CN104622711A - Fibroin shampoo and preparation method thereof - Google Patents
Fibroin shampoo and preparation method thereof Download PDFInfo
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- CN104622711A CN104622711A CN201410835375.XA CN201410835375A CN104622711A CN 104622711 A CN104622711 A CN 104622711A CN 201410835375 A CN201410835375 A CN 201410835375A CN 104622711 A CN104622711 A CN 104622711A
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Abstract
The invention discloses a fibroin shampoo and a preparation method thereof. The shampoo comprises the following components: guar gum, octadecyl trimethyl ammonium chloride, hydroxyethyl cellulose, lecithin, glycerol, propylene glycol, fibroin, vitamin E acetate, essence, diethyl succinate, menthol and deionized water. The preparation method comprises the steps of adding the guar gum, hydroxyethyl cellulose, lecithin, propylene glycol, fibroin, vitamin E acetate, essence, diethyl succinate and menthol into a reactor, adding 30-40 weight parts of deionized water, stirring and mixing uniformly, and then heating and stirring to obtain a mixture I; adding the octadecyl trimethyl ammonium chloride and the glycerol into the mixture I, heating and stirring under vacuum, then adding the remaining deionized water, continuously stirring the mixture, and homogenizing with a high pressure homogenizer to obtain the fibroin shampoo. The shampoo has good stability and hair washing and nourishing performance.
Description
Technical field
The invention belongs to cosmetics of everyday use preparing technical field, be specifically related to a kind of fibroin shampoo and preparation method thereof.
Background technology
Along with improving constantly of living standard, the love of the most attention that cosmetology is subject to people particularly ladies, dye is had a perm number of times showed increased, and has greatly the trend expanding to man and teenager, mid-aged population from Ms.Along with the injury of the chemical composition contained by the hair-washing hair-care in the increase of life stress and market, hair dyeing hair perming products, as cold wave lotion contain strong basicity chemical substance, hair dye contains the oxidation hair-dye material such as p-phenylenediamine (PPD), thus cause that hair is easy to withered and yellow, bifurcated, knotting, not submissive, be easy to fracture, hair caring after scalp scratch where it itches, easily cause scalp inflammation.According to an authoritative professional investigation company, nearly 2,000 investigation that consumer carries out are found, when the interviewee of 46% speaks of the hair in their ideal, answer be submissive, easily arrange, can one comb be the hair quality that current consumer wishes to have most on earth.
China restores vast, natural Chinese medicinal herb plant resources is very abundant, the custom of people's all useful natural Chinese medicinal herb raw material hair care hair caring for thousands of years, therefore, advantageous advantage is had to China with natural Chinese medicinal herb development of raw materials hair-washing hair-care articles for use, relative to the hair-washing hair-care articles for use be made up of chemical stimulating compositions, the hair-washing hair-care articles for use adopting Chinese herbal medicine to form have the advantage such as safety, character gentleness, not easy damaged hair quality.
For the problems that hair-washing hair-care articles for use above occur, the invention provides a kind of novel shampoo, at nourishing hair, improve hair quality, prevent yellow hair, submissive aspect has the effect that modern hair care product does not have.
Summary of the invention
The object of the invention is to provide a kind of fibroin shampoo and preparation method thereof to overcome above the deficiencies in the prior art, adopting fibroin as active material ingredients, improving hair-washing hair-care effect, improving shampoo stability.
Technical scheme of the present invention is as follows:
A kind of fibroin shampoo, comprises in components by weight percent: guar gum 1-5 part, octadecyl trimethyl ammonium chloride 0.2-0.6 part, hydroxyethyl-cellulose 0.2-0.6 part, lecithin 1-4 part, glycerol 1-5 part, propylene glycol 2-4 part, fibroin 2-6 part, vitamin e acetate 0.05-0.1 part, essence 0.1-0.4 part, diethyl succinate 1-4 part, menthol 0.02-0.06 part, deionized water 70-80 part.
Described fibroin shampoo, can preferably comprise in components by weight percent: guar gum 3-5 part, octadecyl trimethyl ammonium chloride 0.3-0.5 part, hydroxyethyl-cellulose 0.4-0.6 part, lecithin 2-4 part, glycerol 3-5 part, propylene glycol 2-3 part, fibroin 4-6 part, vitamin e acetate 0.06-0.08 part, essence 0.2-0.3 part, diethyl succinate 2-4 part, menthol 0.03-0.05 part, deionized water 75-78 part.
Described fibroin shampoo, can more preferably comprise in components by weight percent: guar gum 4 parts, octadecyl trimethyl ammonium chloride 0.4 part, hydroxyethyl-cellulose 0.5 part, 3 parts, lecithin, glycerol 4 parts, propylene glycol 3 parts, fibroin 5 parts, vitamin e acetate 0.07 part, 0.2 part, essence, diethyl succinate 3 parts, menthol 0.04 part, deionized water 76 parts.
The preparation method of described fibroin shampoo, comprises the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 30-40 part deionized water, be uniformly mixed, then 50-60 DEG C is warming up to, stir 100-150 minute, obtain mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 40-50 DEG C under the condition of 0.02-0.08MPa in vacuum, stir 30-50 minute, then add the deionized water of surplus, continue to stir 50-100 minute, obtain mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo.
The preparation method of described fibroin shampoo, the mixing speed be uniformly mixed in step 2 can be 120-150 rev/min.
The preparation method of described fibroin shampoo, the mixing speed stirred described in step 2 100-150 minute can be 70-80 rev/min.
The preparation method of described fibroin shampoo, in step 4, processing condition can be homogenization pressure 30-40MPa, homogenizing time 5-10 minute.
Fibroin has another name called fibroin albumen, it is the natural polymer fibrin extracted from silkworm silk, content accounts for 70% ~ 80% of silkworm silk, containing 18 seed amino acids, wherein glycine (gly), alanine (ala) and serine (ser) account for more than 80% of total composition.Aminoacid contained by these effectively can improve withered short-tempered, the problem such as bifurcated is impaired of hair, and make hair quality wash more glossy and more glossy, abundant foam thoroughly can remove hair oil stain, reaches the object of hair washing hair care.
Fibroin shampoo provided by the invention reaches good physical and chemical index, and wherein pH value is that between 6.5-7.0, working substance reaches more than 26.7%, and foam reaches more than 88mm.The present invention has carried out that in process of the test the vacuum in preparation method step 3 is added reaction and has changed common heating reaction into, result shows that the foaming properties of final products and heat-resisting and resistance to cold are all deteriorated, and therefore shows that the stability of vacuum response step to product of preparation process serves important function.Fibroin shampoo provided by the invention has good heat-resisting and resistance to cold, stable performance, without layering, show through 500 experimenter's result on trial simultaneously, shampoo nonirritant provided by the invention, without anaphylaxis, use rear hair pitch-black, submissive, glossy, naturally straight, reach well hair washing and the effect of taking care of hair.
Detailed description of the invention
Embodiment 1
A kind of fibroin shampoo, comprises in components by weight percent: guar gum 1 part, octadecyl trimethyl ammonium chloride 0.2 part, hydroxyethyl-cellulose 0.2 part, 1 part, lecithin, glycerol 1 part, propylene glycol 2 parts, fibroin 2 parts, vitamin e acetate 0.05 part, 0.1 part, essence, diethyl succinate 1 part, menthol 0.02 part, deionized water 70 parts.
The preparation method of described fibroin shampoo, comprises the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 30 parts of deionized waters, be uniformly mixed, mixing speed is 120 revs/min, is then warming up to 50 DEG C, stirs 100 minutes, mixing speed is 70 revs/min, obtains mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 40 DEG C under the condition of 0.02MPa in vacuum, stirs 30 minutes, then adds the deionized water of surplus, continues stirring 50 minutes, obtains mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo, and wherein processing condition is homogenization pressure 30MPa, homogenizing time 5 minutes.
Embodiment 2
A kind of fibroin shampoo, comprises in components by weight percent: guar gum 3 parts, octadecyl trimethyl ammonium chloride 0.3 part, hydroxyethyl-cellulose 0.4 part, 2 parts, lecithin, glycerol 3 parts, propylene glycol 2 parts, fibroin 4 parts, vitamin e acetate 0.06 part, 0.2 part, essence, diethyl succinate 2 parts, menthol 0.03 part, deionized water 75 parts.
The preparation method of described fibroin shampoo, comprises the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 32 parts of deionized waters, be uniformly mixed, mixing speed is 125 revs/min, is then warming up to 53 DEG C, stirs 110 minutes, mixing speed is 75 revs/min, obtains mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 42 DEG C under the condition of 0.03MPa in vacuum, stirs 35 minutes, then adds the deionized water of surplus, continues stirring 60 minutes, obtains mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo, and wherein processing condition is homogenization pressure 30MPa, homogenizing time 6 minutes.
Embodiment 3
A kind of fibroin shampoo, comprises in components by weight percent: guar gum 4 parts, octadecyl trimethyl ammonium chloride 0.4 part, hydroxyethyl-cellulose 0.5 part, 3 parts, lecithin, glycerol 4 parts, propylene glycol 3 parts, fibroin 5 parts, vitamin e acetate 0.07 part, 0.2 part, essence, diethyl succinate 3 parts, menthol 0.04 part, deionized water 76 parts.
The preparation method of described fibroin shampoo, comprises the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 36 parts of deionized waters, be uniformly mixed, mixing speed is 135 revs/min, is then warming up to 55 DEG C, stirs 130 minutes, mixing speed is 76 revs/min, obtains mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 48 DEG C under the condition of 0.04MPa in vacuum, stirs 40 minutes, then adds the deionized water of surplus, continues stirring 60 minutes, obtains mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo, and wherein processing condition is homogenization pressure 38MPa, homogenizing time 8 minutes.
Embodiment 4
A kind of fibroin shampoo, comprises in components by weight percent: guar gum 5 parts, octadecyl trimethyl ammonium chloride 0.5 part, hydroxyethyl-cellulose 0.6 part, 4 parts, lecithin, glycerol 5 parts, propylene glycol 3 parts, fibroin 6 parts, vitamin e acetate 0.08 part, 0.3 part, essence, diethyl succinate 4 parts, menthol 0.05 part, deionized water 78 parts.
The preparation method of described fibroin shampoo, comprises the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 40 parts of deionized waters, be uniformly mixed, mixing speed is 140 revs/min, is then warming up to 58 DEG C, stirs 140 minutes, mixing speed is 80 revs/min, obtains mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 50 DEG C under the condition of 0.07MPa in vacuum, stirs 48 minutes, then adds the deionized water of surplus, continues stirring 90 minutes, obtains mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo, and wherein processing condition is homogenization pressure 36MPa, homogenizing time 9 minutes.
Embodiment 5
A kind of fibroin shampoo, comprises in components by weight percent: guar gum 5 parts, octadecyl trimethyl ammonium chloride 0.6 part, hydroxyethyl-cellulose 0.6 part, 4 parts, lecithin, glycerol 5 parts, propylene glycol 4 parts, fibroin 6 parts, vitamin e acetate 0.1 part, 0.4 part, essence, diethyl succinate 4 parts, menthol 0.06 part, deionized water 80 parts.
The preparation method of described fibroin shampoo, comprises the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 40 parts of deionized waters, be uniformly mixed, mixing speed is 150 revs/min, is then warming up to 60 DEG C, stirs 150 minutes, mixing speed is 80 revs/min, obtains mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 50 DEG C under the condition of 0.08MPa in vacuum, stirs 50 minutes, then adds the deionized water of surplus, continues stirring 100 minutes, obtains mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo, and wherein processing condition is homogenization pressure 40MPa, homogenizing time 10 minutes.
Carry out physical and chemical index test to the fibroin shampoo that above embodiment prepares, result is as following table:
As can be seen from the above results, fibroin shampoo provided by the invention reaches good physical and chemical index, and wherein pH value is that between 6.5-7.0, working substance reaches more than 26.7%, and foam reaches more than 88mm.The present invention has carried out that in process of the test the vacuum in preparation method step 3 is added reaction and has changed common heating reaction into, result shows that the foaming properties of final products and heat-resisting and resistance to cold are all deteriorated, and therefore shows that the stability of vacuum response step to product of preparation process serves important function.Fibroin shampoo provided by the invention has good heat-resisting and resistance to cold, stable performance, without layering, show through 500 experimenter's result on trial simultaneously, shampoo nonirritant provided by the invention, without anaphylaxis, use rear hair pitch-black, submissive, glossy, naturally straight, reach well hair washing and the effect of taking care of hair.
Claims (7)
1. a fibroin shampoo, is characterized in that, comprises in components by weight percent: guar gum 1-5 part, octadecyl trimethyl ammonium chloride 0.2-0.6 part, hydroxyethyl-cellulose 0.2-0.6 part, lecithin 1-4 part, glycerol 1-5 part, propylene glycol 2-4 part, fibroin 2-6 part, vitamin e acetate 0.05-0.1 part, essence 0.1-0.4 part, diethyl succinate 1-4 part, menthol 0.02-0.06 part, deionized water 70-80 part.
2. fibroin shampoo according to claim 1, is characterized in that, comprise in components by weight percent: guar gum 3-5 part, octadecyl trimethyl ammonium chloride 0.3-0.5 part, hydroxyethyl-cellulose 0.4-0.6 part, lecithin 2-4 part, glycerol 3-5 part, propylene glycol 2-3 part, fibroin 4-6 part, vitamin e acetate 0.06-0.08 part, essence 0.2-0.3 part, diethyl succinate 2-4 part, menthol 0.03-0.05 part, deionized water 75-78 part.
3. fibroin shampoo according to claim 1, is characterized in that, comprise in components by weight percent: guar gum 4 parts, octadecyl trimethyl ammonium chloride 0.4 part, hydroxyethyl-cellulose 0.5 part, 3 parts, lecithin, glycerol 4 parts, propylene glycol 3 parts, fibroin 5 parts, vitamin e acetate 0.07 part, 0.2 part, essence, diethyl succinate 3 parts, menthol 0.04 part, deionized water 76 parts.
4. the preparation method of fibroin shampoo according to claim 1, is characterized in that, comprise the following steps:
Step one, takes each component according to weight portion;
Step 2, guar gum, hydroxyethyl-cellulose, lecithin, propylene glycol, fibroin, vitamin e acetate, essence, diethyl succinate and menthol are joined in reactor, adding weight portion is 30-40 part deionized water, be uniformly mixed, then 50-60 DEG C is warming up to, stir 100-150 minute, obtain mixture one;
Step 3, joins octadecyl trimethyl ammonium chloride and glycerol in mixture one, is to be heated to 40-50 DEG C under the condition of 0.02-0.08MPa in vacuum, stir 30-50 minute, then add the deionized water of surplus, continue to stir 50-100 minute, obtain mixture two;
Step 4, by mixture two after high pressure homogenizer homogenizing, obtains fibroin shampoo.
5. the preparation method of fibroin shampoo according to claim 4, is characterized in that, the mixing speed be uniformly mixed in step 2 is 120-150 rev/min.
6. the preparation method of fibroin shampoo according to claim 4, is characterized in that, the mixing speed stirred described in step 2 100-150 minute is 70-80 rev/min.
7. the preparation method of fibroin shampoo according to claim 4, is characterized in that, in step 4, processing condition is homogenization pressure 30-40MPa, homogenizing time 5-10 minute.
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| CN201410835375.XA CN104622711A (en) | 2014-12-29 | 2014-12-29 | Fibroin shampoo and preparation method thereof |
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| CN201410835375.XA CN104622711A (en) | 2014-12-29 | 2014-12-29 | Fibroin shampoo and preparation method thereof |
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Cited By (4)
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| CN106619172A (en) * | 2016-11-25 | 2017-05-10 | 江苏爱西施科技服务咨询股份有限公司 | Preparation method of hair care article containing fine silk protein powder |
| CN107280994A (en) * | 2017-05-04 | 2017-10-24 | 上海章华保健化妆品有限公司 | One kind hydrolysis fibroin hair conditioner and preparation method thereof |
| CN110075018A (en) * | 2019-04-24 | 2019-08-02 | 杭州犇鑫科技有限公司 | One kind includes tea polyphenols and the micro-nano lotion of fibroin Haircare composition and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106539733A (en) * | 2016-11-25 | 2017-03-29 | 江苏爱西施科技服务咨询股份有限公司 | A kind of anti-dandruff smooth silk gum hair conditioner and preparation method thereof |
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| CN107280994A (en) * | 2017-05-04 | 2017-10-24 | 上海章华保健化妆品有限公司 | One kind hydrolysis fibroin hair conditioner and preparation method thereof |
| CN110075018A (en) * | 2019-04-24 | 2019-08-02 | 杭州犇鑫科技有限公司 | One kind includes tea polyphenols and the micro-nano lotion of fibroin Haircare composition and preparation method thereof |
| CN110075018B (en) * | 2019-04-24 | 2022-09-09 | 杭州犇鑫科技有限公司 | Hair care composition micro-nano emulsion containing tea polyphenol and fibroin and preparation method thereof |
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