CN106727165A - Draft hair care dying cream and its preparation technology containing licorice root extract - Google Patents

Draft hair care dying cream and its preparation technology containing licorice root extract Download PDF

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CN106727165A
CN106727165A CN201710117778.4A CN201710117778A CN106727165A CN 106727165 A CN106727165 A CN 106727165A CN 201710117778 A CN201710117778 A CN 201710117778A CN 106727165 A CN106727165 A CN 106727165A
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hair
mixture
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root extract
stirring
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赵锴
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Guangzhou Peerless Enterprise Group Co Ltd
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Guangzhou Peerless Enterprise Group Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/10Preparations for permanently dyeing the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

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Abstract

The present invention provides a kind of draft hair care dying cream containing licorice root extract and its preparation technology, first to NMF and chelating agent is added in deionized water, heats while stirring, and temperature obtains mixture A after reaching 80 85 DEG C;Thickener, emulsifying agent and conditioner for hair are mixed again, is heated while stirring, temperature obtains mixture B after reaching 80 85 DEG C;Then hair colouring agent and antioxidant are uniformly mixing to obtain mixture C;Again to mixture B and mixture C is added in mixture A, stirring makes to obtain mixture D;Licorice root extract, ginger-root extract, Herb Gynostemmae Pentaphylli extract, aloe barbadensis Miller leaf extract, Flos Nelumbinis extract, pH adjusting agent and aromatic are added in most backward mixture D, draft hair care dying cream is uniformly mixing to obtain.Cream rinse of the present invention contains herbaceous plant, and moderate performance will not produce injury after hair dyeing to hair and scalp, and enemy returns good maintenance effect, moreover it is possible to alleviate itching of the scalp.

Description

Herbal hair care and hair dye cream containing licorice root extract and preparation process thereof
Technical Field
The invention belongs to the technical field of hair dyeing and caring products, and particularly relates to a herbal hair care and dyeing cream containing licorice root extract and a preparation process thereof.
Background
Hair dye is a cosmetic for dyeing hair, and in recent years, dyeing has become a fashionable choice, and according to survey, more than half of people who have dyed hair are on the spot among people who receive the survey. The existing hair dye is divided into: plant hair dyes, metal hair dyes, and oxidative hair dyes. The plant hair dye is used for dyeing by using substances extracted from flower stems and leaves of plants, so that the plant hair dye has small harm to a human body, but has weak coloring capability and quick color falling after hair dyeing. The metal hair dye has the action mechanism that metal ions in the hair dye penetrate into hair and react with sulfur in cysteine in hair protein to generate black lead sulfide and the like, so that the hair is dyed black; the heavy metal ions contained in the metal hair dye are easy to cause accumulation poisoning and great harm to human bodies besides damage to hair health and allergy. The dyes used in various hair dyes or hair dye pastes sold in the market at present are generally oxidative dyes, the oxidative dyes are composed of intermediates, couplers and oxidants, small molecular dye intermediates and couplers firstly permeate into cortex layers and medulla layers of hair, the oxidants oxidize the intermediates, then react with the couplers to form larger dye molecules, and the larger dye molecules permeate into hair fibers, thereby achieving a durable hair dyeing effect. Because of different kinds and content ratios of the dye intermediate and the coupler, reaction products with different hues are generated, and various hue products are combined into different hues, so that the hair is dyed with different colors. Since the dye macromolecules are formed in the hair fibers by the reaction of the dye intermediates and coupler small molecules, the dye macromolecules formed are not easily washed through the pore size of the hair fibers during washing. The hair dye has the condition of permanent hair dyeing, but contains more chemicals, has larger irritation to the scalp, can cause allergic phenomenon to some skin-sensitive people, and can cause harm to human bodies after long-term use.
Disclosure of Invention
The invention aims to provide a herbal hair care and dyeing paste containing licorice root extract, which has small irritation to scalp, strong coloring capability, hair dyeing and hair care.
The invention also aims to provide a preparation method of the herbal hair care and hair dye cream.
The technical scheme adopted by the invention is that,
the herbal hair care and hair dye cream containing the licorice root extract comprises the following raw materials in percentage by mass: 20-28% of base material, 3-5% of licorice root extract, 3-5% of ginger root extract, 3-5% of gynostemma pentaphylla extract, 3-5% of aloe barbadensis leaf extract, 3-5% of lotus flower extract and the balance of deionized water, wherein the sum of the mass percentages of the components is 100%.
The base material comprises the following components in percentage by mass: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent.
The preparation process of the herbal hair care and hair dyeing cream containing the licorice root extract comprises the following specific operation steps:
in the step 1, the method comprises the following steps of,
weighing 20-28% of base material, 3-5% of licorice root extract, 3-5% of ginger root extract, 3-5% of gynostemma pentaphylla extract, 3-5% of aloe barbadensis leaf extract, 3-5% of lotus flower extract and the balance of deionized water according to mass percentage, wherein the sum of the mass percentages of the components is 100%;
wherein, the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent;
in the step 2, the step of mixing the raw materials,
adding a humectant and a chelating agent into deionized water, heating while stirring until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing the thickening agent, the emulsifying agent and the hair conditioner together, heating and stirring the mixture at the same time until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;
in the step 4, the step of,
uniformly stirring a hair colorant and an antioxidant to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
adding Glycyrrhrizae radix extract, rhizoma Zingiberis recens extract, herba Gynostemmatis extract, Aloe Barbadensis leaf extract, flos Nelumbinis extract, pH regulator and aromatic into mixture D, and stirring to obtain herbal hair caring and dyeing paste.
Wherein,
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2-3: 1-2;
the hair conditioner is one of caprylic triglyceride, capric triglyceride or stearic triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4-6: 2-4;
the aromatic is essence;
the chelating agent is disodium EDTA.
The invention has the beneficial effects that:
1. the hair conditioner contains herbaceous plants, has mild performance, does not damage hair and scalp after hair dyeing, has good repairing effect on the hair, and can relieve scalp itch;
2. the coloring capability is strong, the hair can be colored at normal temperature without heating and drying the hair; the dyeing fastness is good, the dyeing effect is durable, and the smell is friendly;
3. the hair dyed is bright, smooth and easy to comb, and the hair is rich in luster; during and after hair dyeing, the scalp has no itching, tightness, irritation and red swelling.
Detailed Description
The invention provides a herbal hair care and hair dyeing paste containing licorice root extract, which comprises the following components in percentage by mass: 20-28% of base material, 3-5% of licorice root extract, 3-5% of ginger root extract, 3-5% of gynostemma pentaphylla extract, 3-5% of aloe barbadensis leaf extract, 3-5% of lotus flower extract and the balance of deionized water, wherein the sum of the mass percentages of the components is 100%.
Wherein, the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent.
Licorice (GLYCYRRHIZA URALENSIS) root extract: the main components are glycyrrhizic acid and liquiritin, and have the effects of resisting inflammation, resisting allergy, clearing heat and removing toxicity; has antipruritic and dandruff removing effects on scalp; and can make hair more soft and healthy.
Ginger (ZINGIBER OFFICINALE) root extract: has effects in promoting blood circulation of head skin, promoting scalp metabolism, activating hair follicle tissue, preventing alopecia and canities, stimulating new hair growth, removing dandruff, relieving itching, and strengthening hairy root.
Gynostemma PENTAPHYLLUM (Gynostemma PENTAPHYLLUM) extract: improving hair microcirculation, promoting hair epidermis germinal layer cell metabolism, enhancing scalp collagen fiber regeneration, and preventing and treating canities and alopecia; in addition, the hair-growing tea also has the effects of inhibiting cell aging and prolonging the cell life, the deposit after scalp cell death forms dandruff, the anti-aging effect of the gynostemma pentaphylla can prolong the scalp cell life, reduce the dandruff generation, and has the functions of sterilization and itching relieving.
Aloe BARBADENSIS (Aloe BARBADENSIS) leaf extract: can supplement water which is lacked in hair and scalp, so that the hair is more smooth and glossy; can regulate scalp sebum, promote scalp metabolism, make tissue blood at hair root well run, make hair fully nutritious, prevent canities and alopecia; aloe also has antibacterial and antiallergic effects, and can be used for inhibiting dandruff, scalp pruritus, etc., keeping scalp healthy, and making hair beautiful.
Extract of lotus (NELUMBO NUCIFERA) flower: can supplement water lost from hair and scalp, and recover smoothness and luster of hair; the hair follicle is balanced in water and oil, more oil is prevented from being secreted by the hair follicle, and the occurrence of folliculitis is reduced; in addition, it has antifungal and antibacterial effects, and can be used for preventing tinea capitis and scalp pruritus.
Thickening agent: the viscosity of the hair care and hair dyeing paste system is increased, the viscosity of the whole system is improved, the content of the thickening agent provided by the invention can ensure that the viscosity of the hair care and hair dyeing paste is between 1000 mPa.s and 100000 mPa.s, the hair care and hair dyeing paste in the range has good adsorbability with hair, is easy to apply to the hair, is not easy to generate dropping liquid, cannot flow, and can prevent the skin from being stained.
pH regulator: the pH value of the hair care and hair dyeing paste system is adjusted to be 7.0-11.0, because the hair can be expanded and softened only under the alkaline condition, and the hair scales are opened, so that the dye can be better diffused and permeated into the cortex.
Humectant: has effects of lubricating and moisturizing hair, and preventing frizziness of hair.
Emulsifier: the oil phase and the water phase in the hair care and hair dyeing cream can be mixed with each other to form a completely dispersed emulsion.
Conditioner for hair: because the hair care and dyeing cream is alkaline and can damage hair to a certain extent in the hair dyeing process, the hair conditioner added has certain protection and moistening effects on the hair.
Hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine in the hair colorant are hair dye intermediates; wherein, the 'hydroxyethyl-p-phenylenediamine sulfate' is used as an intermediate of the hair dye, the oxidation process is the fixation process of the color during the hair dyeing, and the method has the advantages that: 1. the antioxidant capacity is strong, 2, the damage to hair is small, 3, the damage to hair structure is small, 4, the ultraviolet resistance is strong (the advantages are obtained by comparing another similar intermediate p-phenylenediamine); the resorcinol is also a hair dye intermediate and is used as a complex dye, and has a sterilization function. The mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3:1, and the mixture prepared by the ratio is used as a hair dye intermediate, so that the toxicity of the hair dye intermediate is much lower than that of the common p-phenylenediamine in the existing market, the hair dye intermediate has small stimulation to scalp and hair, the hair dye intermediate does not damage the structure of the hair, does not cause discomfort to the scalp, does not cause harm to human bodies, and has strong oxidation resistance.
Antioxidant: can avoid sending out and lead to the inhomogeneous phenomenon of dyeing with colorant oxidation rate at the excessive speed, the antioxidant can make sending out and use colorant oxidation rate to slow down, guarantees to send out and has abundant time infiltration into the hair core with the colorant for it is more even to dye, and the dyeing is more bright.
Aromatic agent: the hair care and dyeing cream has fragrant smell and is not pungent.
Chelating agent: can chelate metal ions, so that the metal ions are difficult to have normal valence state reaction, thereby maintaining the stability of the hair care and hair dyeing cream and reducing the damage of the metal ions to hair and scalp. The chelating agent of the hair care and hair dyeing cream disclosed by the invention selects disodium EDTA, and the disodium EDTA has a chelating effect, a preservative effect and a good bacteriostatic ability on gram-negative bacteria.
Example 1
A preparation process of herbal hair care and hair dye cream containing licorice root extract comprises the following specific operation steps:
in the step 1, the method comprises the following steps of,
weighing 24.3% of base material, 3% of licorice root extract, 3% of ginger root extract, 3% of gynostemma pentaphylla extract, 3% of aloe barbadensis leaf extract, 3% of lotus flower extract and 60.7% of deionized water according to mass percentage;
the purchase information of licorice root extract, ginger root extract, gynostemma pentaphyllum extract, aloe barbadensis leaf extract and lotus flower extract used in this example is:
licorice (GLYCYRRHIZA URALENSIS) root extract-manufacturer: shanxi three-primitive-Tian-Domain biologicals, Inc.; the product name is as follows: licorice root extract; production batch number: TY 147546-G20170817;
ginger (ZINGIBER OFFICINALE) root extract-manufacturer: ganzhou Huahan Biotech Co., Ltd; the product name is as follows: ginger root extract (extracted from ginger root); production batch number: HH 15762120715;
GYNOSTEMMA pentaphylla (gynostem PENTAPHYLLUM) extract-manufacturer: ganzhou Huahan Biotech Co., Ltd; the product name is as follows: gynostemma pentaphyllum extract; production batch number: HH 17626720170411;
ALOE BARBADENSIS (ALOE BARBADENSIS) leaf extract-manufacturer: west ann tianfeng biotechnology limited; the product name is as follows: aloe vera leaf extract (barbaloin); production batch number: TF 42375720171108;
lotus (NELUMBO NUCIFERA) flower extract-manufacturer: sienna Tianrui Biotechnology, Inc.; the product name is as follows: lotus flower extract; production batch number: TR 34215-L20171214;
wherein, the base material comprises the following components by mass percent: 41.2% of a thickening agent, 10.3% of a pH regulator, 10.3% of a humectant, 16.5% of an emulsifier, 4.1% of a hair conditioner, 12.3% of a hair colorant, 3.3% of an antioxidant, 1.2% of a fragrance, 0.8% of a chelating agent;
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of ceteareth-20 to glyceryl stearate is 2.5: 1.5;
the hair conditioner is caprylic triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 5: 3;
the aromatic is essence;
the chelating agent is EDTA disodium;
in the step 2, the step of mixing the raw materials,
adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and caprylic triglyceride together, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;
in the step 4, the step of,
uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
adding Glycyrrhrizae radix extract, rhizoma Zingiberis recens extract, herba Gynostemmatis extract, Aloe Barbadensis leaf extract, flos Nelumbinis extract, ammonium hydroxide and essence into mixture D, and stirring to obtain herbal hair caring and dyeing paste A.
Example 2
A preparation process of herbal hair care and hair dye cream containing licorice root extract comprises the following specific operation steps:
in the step 1, the method comprises the following steps of,
weighing 24.3% of base material, 4% of licorice root extract, 4% of ginger root extract, 4% of gynostemma pentaphylla extract, 4% of aloe barbadensis leaf extract, 4% of lotus flower extract and 55.7% of deionized water according to mass percentage;
the purchase information of the licorice root extract, ginger root extract, gynostemma pentaphyllum extract, aloe barbadensis leaf extract and lotus flower extract used in this example is the same as that of example 1;
wherein, the base material comprises the following components by mass percent: 41.2% of a thickening agent, 10.3% of a pH regulator, 10.3% of a humectant, 16.5% of an emulsifier, 4.1% of a hair conditioner, 12.3% of a hair colorant, 3.3% of an antioxidant, 1.2% of a fragrance, 0.8% of a chelating agent;
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, and the mass ratio of the ceteareth-20 to the glyceryl stearate is 2.5: 1.5;
the hair conditioner is caprylic triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 5: 3;
the aromatic is essence;
the chelating agent is EDTA disodium;
in the step 2, the step of mixing the raw materials,
adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and caprylic triglyceride together, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;
in the step 4, the step of,
uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
and adding the licorice root extract, the ginger root extract, the gynostemma pentaphylla extract, the aloe barbadensis leaf extract, the lotus flower extract, ammonium hydroxide and essence into the mixture D, and uniformly stirring to obtain the herbal hair care and hair dyeing paste B.
Example 3
A preparation process of herbal hair care and hair dye cream containing licorice root extract comprises the following specific operation steps:
in the step 1, the method comprises the following steps of,
weighing 24.3% of base material, 5% of licorice root extract, 5% of ginger root extract, 5% of gynostemma pentaphylla extract, 5% of aloe barbadensis leaf extract, 5% of lotus flower extract and 50.7% of deionized water according to mass percentage;
the purchase information of the licorice root extract, ginger root extract, gynostemma pentaphyllum extract, aloe barbadensis leaf extract and lotus flower extract used in this example is the same as that of example 1;
wherein, the base material comprises the following components by mass percent: 41.2% of a thickening agent, 10.3% of a pH regulator, 10.3% of a humectant, 16.5% of an emulsifier, 4.1% of a hair conditioner, 12.3% of a hair colorant, 3.3% of an antioxidant, 1.2% of a fragrance, 0.8% of a chelating agent;
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, and the mass ratio of the ceteareth-20 to the glyceryl stearate is 2.5: 1.5;
the hair conditioner is caprylic triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 5: 3;
the aromatic is essence;
the chelating agent is EDTA disodium;
in the step 2, the step of mixing the raw materials,
adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and caprylic triglyceride together, heating while stirring until the temperature of the mixture reaches 85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;
in the step 4, the step of,
uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
and adding the licorice root extract, the ginger root extract, the gynostemma pentaphylla extract, the aloe barbadensis leaf extract, the lotus flower extract, ammonium hydroxide and essence into the mixture D, and uniformly stirring to obtain the herbal hair care and hair dyeing paste C.
Tests prove that the hair care and hair care effects of the hair care and hair dye cream prepared by the three embodiments are as follows:
under an indoor environment with the temperature of 25 ℃, on the hair of the same tester, the herbal hair care and hair dye cream A is uniformly smeared on the No. 1 area white hair of the tester, the herbal hair care and hair dye cream B is uniformly smeared on the No. 2 area white hair of the tester, and the herbal hair care and hair dye cream C is uniformly smeared on the No. 3 area white hair of the tester; after standing for 20 minutes, washing off the paste with clear water, and observing the paste with naked eyes when the hair of a tester is air-dried: the white hair in the area No. 1 is dyed black, the color is uniform, the hair is black, and the hair has slight luster; the white hair in the No. 2 area is dyed black, the color is uniform, the hair quality is black, the white hair is shinier than that in the No. 1 area, and the hair is smoother; the white hair in the No. 3 area is dyed black, the color is uniform, the hair is naturally black, the color is full, the glossiness is full, and the hair is light and smooth.
As can be seen from the above tests, the herbal hair care and dyeing cream C contains the most herbal extracts, and after dyeing, the hair in the area No. 3 is the most glossy, the most smooth and the most smooth, and the hair dyeing effect is the best; the herbaceous plants in the herbaceous hair care and hair dyeing cream have the hair care effect.
Example 4
A preparation process of herbal hair care and hair dye cream containing licorice root extract comprises the following specific operation steps:
in the step 1, the method comprises the following steps of,
weighing 20% of base material, 5% of licorice root extract, 5% of ginger root extract, 5% of gynostemma pentaphylla extract, 5% of aloe barbadensis leaf extract, 5% of lotus flower extract and 55% of deionized water according to mass percentage;
the purchase information of the licorice root extract, ginger root extract, gynostemma pentaphyllum extract, aloe barbadensis leaf extract and lotus flower extract used in this example was the same as that of example 1.
Wherein, the base material comprises the following components by mass percent: 38% of a thickener, 12% of a pH adjuster, 12% of a humectant, 17.5% of an emulsifier, 5% of a hair conditioner, 10% of a hair colorant, 4% of an antioxidant, 1% of a fragrance, 0.5% of a chelating agent;
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2: 1;
the hair conditioner is capric triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4: 2;
the aromatic is essence;
the chelating agent is EDTA disodium;
in the step 2, the step of mixing the raw materials,
adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 82 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and capric triglyceride together, heating while stirring until the temperature of the mixture reaches 82 deg.C, and stopping heating and stirring to obtain uniformly stirred mixture B;
in the step 4, the step of,
uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
adding Glycyrrhrizae radix extract, rhizoma Zingiberis recens extract, herba Gynostemmatis extract, Aloe Barbadensis leaf extract, flos Nelumbinis extract, ammonium hydroxide and essence into mixture D, and stirring to obtain herbal hair caring and dyeing paste D.
Example 5
A preparation process of herbal hair care and hair dye cream containing licorice root extract comprises the following specific operation steps:
in the step 1, the method comprises the following steps of,
weighing 28% of base material, 5% of licorice root extract, 5% of ginger root extract, 5% of gynostemma pentaphylla extract, 5% of aloe barbadensis leaf extract, 5% of lotus flower extract and 47% of deionized water according to mass percentage;
the purchase information of the licorice root extract, ginger root extract, gynostemma pentaphyllum extract, aloe barbadensis leaf extract and lotus flower extract used in this example is the same as that of example 1;
wherein, the base material comprises the following components by mass percent: 45% of a thickener, 8% of a pH adjuster, 8% of a humectant, 14% of an emulsifier, 3% of a hair conditioner, 15% of a hair colorant, 2% of an antioxidant, 3% of a fragrance, 2% of a chelating agent;
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 3: 2;
the hair conditioner is stearic acid triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 6: 4;
the aromatic is essence;
the chelating agent is EDTA disodium;
in the step 2, the step of mixing the raw materials,
adding propylene glycol and EDTA disodium into deionized water, heating while stirring until the temperature of the mixture reaches 80 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing cetearyl alcohol, ceteareth-20, glyceryl stearate and glyceryl tristearate together, heating while stirring until the temperature of the mixture reaches 80 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;
in the step 4, the step of,
uniformly stirring hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol, 2-amino-3-hydroxypyridine, sodium sulfite and sodium erythorbate to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
adding Glycyrrhrizae radix extract, rhizoma Zingiberis recens extract, herba Gynostemmatis extract, Aloe Barbadensis leaf extract, flos Nelumbinis extract, ammonium hydroxide and essence into mixture D, and stirring to obtain herbal hair caring and dyeing paste E.
The hair care and hair dyeing cream is kept at the temperature of 40 +/-2 ℃ for 6 hours, has no oil-water separation phenomenon after the room temperature is recovered, is kept at the temperature of-10 +/-2 ℃ for 24 hours, and has no oil-water separation phenomenon after the room temperature is recovered. In the process of dyeing hair, the hair dye is easy to apply to hair, does not easily generate dropping liquid, does not flow, and does not stain skin and clothes. The coloring capability is strong, the hair can be colored at normal temperature without heating and drying the hair; the dyeing fastness is good, the dyeing effect is durable, and the hair color and the glossiness are not obviously changed after 50 times of hair washing; after dyeing, the hair is bright, smooth, easy to comb and rich in luster. The hair dye has mild performance, and has no itching, no tension, no irritation and no red swelling of scalp during and after hair dyeing.

Claims (5)

1. The herbal hair care and hair dye cream containing the licorice root extract is characterized in that the raw materials consist of the following components in percentage by mass: 20-28% of base material, 3-5% of licorice root extract, 3-5% of ginger root extract, 3-5% of gynostemma pentaphylla extract, 3-5% of aloe barbadensis leaf extract, 3-5% of lotus flower extract and the balance of deionized water, wherein the sum of the mass percentages of the components is 100%.
2. The herbal hair care and hair dye cream containing licorice root extract according to claim 1, wherein the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent.
3. The herbal hair care and hair dye cream containing licorice root extract according to claim 2, wherein:
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2-3: 1-2;
the hair conditioner is one of caprylic triglyceride, capric triglyceride or stearic triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4-6: 2-4;
the aromatic is essence;
the chelating agent is disodium EDTA.
4. A process for preparing herbal hair care and hair dye cream containing licorice root extract according to claim 2, wherein the process comprises the following steps:
in the step 1, the method comprises the following steps of,
weighing 20-28% of base material, 3-5% of licorice root extract, 3-5% of ginger root extract, 3-5% of gynostemma pentaphylla extract, 3-5% of aloe barbadensis leaf extract, 3-5% of lotus flower extract and the balance of deionized water according to mass percentage, wherein the sum of the mass percentages of the components is 100%;
wherein, the base material comprises the following components by mass percent: 38-45% of a thickening agent, 8-12% of a pH regulator, 8-12% of a humectant, 14-17.5% of an emulsifier, 3-5% of a hair conditioner, 10-15% of a hair colorant, 2-4% of an antioxidant, 1-3% of an aromatic and 0.5-2% of a chelating agent; the sum of the mass percentages of the components is 100 percent;
in the step 2, the step of mixing the raw materials,
adding a humectant and a chelating agent into deionized water, heating while stirring until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture A for later use;
in the step 3, the step of,
mixing the thickening agent, the emulsifying agent and the hair conditioner together, heating and stirring the mixture at the same time until the temperature of the mixture reaches 80-85 ℃, and stopping heating and stirring to obtain a uniformly stirred mixture B for later use;
in the step 4, the step of,
uniformly stirring a hair colorant and an antioxidant to obtain a mixture C for later use;
in the step 5, the step of the method is that,
adding the mixture B and the mixture C into the mixture A, and stirring uniformly to fully emulsify the mixture A, the mixture B and the mixture C to obtain a mixture D;
in the step 6, the step of,
adding Glycyrrhrizae radix extract, rhizoma Zingiberis recens extract, herba Gynostemmatis extract, Aloe Barbadensis leaf extract, flos Nelumbinis extract, pH regulator and aromatic into mixture D, and stirring to obtain herbal hair caring and dyeing paste.
5. The process for preparing herbal hair care and hair dye cream containing licorice root extract according to claim 4, wherein the herbal hair care and hair dye cream comprises the following steps:
the thickening agent is cetostearyl alcohol;
the pH regulator is ammonium hydroxide;
the humectant is propylene glycol;
the emulsifier is ceteareth-20 and glyceryl stearate, wherein the mass ratio of the ceteareth-20 to the glyceryl stearate is 2-3: 1-2;
the hair conditioner is one of caprylic triglyceride, capric triglyceride or stearic triglyceride;
the hair colorant is hydroxyethyl-p-phenylenediamine sulfate, resorcinol, 2, 4-diaminophenoxyethanol and 2-amino-3-hydroxypyridine; wherein the mass ratio of the hydroxyethyl-p-phenylenediamine sulfate to the resorcinol to the 2, 4-diaminophenoxyethanol to the 2-amino-3-hydroxypyridine is 20:6:3: 1;
the antioxidant is sodium sulfite and sodium erythorbate, and the mass ratio of the sodium sulfite to the sodium erythorbate is 4-6: 2-4;
the aromatic is essence;
the chelating agent is disodium EDTA.
CN201710117778.4A 2017-03-01 2017-03-01 Draft hair care dying cream and its preparation technology containing licorice root extract Pending CN106727165A (en)

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CN112641662A (en) * 2020-12-31 2021-04-13 泉后(广州)生物科技研究院有限公司 Soothing and anti-allergy composition and application thereof
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CN118021695A (en) * 2024-01-17 2024-05-14 广东领康日用品有限公司 Comfortable and dyed hair care composition and preparation method and application thereof

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