CN111920696B - Artificial melanin hair-perming and dyeing agent and preparation and hair-perming and dyeing integrated use method thereof - Google Patents

Artificial melanin hair-perming and dyeing agent and preparation and hair-perming and dyeing integrated use method thereof Download PDF

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CN111920696B
CN111920696B CN202010958221.5A CN202010958221A CN111920696B CN 111920696 B CN111920696 B CN 111920696B CN 202010958221 A CN202010958221 A CN 202010958221A CN 111920696 B CN111920696 B CN 111920696B
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CN111920696A (en
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李乙文
胡俊飞
郭万才
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Sichuan meilaning polymer material Co.,Ltd.
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Sichuan University
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    • A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
    • A61K8/492—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid having condensed rings, e.g. indol
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/22—Peroxides; Oxygen; Ozone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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    • A—HUMAN NECESSITIES
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    • A—HUMAN NECESSITIES
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    • A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
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    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/10—Preparations for permanently dyeing the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42—Colour properties
    • A61K2800/43—Pigments; Dyes
    • A61K2800/432—Direct dyes
    • A61K2800/4324—Direct dyes in preparations for permanently dyeing the hair

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Abstract

The invention discloses an integrated use method of artificial melanin hair perming and dyeing, which comprises an agent A and an agent B, wherein the agent A mainly comprises the following components: 5, 6-dihydroxyindole, stearic acid, cetyl alcohol, sodium dodecyl benzene sulfonate, propylene glycol, cysteine, hydrolyzed keratin, ammonia water and water; the agent B mainly comprises the following components: hydrogen peroxide, stearic acid, cetyl alcohol, propylene glycol, sodium dodecyl benzene sulfonate and water; cleaning hair, applying agent A on hair, fixing with a winding bar, shaping, and infrared heating for 20 min; then smearing the agent B on hair, permanently shaping hair, and staying for 15 min. The preparation method of the artificial melanin hair dye comprises the following steps: (1) preparation of an agent A; (2) preparation of agent B; the invention can simultaneously dye hair and perm hair, effectively reduces the damage caused by multiple treatments of hair, and saves time and labor.

Description

Artificial melanin hair-perming and dyeing agent and preparation and hair-perming and dyeing integrated use method thereof
Technical Field
The invention relates to the technical field of hair dyeing and permanent wave agents, in particular to an artificial melanin permanent wave hair dye and a preparation and permanent wave integrated use method thereof.
Background
Hair coloring and perming have become an important cosmetic art for beautifying hair. With the improvement of living standard of people, the beautification of hair becomes fashion pursued by people no matter men, women, old and young, and the pursuit of beauty is higher and higher. Consumers are generally required to go to barbershops to change hairstyles, but meanwhile people pay more attention to the safety of hair dyeing and permanent waving on one hand, and the hair dyeing and permanent waving are required to be more efficient and quicker on the other hand due to the quick life rhythm.
The primary target of action of hair coloring products is the "inanimate" visible portion of the hair, namely the hair shaft and hair fibers. Hair is a complex biological unit, the protein content in hair is 65% -95% according to the type, and the cuticle scale layer on the hair surface has protection effect on hair. The existing hair dye generally contains p-phenylenediamine which is a carcinogenic substance, which causes obstruction to the development of the hair dye.
The hair dye containing 5, 6-dihydroxyindole melanin gradually exposes the horns, and researches show that tyrosine in a human body is catalyzed and oxidized to form an active intermediate 5, 6-dihydroxyindole, and further oxidized to form melanin. The bionic hair dyeing by using the active intermediate in vitro is not only green but also safe as a permanent hair dye, and the hair dye has the same hair dyeing mechanism with the p-phenylenediamine and the derivatives thereof, and acts on the hair keratin fiber.
The Chinese invention with the invention name of 'a hair dye based on phenylboronic acid and a preparation and use method thereof' of the publication No. CN110200823A discloses a hair dye based on phenylboronic acid and a preparation and use method thereof, wherein the hair dye comprises an agent A and an agent B, and the agent A comprises the following components: 5, 6-dihydroxyindole, phenylboronic acid, oleyl alcohol, oleic acid, propylene glycol, isopropanol, sodium dodecyl sulfate, ammonia water and water; the agent B consists of the following components: hydrogen peroxide, oleyl alcohol, oleic acid, propylene glycol, isopropanol, sodium dodecyl sulfate, phosphoric acid and water.
The Chinese invention with the invention name of 'a hair dye based on macromolecular amine and a preparation and use method thereof' in the publication No. CN110151599A discloses a hair dye based on macromolecular amine and a preparation and use method thereof, which comprises an agent A and an agent B, wherein the agent A comprises the following components: 5, 6-dihydroxyindole, cetostearyl alcohol, oleic acid, propylene glycol, isopropanol, sodium dodecyl sulfate, high molecular amine, ammonia water and water; the agent B consists of the following components: hydrogen peroxide, oleyl alcohol, oleic acid, propylene glycol, isopropanol and sodium dodecyl sulfate.
The Chinese invention with the invention name of 'a dendritic macromolecule catalytic hair dye and a preparation and use method thereof' of the publication No. CN110123670A discloses a dendritic macromolecule catalytic hair dye and a preparation and use method thereof, wherein the preparation and use method comprises an agent A and an agent B, and the agent A comprises the following components: 5, 6-dihydroxyindole, cetostearyl alcohol, oleic acid, propylene glycol, isopropanol, sodium dodecyl sulfate, polyethylene diamine dendrimer, ammonia water and water; the agent B consists of the following components: hydrogen peroxide, cetostearyl alcohol, oleic acid, propylene glycol, isopropanol, sodium dodecyl sulfate, a proper amount of phosphoric acid and the balance of water.
Although the three hair dyes have good overall hair dyeing effect, the conventional hair perming operation is carried out after hair dyeing is finished. For consumers who have the needs of hair perming and dyeing, the operation of hair perming after hair dyeing is finished undoubtedly consumes a great deal of time, wastes time and labor and can not avoid the damage caused by multiple times of hair treatment.
Disclosure of Invention
Aiming at the defects of the prior art, the invention solves the technical problems that hair dyeing and perming are carried out simultaneously, reduces the damage caused by multiple treatments of the hair and saves time and labor.
In order to solve the technical problems, the technical scheme adopted by the invention is that the artificial melanin hair-scalding dye comprises an agent A and an agent B, wherein:
the agent A mainly comprises the following components in percentage by mass:
0.5 to 3 percent of 5, 6-dihydroxyindole,
5 to 10 percent of stearic acid,
5 to 10 percent of cetyl alcohol,
0.2 to 1.5 percent of sodium dodecyl benzene sulfonate,
4 to 9 percent of propylene glycol,
1 to 3 percent of cysteine,
1 percent of hydrolyzed keratin,
a proper amount of ammonia water is added,
the balance of water is water,
the mass percentage of each component is 100 percent;
the agent B mainly comprises the following components in percentage by mass:
8 to 20 percent of hydrogen peroxide,
5 to 10 percent of stearic acid,
5 to 10 percent of cetyl alcohol,
4 to 9 percent of propylene glycol,
0.2 to 1.5 percent of sodium dodecyl benzene sulfonate,
the balance of water is water,
the mass percentage of each component is 100 percent.
The invention also provides a use method of the artificial melanin hair-scalding dye.
Therefore, the technical scheme adopted by the invention is an integrated use method for the artificial melanin hair waving and dyeing, in the use process of the artificial melanin hair waving and dyeing agent, tyrosine in a human body is catalyzed and oxidized to form an active intermediate 5, 6-dihydroxyindole, then the oxidized melanin is converted into heat by near infrared light, the hair style is changed by rapidly heating to destroy hydrogen bonds and disulfide bonds between hair fibers, and the scalp irritation is reduced, and the specific process is as follows: cleaning hair, applying agent A on hair, fixing with a winding bar, shaping, and infrared heating for 20 min; then smearing the agent B on hair, permanently shaping hair, and staying for 15 min.
The invention also aims to solve the technical problem of providing a preparation method of the artificial melanin hair-scalding dye.
Therefore, the technical scheme provided by the invention is a preparation method of the artificial melanin hair-scalding dye, which comprises the following specific steps:
(1) the preparation of the agent A comprises the following steps:
a. mixing stearic acid and cetyl alcohol, heating to 80 ℃ to obtain an oil phase,
b. mixing sodium dodecyl benzene sulfonate, propylene glycol, cysteine, hydrolyzed keratin, D-panthenol and water, heating to 80 ℃ to obtain a water phase,
c. adding the water phase into the oil phase, stirring for 5min, cooling to room temperature,
d. adding ammonia water to regulate pH value to 9-10, adding 5, 6-dihydroxyindole, and mixing to obtain the preparation A.
(2) The preparation of the agent B comprises the following steps:
a. mixing stearic acid and cetyl alcohol, heating to 80 ℃ to obtain an oil phase,
b. mixing sodium dodecyl benzene sulfonate, propylene glycol and water, heating to 80 ℃ to obtain a water phase,
c. adding the water phase into the oil phase, stirring for 5min, cooling to room temperature,
d. adding a proper amount of hydrogen peroxide and mixing to obtain the agent B.
Compared with the prior art, the product of the invention can simultaneously dye hair and perm hair, effectively reduces the damage caused by multiple treatments of hair, and saves time and labor.
Detailed Description
The following examples are given to further illustrate the embodiments of the present invention, but are not intended to limit the invention.
Example 1
An artificial melanin hair-scalding dye comprises an agent A and an agent B, wherein:
the agent A mainly comprises the following components in percentage by mass:
0.5 percent of 5, 6-dihydroxyindole,
10 percent of stearic acid,
5 percent of cetyl alcohol,
1.5 percent of sodium dodecyl benzene sulfonate,
4 percent of propylene glycol,
3 percent of cysteine,
1 percent of hydrolyzed keratin,
a proper amount of ammonia water is added,
the balance of water is water,
the mass percentage of each component is 100 percent;
the agent B mainly comprises the following components in percentage by mass:
8 percent of hydrogen peroxide,
10 percent of stearic acid,
5 percent of cetyl alcohol,
9 percent of propylene glycol,
0.2 percent of sodium dodecyl benzene sulfonate,
the balance of water is water,
the mass percentage of each component is 100 percent.
Example 2
An artificial melanin hair-scalding dye comprises an agent A and an agent B, wherein:
the agent A mainly comprises the following components in percentage by mass:
2 percent of 5, 6-dihydroxyindole,
7 percent of stearic acid,
7 percent of cetyl alcohol,
1 percent of sodium dodecyl benzene sulfonate,
5 percent of propylene glycol,
2 percent of cysteine,
1 percent of hydrolyzed keratin,
a proper amount of ammonia water is added,
the balance of water is water,
the mass percentage of each component is 100 percent;
the agent B mainly comprises the following components in percentage by mass:
10 percent of hydrogen peroxide,
7 percent of stearic acid,
7 percent of cetyl alcohol,
6 percent of propylene glycol,
1 percent of sodium dodecyl benzene sulfonate,
the balance of water is water,
the mass percentage of each component is 100 percent.
Example 3
An artificial melanin hair-scalding dye comprises an agent A and an agent B, wherein:
the agent A mainly comprises the following components in percentage by mass:
3 percent of 5, 6-dihydroxyindole,
5 percent of stearic acid,
10 percent of cetyl alcohol,
0.2 percent of sodium dodecyl benzene sulfonate,
9 percent of propylene glycol,
1 percent of cysteine,
1 percent of hydrolyzed keratin,
a proper amount of ammonia water is added,
the balance of water is water,
the mass percentage of each component is 100 percent;
the agent B mainly comprises the following components in percentage by mass:
20 percent of hydrogen peroxide,
5 percent of stearic acid,
10 percent of cetyl alcohol,
4 percent of propylene glycol,
1.5 percent of sodium dodecyl benzene sulfonate,
the balance of water is water,
the mass percentage of each component is 100 percent.
The integrated use method of the artificial melanin hair perming and dyeing of the embodiments 1 to 3 comprises the following specific steps:
cleaning hair, applying agent A on hair, fixing with a winding bar, shaping, and infrared heating for 20 min. Then smearing the agent B on hair, permanently shaping hair, and staying for 15 min.
The preparation method of the artificial melanin hair-waving dye of the above embodiments 1 to 3 includes the following specific steps:
(1) the preparation of the agent A comprises the following steps:
a. mixing stearic acid and cetyl alcohol, heating to 80 ℃ to obtain an oil phase,
b. mixing sodium dodecyl benzene sulfonate, propylene glycol, cysteine, hydrolyzed keratin, D-panthenol and water, heating to 80 ℃ to obtain a water phase,
c. adding the water phase into the oil phase, stirring for 5min, cooling to room temperature,
d. adding ammonia water to regulate pH value to 9-10, adding 5, 6-dihydroxyindole, and mixing to obtain the preparation A.
(2) The preparation of the agent B comprises the following steps:
a. mixing stearic acid and cetyl alcohol, heating to 80 ℃ to obtain an oil phase,
b. mixing sodium dodecyl benzene sulfonate, propylene glycol and water, heating to 80 ℃ to obtain a water phase,
c. adding the water phase into the oil phase, stirring for 5min, cooling to room temperature,
d. adding a proper amount of hydrogen peroxide and mixing to obtain the agent B.
Comparative example 1
A hair dye comprises an agent A and an agent B, wherein:
the agent A mainly comprises the following components in percentage by mass:
6 percent of stearic acid,
the content of the cetyl alcohol is 6 percent,
0.6 percent of sodium dodecyl benzene sulfonate,
5 percent of propylene glycol,
4 percent of cysteine,
1 percent of hydrolyzed keratin,
a proper amount of ammonia water is added,
the balance of water is water,
the mass percentage of each component is 100 percent;
the agent B mainly comprises the following components in percentage by mass:
10 percent of hydrogen peroxide,
6 percent of stearic acid,
the content of the cetyl alcohol is 6 percent,
5 percent of propylene glycol,
0.6 percent of sodium dodecyl benzene sulfonate,
the balance of water is water,
the mass percentage of each component is 100 percent.
To better illustrate the beneficial effects of the present invention, the following comparison of the use effects of the inventive product with the comparative product was performed.
The original length of hair is 30cm, the vertical distance from the top of the head to the tip of the hair is measured by whether infrared rays are added during perming to evaluate the perming effect, the hair blackening degree L value is evaluated, the hair blackening degree L value is tested for 3 times by using a color difference meter, the average value is obtained, and the average value is referred to a chromaticity board. Results statistical comparison the results are given in table 1 below:
table 1:
Figure BDA0002679331010000091
as can be seen from the above Table 1, the hair dyeing effect of the product of the present invention is remarkable after the infrared ray is added, and when the melanin exists, the infrared ray is converted into heat through the melanin to make the hair waving effect remarkable. And the hair-waving effect is not obvious when only infrared rays are added and no melanin exists.
Compared with the prior art, the integrated use method for hair perming and dyeing is particularly suitable for people who need hair dyeing and perming, and has the advantages of simple perming process and short time consumption.
The embodiments of the present invention have been described in detail with reference to the examples, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention.

Claims (2)

1. The ironing and dyeing integrated use method of the artificial melanin ironing and dyeing agent is characterized in that the artificial melanin ironing and dyeing agent comprises an agent A and an agent B, wherein the agent A mainly comprises the following components in percentage by mass:
0.5 to 3 percent of 5, 6-dihydroxyindole,
5 to 10 percent of stearic acid,
5 to 10 percent of cetyl alcohol,
0.2 to 1.5 percent of sodium dodecyl benzene sulfonate,
4 to 9 percent of propylene glycol,
1 to 3 percent of cysteine,
1 percent of hydrolyzed keratin,
a proper amount of ammonia water is added,
the balance of water is water,
the mass percentage of each component is 100 percent;
the agent B mainly comprises the following components in percentage by mass:
8 to 20 percent of hydrogen peroxide,
5 to 10 percent of stearic acid,
5 to 10 percent of cetyl alcohol,
4 to 9 percent of propylene glycol,
0.2 to 1.5 percent of sodium dodecyl benzene sulfonate,
the balance of water is water,
the mass percentage of each component is 100 percent;
in the using process, tyrosine in a human body is catalyzed and oxidized to form an active intermediate 5, 6-dihydroxyindole, then melanin formed by oxidation is converted into heat by near infrared light, the hair style is changed by rapidly heating to destroy hydrogen bonds and disulfide bonds between hair fibers, and the scalp irritation is reduced, and the specific process is as follows: cleaning hair, applying agent A on hair, fixing with a winding bar, shaping, heating with infrared ray for 20min, applying agent B on hair, permanently shaping, and standing for 15 min.
2. A method for preparing the artificial melanin hair-waving dye according to claim 1, which comprises the following specific steps:
(1) the preparation of the agent A comprises the following steps:
a. mixing stearic acid and cetyl alcohol, and heating to 80 ℃ to obtain an oil phase;
b. mixing sodium dodecyl benzene sulfonate, propylene glycol, cysteine, hydrolyzed keratin, D-panthenol and water, and heating to 80 ℃ to obtain a water phase;
c. adding the water phase into the oil phase, stirring for 5min, and then cooling to room temperature;
d. adding a proper amount of ammonia water to adjust the pH value to 9-10, and adding 5, 6-dihydroxyindole to mix to obtain an agent A;
(2) the preparation of the agent B comprises the following steps:
a. mixing stearic acid and cetyl alcohol, and heating to 80 ℃ to obtain an oil phase;
b. mixing sodium dodecyl benzene sulfonate, propylene glycol and water, and heating to 80 ℃ to obtain a water phase;
c. adding the water phase into the oil phase, stirring for 5min, and then cooling to room temperature;
d. adding a proper amount of hydrogen peroxide and mixing to obtain the agent B.
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CN114028275B (en) * 2021-12-16 2022-11-29 四川大学 Hair dye with soap catalyzing melanin polymerization, preparation method and use method thereof
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