CN110075018A - One kind includes tea polyphenols and the micro-nano lotion of fibroin Haircare composition and preparation method thereof - Google Patents
One kind includes tea polyphenols and the micro-nano lotion of fibroin Haircare composition and preparation method thereof Download PDFInfo
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- CN110075018A CN110075018A CN201910332236.8A CN201910332236A CN110075018A CN 110075018 A CN110075018 A CN 110075018A CN 201910332236 A CN201910332236 A CN 201910332236A CN 110075018 A CN110075018 A CN 110075018A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/068—Microemulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
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Abstract
It include tea polyphenols and the micro-nano lotion of fibroin Haircare composition and preparation method thereof the invention discloses one kind, the tea polyphenols for being 0.2~8 part including weight ratio, 0.4~24 part of fibroin, 10~30 parts of grease, 2~10 parts of emulsifier, 5~10 parts of polyalcohol, 0.2~1 part of preservative and 17~82.2 parts of water, the mass ratio of the tea polyphenols and fibroin is 1:2~1:3, it further include that suitable PH regulator makes final composition PH scope control 4~6, by the way that tea polyphenols and fibroin are compounded according to a certain percentage, it is prepared into micro-nano lotion, form micro-nano lotion delivery system, using the particle of small particle come carrying active ingredients, on the one hand the stability of tea polyphenols can be promoted, it is not easily decomposed and changes colour；In addition during hair washing, little particle can be rapidly and uniformly bonded with hair and scalp, so as to more preferably play oil-control, reparation and submissive effect.
Description
[technical field]
The present invention relates to the technical fields that hair washes shield, and especially a kind of includes tea polyphenols and fibroin Haircare composition
The technical field of micro-nano lotion and preparation method thereof.
[background technique]
Tea polyphenols are most important active materials in tealeaves, research shows that tea polyphenols have anti-oxidant, anticancer, it is anti-radiation and
Prevent more health efficacies such as cardiovascular disease.In hair product, it is greasy that tea polyphenols can remove scalp, restrains pore, have and disappear
Poison sterilizes, effect of the ultraviolet radiation in resisting age of skin and reduction daylight to the damage of skin, because it is with very strong
Oxygen delivery capacity can stop ultraviolet light and remove the free radical of ultraviolet induction, kill dark sore corynebacteria etc..But tea polyphenols
Itself is unstable, is easy inactivation and discoloration in the product, thus limits its application in hair products.Fibroin application
There is long history in cosmetics, once had fibroin that can remove skin blackspot in Compendium of Material Medica, and treated the record of suppurative dermatitis.
It was found that fibroin can make hair from damage, permanent hair styling can be effectively repaired, chemistry scalds and hair dyeing damage caused by hair
Wound makes hair that healthy nature be presented.
Patent CN103720637B provides a kind of natural plant extract and closes hair conditioner and preparation method thereof.The program contains
Some fibroins and tea polyphenols, but only simple mixing, cannot promote the stability of tea polyphenols, oil-control, hair care well
Effect it is limited.
Patent CN103110107A provide it is a kind of using protein gel package tea polyphenols method, however its do not carry out it is micro-
Nanosizing, partial size is larger, and the soybean protein and fibroin applied differ greatly.
[summary of the invention]
The object of the invention is to solve the problems of the prior art, propose a kind of comprising tea polyphenols and fibroin hair care
Micro-nano lotion of composition and preparation method thereof, tea polyphenols and fibroin are compounded according to a certain percentage, are prepared into micro-nano
Rice milk liquid, on the one hand forming micro-nano lotion delivery system using the particle of small particle come carrying active ingredients, it is more can to promote tea
The stability of phenol, in addition during hair washing, little particle can be rapidly and uniformly bonded with hair and scalp, to play hair care function
Effect.
To achieve the above object, the present invention is achieved through the following technical solutions:
One kind includes tea polyphenols and the micro-nano lotion of fibroin Haircare composition, is 0.2~8 part including weight ratio
Tea polyphenols, 0.4~24 part of fibroin, 10~30 parts of grease, 2~10 parts of emulsifier, 5~10 parts of polyalcohol, 0.2
The mass ratio of~1 part of preservative and 17~82.2 parts of water, the tea polyphenols and fibroin is 1:2~1:3, further includes
Suitable PH regulator makes final composition PH scope control 4~6.
Preferably, being 0.5~5 part of tea polyphenols, 1~15 part of fibroin, 12~20 parts including weight ratio
Grease, 5~10 parts of emulsifier, 5~10 parts of polyalcohol, 0.2~0.8 part of preservative and 39.2~76.3 parts of water, institute
The mass ratio for stating tea polyphenols and fibroin is 1:2~1:3, further includes that suitable PH regulator makes final composition PH range
Control is 4~6.
Preferably, content >=50wt% of content >=80wt% of the catechin of the tea polyphenols, EGCG.
Preferably, the fibroin is powdered and fibroin albumen content >=70wt%.
Preferably, the emulsifier be glycerin fatty acids, polyglycereol esters, sucrose ester, lecithin, fatty acid and
Fatty alcohol is one such or multiple combinations, the polyalcohol are glycerol, 1,3-PD, butanediol, pentanediol, hexylene glycol
With pungent glycol is one such or multiple combinations, the preservative be dehydroactic acid sodium, sodium benzoate, potassium sorbate, to hydroxyl
Benzoylformaldoxime and Phenoxyethanol is one such or multiple combinations, the grease is glycerol caprylate, glycerol decanoate, camellia
Seed oil, saualane, shea butter, linseed oil, evening primrose oil and olive oil is one such or multiple combinations, the pH tune
Agent is saved as citric acid and sodium citrate is one such or two kinds are combined.
Preferably, ultimately joining the ratio in cosmetic product such as shampoo or hair conditioner is 1%~10%.
A kind of preparation method comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, includes the following steps:
A) it is that 0.4~24 part of fibroin is dissolved in 17~82.2 parts of water by weight ratio, 5~10 parts more is added
Then 0.2~8 part of tea polyphenols are added while stirring, 60~65 DEG C are heated to, as A phase for first alcohol；
B) 2~10 parts of emulsifier and 10~30 parts of grease are uniformly mixed, are heated to 60~65 DEG C, be dispersed with stirring
It is even, as B phase, B is added to A phase high speed and is stirred 5~10 minutes, revolving speed 5000-6000rpm obtains pretreatment fluid；
C) pretreatment fluid is handled by microjet high pressure homogenizer, pressure is set as 150~250MPa, recycles 2~5 times；
D) 50 DEG C are cooled to after discharging hereinafter, 0.2~1 part of preservative is added, recycle pH adjusting agent pH is adjusted to 4~
6, it stirs evenly, is cooled to≤35 DEG C up to micro-nano lotion.
Preferably, the average grain diameter of the micro-nano lotion is between 50~200nm.
Beneficial effects of the present invention: the present invention compounds tea polyphenols and fibroin according to a certain percentage, is prepared into micro-
Nanoemulsions form micro-nano lotion delivery system, using the particle of small particle come carrying active ingredients, on the one hand can be promoted
The stability of tea polyphenols, in addition during hair washing, little particle can be rapidly and uniformly bonded with hair and scalp, to play shield
Send out effect.
[specific embodiment]
Embodiment one:
Prepare the micro-nano lotion of 1Kg
Preparation formula:
Tea polyphenols 10g, fibroin 30g, Trivent OCG or Triglyceride DDD 150g, sucrose stearate
50g, glycerol 100g, dehydroactic acid sodium 5g, citric acid 8g and water 647g.
Preparation method:
A) 30g fibroin is dissolved in 647g water, 100g glycerol is added, 10g tea polyphenols are then added while stirring, add
Heat is to 60~65 DEG C, as A phase；
B) 50g sucrose stearate and 150g Trivent OCG or Triglyceride DDD are uniformly mixed, are heated to
It 60~65 DEG C, is dispersed with stirring uniformly, as B phase, B is added to A phase high speed and is stirred 5 minutes, revolving speed 6000rpm is obtained
To pretreatment fluid；
C) pretreatment fluid is handled by microjet high pressure homogenizer, pressure is set as 150MPa, recycles 3 times；
D) 50 DEG C are cooled to after discharging hereinafter, addition 5g dehydroactic acid sodium and 8g citric acid, stir evenly, be cooled to≤35
DEG C up to micro-nano lotion.
The micro-nano lotion tests to obtain average grain diameter to be 153nm through Malvern nano particle size instrument.
Embodiment two:
Prepare the micro-nano lotion of 1Kg
Preparation formula:
Tea polyphenols 50g, fibroin 100g, camellia seed oil 50g, linseed oil 50g, Natrulon H-10 laurate 30g,
- 2 diisopstearate 10g of polyglycereol, 1,3-PD 80g, potassium sorbate 5g, citric acid 4g and water 621g.
Preparation method:
A) 100g fibroin is dissolved in 621g water, 80g 1,3-PD is added, 50g tea is then added while stirring
Polyphenol is heated to 60~65 DEG C, as A phase；
B) by 30g Natrulon H-10 laurate, -2 diisopstearate of 10g polyglycereol, 50g camellia seed oil and 50g flax
Seed oil is uniformly mixed, and is heated to 60~65 DEG C, is dispersed with stirring uniformly, as B phase, B is added to A phase high speed and stirs 10 points
Clock, revolving speed 5000rpm, obtains pretreatment fluid；
C) pretreatment fluid is handled by microjet high pressure homogenizer, pressure is set as 250MPa, recycles 2 times；
D) 50 DEG C are cooled to after discharging hereinafter, addition 5g potassium sorbate and 4g citric acid, stir evenly, be cooled to≤35 DEG C
Obtain micro-nano lotion.
The micro-nano lotion tests to obtain average grain diameter to be 116nm through Malvern nano particle size instrument.
Embodiment three:
Prepare the micro-nano lotion of 1Kg
Preparation formula:
Tea polyphenols 30g, fibroin: 80g, saualane 100g, evening primrose oil 20g, Glyceryl stearate citrate
30g, lecithin 5g, glycerol 80g, hexylene glycol 3g, Phenoxyethanol 5g, citric acid 1g and water 646g.
Preparation method:
A) 80g fibroin is dissolved in 646g water, 80g glycerol and 3g hexylene glycol is added, 30g is then added while stirring
Tea polyphenols are heated to 60~65 DEG C, as A phase；
B) 30g Glyceryl stearate citrate, 5g lecithin, 100g saualane and 20g evening primrose oil are uniformly mixed,
60~65 DEG C are heated to, is dispersed with stirring uniformly, as B phase, B is added to A phase high speed and is stirred 8 minutes, revolving speed is
5500rpm obtains pretreatment fluid；
C) pretreatment fluid is handled by microjet high pressure homogenizer, pressure is set as 200MPa, recycles 3 times；
D) 50 DEG C are cooled to after discharging hereinafter, addition 5g Phenoxyethanol and 1g citric acid, stir evenly, be cooled to≤35 DEG C
Obtain micro-nano lotion.
The micro-nano lotion tests to obtain average grain diameter to be 86nm through Malvern nano particle size instrument.
Example IV:
Prepare the micro-nano lotion of 1Kg
Preparation formula:
Tea polyphenols 80g, fibroin 200g, Trivent OCG or Triglyceride DDD 50g, Natrulon H-10 Pork and beans
Cool acid esters 20g, glycerol hard acid ester 10g, glycerol 20g, pentanediol 20g, sodium benzoate 3g, citric acid 3g and water 596g.
Preparation method:
A) 200g fibroin is dissolved in 596g water, 20g glycerol and 20g pentanediol is added, is then added while stirring
80g tea polyphenols are heated to 60~65 DEG C, as A phase；
B) 20g Natrulon H-10 myristinate, 10g stearine, 50g Trivent OCG or capric acid is sweet
Oily three esters are uniformly mixed, and are heated to 60~65 DEG C, are dispersed with stirring uniformly, as B phase, B is added to A phase high speed stirring 10
Minute, revolving speed 6000rpm obtains pretreatment fluid；
C) pretreatment fluid is handled by microjet high pressure homogenizer, pressure is set as 200MPa, recycles 5 times；
D) 50 DEG C are cooled to after discharging hereinafter, addition 3g sodium benzoate and 3g citric acid, stir evenly, be cooled to≤35 DEG C
Obtain the micro-nano lotion of the composition.
The micro-nano lotion tests to obtain average grain diameter to be 93nm through Malvern nano particle size instrument.
Embodiment five:
Preparing the shampoo containing the micro-nano lotion in embodiment 3 is embodiment 5 and comparative example shampoo.Wherein implement
Example 5 and each ingredient of comparative example are same batch, and proportion is consistent, referring to table 1:
The formula of table 1 embodiment 5 and comparative example
(1) performance test 1: stability experiment
Stability test experiment condition is respectively as follows:
Shampoo is placed on 40 DEG C of next months, measures the content retention rate of catechin by 1 heat-resistant stability of experiment condition
And observation color change；
Experiment condition 2 under room temperature, stores 3 months, measures the content retention rate and observation color change of catechin.
Test result such as table 2
(2) performance test 2: in-service evaluation
It selects the female volunteers of 20 long hairs, oily hair to be tested, above-mentioned volunteer is divided into 2 test groups,
Every group 10, respectively using the shampoo in embodiment 5 and comparative example.Shampoo two weeks of embodiment are used continuously in volunteer
Afterwards, using subjectivity inquiry answer by the way of evaluated, evaluation be divided into, general and bad three grades, evaluation result such as table 3
The results show that the present invention is first by tea polyphenols compared with being directly added into tea polyphenols and fibroin in comparative formulation
Micro-nano lotion is prepared into according to a certain percentage with fibroin, using the particle of small particle come carrying active ingredients, a side
Face can be effectively improved the stability of tea polyphenols, be not easily decomposed and change colour；In addition during hair washing, little particle can be rapidly and uniformly
It is bonded with hair and scalp, so as to more preferably play oil-control, reparation and submissive effect.
Above-described embodiment is the description of the invention, is not limitation of the invention, after any pair of simple transformation of the present invention
Scheme all belong to the scope of protection of the present invention.
Claims (8)
1. one kind includes tea polyphenols and the micro-nano lotion of fibroin Haircare composition, it is characterised in that: be including weight ratio
0.2~8 part of tea polyphenols, 0.4~24 part of fibroin, 10~30 parts of grease, 2~10 parts of emulsifier, 5~10 parts
The mass ratio of polyalcohol, 0.2~1 part of preservative and 17~82.2 parts of water, the tea polyphenols and fibroin be 1:2~
1:3 further includes that suitable PH regulator makes final composition PH scope control 4~6.
2. one kind as described in claim 1 exists comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, feature
In: it is 0.5~5 part of tea polyphenols, 1~15 part of fibroin, 12~20 parts of grease, 5~10 parts including weight ratio
Emulsifier, 5~10 parts of polyalcohol, 0.2~0.8 part of preservative and 39.2~76.3 parts of water, the tea polyphenols and silk
The mass ratio of albumen is 1:2~1:3, further includes that suitable PH regulator makes final composition PH scope control 4~6.
3. one kind as described in claim 1 exists comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, feature
In: content >=50wt% of content >=80wt% of the catechin of the tea polyphenols, EGCG.
4. one kind as described in claim 1 exists comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, feature
In: the fibroin is powdered and fibroin albumen content >=70wt%.
5. one kind as described in claim 1 exists comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, feature
In: the emulsifier is glycerin fatty acids, polyglycereol esters, sucrose ester, lecithin, fatty acid and fatty alcohol therein one
Kind or multiple combinations, the polyalcohol are that glycerol, 1,3-PD, butanediol, pentanediol, hexylene glycol and pungent glycol are therein
One or more combination, the preservative are dehydroactic acid sodium, sodium benzoate, potassium sorbate, parahydroxyacet-ophenone and benzene oxygen
Ethyl alcohol is one such or multiple combinations, the grease are glycerol caprylate, glycerol decanoate, camellia seed oil, saualane, cream
The wooden fruit oil, linseed oil, evening primrose oil and olive oil is one such or multiple combinations, the pH adjusting agent be citric acid and
Sodium citrate is one such or two kinds are combined.
6. one kind as described in claim 1 exists comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, feature
In: ultimately joining the ratio in cosmetic product such as shampoo or hair conditioner is 1%~10%.
7. a kind of preparation method comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition, it is characterised in that including such as
Lower step:
A) it is that 0.4~24 part of fibroin is dissolved in 17~82.2 parts of water by weight ratio, 5~10 parts polynary is added
Then 0.2~8 part of tea polyphenols are added while stirring, 60~65 DEG C are heated to, as A phase for alcohol；
B) 2~10 parts of emulsifier and 10~30 parts of grease are uniformly mixed, are heated to 60~65 DEG C, be dispersed with stirring uniformly,
As B phase, B is added to A phase high speed and is stirred 5~10 minutes, revolving speed 5000-6000rpm obtains pretreatment fluid；
C) pretreatment fluid is handled by microjet high pressure homogenizer, pressure is set as 150~250MPa, recycles 2~5 times；
D) 50 DEG C are cooled to after discharging hereinafter, 0.2~1 part of preservative is added, pH is adjusted to 4~6 by recycling pH adjusting agent, is stirred
It mixes uniformly, is cooled to≤35 DEG C up to micro-nano lotion.
8. a kind of preparation side comprising tea polyphenols and the micro-nano lotion of fibroin Haircare composition as claimed in claim 7
Method, it is characterised in that: the average grain diameter of the micro-nano lotion is between 50~200nm.
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| CN110507555A (en) * | 2019-09-18 | 2019-11-29 | 贵州沐木皙颜生物科技有限公司 | A kind of anhydrous amino acid ginger tea shampoo and its processing method |
| CN113730303A (en) * | 2021-09-17 | 2021-12-03 | 欧诗漫生物股份有限公司 | Method for preparing multiple emulsions by using single type emulsifier and ice crystal cream for repairing after-sun |
| CN114272153A (en) * | 2021-12-29 | 2022-04-05 | 浙江宜格企业管理集团有限公司 | Nano emulsion with antioxidant effect and preparation method thereof |
| CN115778882A (en) * | 2023-02-09 | 2023-03-14 | 北京普世安生物科技有限公司 | Hair-growing essence and preparation method thereof |
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| CN114272153A (en) * | 2021-12-29 | 2022-04-05 | 浙江宜格企业管理集团有限公司 | Nano emulsion with antioxidant effect and preparation method thereof |
| CN114272153B (en) * | 2021-12-29 | 2023-09-01 | 浙江宜格企业管理集团有限公司 | Nanometer emulsion with antioxidation effect and preparation method thereof |
| CN115778882A (en) * | 2023-02-09 | 2023-03-14 | 北京普世安生物科技有限公司 | Hair-growing essence and preparation method thereof |
| CN115778882B (en) * | 2023-02-09 | 2023-04-28 | 北京普世安生物科技有限公司 | Hair-growing essence and preparation method thereof |
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