CN103735430A - Three-in-one liquid shampoo and preparation method thereof - Google Patents
Three-in-one liquid shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a three-in-one liquid shampoo and a preparation method thereof. The three-in-one liquid shampoo is prepared from the following raw materials: sodium laureth sulfate, ammonium lauryl sulfate, behentrimonium chloride, cocamidopropyl MEA, cetanol, guar hydroxypropyltrimonium chloride, polyquaternium-10, allantoin, trimethylol propane octanoate ester, methylparaben, propyl hydroxybenzoate, C12-20 alkyl polyglycoside, cocamidopropyl betaine, cocamidopropyl dimethylamine oxide, dimethiconol or dodecylbenzene sulfonic acid TEA salt, zinc pyrithione, hydrolyzed keratin, hydrolyzed silk protein, methyl-isothiazol-ketamine, polyquaternium-7, essence, crylic acid (ester)/C10-30 alkanol acrylic ester cross-linked polymer and deionized water. By adopting the three-in-one liquid shampoo, the stability of the product and the use effects of the raw materials can be improved, the three-in-one liquid shampoo achieves good cleaning and nursing effects, does not generate aggregation and stimulation problems after being used for a long period of time, and achieves the three-in-one effect of cleaning, nursing and conditioning.
Description
Technical field
The present invention relates to the shampoo in a kind of personal care articles, be specially a kind of three-in-one shampoo simultaneously with clean, nursing, protective effect and preparation method thereof.
Background technology
Shampoo as human lives's essential product, receives the concern of consumer always.Shampoo can be divided into clean shampoo and two-in-one shampoo, and the clean main demand of shampoo is clean hair dirt, need to coordinate hair conditioner to use together; And two-in-one shampoo is in clean hair dirt, can bring nursing to hair, improve smoothness, the lifting carding power of the rear hair of washing, improve dry compliance and the easy cardability sent out, prevent generation of static electricity.But the two-in-one shampoo of selling on market now mostly exists nursing efficacy inadequate, large to scalp irritation, the shortcoming that product long-time stability are inadequate.Analyze its main cause have following some: 1, shampoo main body composition is anion surfactant and water, and have the material of opsonic action mostly to be cation and lipophilicity substance to hair, both mix very difficult long-time stable, therefore the dosage of conditioner is restricted, there is the bad .2 of conditioning effect, after adding stabilizing agent, add a large amount of conditioners, a large amount of cationes and silicone oil conditioner are assembled and are caused nose heave and hair to become fragile easily broken on hair, 3, a large amount of cationes and silicone oil conditioner also produce and stimulate scalp, life-time service easily causes head pruritus and dandruff problem.
Summary of the invention
For overcoming the defect of prior art, be of the present inventionly to provide a kind of three-in-one shampoo, it can improve the stability of integral product and the result of use of raw material, reaches clean, nursing efficacy good, and life-time service can not cause to be assembled and stimulation problem; Can accomplish the real triple effect unification of cleaning, nurse, nurse one's health.
Another object of the present invention is to provide a kind of preparation method of three-in-one shampoo.
The technical solution adopted in the present invention is as follows for achieving the above object:
A kind of three-in-one shampoo, is characterized in that: it be by sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol, guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, dimethiconol or DBSA TEA salt, Zinc Pyrithione, hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, deionized water are prepared from.
Preferably, inventor finds through great many of experiments,, nursing real clean in order to accomplish, the unification of conditioning triple effect, and it is comprised of the following component in quality percentage composition:
In the present invention, above-mentioned raw materials all can obtain by purchase.As: hydrolyzed silkworm silk albumen is optional purchased from Huzhou Xintiansi Biotechnology Co. Ltd., and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is optional purchased from Lubrizol company
ultrez 20 Polymer.
A preparation method for three-in-one shampoo, its concrete steps are as follows:
1) the A component cold water soak being comprised of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is disperseed, standby;
2) add liquid to wash in pot the B component being formed by deionized water, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol; stirring is warmed up to 75-85 degree; after insulated and stirred is dissolved extremely completely, then add standby A component;
3) after the C component being comprised of guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10 is disperseed with cold water respectively, add liquid to wash in pot, insulated and stirred is even;
4) add liquid to wash in pot the D component being comprised of allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, processing cools;
5) will be by C12-20 alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, and the E component of dimethiconol or DBSA TEA salt composition adds liquid to wash in pot, stirs, processing cools;
6) after the F component cold water being comprised of Zinc Pyrithione is disperseed, add liquid to wash in pot, homogenizing 2-5 minute;
7) the G component being comprised of hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence is added in pot, stir;
8) sampling detect, qualified after, discharging, obtains three-in-one shampoo.
Preferably, in step 2) in, stir and be warmed up to 80 degree.
Preferably, in step 3), C component adds liquid to wash after pot, need to stir 2 hours.
Preferably, in step 4), D component adds liquid to wash after pot, and 50 degree cool.
Preferably, in step 5), E component adds liquid to wash after pot, cools below 45 degree.
Preferably, in step 6), homogenizing 3 minutes;
Preferably, in step 8), need to continue low rate mixing after 2 hours, resampling detects; Wherein, controlling mixing speed is 20～40r/min.
Beneficial effect of the present invention is:
1, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, the C in the present invention's formula
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide play cleaning action, wherein C in product
12 -20alkyl androstanediol can effectively reduce the stimulation of other surfactants, cocamidopropyl propyl amide amine oxide add the lather quickness that can improve product. the collocation of above component is used, and when product is used, bubbles rapidly, and foam is abundant, and clean power is strong and zest is little.
2, mountain Yu base trimethyl ammonium chloride, trimethylolpropane tris caprylate, coconut oleoyl amine MEA, spermol, dimethiconol or the DBSA TEA salt in the present invention's formula forms polynary conditioner, wherein spermol, coconut oleoyl amine MEA adds the whole polynary conditioner of effective promotion more formation liquid crystal structure in integral product, while being in use diluted, this liquid crystal structure is destroyed very soon, and discharge the conditioner of parcel, reach conditioning effect obvious, rapidly object.And trimethylolpropane tris caprylate is a kind of efficient salubrious humectants and emollients, can improve rapidly the moisture holding capacity of hair and skin, activate scalp cells vigor, improve the lubricated sense of bath of product, improve the dry soft feeling of sending out. make scalp more healthy.It is steady in a long-term that trimethylolpropane tris caprylate is difficult to reach in general system, this product can cross said components collocation, make it form liquid crystal structure and can discharge fast onset while reaching steady in a long-term dilution.
3, guar gum hydroxypropyl-trimethyl ammonium chloride, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, the Polyquaternium-10 in the present invention's formula forms a solid netted system in product, play the Stabilization of a suspension, form a polynary stabilising system together with polynary conditioner, make this product long-term stability and result of use rapid.
4, ZPT, allantoin, hydrolysis of keratin, the hydrolyzed silkworm silk albumen in the present invention's formula plays removing scurf and relieving itching effect in this product; adding of allantoin and albumen plays the anti-scorching effect of antiinflammatory to scalp; for scalp has been constructed a protection, repair barrier together with trimethylolpropane tris caprylate.
5, methyl hydroxybenzoate, propyl hydroxybenzoate, the methylchloroisothiazandnone in the present invention's formula plays protective system, and the composite use of several antiseptic has synergistic function.
6, adjusting product rheology is played in polyquaternary ammonium salt-7 in the present invention's formula in this product, increases product and uses the sliding sense of bath.
In sum, the compatibility of the present invention by above-mentioned raw materials and the present invention is directed to the production technology of above-mentioned recipe design, make whole interiors of products structure form diversification structure, can improve the stability of integral product and the result of use of raw material, reach clean, nursing efficacy good, life-time service can not cause assemble and stimulation problem; Can accomplish the real triple effect unification of cleaning, nurse, nurse one's health.
Below in conjunction with concrete embodiment, the present invention is described in further detail.
The specific embodiment
Embodiment 1-3:
Get respectively the following raw material in quality percentage composition: sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol, guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, dimethiconol or DBSA TEA salt, Zinc Pyrithione, hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, deionized water.
Concrete proportioning is in Table 1.
The proportioning table of table 1 embodiment 1-3
Above-mentioned raw materials is followed these steps to prepare three-in-one shampoo as follows:
1) the A component cold water soak being comprised of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is disperseed, standby;
2) add liquid to wash in pot the B component being formed by deionized water, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol; stirring is warmed up to 80 degree; after insulated and stirred is dissolved extremely completely, then add standby A component;
3) after the C component being comprised of guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10 is disperseed with cold water respectively, add liquid to wash in pot, insulated and stirred is even; Stir 2 hours.
4) add liquid to wash in pot the D component being comprised of allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, processing cools; 50 degree cool.
5) will be by C12-20 alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, and the E component of dimethiconol or DBSA TEA salt composition adds liquid to wash in pot, stirs, processing cools; Cool below 45 degree.
6) after the F component cold water being comprised of Zinc Pyrithione is disperseed, add liquid to wash in pot, homogenizing 3 minutes;
7) the G component being comprised of hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence is added in pot, stir;
8) continue low rate mixing after 2 hours, sampling detects, qualified after, discharging, obtains three-in-one shampoo.
Test implementation example 1: stability experiment.
Table 2 embodiment 1 stability test result table
Table 3 embodiment 2 stability test result tables
Table 4 embodiment 3 stability test result tables
Remarks explanation: 1 grade: unchanged, 2 grades: slightly change 3 grades: changes larger, 4 grades: seriously variation; 1, can go into operation for 2 grades, can spy adopt for 3 grades.
From table, 2-4 can find out, the shampoo described in embodiment of the present invention 1-3 is highly stable, can go into operation.
Test implementation example 2: application experiment.
This product application experiment contrast (A is commercially available prod, and B is shampoo described in embodiment 1-3) must be divided into 0-5 and divide, and the high score of performance is high.
1, choose the volunteer of 20 impaired hair qualitys, every ten become a group, respectively corresponding these four groups, these volunteers are used respectively to shampoo and commercially available prod described in embodiment 1-3, to foam, the sliding sense of bath, wetly send out a feel, half-dried feel, dryly send out a feel, scalp is felt to test, method of testing is sensory testing, and test result is as shown 5-7:
The comparison of test results table of shampoo described in table 5 commercially available prod and embodiment 1
The comparison of test results table of shampoo described in table 6 commercially available prod and embodiment 2
The comparison of test results table of shampoo described in table 7 commercially available prod and embodiment 3
2, choose the volunteer of 20 healthy hair qualitys, every ten become a group, respectively corresponding these four groups, these volunteers are used respectively to shampoo and commercially available prod described in embodiment 1-3, to foam, the sliding sense of bath, wetly send out a feel, half-dried feel, dryly send out a feel, scalp is felt to test, method of testing is sensory testing, and test result is as shown 8-10:
The comparison of test results table of shampoo described in table 8 commercially available prod and embodiment 1
The comparison of test results table of shampoo described in table 9 commercially available prod and embodiment 2
The comparison of test results table of shampoo described in table 10 commercially available prod and embodiment 3
From above application experiment result, reach a conclusion: the neatly sense that liquidates in the use of this product, the wet feel of sending out, half-dried feel, the dry feel of sending out, scalp sensuously has lifting, obvious especially to impaired hair quality.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, the variation of any unsubstantiality that those skilled in the art does on basis of the present invention and replacement all belong to the present invention's scope required for protection.
Claims (9)
1. a three-in-one shampoo, is characterized in that: it is by sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol, guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, dimethiconol or DBSA TEA salt, Zinc Pyrithione, hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, deionized water are prepared from.
2. three-in-one shampoo according to claim 1, is characterized in that, it is comprised of the following component in quality percentage composition:
Sodium laureth sulfate 15-18%
Lauryl alcohol sulfuric ester ammonium 2-4%
Mountain Yu base trimethyl ammonium chloride 0.2-0.5%
Coconut oleoyl amine MEA 0.5-1.0%
Spermol 0.5-1.0%
Guar gum hydroxypropyl-trimethyl ammonium chloride 0.3-0.6%
Polyquaternium-10 0.15-0.25%
Allantoin 0.2-0.4%
Trimethylolpropane tris caprylate 0.2-0.5%
Methyl hydroxybenzoate 0.1-0.2%
Propyl hydroxybenzoate 0.1-0.2%
C
12-20alkyl androstanediol 3.0-5.0%
Cocamido propyl betaine 2-5%
Cocamidopropyl propyl amide amine oxide 1.0-4.0%
Dimethiconol or DBSA TEA salt 1.0-2.0%
Zinc Pyrithione 1.0-2.0%
Hydrolysis of keratin 0.5-2%
Hydrolyzed silkworm silk albumen 0.5-2%
Methylchloroisothiazandnone 0.05-0.1%
Polyquaternary ammonium salt-7 1.0-3.0%
Essence 0.8-1.5%
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2-0.4%
Deionized water surplus.
3. the preparation method of three-in-one shampoo according to claim 2, is characterized in that, its concrete steps are as follows:
1) the A component cold water soak being comprised of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is disperseed, standby;
2) add liquid to wash in pot the B component being formed by deionized water, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol; stirring is warmed up to 75-85 degree; after insulated and stirred is dissolved extremely completely, then add standby A component;
3) after the C component being comprised of guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10 is disperseed with cold water respectively, add liquid to wash in pot, insulated and stirred is even;
4) add liquid to wash in pot the D component being comprised of allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, processing cools;
5) will be by C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, and the E component of dimethiconol or DBSA TEA salt composition adds liquid to wash in pot, stirs, processing cools;
6) after the F component cold water being comprised of Zinc Pyrithione is disperseed, add liquid to wash in pot, homogenizing 2-5 minute;
7) the G component being comprised of hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence is added in pot, stir;
8) sampling detect, qualified after, discharging, obtains three-in-one shampoo.
4. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 2) in, stir and be warmed up to 80 degree.
5. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 3), C component adds liquid to wash after pot, need to stir 2 hours.
6. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 4), D component adds liquid to wash after pot, and 50 degree cool.
7. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 5), E component adds liquid to wash after pot, cools below 45 degree.
8. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 6), and homogenizing 3 minutes.
9. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 8), need to continue low rate mixing after 2 hours, resampling detects; Wherein, controlling mixing speed is 20 ~ 40 r/min.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104622711A (en) * | 2014-12-29 | 2015-05-20 | 无锡蚕魅科技有限公司 | Fibroin shampoo and preparation method thereof |
| CN105769615A (en) * | 2016-04-12 | 2016-07-20 | 谢文福 | Portable hair washing sheet and preparing method thereof |
| CN106344434A (en) * | 2016-10-12 | 2017-01-25 | 广州丹奇日用化工厂有限公司 | Nutritious supple shampoo without silicon oil and preparation method thereof |
| CN106420511A (en) * | 2016-12-12 | 2017-02-22 | 德阳力久云智知识产权运营有限公司 | Antidandruff and antipruritic silicone-oil-free shampoo and preparation method thereof |
| CN106580863A (en) * | 2017-02-24 | 2017-04-26 | 李忠泽 | Scurf removing and brain strengthening sapindus silk protein shampoo |
| CN106726712A (en) * | 2016-11-30 | 2017-05-31 | 钟梅 | A kind of maintenance shampoo |
| CN107184413A (en) * | 2017-05-11 | 2017-09-22 | 曾万祥 | It is a kind of to repair moist hair film of root of hair and preparation method thereof without anti-corrosion depth |
| CN107550770A (en) * | 2016-06-30 | 2018-01-09 | 王文军 | A kind of preparation method of peony oil-control anti-dandruff shampoo |
| CN107811886A (en) * | 2017-11-15 | 2018-03-20 | 陈荷芬 | A kind of nourishing osmosis type shampoo with massage powder |
| CN108354852A (en) * | 2018-04-09 | 2018-08-03 | 广州奥蓓斯化妆品有限公司 | A kind of shampoo |
| CN110585087A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil shampoo and preparation method thereof |
| CN111743806A (en) * | 2020-08-01 | 2020-10-09 | 广州市舒悦化妆品有限公司 | Gemini process mild nourishing and softening shampoo and preparation method thereof |
| CN111973542A (en) * | 2020-08-27 | 2020-11-24 | 刘克武 | Shampoo containing wormwood extract for infants |
| CN113908101A (en) * | 2021-11-09 | 2022-01-11 | 广州大唐化妆品有限公司 | Anti-dandruff composition containing ginger granules and application thereof |
| CN114209619A (en) * | 2021-11-30 | 2022-03-22 | 重庆创园生物科技有限公司 | Liquid shampoo |
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| CN103169631A (en) * | 2011-12-22 | 2013-06-26 | 天津天狮生物发展有限公司 | Softening and shining shampoo containing traditional Chinese medicine composition and preparation method thereof |
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| CN1114181A (en) * | 1994-06-28 | 1996-01-03 | 乌力吉 | 6-in-1 long-acting nutritious shampoo containing extract liquid of snail |
| CN103169631A (en) * | 2011-12-22 | 2013-06-26 | 天津天狮生物发展有限公司 | Softening and shining shampoo containing traditional Chinese medicine composition and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104622711A (en) * | 2014-12-29 | 2015-05-20 | 无锡蚕魅科技有限公司 | Fibroin shampoo and preparation method thereof |
| CN105769615B (en) * | 2016-04-12 | 2019-02-22 | 谢文福 | A kind of Portable shampooing piece and preparation method thereof |
| CN105769615A (en) * | 2016-04-12 | 2016-07-20 | 谢文福 | Portable hair washing sheet and preparing method thereof |
| CN107550770A (en) * | 2016-06-30 | 2018-01-09 | 王文军 | A kind of preparation method of peony oil-control anti-dandruff shampoo |
| CN106344434A (en) * | 2016-10-12 | 2017-01-25 | 广州丹奇日用化工厂有限公司 | Nutritious supple shampoo without silicon oil and preparation method thereof |
| CN106726712A (en) * | 2016-11-30 | 2017-05-31 | 钟梅 | A kind of maintenance shampoo |
| CN106420511A (en) * | 2016-12-12 | 2017-02-22 | 德阳力久云智知识产权运营有限公司 | Antidandruff and antipruritic silicone-oil-free shampoo and preparation method thereof |
| CN106580863A (en) * | 2017-02-24 | 2017-04-26 | 李忠泽 | Scurf removing and brain strengthening sapindus silk protein shampoo |
| CN107184413A (en) * | 2017-05-11 | 2017-09-22 | 曾万祥 | It is a kind of to repair moist hair film of root of hair and preparation method thereof without anti-corrosion depth |
| CN107811886A (en) * | 2017-11-15 | 2018-03-20 | 陈荷芬 | A kind of nourishing osmosis type shampoo with massage powder |
| CN108354852A (en) * | 2018-04-09 | 2018-08-03 | 广州奥蓓斯化妆品有限公司 | A kind of shampoo |
| CN110585087A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil shampoo and preparation method thereof |
| CN111743806A (en) * | 2020-08-01 | 2020-10-09 | 广州市舒悦化妆品有限公司 | Gemini process mild nourishing and softening shampoo and preparation method thereof |
| CN111973542A (en) * | 2020-08-27 | 2020-11-24 | 刘克武 | Shampoo containing wormwood extract for infants |
| CN113908101A (en) * | 2021-11-09 | 2022-01-11 | 广州大唐化妆品有限公司 | Anti-dandruff composition containing ginger granules and application thereof |
| CN114209619A (en) * | 2021-11-30 | 2022-03-22 | 重庆创园生物科技有限公司 | Liquid shampoo |
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