agent is disodium EDTA.

4. A process for preparing the herbal hair care and hair dye cream containing the Chinese gall extract according to claim 2, which is characterized by comprising the following specific operation steps:

in the step 1, the method comprises the following steps of,

weighing 20-28% of base material, 3-5% of nutgall extract, 3-5% of walnut leaf (seed) extract, 3-5% of lotus flower extract, 3-5% of tea extract, 3-5% of ginseng root extract and the balance of deionized water according to mass percentage, wherein the sum of the mass percentages of the components is 100%;

wherein, the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent;

in the step 2, the step of mixing the raw materials,

adding a humectant and a chelating agent into deionized water, heating while stirring until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;

in the step 3, the step of,

mixing the thickening agent, the emulsifying agent and the hair conditioner together, heating and stirring the mixture at the same time until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;

in the step 4, the step of,

uniformly stirring a hair colorant and an antioxidant to obtain a mixture C for later use;

in the step 5, the step of the method is that,

adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;

in the step 6, the step of,

adding Galla chinensis extract, folium Juglandis (seed) extract, flos Nelumbinis extract, folium Camelliae sinensis extract, radix Ginseng extract, pH regulator and aromatic into mixture D, and stirring to obtain herbal hair caring and dyeing cream.

5. The process for preparing herbal hair care and hair dye cream containing gallnut extract according to claim 4, wherein the process comprises the following steps:

the thickening agent is cetostearyl alcohol;

the pH regulator is ammonium hydroxide;

the humectant is propylene glycol;

the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2-3: 1-2;

the hair conditioner is one of caprylic triglyceride, capric triglyceride or stearic triglyceride;

the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;

the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4-6: 2-4;

the aromatic is essence;

the chelating agent is disodium EDTA.