CN103735430A - Three-in-one liquid shampoo and preparation method thereof - Google Patents
Three-in-one liquid shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN103735430A CN103735430A CN201310754480.6A CN201310754480A CN103735430A CN 103735430 A CN103735430 A CN 103735430A CN 201310754480 A CN201310754480 A CN 201310754480A CN 103735430 A CN103735430 A CN 103735430A
- Authority
- CN
- China
- Prior art keywords
- component
- pot
- shampoo
- wash
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002453 shampoo Substances 0.000 title claims abstract description 43
- 239000007788 liquid Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 150000002148 esters Chemical class 0.000 claims abstract description 27
- -1 polyquaternium-10 Chemical compound 0.000 claims abstract description 26
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims abstract description 10
- 239000002253 acid Substances 0.000 claims abstract description 10
- 229960000458 allantoin Drugs 0.000 claims abstract description 10
- 229920006037 cross link polymer Polymers 0.000 claims abstract description 10
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 102000011782 Keratins Human genes 0.000 claims abstract description 9
- 108010076876 Keratins Proteins 0.000 claims abstract description 9
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims abstract description 9
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960003415 propylparaben Drugs 0.000 claims abstract description 9
- 229940057950 sodium laureth sulfate Drugs 0.000 claims abstract description 9
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims abstract description 9
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 229940043810 zinc pyrithione Drugs 0.000 claims abstract description 8
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 14
- SHWDCLQRSWTSRE-UHFFFAOYSA-N CCC(CO)(CO)CO.CCCCCCCC(O)=O.CCCCCCCC(O)=O.CCCCCCCC(O)=O Chemical compound CCC(CO)(CO)CO.CCCCCCCC(O)=O.CCCCCCCC(O)=O.CCCCCCCC(O)=O SHWDCLQRSWTSRE-UHFFFAOYSA-N 0.000 claims description 11
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 9
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 9
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 9
- 241000255789 Bombyx mori Species 0.000 claims description 9
- 244000060011 Cocos nucifera Species 0.000 claims description 9
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 9
- MPNXSZJPSVBLHP-UHFFFAOYSA-N 2-chloro-n-phenylpyridine-3-carboxamide Chemical compound ClC1=NC=CC=C1C(=O)NC1=CC=CC=C1 MPNXSZJPSVBLHP-UHFFFAOYSA-N 0.000 claims description 8
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims description 8
- 229920002907 Guar gum Polymers 0.000 claims description 8
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 8
- 239000000665 guar gum Substances 0.000 claims description 8
- 229960002154 guar gum Drugs 0.000 claims description 8
- 235000010417 guar gum Nutrition 0.000 claims description 8
- 230000007062 hydrolysis Effects 0.000 claims description 8
- 238000006460 hydrolysis reaction Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- CBMYJHIOYJEBSB-YSZCXEEOSA-N 5alpha-androstane-3beta,17beta-diol Chemical compound C1[C@@H](O)CC[C@]2(C)[C@H]3CC[C@](C)([C@H](CC4)O)[C@@H]4[C@@H]3CC[C@H]21 CBMYJHIOYJEBSB-YSZCXEEOSA-N 0.000 claims description 7
- 238000012545 processing Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 3
- 238000005070 sampling Methods 0.000 claims description 3
- 238000012952 Resampling Methods 0.000 claims description 2
- 230000000474 nursing effect Effects 0.000 abstract description 8
- 239000002994 raw material Substances 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 7
- 238000004140 cleaning Methods 0.000 abstract description 5
- 230000003750 conditioning effect Effects 0.000 abstract description 4
- 230000000638 stimulation Effects 0.000 abstract description 4
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 abstract 1
- 244000007835 Cyamopsis tetragonoloba Species 0.000 abstract 1
- 238000004220 aggregation Methods 0.000 abstract 1
- 230000002776 aggregation Effects 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 abstract 1
- 229940063953 ammonium lauryl sulfate Drugs 0.000 abstract 1
- YSJGOMATDFSEED-UHFFFAOYSA-M behentrimonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCCCCCC[N+](C)(C)C YSJGOMATDFSEED-UHFFFAOYSA-M 0.000 abstract 1
- 229940075506 behentrimonium chloride Drugs 0.000 abstract 1
- 229960000541 cetyl alcohol Drugs 0.000 abstract 1
- 229940060296 dodecylbenzenesulfonic acid Drugs 0.000 abstract 1
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 abstract 1
- 229960003299 ketamine Drugs 0.000 abstract 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 abstract 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 abstract 1
- 229960002216 methylparaben Drugs 0.000 abstract 1
- ONLRKTIYOMZEJM-UHFFFAOYSA-N n-methylmethanamine oxide Chemical compound C[NH+](C)[O-] ONLRKTIYOMZEJM-UHFFFAOYSA-N 0.000 abstract 1
- 102000004169 proteins and genes Human genes 0.000 abstract 1
- 108090000623 proteins and genes Proteins 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 14
- 210000004761 scalp Anatomy 0.000 description 9
- 238000002474 experimental method Methods 0.000 description 5
- 239000006260 foam Substances 0.000 description 3
- 230000003648 hair appearance Effects 0.000 description 3
- 239000004973 liquid crystal related substance Substances 0.000 description 3
- 230000007774 longterm Effects 0.000 description 3
- 238000013112 stability test Methods 0.000 description 3
- 208000001840 Dandruff Diseases 0.000 description 2
- 208000003251 Pruritus Diseases 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 229920002545 silicone oil Polymers 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009960 carding Methods 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 210000003128 head Anatomy 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001662 opsonic effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 230000003019 stabilising effect Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a three-in-one liquid shampoo and a preparation method thereof. The three-in-one liquid shampoo is prepared from the following raw materials: sodium laureth sulfate, ammonium lauryl sulfate, behentrimonium chloride, cocamidopropyl MEA, cetanol, guar hydroxypropyltrimonium chloride, polyquaternium-10, allantoin, trimethylol propane octanoate ester, methylparaben, propyl hydroxybenzoate, C12-20 alkyl polyglycoside, cocamidopropyl betaine, cocamidopropyl dimethylamine oxide, dimethiconol or dodecylbenzene sulfonic acid TEA salt, zinc pyrithione, hydrolyzed keratin, hydrolyzed silk protein, methyl-isothiazol-ketamine, polyquaternium-7, essence, crylic acid (ester)/C10-30 alkanol acrylic ester cross-linked polymer and deionized water. By adopting the three-in-one liquid shampoo, the stability of the product and the use effects of the raw materials can be improved, the three-in-one liquid shampoo achieves good cleaning and nursing effects, does not generate aggregation and stimulation problems after being used for a long period of time, and achieves the three-in-one effect of cleaning, nursing and conditioning.
Description
Technical field
The present invention relates to the shampoo in a kind of personal care articles, be specially a kind of three-in-one shampoo simultaneously with clean, nursing, protective effect and preparation method thereof.
Background technology
Shampoo as human lives's essential product, receives the concern of consumer always.Shampoo can be divided into clean shampoo and two-in-one shampoo, and the clean main demand of shampoo is clean hair dirt, need to coordinate hair conditioner to use together; And two-in-one shampoo is in clean hair dirt, can bring nursing to hair, improve smoothness, the lifting carding power of the rear hair of washing, improve dry compliance and the easy cardability sent out, prevent generation of static electricity.But the two-in-one shampoo of selling on market now mostly exists nursing efficacy inadequate, large to scalp irritation, the shortcoming that product long-time stability are inadequate.Analyze its main cause have following some: 1, shampoo main body composition is anion surfactant and water, and have the material of opsonic action mostly to be cation and lipophilicity substance to hair, both mix very difficult long-time stable, therefore the dosage of conditioner is restricted, there is the bad .2 of conditioning effect, after adding stabilizing agent, add a large amount of conditioners, a large amount of cationes and silicone oil conditioner are assembled and are caused nose heave and hair to become fragile easily broken on hair, 3, a large amount of cationes and silicone oil conditioner also produce and stimulate scalp, life-time service easily causes head pruritus and dandruff problem.
Summary of the invention
For overcoming the defect of prior art, be of the present inventionly to provide a kind of three-in-one shampoo, it can improve the stability of integral product and the result of use of raw material, reaches clean, nursing efficacy good, and life-time service can not cause to be assembled and stimulation problem; Can accomplish the real triple effect unification of cleaning, nurse, nurse one's health.
Another object of the present invention is to provide a kind of preparation method of three-in-one shampoo.
The technical solution adopted in the present invention is as follows for achieving the above object:
A kind of three-in-one shampoo, is characterized in that: it be by sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol, guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, dimethiconol or DBSA TEA salt, Zinc Pyrithione, hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, deionized water are prepared from.
Preferably, inventor finds through great many of experiments,, nursing real clean in order to accomplish, the unification of conditioning triple effect, and it is comprised of the following component in quality percentage composition:
In the present invention, above-mentioned raw materials all can obtain by purchase.As: hydrolyzed silkworm silk albumen is optional purchased from Huzhou Xintiansi Biotechnology Co. Ltd., and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is optional purchased from Lubrizol company
ultrez 20 Polymer.
A preparation method for three-in-one shampoo, its concrete steps are as follows:
1) the A component cold water soak being comprised of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is disperseed, standby;
2) add liquid to wash in pot the B component being formed by deionized water, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol; stirring is warmed up to 75-85 degree; after insulated and stirred is dissolved extremely completely, then add standby A component;
3) after the C component being comprised of guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10 is disperseed with cold water respectively, add liquid to wash in pot, insulated and stirred is even;
4) add liquid to wash in pot the D component being comprised of allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, processing cools;
5) will be by C12-20 alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, and the E component of dimethiconol or DBSA TEA salt composition adds liquid to wash in pot, stirs, processing cools;
6) after the F component cold water being comprised of Zinc Pyrithione is disperseed, add liquid to wash in pot, homogenizing 2-5 minute;
7) the G component being comprised of hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence is added in pot, stir;
8) sampling detect, qualified after, discharging, obtains three-in-one shampoo.
Preferably, in step 2) in, stir and be warmed up to 80 degree.
Preferably, in step 3), C component adds liquid to wash after pot, need to stir 2 hours.
Preferably, in step 4), D component adds liquid to wash after pot, and 50 degree cool.
Preferably, in step 5), E component adds liquid to wash after pot, cools below 45 degree.
Preferably, in step 6), homogenizing 3 minutes;
Preferably, in step 8), need to continue low rate mixing after 2 hours, resampling detects; Wherein, controlling mixing speed is 20～40r/min.
Beneficial effect of the present invention is:
1, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, the C in the present invention's formula
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide play cleaning action, wherein C in product
12 -20alkyl androstanediol can effectively reduce the stimulation of other surfactants, cocamidopropyl propyl amide amine oxide add the lather quickness that can improve product. the collocation of above component is used, and when product is used, bubbles rapidly, and foam is abundant, and clean power is strong and zest is little.
2, mountain Yu base trimethyl ammonium chloride, trimethylolpropane tris caprylate, coconut oleoyl amine MEA, spermol, dimethiconol or the DBSA TEA salt in the present invention's formula forms polynary conditioner, wherein spermol, coconut oleoyl amine MEA adds the whole polynary conditioner of effective promotion more formation liquid crystal structure in integral product, while being in use diluted, this liquid crystal structure is destroyed very soon, and discharge the conditioner of parcel, reach conditioning effect obvious, rapidly object.And trimethylolpropane tris caprylate is a kind of efficient salubrious humectants and emollients, can improve rapidly the moisture holding capacity of hair and skin, activate scalp cells vigor, improve the lubricated sense of bath of product, improve the dry soft feeling of sending out. make scalp more healthy.It is steady in a long-term that trimethylolpropane tris caprylate is difficult to reach in general system, this product can cross said components collocation, make it form liquid crystal structure and can discharge fast onset while reaching steady in a long-term dilution.
3, guar gum hydroxypropyl-trimethyl ammonium chloride, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, the Polyquaternium-10 in the present invention's formula forms a solid netted system in product, play the Stabilization of a suspension, form a polynary stabilising system together with polynary conditioner, make this product long-term stability and result of use rapid.
4, ZPT, allantoin, hydrolysis of keratin, the hydrolyzed silkworm silk albumen in the present invention's formula plays removing scurf and relieving itching effect in this product; adding of allantoin and albumen plays the anti-scorching effect of antiinflammatory to scalp; for scalp has been constructed a protection, repair barrier together with trimethylolpropane tris caprylate.
5, methyl hydroxybenzoate, propyl hydroxybenzoate, the methylchloroisothiazandnone in the present invention's formula plays protective system, and the composite use of several antiseptic has synergistic function.
6, adjusting product rheology is played in polyquaternary ammonium salt-7 in the present invention's formula in this product, increases product and uses the sliding sense of bath.
In sum, the compatibility of the present invention by above-mentioned raw materials and the present invention is directed to the production technology of above-mentioned recipe design, make whole interiors of products structure form diversification structure, can improve the stability of integral product and the result of use of raw material, reach clean, nursing efficacy good, life-time service can not cause assemble and stimulation problem; Can accomplish the real triple effect unification of cleaning, nurse, nurse one's health.
Below in conjunction with concrete embodiment, the present invention is described in further detail.
The specific embodiment
Embodiment 1-3:
Get respectively the following raw material in quality percentage composition: sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol, guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, dimethiconol or DBSA TEA salt, Zinc Pyrithione, hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, deionized water.
Concrete proportioning is in Table 1.
The proportioning table of table 1 embodiment 1-3
Above-mentioned raw materials is followed these steps to prepare three-in-one shampoo as follows:
1) the A component cold water soak being comprised of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is disperseed, standby;
2) add liquid to wash in pot the B component being formed by deionized water, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol; stirring is warmed up to 80 degree; after insulated and stirred is dissolved extremely completely, then add standby A component;
3) after the C component being comprised of guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10 is disperseed with cold water respectively, add liquid to wash in pot, insulated and stirred is even; Stir 2 hours.
4) add liquid to wash in pot the D component being comprised of allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, processing cools; 50 degree cool.
5) will be by C12-20 alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, and the E component of dimethiconol or DBSA TEA salt composition adds liquid to wash in pot, stirs, processing cools; Cool below 45 degree.
6) after the F component cold water being comprised of Zinc Pyrithione is disperseed, add liquid to wash in pot, homogenizing 3 minutes;
7) the G component being comprised of hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence is added in pot, stir;
8) continue low rate mixing after 2 hours, sampling detects, qualified after, discharging, obtains three-in-one shampoo.
Test implementation example 1: stability experiment.
Table 2 embodiment 1 stability test result table
Table 3 embodiment 2 stability test result tables
Table 4 embodiment 3 stability test result tables
Remarks explanation: 1 grade: unchanged, 2 grades: slightly change 3 grades: changes larger, 4 grades: seriously variation; 1, can go into operation for 2 grades, can spy adopt for 3 grades.
From table, 2-4 can find out, the shampoo described in embodiment of the present invention 1-3 is highly stable, can go into operation.
Test implementation example 2: application experiment.
This product application experiment contrast (A is commercially available prod, and B is shampoo described in embodiment 1-3) must be divided into 0-5 and divide, and the high score of performance is high.
1, choose the volunteer of 20 impaired hair qualitys, every ten become a group, respectively corresponding these four groups, these volunteers are used respectively to shampoo and commercially available prod described in embodiment 1-3, to foam, the sliding sense of bath, wetly send out a feel, half-dried feel, dryly send out a feel, scalp is felt to test, method of testing is sensory testing, and test result is as shown 5-7:
The comparison of test results table of shampoo described in table 5 commercially available prod and embodiment 1
The comparison of test results table of shampoo described in table 6 commercially available prod and embodiment 2
The comparison of test results table of shampoo described in table 7 commercially available prod and embodiment 3
2, choose the volunteer of 20 healthy hair qualitys, every ten become a group, respectively corresponding these four groups, these volunteers are used respectively to shampoo and commercially available prod described in embodiment 1-3, to foam, the sliding sense of bath, wetly send out a feel, half-dried feel, dryly send out a feel, scalp is felt to test, method of testing is sensory testing, and test result is as shown 8-10:
The comparison of test results table of shampoo described in table 8 commercially available prod and embodiment 1
The comparison of test results table of shampoo described in table 9 commercially available prod and embodiment 2
The comparison of test results table of shampoo described in table 10 commercially available prod and embodiment 3
From above application experiment result, reach a conclusion: the neatly sense that liquidates in the use of this product, the wet feel of sending out, half-dried feel, the dry feel of sending out, scalp sensuously has lifting, obvious especially to impaired hair quality.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, the variation of any unsubstantiality that those skilled in the art does on basis of the present invention and replacement all belong to the present invention's scope required for protection.
Claims (9)
1. a three-in-one shampoo, is characterized in that: it is by sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol, guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, dimethiconol or DBSA TEA salt, Zinc Pyrithione, hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, deionized water are prepared from.
2. three-in-one shampoo according to claim 1, is characterized in that, it is comprised of the following component in quality percentage composition:
Sodium laureth sulfate 15-18%
Lauryl alcohol sulfuric ester ammonium 2-4%
Mountain Yu base trimethyl ammonium chloride 0.2-0.5%
Coconut oleoyl amine MEA 0.5-1.0%
Spermol 0.5-1.0%
Guar gum hydroxypropyl-trimethyl ammonium chloride 0.3-0.6%
Polyquaternium-10 0.15-0.25%
Allantoin 0.2-0.4%
Trimethylolpropane tris caprylate 0.2-0.5%
Methyl hydroxybenzoate 0.1-0.2%
Propyl hydroxybenzoate 0.1-0.2%
C
12-20alkyl androstanediol 3.0-5.0%
Cocamido propyl betaine 2-5%
Cocamidopropyl propyl amide amine oxide 1.0-4.0%
Dimethiconol or DBSA TEA salt 1.0-2.0%
Zinc Pyrithione 1.0-2.0%
Hydrolysis of keratin 0.5-2%
Hydrolyzed silkworm silk albumen 0.5-2%
Methylchloroisothiazandnone 0.05-0.1%
Polyquaternary ammonium salt-7 1.0-3.0%
Essence 0.8-1.5%
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2-0.4%
Deionized water surplus.
3. the preparation method of three-in-one shampoo according to claim 2, is characterized in that, its concrete steps are as follows:
1) the A component cold water soak being comprised of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer is disperseed, standby;
2) add liquid to wash in pot the B component being formed by deionized water, sodium laureth sulfate, lauryl alcohol sulfuric ester ammonium, mountain Yu base trimethyl ammonium chloride, coconut oleoyl amine MEA, spermol; stirring is warmed up to 75-85 degree; after insulated and stirred is dissolved extremely completely, then add standby A component;
3) after the C component being comprised of guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10 is disperseed with cold water respectively, add liquid to wash in pot, insulated and stirred is even;
4) add liquid to wash in pot the D component being comprised of allantoin, trimethylolpropane tris caprylate, methyl hydroxybenzoate, propyl hydroxybenzoate, processing cools;
5) will be by C
12-20alkyl androstanediol, cocamido propyl betaine, cocamidopropyl propyl amide amine oxide, and the E component of dimethiconol or DBSA TEA salt composition adds liquid to wash in pot, stirs, processing cools;
6) after the F component cold water being comprised of Zinc Pyrithione is disperseed, add liquid to wash in pot, homogenizing 2-5 minute;
7) the G component being comprised of hydrolysis of keratin, hydrolyzed silkworm silk albumen, methylchloroisothiazandnone, polyquaternary ammonium salt-7, essence is added in pot, stir;
8) sampling detect, qualified after, discharging, obtains three-in-one shampoo.
4. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 2) in, stir and be warmed up to 80 degree.
5. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 3), C component adds liquid to wash after pot, need to stir 2 hours.
6. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 4), D component adds liquid to wash after pot, and 50 degree cool.
7. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 5), E component adds liquid to wash after pot, cools below 45 degree.
8. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 6), and homogenizing 3 minutes.
9. the preparation method of three-in-one shampoo according to claim 3, is characterized in that: in step 8), need to continue low rate mixing after 2 hours, resampling detects; Wherein, controlling mixing speed is 20 ~ 40 r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310754480.6A CN103735430B (en) | 2013-12-31 | 2013-12-31 | Three-in-one liquid shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310754480.6A CN103735430B (en) | 2013-12-31 | 2013-12-31 | Three-in-one liquid shampoo and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103735430A true CN103735430A (en) | 2014-04-23 |
| CN103735430B CN103735430B (en) | 2015-06-03 |
Family
ID=50492552
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310754480.6A Active CN103735430B (en) | 2013-12-31 | 2013-12-31 | Three-in-one liquid shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103735430B (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104622711A (en) * | 2014-12-29 | 2015-05-20 | 无锡蚕魅科技有限公司 | Fibroin shampoo and preparation method thereof |
| CN105769615A (en) * | 2016-04-12 | 2016-07-20 | 谢文福 | Portable hair washing sheet and preparing method thereof |
| CN106344434A (en) * | 2016-10-12 | 2017-01-25 | 广州丹奇日用化工厂有限公司 | Nutritious supple shampoo without silicon oil and preparation method thereof |
| CN106420511A (en) * | 2016-12-12 | 2017-02-22 | 德阳力久云智知识产权运营有限公司 | Antidandruff and antipruritic silicone-oil-free shampoo and preparation method thereof |
| CN106580863A (en) * | 2017-02-24 | 2017-04-26 | 李忠泽 | Scurf removing and brain strengthening sapindus silk protein shampoo |
| CN106726712A (en) * | 2016-11-30 | 2017-05-31 | 钟梅 | A kind of maintenance shampoo |
| CN107184413A (en) * | 2017-05-11 | 2017-09-22 | 曾万祥 | It is a kind of to repair moist hair film of root of hair and preparation method thereof without anti-corrosion depth |
| CN107550770A (en) * | 2016-06-30 | 2018-01-09 | 王文军 | A kind of preparation method of peony oil-control anti-dandruff shampoo |
| CN107811886A (en) * | 2017-11-15 | 2018-03-20 | 陈荷芬 | A kind of nourishing osmosis type shampoo with massage powder |
| CN108354852A (en) * | 2018-04-09 | 2018-08-03 | 广州奥蓓斯化妆品有限公司 | A kind of shampoo |
| CN110585087A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil shampoo and preparation method thereof |
| CN111743806A (en) * | 2020-08-01 | 2020-10-09 | 广州市舒悦化妆品有限公司 | Gemini process mild nourishing and softening shampoo and preparation method thereof |
| CN111973542A (en) * | 2020-08-27 | 2020-11-24 | 刘克武 | Shampoo containing wormwood extract for infants |
| CN113908101A (en) * | 2021-11-09 | 2022-01-11 | 广州大唐化妆品有限公司 | Anti-dandruff composition containing ginger granules and application thereof |
| CN114209619A (en) * | 2021-11-30 | 2022-03-22 | 重庆创园生物科技有限公司 | Liquid shampoo |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114181A (en) * | 1994-06-28 | 1996-01-03 | 乌力吉 | 6-in-1 long-acting nutritious shampoo containing extract liquid of snail |
| CN103169631A (en) * | 2011-12-22 | 2013-06-26 | 天津天狮生物发展有限公司 | Softening and shining shampoo containing traditional Chinese medicine composition and preparation method thereof |
-
2013
- 2013-12-31 CN CN201310754480.6A patent/CN103735430B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114181A (en) * | 1994-06-28 | 1996-01-03 | 乌力吉 | 6-in-1 long-acting nutritious shampoo containing extract liquid of snail |
| CN103169631A (en) * | 2011-12-22 | 2013-06-26 | 天津天狮生物发展有限公司 | Softening and shining shampoo containing traditional Chinese medicine composition and preparation method thereof |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104622711A (en) * | 2014-12-29 | 2015-05-20 | 无锡蚕魅科技有限公司 | Fibroin shampoo and preparation method thereof |
| CN105769615B (en) * | 2016-04-12 | 2019-02-22 | 谢文福 | A kind of Portable shampooing piece and preparation method thereof |
| CN105769615A (en) * | 2016-04-12 | 2016-07-20 | 谢文福 | Portable hair washing sheet and preparing method thereof |
| CN107550770A (en) * | 2016-06-30 | 2018-01-09 | 王文军 | A kind of preparation method of peony oil-control anti-dandruff shampoo |
| CN106344434A (en) * | 2016-10-12 | 2017-01-25 | 广州丹奇日用化工厂有限公司 | Nutritious supple shampoo without silicon oil and preparation method thereof |
| CN106726712A (en) * | 2016-11-30 | 2017-05-31 | 钟梅 | A kind of maintenance shampoo |
| CN106420511A (en) * | 2016-12-12 | 2017-02-22 | 德阳力久云智知识产权运营有限公司 | Antidandruff and antipruritic silicone-oil-free shampoo and preparation method thereof |
| CN106580863A (en) * | 2017-02-24 | 2017-04-26 | 李忠泽 | Scurf removing and brain strengthening sapindus silk protein shampoo |
| CN107184413A (en) * | 2017-05-11 | 2017-09-22 | 曾万祥 | It is a kind of to repair moist hair film of root of hair and preparation method thereof without anti-corrosion depth |
| CN107811886A (en) * | 2017-11-15 | 2018-03-20 | 陈荷芬 | A kind of nourishing osmosis type shampoo with massage powder |
| CN108354852A (en) * | 2018-04-09 | 2018-08-03 | 广州奥蓓斯化妆品有限公司 | A kind of shampoo |
| CN110585087A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil shampoo and preparation method thereof |
| CN111743806A (en) * | 2020-08-01 | 2020-10-09 | 广州市舒悦化妆品有限公司 | Gemini process mild nourishing and softening shampoo and preparation method thereof |
| CN111973542A (en) * | 2020-08-27 | 2020-11-24 | 刘克武 | Shampoo containing wormwood extract for infants |
| CN113908101A (en) * | 2021-11-09 | 2022-01-11 | 广州大唐化妆品有限公司 | Anti-dandruff composition containing ginger granules and application thereof |
| CN114209619A (en) * | 2021-11-30 | 2022-03-22 | 重庆创园生物科技有限公司 | Liquid shampoo |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103735430B (en) | 2015-06-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103735430B (en) | Three-in-one liquid shampoo and preparation method thereof | |
| CN102895151B (en) | Sulfate-free hair cleanser and preparation method thereof | |
| CN102716045B (en) | Shampoo composition containing double anti-dandruff agents | |
| CN103251523B (en) | Oil-control shampoo composite | |
| CN110123721B (en) | Shampoo composition for improving oily scalp | |
| CN108619053A (en) | Desquamation compositions, leaves shampoo and preparation method thereof | |
| CN104523450B (en) | A kind of new hair washing hair care and nourishing combination | |
| CN102920619A (en) | Conditioning shampoo composition containing small amount of sulfate anionic surfactant | |
| CN106361596A (en) | Amino acid foaming cleansing gel and preparation method thereof | |
| CN104940071A (en) | Mild antidandruff shampoo and preparation method thereof | |
| CN107281014A (en) | One kind nourishes strong hair without silicone oil shampoo | |
| CN113332191A (en) | Shampoo and preparation method thereof | |
| CN102488634B (en) | Wild camellia oil shampoo | |
| CN108904311A (en) | A kind of no silicone oil shampoo | |
| CN108992357A (en) | A kind of anti-dandruff and itching-relieving shampoo containing silk hydroiyzing liquid | |
| CN104940039B (en) | Ketoconazol/Clobetasol Propionate hair lotion | |
| CN115581650A (en) | High-safety anti-dandruff composition and preparation method and application thereof | |
| CN106344423A (en) | Composition with dandruff removal and itch relieving effects and hair shampooing care product containing composition | |
| CN114010520A (en) | Personal care composition, preparation method and application | |
| KR102809026B1 (en) | Dandruff Relieving Scalp Cleansing Composition | |
| CN116035933B (en) | Personal cleaning care composition and preparation method and application thereof | |
| CN104352392A (en) | Preparation method of dandruff removing and itching relieving plant shampoo | |
| CN103251517A (en) | Applications of zinc glycyrrhetate, and zinc glycyrrhetate-containing composition | |
| CN103251514A (en) | Anti-dandruff shampoo composition | |
| CN112120985A (en) | Oil-control facial cleanser and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |