CN105232402B - A kind of composition with skin-care effect - Google Patents
A kind of composition with skin-care effect Download PDFInfo
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- CN105232402B CN105232402B CN201510759942.2A CN201510759942A CN105232402B CN 105232402 B CN105232402 B CN 105232402B CN 201510759942 A CN201510759942 A CN 201510759942A CN 105232402 B CN105232402 B CN 105232402B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention provides a kind of compositions with skin-care effect, it is formed by the component combine of following weight proportion：10~25 parts of black fruit fructus lycii Aqueous extracts, 10~16 parts of sea-buckthorn Aqueous extracts, 5~10 parts of licorice water extract.After black fruit fructus lycii, sea-buckthorn and Radix Glycyrrhizae are applied in combination the present invention, with use black fruit fructus lycii, sea-buckthorn, Radix Glycyrrhizae the group of compatibility two-by-two compared with, the beauty functions that the present invention combines the facial mask to be formed, Essence etc. greatly improve, and illustrate that black fruit fructus lycii, sea-buckthorn and Radix Glycyrrhizae compatible use have been played synergistic function by the present invention；Meanwhile it is mildly non-stimulated by skin care item prepared by composition, side effect is not generated, and splendid to the skin care effect of dry skin, there are good market prospects.
Description
Technical field
The present invention relates to a kind of compositions with skin-care effect.
Background technology
Presently commercially available skin care item are dazzling, are divided into whitening, moisturizing, cleaning, Sage Extract, anti-ageing according to different efficacies
Always, it releives, the facial mask that compacts etc., lead, mercury, benzene in most products, phenol content are exceeded, although temporarily skin can be made to present
Glossy soft state, but it is used for a long time that cuticula can be made to fall off is thinning, lead to red swelling of the skin, forms color spot, be unfavorable for skin
Health.
Black fruit fructus lycii and sea-buckthorn are distributed across the characteristic berry in northwest China area, they are grown in salinization wasteland, salinization
In the salination ambient soil such as sand ground, growth conditions is arduous, and vitality is extremely strong, drought-enduring, the cold-resistant, high temperature resistant of energy, very precious.It is black
Fruit Chinese wolfberry fruit is rich in anthocyanidin, being capable of anti-aging, beautifying face and moistering lotion.Vitamin C content is high in sea buckthorn fruit, skin can be made to be full of
Vigor.Two kinds of berries all can be used as skin care item, also edible.
It is combined currently on the market still without using black fruit fructus lycii and sea-buckthorn, the skin care item for being used as main skin care ingredient go out
It is existing.
Invention content
In order to increase the added value of product of black fruit fructus lycii, sea-buckthorn, the present invention plans the two and is applied in combination to prepare skin care item,
However, only whether both above-mentioned combination can reach good skin care effect, someone's research yet there are no.Before inventor
Phase experiment is found, if only by the compatible use of both black fruit fructus lycii and sea-buckthorn, although also there is certain skin care effect, in different skins
Show different in matter, especially not ideal enough to the whitening and anti-aging of dry skin and other effects, target user's range is relatively narrow.For
This, inventor passes through a large amount of experiment screening, final to confirm, only on the basis of black fruit fructus lycii, sea-buckthorn, add Radix Glycyrrhizae into
Row compatibility can play the skin care effect of each raw material to the maximum extent in the case of minimum raw material type.
For these reasons, the present invention is practical provides a kind of composition with skin-care effect, it is by following weight
The component combine of proportioning forms：
10~25 parts of black fruit fructus lycii Aqueous extracts, 10~16 parts of sea-buckthorn Aqueous extracts, 5~10 parts of licorice water extract.
In a specific implementation mode of the invention, composition is formed by the component combine of following weight proportion：
10 parts of black fruit fructus lycii Aqueous extracts, 10 parts of sea-buckthorn Aqueous extracts, 5 parts of licorice water extract.
Wherein, the black fruit fructus lycii Aqueous extracts are prepared by the following method：
Fresh black fruit fructus lycii is taken, appropriate antioxidant, grinding or crushing is added；Deionized water is added to be uniformly mixed, filtering
Or centrifugation, this step carry out 1~3 time, merge supernatant, are concentrated under reduced pressure into 1.5~2.2g/mL, preferably 2g/mL is to get black
Fruit matrimony vine Aqueous extracts.
Wherein, the use of antioxidant is to protect the anthocyanidin isoreactivity ingredient in black fruit fructus lycii, and antioxidant can
To select the composition of one or more of vitamin C, glutathione, lipoic acid or uric acid.
In a specific implementation mode of the invention, antioxidant selects vitamin C；Further, ascorbic dosage is
10%~50%w/w of fresh black fruit fructus lycii weight, preferably 40%w/w.
Wherein, the sea-buckthorn Aqueous extracts are prepared by the following method：
Fresh sea-buckthorn is taken, the extraction of deionization water temperature is added to take, extracting solution filtering or centrifugation, supernatant is concentrated under reduced pressure into 1.5~
2.2g/mL, preferably 2g/mL are to get sea-buckthorn Aqueous extracts.
Wherein, the temperature that temperature extraction takes is 50~70 DEG C, is further 55~65 DEG C, a specific implementation mode of the invention
It is middle to select temperature for 60 ± 2 DEG C.
Wherein, the licorice water extract is prepared by the following method：Extracting liquorice medicine materical crude slice, adds water to cook extraction, filtering or
Centrifugation, supernatant are concentrated under reduced pressure into 1.0~2.0g/mL, and preferably 1.5g/mL is to get licorice water extract.
The present invention also provides use of the above-mentioned composition in preparing the skin care item with whitening or/and senile-resistant efficacy
On the way.
Present composition skin effect is good, can it be prepared into skin care item together with other conventional skin care product ingredients,
To play wider range of skin effect simultaneously.
Wherein, the skin care item include facial mask, Essence, face cream, facial cleanser, smoothing toner, reparation dew etc..Conventional skin care
Product ingredient has hyaluronic acid, glycerine, PEG, elastin laminin, tocopherol etc..Further include other conventional kinds in addition to mentioned kind,
And will not be described here in detail.
The present invention the study found that the skin care item have good skin effect for dryness, neutrality or Oily, but
It is, if compared with the skin care item of other material combinations, using the skin care item of the present composition to the skin care effect of dry skin
It is even more ideal, more suitable for the use of dry skin.
After black fruit fructus lycii, sea-buckthorn and Radix Glycyrrhizae are applied in combination the present invention, and black fruit fructus lycii, sea-buckthorn, Radix Glycyrrhizae are used two-by-two
Compatibility group is compared, and the beauty functions that the present invention combines the facial mask to be formed, Essence etc. greatly improve, and illustrates the present invention by black fruit Chinese holly
Qi, sea-buckthorn and Radix Glycyrrhizae compatible use have played synergistic function；Meanwhile it is mildly non-stimulated by skin care item prepared by composition,
Side effect is not generated, and splendid to the skin care effect of dry skin, there are good market prospects.
Specific implementation mode
Specific embodiments of the present invention are described in detail below：
In the present invention, black fruit fructus lycii Aqueous extracts are to prepare in the following manner：The fresh black fruit fructus lyciis of 10g accurately are weighed,
To keep the stability of anthocyanidin in black fruit fructus lycii, addition 4g vitamin Cs are broken with mortar grinder, obtain black fruit fructus lycii pulp,
100mL deionized waters are added to stir evenly, filter, residue adds 100mL deionized waters again, filters, and merges supernatant twice, decompression
2g/mL is concentrated into get black fruit fructus lycii Aqueous extracts.
The preparation method of sea-buckthorn Aqueous extracts：Precision weighs the fresh sea-buckthorns of 10g, 200mL deionized waters is added, in 60 DEG C of water
2h is extracted in bath, has extracted and extracting solution 3000r/mim is centrifuged into 5min, and supernatant reduction vaporization is concentrated into 2g/mL to get sand
Spine Aqueous extracts.
Licorice water extract preparation method：Licorice piece 10g is weighed, be soaked in water 30min, heating and refluxing extraction 1h, filtering,
Supernatant is concentrated under reduced pressure into 1.5g/mL to get licorice water extract.
Concentration in the present invention after extract concentration is calculated by the following formula：
Quality (g)/volume (mL) of concentration (g/mL)=concentrate.
The preparation of 1 present composition of embodiment
Black fruit fructus lycii Aqueous extracts 100g, sea-buckthorn Aqueous extracts 100g, licorice water extract 50g are taken, after mixing, as this hair
The bright composition with skin-care effect.
The composition can be used directly, after other conventional skin care product ingredients can also be added, with the presence of conventional skin care product
Form is used, such as facial mask, Essence.
The preparation of 2 facial mask of embodiment
The present composition is prepared into facial mask, and corresponding efficacy test is carried out to facial mask.
1 each embodiment facial mask essence of table matches
| Constituent | Formula 1 | Formula 2 | Formula 3 | Formula 4 |
| Deionized water | 10 parts | 15 parts | 20 parts | 25 parts |
| Hyaluronic acid | 8 parts | 9 parts | 10 parts | 12 parts |
| Glycerine | 8 parts | 9 parts | 10 parts | 12 parts |
| Polyethylene glycol PEG-400 | 5 parts | 7 parts | 9 parts | 10 parts |
| Elastin hydrolysis | 3 parts | 3 parts | 4 parts | 5 parts |
| Black fruit fructus lycii extracting solution | 10 parts | 15 parts | 20 parts | 25 parts |
| Sea-buckthorn extracting solution | 10 parts | 12 parts | 14 parts | 16 parts |
| Licorice extract | 5 parts | 7 parts | 9 parts | 10 parts |
Preparation method：Essence is uniformly mixed, is sterilized, then face paper is impregnated 20~25 minutes in Essence, most
Vacuum Package is to get facial mask of the present invention afterwards.
In order to verify whether product of the present invention meets hygienic practice, the sample prepared by formula 1~4 is sent to third party's inspection
Mechanism is surveyed, whether detection product meets corresponding hygienic practice, and third party testing agency ties by being detected to indices
Fruit shows to meet corresponding specification, and finally the sample prepared by judgement formula 1~4 meets《Facial mask》(QB/T2872-
2007) limitation requirement.
In order to test the whitening anti-aging effect of facial mask of the present invention, choose the dry skin of areal, Oily, in
Property skin volunteer, being divided into four groups, (every group to respectively include 10 dry skins, 10 neutral skins, 10 Oilys on probation
Volunteer), utility efficiency experiment has been carried out to A, B, C, D product respectively：
1. test period：28 days
2. Evaluation product：
A products are the black fruit fructus lycii sea-buckthorn facial masks prepared with inventive formulation 1.
B products are the facial masks that the preparation of sea-buckthorn extracting solution is not added with inventive formulation 1, and the weight point of sea-buckthorn extracting solution is by black fruit
Fructus lycii extracted solution：Licorice extract=2：1 replaces, and other compositions are identical as A.
C products are the facial mask that the preparation of black fruit fructus lycii extracting solution is not added with inventive formulation 1, the weight of black fruit fructus lycii extracting solution
Divide by sea-buckthorn extracting solution：Licorice extract=2：1 replaces, and other compositions are identical as A.
D products are the facial masks that licorice extract preparation is not added with inventive formulation 1, and the weight point of licorice extract is by black fruit
Fructus lycii extracted solution：Sea-buckthorn extracting solution=1：1 replaces, and other compositions are identical as A.
3. test method：After each group tries out volunteer's cleaning face, A, B, C, D product are spread on into facial 15min respectively, often
It is primary, using 28 days, observes and investigates trial effect；
4. it is as follows to test effect statistics：
2 A product service conditions of table are fed back
3 B product service conditions of table are fed back
4 C product service conditions of table are fed back
5 D product service conditions of table are fed back
5. feeding back conclusion：
(1) using no after four kinds of products the allergic phenomenas such as red and swollen, husking occur for volunteer, illustrate above-mentioned facial mask safety
Property is good.
(2) first groups of triers indicate that A product whitening anti-aging moistening effects are fine, and skin quality is bright after a week for continuous use
Aobvious to improve, microgroove is reduced, and skin restores elastic and glossy.Second group of trier indicates that B products have certain wrinkle resistant moisturizing effect
Fruit, facial lines are reduced, but whitening effect unobvious, and most triers improve unobvious using rear skin lightening degree.
Third group trier indicates that C products have certain skin whitening, moisturizing effect, but goes wrinkle effect unobvious, uses front and back facial lines
It has no and significantly reduces.4th group of trier indicates that D products have certain skin whitening, moisturizing effect and go wrinkle effect, but not as good as A groups are imitated
Fruit is apparent.
By first group and other three groups relatively from the point of view of, for the skin care effect of dry skin volunteer, the effect of A products is bright
It is aobvious more preferable, illustrate A products compared with other 3 kinds of compatibility products more suitable for dry skin, this makes the target user of the present invention more
Comprehensively.
The preparation of 3 Essence of embodiment
6 each embodiment Essence of table matches
| Constituent | Essence formula of liquid 1 | Essence formula of liquid 2 | Essence formula of liquid 3 | Essence formula of liquid 4 |
| Deionized water | 10 parts | 15 parts | 20 parts | 25 parts |
| Hyaluronic acid | 8 parts | 9 parts | 10 parts | 12 parts |
| Glycerine | 8 parts | 9 parts | 10 parts | 12 parts |
| Polyethylene glycol PEG-400 | 5 parts | 7 parts | 9 parts | 10 parts |
| Elastin hydrolysis | 3 parts | 3 parts | 4 parts | 5 parts |
| Black fruit fructus lycii extracting solution | 10 parts | 15 parts | 20 parts | 25 parts |
| Sea-buckthorn extracting solution | 10 parts | 12 parts | 14 parts | 16 parts |
| Licorice extract | 5 parts | 7 parts | 9 parts | 10 parts |
| Vitamin E | 3 parts | 4 parts | 5 parts | 6 parts |
Preparation method：Above-mentioned each ingredient mixing is packed to get Essence of the present invention.
In order to test the whitening anti-aging effect of Essence of the present invention, choose the dry skin of areal, Oily,
Neutral skin volunteer, being divided into four groups, (every group respectively includes 10 dry skins, 10 neutral skins, 10 Oily examinations
With volunteer), utility efficiency experiment has been carried out to A, B, C, D product respectively：
1. test period：28 days
2. Evaluation product：
A products are the Essences prepared with essence formula of liquid 1 of the present invention.
B products are the Essence that the preparation of sea-buckthorn extracting solution is not added with essence formula of liquid 1 of the present invention, the weight of sea-buckthorn extracting solution
Divide by black fruit fructus lycii extracting solution：Licorice extract=2：1 replaces, and other compositions are identical as A.
C products are the Essence that the preparation of black fruit fructus lycii extracting solution is not added with essence formula of liquid 1 of the present invention, black fruit fructus lycii extraction
The weight of liquid point is by sea-buckthorn extracting solution：Licorice extract=2：1 replaces, and other compositions are identical as A.
D products are the Essence that licorice extract preparation is not added with essence formula of liquid 1 of the present invention, the weight of licorice extract
Divide by black fruit fructus lycii extracting solution：Sea-buckthorn extracting solution=1：1 replaces, and other compositions are identical as A.
3. test method：After each group tries out volunteer's cleaning face, A, B, C, D product are spread on into facial 15min respectively, often
It is primary, using 28 days, observes and investigates trial effect；
4. it is as follows to test effect statistics：
7 A product service conditions of table are fed back
8 B product service conditions of table are fed back
9 C product service conditions of table are fed back
10 D product service conditions of table are fed back
5. feeding back conclusion：
(1) using no after four kinds of products the allergic phenomenas such as red and swollen, husking occur for volunteer, illustrate above-mentioned Essence peace
Full property is good.Essence of the present invention can inhibit the formation of harmful free radicals and melanin, nutrition be injected for skin, so as to nti-freckle
Whitening, anti-aging, replenishing water and preserving moisture make skin gloss high resilience, and the young state of health is presented.
(2) first groups of triers indicate that A product whitening anti-aging moistening effects are fine, and skin quality is bright after a week for continuous use
Aobvious to improve, microgroove is reduced, and skin restores elastic and glossy.Second group of trier indicates that B products have certain wrinkle resistant moisturizing effect
Fruit, facial lines are reduced, but whitening effect unobvious, and most triers improve unobvious using rear skin lightening degree.
Third group trier indicates that C products have certain skin whitening, moisturizing effect, but goes wrinkle effect unobvious, uses front and back facial lines
It has no and significantly reduces.4th group of trier indicates that D products have certain skin whitening, moisturizing effect and go wrinkle effect, but not as good as A groups are imitated
Fruit is apparent.
(3) Essence of the present invention is good to the skin effect of various skin quality, this makes the target user of the present invention more
Comprehensively.
The preparation of 4 disposable sleep mask of embodiment
11 raw material proportioning of table
For the whitening anti-aging effect of the disposable sleep mask of the test present invention, dry skin, the oiliness of areal are chosen
Skin, neutral skin volunteer, being divided into two groups, (every group respectively includes 10 dry skins, 10 neutral skins, 10 oiliness skins
Skin tries out volunteer), utility efficiency has been carried out to A, B product obtained by Wash-free mask formula 1 and Wash-free mask formula 3 respectively
Experiment：
1. test period：28 days
2. test method：After each group volunteer on probation cleans face every night, A, B product are uniformly applied to face respectively,
The next morning normally washes one's face, and observes and investigates trial effect；
3. it is as follows to test effect statistics：
12 A product service conditions of table are fed back
13 B product service conditions of table are fed back
4. feeding back conclusion：
After 28 days, the facial lines of every group of volunteer are reduced, generally all relatively using more delicate before this product
Glossy and high resilience.And the resultant effect ratio A products of B products are more preferably.
In conclusion after black fruit fructus lycii, sea-buckthorn and Radix Glycyrrhizae are applied in combination the present invention, and black fruit fructus lycii, sea-buckthorn, sweet is used
The group of compatibility two-by-two of grass is compared, and the beauty functions that the present invention combines the facial mask to be formed, Essence etc. greatly improve, and illustrate the present invention
Black fruit fructus lycii, sea-buckthorn and Radix Glycyrrhizae compatible use synergistic function has been played into；Meanwhile it is mild by skin care item prepared by composition
It is non-stimulated, side effect is not generated, and splendid to the skin care effect of dry skin, there are good market prospects.
Claims (17)
1. a kind of composition with skin-care effect, it is characterised in that：It is formed by the component combine of following weight proportion：
10~25 parts of black fruit fructus lycii Aqueous extracts, 10~16 parts of sea-buckthorn Aqueous extracts, 5~10 parts of licorice water extract.
2. composition according to claim 1, it is characterised in that：It is formed by the component combine of following weight proportion：
10 parts of black fruit fructus lycii Aqueous extracts, 10 parts of sea-buckthorn Aqueous extracts, 5 parts of licorice water extract.
3. composition according to claim 1 or 2, it is characterised in that：The black fruit fructus lycii Aqueous extracts are made by the following method
It is standby to obtain：
Fresh black fruit fructus lycii is taken, appropriate antioxidant, grinding or crushing is added；Be added deionized water be uniformly mixed, filtering or from
The heart, this step carry out 1~3 time, merge supernatant, are concentrated under reduced pressure into 1.5~2.2g/mL to get black fruit fructus lycii Aqueous extracts；Its
In, the antioxidant is selected from the composition of one or more of vitamin C, glutathione, lipoic acid, uric acid.
4. composition according to claim 3, it is characterised in that：It is concentrated under reduced pressure into 2g/mL.
5. composition according to claim 3, it is characterised in that：The antioxidant is selected from vitamin C.
6. composition according to claim 5, it is characterised in that：Ascorbic dosage is fresh black fruit fructus lycii weight
10%~50%w/w.
7. composition according to claim 6, it is characterised in that：Ascorbic dosage is fresh black fruit fructus lycii weight
40%w/w.
8. composition according to claim 1 or 2, it is characterised in that：The sea-buckthorn Aqueous extracts are prepared by the following method
It arrives：
Fresh sea-buckthorn is taken, the extraction of deionization water temperature is added to take, extracting solution filtering or centrifugation, supernatant is concentrated under reduced pressure into 1.5~
2.2g/mL is to get sea-buckthorn Aqueous extracts.
9. composition according to claim 8, it is characterised in that：The supernatant is concentrated under reduced pressure into 2g/mL.
10. composition according to claim 8, it is characterised in that：The temperature that temperature extraction takes is 50~70 DEG C.
11. composition according to claim 10, it is characterised in that：The temperature that temperature extraction takes is 55~65 DEG C.
12. composition according to claim 11, it is characterised in that：The temperature that temperature extraction takes is 60 ± 2 DEG C.
13. composition according to claim 1 or 2, it is characterised in that：The licorice water extract is prepared by the following method
It arrives：Extracting liquorice medicine materical crude slice, adds water to cook extraction, and filtering or centrifugation, supernatant are concentrated under reduced pressure into 1.0~2.0g/mL to get liquorice beverage
Extract.
14. composition according to claim 13, it is characterised in that：Supernatant is concentrated under reduced pressure into 1.5g/mL.
15. composition described in claim 1~14 any one is in preparing the skin care item with whitening or/and senile-resistant efficacy
Purposes.
16. purposes according to claim 15, it is characterised in that：The skin care item are the skin cares that dry skin crowd uses
Product.
17. purposes according to claim 15 or 16, it is characterised in that：The skin care item be facial mask, Essence, face cream,
Facial cleanser, smoothing toner repair dew.
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| CN201510759942.2A CN105232402B (en) | 2015-11-10 | 2015-11-10 | A kind of composition with skin-care effect |
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| CN201510759942.2A CN105232402B (en) | 2015-11-10 | 2015-11-10 | A kind of composition with skin-care effect |
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| CN105232402A CN105232402A (en) | 2016-01-13 |
| CN105232402B true CN105232402B (en) | 2018-09-18 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106265286A (en) * | 2016-08-31 | 2017-01-04 | 青海新泰行生物科技有限公司 | A kind of cosmetic composition containing black Fructus Lycii extract and eye cream |
| CN108175723A (en) * | 2017-12-11 | 2018-06-19 | 百朗德生物化学(海门)有限公司 | With whitening and prevent the composition of skin aging and its application in cosmetics |
| CN111407695B (en) * | 2020-03-27 | 2022-09-30 | 陕西海天制药有限公司 | Sea-buckthorn water and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1799533A (en) * | 2005-01-07 | 2006-07-12 | 张善领 | Spot-removing and whitening essence liquid |
| CN103565699A (en) * | 2013-11-06 | 2014-02-12 | 中国科学院西北高原生物研究所 | Lycium ruthenicum mill freckle-removing and whitening anti-aging essence and preparation method of essence |
| CN104434741A (en) * | 2014-12-23 | 2015-03-25 | 吴辰 | Black wolfberry facial mask |
-
2015
- 2015-11-10 CN CN201510759942.2A patent/CN105232402B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1799533A (en) * | 2005-01-07 | 2006-07-12 | 张善领 | Spot-removing and whitening essence liquid |
| CN103565699A (en) * | 2013-11-06 | 2014-02-12 | 中国科学院西北高原生物研究所 | Lycium ruthenicum mill freckle-removing and whitening anti-aging essence and preparation method of essence |
| CN104434741A (en) * | 2014-12-23 | 2015-03-25 | 吴辰 | Black wolfberry facial mask |
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