CN112120985A - Oil-control facial cleanser and preparation method thereof - Google Patents
Oil-control facial cleanser and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses an oil-control facial cleanser and a preparation method thereof, wherein the oil-control facial cleanser is prepared from the following raw materials in parts by weight: 12-25 parts of surfactant, 3-6 parts of glycerol, 2-5 parts of Tween 60, 1-4 parts of butanediol, 1-3 parts of nicotinamide, 1-4 parts of Hamamelis virginiana extract, 1-4 parts of brown algae extract, 0.8-2 parts of jojoba oil, 0.5-1.5 parts of cetostearyl alcohol, 0.5-1.2 parts of retinol palmitate, 0.5-1 part of squalane, 0.4-0.8 part of hydrogenated lecithin, 0.2-1 part of thickener, 0.2-0.5 part of vitamin E, 0.04-0.08 part of sodium hyaluronate, 0.04-0.08 part of disodium edetate and 60-75 parts of deionized water. The facial cleanser with good oil control effect is prepared by matching the components; by combining multiple oil control factors, oil control is balanced from multiple dimensions, synergistic with each other.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to an oil-control facial cleanser and a preparation method thereof.
Background
Beauty is the nature of people, the first thing to keep the appearance beautiful is to keep clean, the face is used as the face of people, the face is particularly important to keep clean, and in order to realize effective cleaning of the face and fully remove stains and grease on the face, people invent a cleaning product which is a facial cleanser and is specially used for cleaning the face. The facial cleanser is accepted by consumers as a facial cleanser, and is a facial cleaning product for cleaning skin, which not only has good cleaning ability of soap, but also has a certain nursing function.
The existing oil control product takes inorganic powder as a pore astringing component, the function of the component is similar to that of a water tap blocked by a wooden plug, the oil control value of the pore of the oil outlet is not real, the skin burden and the skin quality are deteriorated after long-term use, and the oil gloss is still remained. And the oil is controlled by using algefacients, wherein the algefacients mainly comprise alcohol and mint, and both of the algefacients have the effect of instantly shrinking pores. However, the cooling effect is only palliative, i.e., the astringent effect disappears after a short time, and the subsequent exuded oil cannot be effectively controlled.
Disclosure of Invention
The oil-control facial cleanser has a good oil-control effect.
The invention adopts the following technical scheme for solving the technical problems:
the oil-control facial cleanser is prepared from the following raw materials in parts by weight: 12-25 parts of surfactant, 3-6 parts of glycerol, 2-5 parts of Tween 60, 1-4 parts of butanediol, 1-3 parts of nicotinamide, 1-4 parts of Hamamelis virginiana extract, 1-4 parts of brown algae extract, 0.8-2 parts of jojoba oil, 0.5-1.5 parts of cetostearyl alcohol, 0.5-1.2 parts of retinol palmitate, 0.5-1 part of squalane, 0.4-0.8 part of hydrogenated lecithin, 0.2-1 part of thickener, 0.2-0.5 part of vitamin E, 0.04-0.08 part of sodium hyaluronate, 0.04-0.08 part of disodium edetate and 60-75 parts of deionized water.
As a preferable scheme, the oil-control facial cleanser is prepared from the following raw materials in parts by weight: 15-25 parts of surfactant, 3-5 parts of glycerol, 2-4 parts of Tween 60, 1-3 parts of butanediol, 1-2 parts of nicotinamide, 1-3 parts of Hamamelis virginiana extract, 1-3 parts of brown algae extract, 0.8-1.5 parts of jojoba oil, 0.5-1.2 parts of cetostearyl alcohol, 0.5-1 part of retinol palmitate, 0.5-0.8 part of squalane, 0.5-0.8 part of hydrogenated lecithin, 0.2-0.8 part of thickener, 0.2-0.4 part of vitamin E, 0.04-0.07 part of sodium hyaluronate, 0.04-0.06 part of disodium edetate and 60-70 parts of deionized water.
As a preferable scheme, the oil-control facial cleanser is prepared from the following raw materials in parts by weight: 18 parts of surfactant, 4 parts of glycerol, 2.5 parts of tween 60, 2 parts of butanediol, 1.5 parts of nicotinamide, 2 parts of witch hazel extract, 2 parts of brown algae extract, 1 part of jojoba oil, 1 part of cetostearyl alcohol, 0.8 part of retinol palmitate, 0.6 part of squalane, 0.5 part of hydrogenated lecithin, 0.4 part of thickening agent, 0.3 part of vitamin E, 0.05 part of sodium hyaluronate, 0.05 part of disodium ethylenediamine tetraacetic acid and 63.3 parts of deionized water.
As a preferred embodiment, the surfactant consists of cocamidopropyl betaine, cocomonoethanolamide, sodium methylcocoyl taurate.
As a preferred embodiment, the surfactant is prepared from cocamidopropyl betaine, cocomonoethanolamide, sodium methylcocoyltaurate in a weight ratio of 9: 8: 1.
6. An oil-controlling facial cleanser according to claim 1, wherein said thickener is one of xanthan gum, carboxymethyl cellulose and inorganic salt.
As a preferred embodiment, the preparation method of the brown algae extract comprises the following steps: cleaning fresh brown algae, drying, crushing to 50-100 meshes to obtain brown algae powder, adding the brown algae powder and mixed enzyme into deionized water, stirring for 60-100 min in a water bath at 55-65 ℃ at a rotating speed of 60-150 rpm, adding the stirred liquid into absolute ethyl alcohol with the weight of 3-5 times of that of the liquid, performing ultrasonic treatment for 25-40 min at 500-800W, filtering, and drying to obtain the brown algae extract.
As a preferred scheme, the weight ratio of the brown algae powder, the mixed enzyme and the deionized water is 1: 0.01-0.04: 16-20, wherein the mixed enzyme is prepared from cellulase and pectinase according to a weight ratio of 1: 0.5 to 2.
The invention also provides a preparation method of the oil-control facial cleanser, which comprises the following steps:
(1) adding deionized water, hydrogenated lecithin, disodium ethylene diamine tetraacetate, sodium hyaluronate, a thickening agent, tween 60, jojoba oil and cetostearyl alcohol into a reaction kettle, heating to 75-85 ℃, and uniformly stirring;
(2) adding surfactant, glycerol and squalane, and stirring;
(3) cooling to 42-50 ℃, adding butanediol, nicotinamide, retinol palmitate and vitamin E, and uniformly stirring;
(4) and cooling to 35-40 ℃, adding the witch hazel extract and the brown algae extract, and uniformly stirring to obtain the oil-controlling facial cleanser.
Preferably, the stirring speed is 100-200 rpm.
The invention has the beneficial effects that: (1) the oil control facial cleanser consists of a surfactant, glycerin, Tween 60, butanediol, nicotinamide, a Hamamelis virginiana extract, a brown algae extract, jojoba oil, cetearyl alcohol, retinol palmitate, squalane, hydrogenated lecithin, a thickening agent, vitamin E, sodium hyaluronate, disodium edetate and deionized water, and the facial cleanser with a good oil control effect is prepared by matching; (2) the invention balances oil control from multiple dimensions by using nicotinamide, witch hazel extract, brown algae extract and retinol palmitate in combination, and realizes synergistic interaction; (3) the brown algae extract mainly contains glucuronide, can form a biological membrane with excellent moisturizing effect with protein in skin, and is rich in Na+And K+The ions can help the skin to keep osmotic pressure balance, reduce excessive secreted oil and regulate physiological balance.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The oil-control facial cleanser is prepared from the following raw materials in parts by weight: 18 parts of surfactant, 4 parts of glycerol, 2.5 parts of tween 60, 2 parts of butanediol, 1.5 parts of nicotinamide, 2 parts of witch hazel extract, 2 parts of brown algae extract, 1 part of jojoba oil, 1 part of cetostearyl alcohol, 0.8 part of retinol palmitate, 0.6 part of squalane, 0.5 part of hydrogenated lecithin, 0.4 part of thickening agent, 0.3 part of vitamin E, 0.05 part of sodium hyaluronate, 0.05 part of disodium ethylenediamine tetraacetic acid and 63.3 parts of deionized water.
In this example, the surfactant was prepared from cocamidopropyl betaine, cocomonoethanolamide, sodium methylcocoyl taurate in a weight ratio of 9: 8: 1.
In this example, the thickener is xanthan gum.
In this embodiment, the preparation method of the brown algae extract comprises: cleaning fresh brown algae, drying, pulverizing to 80 mesh to obtain brown algae powder, adding brown algae powder and mixed enzyme into deionized water, stirring in 60 deg.C water bath at 100rpm for 80min, adding the stirred liquid into anhydrous ethanol 4 times the weight of the liquid, treating with 600W ultrasound for 35min, filtering, and drying to obtain brown algae extract.
The weight ratio of the brown algae powder to the mixed enzyme to the deionized water is 1: 0.02: 19, the mixed enzyme is prepared from cellulase and pectinase according to the weight ratio of 1: 1.
The preparation method of the oil-control facial cleanser comprises the following steps:
(1) adding deionized water, hydrogenated lecithin, disodium ethylene diamine tetraacetate, sodium hyaluronate, a thickening agent, tween 60, jojoba oil and cetearyl alcohol into a reaction kettle, heating to 80 ℃, and uniformly stirring;
(2) adding surfactant, glycerol and squalane, and stirring;
(3) cooling to 45 deg.C, adding butanediol, nicotinamide, retinol palmitate, and vitamin E, and stirring;
(4) cooling to 38 deg.C, adding Hamamelis virginiana extract and brown algae extract, and stirring to obtain oil-controlling facial cleanser.
In this example, the stirring rates were all 150 rpm.
Example 2
The oil-control facial cleanser is prepared from the following raw materials in parts by weight: 12 parts of surfactant, 3 parts of glycerol, 2 parts of tween 60, 1 part of butanediol, 1 part of nicotinamide, 1 part of hamamelis virginiana extract, 1 part of brown algae extract, 0.8 part of jojoba oil, 0.5 part of cetostearyl alcohol, 0.5 part of retinol palmitate, 0.5 part of squalane, 0.4 part of hydrogenated lecithin, 0.2 part of thickening agent, 0.2 part of vitamin E, 0.04 part of sodium hyaluronate, 0.04 part of disodium ethylenediamine tetraacetic acid and 60 parts of deionized water.
In this example, the surfactant was prepared from cocamidopropyl betaine, cocomonoethanolamide, sodium methylcocoyl taurate in a weight ratio of 9: 8: 1.
In this example, the thickener is xanthan gum.
In this embodiment, the preparation method of the brown algae extract comprises: cleaning fresh brown algae, drying, pulverizing to 80 mesh to obtain brown algae powder, adding brown algae powder and mixed enzyme into deionized water, stirring in 60 deg.C water bath at 100rpm for 80min, adding the stirred liquid into anhydrous ethanol 4 times the weight of the liquid, treating with 600W ultrasound for 35min, filtering, and drying to obtain brown algae extract.
The weight ratio of the brown algae powder to the mixed enzyme to the deionized water is 1: 0.02: 19, the mixed enzyme is prepared from cellulase and pectinase according to the weight ratio of 1: 1.
The preparation method of the oil-control facial cleanser comprises the following steps:
(1) adding deionized water, hydrogenated lecithin, disodium ethylene diamine tetraacetate, sodium hyaluronate, a thickening agent, tween 60, jojoba oil and cetearyl alcohol into a reaction kettle, heating to 80 ℃, and uniformly stirring;
(2) adding surfactant, glycerol and squalane, and stirring;
(3) cooling to 45 deg.C, adding butanediol, nicotinamide, retinol palmitate, and vitamin E, and stirring;
(4) cooling to 38 deg.C, adding Hamamelis virginiana extract and brown algae extract, and stirring to obtain oil-controlling facial cleanser.
In this example, the stirring rates were all 150 rpm.
Example 3
The oil-control facial cleanser is prepared from the following raw materials in parts by weight: 25 parts of surfactant, 6 parts of glycerol, 5 parts of tween 60, 4 parts of butanediol, 3 parts of nicotinamide, 4 parts of hamamelis virginiana extract, 4 parts of brown algae extract, 2 parts of jojoba oil, 1.5 parts of cetostearyl alcohol, 1.2 parts of retinol palmitate, 1 part of squalane, 0.8 part of hydrogenated lecithin, 1 part of thickener, 0.5 part of vitamin E, 0.08 part of sodium hyaluronate, 0.08 part of disodium ethylenediamine tetraacetic acid and 75 parts of deionized water.
In this example, the surfactant was prepared from cocamidopropyl betaine, cocomonoethanolamide, sodium methylcocoyl taurate in a weight ratio of 9: 8: 1.
In this example, the thickener is xanthan gum.
In this embodiment, the preparation method of the brown algae extract comprises: cleaning fresh brown algae, drying, pulverizing to 80 mesh to obtain brown algae powder, adding brown algae powder and mixed enzyme into deionized water, stirring in 60 deg.C water bath at 100rpm for 80min, adding the stirred liquid into anhydrous ethanol 4 times the weight of the liquid, treating with 600W ultrasound for 35min, filtering, and drying to obtain brown algae extract.
The weight ratio of the brown algae powder to the mixed enzyme to the deionized water is 1: 0.02: 19, the mixed enzyme is prepared from cellulase and pectinase according to the weight ratio of 1: 1.
The preparation method of the oil-control facial cleanser comprises the following steps:
(1) adding deionized water, hydrogenated lecithin, disodium ethylene diamine tetraacetate, sodium hyaluronate, a thickening agent, tween 60, jojoba oil and cetearyl alcohol into a reaction kettle, heating to 80 ℃, and uniformly stirring;
(2) adding surfactant, glycerol and squalane, and stirring;
(3) cooling to 45 deg.C, adding butanediol, nicotinamide, retinol palmitate, and vitamin E, and stirring;
(4) cooling to 38 deg.C, adding Hamamelis virginiana extract and brown algae extract, and stirring to obtain oil-controlling facial cleanser.
In this example, the stirring rates were all 150 rpm.
Example 4
The oil-control facial cleanser is prepared from the following raw materials in parts by weight: 15 parts of surfactant, 3 parts of glycerol, 2 parts of tween 60, 1 part of butanediol, 1 part of nicotinamide, 1 part of hamamelis virginiana extract, 1 part of brown algae extract, 0.8 part of jojoba oil, 0.5 part of cetostearyl alcohol, 0.5 part of retinol palmitate, 0.5 part of squalane, 0.5 part of hydrogenated lecithin, 0.2 part of thickening agent, 0.2 part of vitamin E, 0.04 part of sodium hyaluronate, 0.04 part of disodium ethylenediamine tetraacetic acid and 60 parts of deionized water.
In this example, the surfactant was prepared from cocamidopropyl betaine, cocomonoethanolamide, sodium methylcocoyl taurate in a weight ratio of 9: 8: 1.
In this example, the thickener is xanthan gum.
In this embodiment, the preparation method of the brown algae extract comprises: cleaning fresh brown algae, drying, pulverizing to 80 mesh to obtain brown algae powder, adding brown algae powder and mixed enzyme into deionized water, stirring in 60 deg.C water bath at 100rpm for 80min, adding the stirred liquid into anhydrous ethanol 4 times the weight of the liquid, treating with 600W ultrasound for 35min, filtering, and drying to obtain brown algae extract.
The weight ratio of the brown algae powder to the mixed enzyme to the deionized water is 1: 0.02: 19, the mixed enzyme is prepared from cellulase and pectinase according to the weight ratio of 1: 1.
The preparation method of the oil-control facial cleanser comprises the following steps:
(1) adding deionized water, hydrogenated lecithin, disodium ethylene diamine tetraacetate, sodium hyaluronate, a thickening agent, tween 60, jojoba oil and cetearyl alcohol into a reaction kettle, heating to 80 ℃, and uniformly stirring;
(2) adding surfactant, glycerol and squalane, and stirring;
(3) cooling to 45 deg.C, adding butanediol, nicotinamide, retinol palmitate, and vitamin E, and stirring;
(4) cooling to 38 deg.C, adding Hamamelis virginiana extract and brown algae extract, and stirring to obtain oil-controlling facial cleanser.
In this example, the stirring rates were all 150 rpm.
Comparative example 1
Comparative example 1 is different from example 1 in that comparative example 1 does not contain hamamelis virginiana extract, and the others are the same.
Comparative example 2
Comparative example 2 is different from example 1 in that comparative example 2 does not contain the brown algae extract, and the others are the same.
Comparative example 3
Comparative example 3 differs from the examples in that the brown algae extract described in comparative example 3 is commercially available, and the others are the same.
In this comparative example, the brown algae extract of example 1 was replaced with a brown algae extract purchased from sealimei biotechnology limited of Qingdao.
Comparative example 4
Comparative example 4 differs from example 1 in that comparative example 4 does not contain retinol palmitate, and the other things are the same.
To further demonstrate the effect of the present invention, the following test methods were provided:
1. a skin oil and water pH value tester is adopted to monitor the volunteer using the facial cleanser for 4 hours, and the facial water content and the oil content of the volunteer are evaluated. The method comprises the steps of respectively sampling the oil-control facial cleanser described in examples 1-4 and comparative examples 1-4 for 10 persons in each group, washing the face with the clean water at 25 +/-2 ℃ and the facial cleanser described in examples 1-4 and comparative examples 1-4 in a closed space at 25 +/-2 ℃ and 50 +/-5% of humidity, and then respectively testing oil on the forehead, the chin and the two side cheeks from 0 hour (before testing) to 4 hours (after testing), wherein the average of 10 persons is taken to obtain the following table. The test results are shown in Table 1.
TABLE 1 test results
As can be seen from the table 1, the oil-control facial cleanser disclosed by the invention has a good oil-control effect, and as can be seen from comparative examples 1-4, the oil-control effect can be influenced by different raw material proportions, wherein the example 1 is the optimal proportion and has the optimal oil-control effect; compared with comparative examples 1 to 4, the oil control effect can be obviously improved by adding the witch hazel extract, the brown algae extract and the retinol palmitate, wherein the influence of the brown algae extract is the largest, and the brown algae extract prepared by the method has a better oil control effect compared with the commercially available brown algae extract.
In light of the foregoing description of preferred embodiments according to the invention, it is clear that many changes and modifications can be made by the person skilled in the art without departing from the scope of the invention. The technical scope of the present invention is not limited to the contents of the specification, and must be determined according to the scope of the claims.
Claims (10)
1. The oil-control facial cleanser is characterized by being prepared from the following raw materials in parts by weight: 12-25 parts of surfactant, 3-6 parts of glycerol, 2-5 parts of Tween 60, 1-4 parts of butanediol, 1-3 parts of nicotinamide, 1-4 parts of Hamamelis virginiana extract, 1-4 parts of brown algae extract, 0.8-2 parts of jojoba oil, 0.5-1.5 parts of cetostearyl alcohol, 0.5-1.2 parts of retinol palmitate, 0.5-1 part of squalane, 0.4-0.8 part of hydrogenated lecithin, 0.2-1 part of thickener, 0.2-0.5 part of vitamin E, 0.04-0.08 part of sodium hyaluronate, 0.04-0.08 part of disodium edetate and 60-75 parts of deionized water.
2. The oil-control facial cleanser according to claim 1, wherein the oil-control facial cleanser is prepared from the following raw materials in parts by weight: 15-25 parts of surfactant, 3-5 parts of glycerol, 2-4 parts of Tween 60, 1-3 parts of butanediol, 1-2 parts of nicotinamide, 1-3 parts of Hamamelis virginiana extract, 1-3 parts of brown algae extract, 0.8-1.5 parts of jojoba oil, 0.5-1.2 parts of cetostearyl alcohol, 0.5-1 part of retinol palmitate, 0.5-0.8 part of squalane, 0.5-0.8 part of hydrogenated lecithin, 0.2-0.8 part of thickener, 0.2-0.4 part of vitamin E, 0.04-0.07 part of sodium hyaluronate, 0.04-0.06 part of disodium edetate and 60-70 parts of deionized water.
3. The oil-control facial cleanser according to claim 1, wherein the oil-control facial cleanser is prepared from the following raw materials in parts by weight: 18 parts of surfactant, 4 parts of glycerol, 2.5 parts of tween 60, 2 parts of butanediol, 1.5 parts of nicotinamide, 2 parts of witch hazel extract, 2 parts of brown algae extract, 1 part of jojoba oil, 1 part of cetostearyl alcohol, 0.8 part of retinol palmitate, 0.6 part of squalane, 0.5 part of hydrogenated lecithin, 0.4 part of thickening agent, 0.3 part of vitamin E, 0.05 part of sodium hyaluronate, 0.05 part of disodium ethylenediamine tetraacetic acid and 63.3 parts of deionized water.
4. An oil-controlling facial cleanser according to claim 1, characterized in that said surfactant consists of cocamidopropyl betaine, coconut monoethanolamide, sodium methylcocoyl taurate.
5. An oil-controlling facial cleanser according to claim 1, wherein said surfactant is prepared from cocamidopropyl betaine, coconut monoethanolamide, sodium methylcocoyl taurate in a weight ratio of 9: 8: 1.
6. An oil-controlling facial cleanser according to claim 1, wherein said thickener is one of xanthan gum, carboxymethyl cellulose and inorganic salt.
7. The oil-control facial cleanser of claim 1, wherein the brown algae extract is prepared by the following steps: cleaning fresh brown algae, drying, crushing to 50-100 meshes to obtain brown algae powder, adding the brown algae powder and mixed enzyme into deionized water, stirring for 60-100 min in a water bath at 55-65 ℃ at a rotating speed of 60-150 rpm, adding the stirred liquid into absolute ethyl alcohol with the weight of 3-5 times of that of the liquid, performing ultrasonic treatment for 25-40 min at 500-800W, filtering, and drying to obtain the brown algae extract.
8. The oil-control facial cleanser according to claim 1, wherein the weight ratio of the brown algae powder, the mixed enzyme and the deionized water is 1: 0.01-0.04: 16-20, wherein the mixed enzyme is prepared from cellulase and pectinase according to a weight ratio of 1: 0.5 to 2.
9. The preparation method of the oil-control facial cleanser according to any one of claims 1 to 8, characterized by comprising the following steps:
(1) adding deionized water, hydrogenated lecithin, disodium ethylene diamine tetraacetate, sodium hyaluronate, a thickening agent, tween 60, jojoba oil and cetostearyl alcohol into a reaction kettle, heating to 75-85 ℃, and uniformly stirring;
(2) adding surfactant, glycerol and squalane, and stirring;
(3) cooling to 42-50 ℃, adding butanediol, nicotinamide, retinol palmitate and vitamin E, and uniformly stirring;
(4) and cooling to 35-40 ℃, adding the witch hazel extract and the brown algae extract, and uniformly stirring to obtain the oil-controlling facial cleanser.
10. The preparation method of the oil-control facial cleanser according to claim 9, wherein the stirring speed is 100-200 rpm.
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