CN104546610A - Anti-aging facial cleanser and preparation method thereof - Google Patents
Anti-aging facial cleanser and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an anti-aging facial cleanser and a preparation method thereof and relates to the technical field of cosmetics in daily-use chemical industry. The anti-aging facial cleanser is prepared from the following raw materials: surface active components comprising sodium lauroyl glutamate, cocamidopropyl betaine, coconut oil momoethanolamide and sodium methyl cocoyl taurate, waterborne components comprising glycerin, propylene glycol and 1,3-butanediol, nutrition components comprising hyaluronic acid, squalane, oil tea camellia extract and tea-seed protein hydrolysate, adjuvant components comprising citric acid, sodium chloride, essence and preservatives, and the balance of deionized water, totaling 100 parts. The method comprises the following preparation steps: (1) preparing materials; (2) preparing the surface active components; (3) preparing the waterborne components; (4) mixing the components; (5) homogenizing; and (6) mixing. The anti-aging facial cleanser has good moisturizing and nourishing effects, also has the characteristics of aging resistance and the like and is suitable to be used by people of different skins and different ages.
Description
Technical field
The present invention relates to the cosmetics processing technique field in daily-use chemical industry, particularly a kind of defying age cleansing milk and preparation method thereof.
Technical background
Skin clean is an important step in skin protection, dust in daily life, air atom etc. are all easily adsorbed in skin surface, blocking pore, cause various skin problem, especially along with the age increases, skin metabolism is slowed down, and uses the cleansing milk containing too much soap base composition or surfactant component cause skin water loss thus produce wrinkle, therefore a be suitable for skin crowd in ripe age can cleaning skin, can the cleansing milk of moisture-keeping crease-shedding be absolutely necessary again.Have some to possess the cleansing milk of senile-resistant efficacy on the market at present, but can find by analyzing its composition, all more rearward, its anti-aging effects declared remains to be discussed the rank of its aging ingredient in component list.In patented product, as Chinese patent (ZL201310708301.5) disclosed " defying age cleansing milk and preparation method thereof ", the mass ratio of each component is: Herba Houttuyniae 10 ~ 20 parts, citric acid 10 ~ 15 parts, cherry juice 10 ~ 15 parts, vitamin E 8 ~ 15 parts, 10 ~ 15 parts, lecithin, 10 ~ 18 parts, surfactant, deionized water 40 ~ 80 parts; Its preparation method comprises: pulverize after being dried by Herba Houttuyniae; Fructus Pruni pseudocerasi extracting juice; Add lecithin, Herba Houttuyniae and the surfactant reactor to deionized water in proportion, successively carry out stirring, heating up; Adding citric acid after cooling, stirs; Continue cooling, stir with cherry juice and vitamin E; Add deionized water and stirring, after being cooled to 38 DEG C, discharging can obtain this product; The preparation method of this invention is simple to operation; Its product is without any harmful chemical additive, naturally has no side effect, and has antidotal high-quality cleansing milk, can strengthen the immunity of skin after life-time service.And for example Chinese patent (ZL201210485253.3) disclosed " a kind of defying age cleansing milk ", be made up of according to parts by weight following component: Aloe 12-14 part, Radix Ginseng 11-14 part, tasteless mineral oil 8-15 part, ammonium hydroxide 6-13 part, HANSHENGJIAO 7-12 part, Oleum menthae 6-10 part, surplus is water; This invention has effect of slow down aging, and has the various active such as antiinflammatory, antiallergic, free radical resisting and antioxidation, is especially applicable to allergy, long small pox, the problematic skin quality of acne class.Supplement the nutrient needed for skin, after washing, make face skin moisten bright and clean, soft smooth.
Technology contents
The object of the present invention is to provide a kind of existing good moisturizing, moisturizing effect, there is again the facial cleansing product of senile-resistant efficacy; Meanwhile, also its preparation method is provided.
For achieving the above object, the technical solution used in the present invention is a kind of defying age cleansing milk of invention, is be prepared from by following raw material by weight:
Surface active composition:
Sodium lauroyl glutamate 1-10 cocamido propyl betaine 1-5
Coconut monoethanol amide 1-3 sodium methyl cocoyl taurate 1-10;
Aqueous components:
Glycerol 1-5 propylene glycol 1-5 1,3 butanediol 1-5;
Nutrition composition:
Hyaluronic acid 0.1-0.5 squalane 0.1-1
Camellia Leaves extract 1-10 camellia oleosa seed protein hydrolyzate 1-10;
Aid component:
Citric acid 0.1-0.5 sodium chloride 0.1-1 essence 0.05-0.2
Antiseptic 0.1-0.5;
Surplus is deionized water, adds up to 100 parts.
Described Camellia Leaves extract is prepared from as follows: choose fresh, healthy free of contamination oil tea Lao Ye, and dry at 40-50 DEG C to moisture lower than 10%, then pulverize, 50-70 mesh sieve, obtains oil tea Lao Ye powder excessively; Thereafter, add according to every 50g oil tea Lao Ye powder the ratio that volumetric concentration is the edible ethanol 350-450ml of 60-80%, filter after water-bath reflux, extract, 2-4h at 80-90 DEG C; Its filtering residue adds according to former every 50g oil tea Lao Ye powder the ratio that volumetric concentration is the edible ethanol 150-250ml of 60-80% again, and filters after water-bath reflux, extract, 0.5-1.5h at 80-90 DEG C; Merge twice filtrate, obtain Camellia Leaves extracting solution; Again Camellia Leaves extracting solution is evaporated to the 20-50% of original volume, obtains Camellia Leaves extract, under being stored in aseptic condition.
Described camellia oleosa seed protein hydrolyzate is prepared from as follows: will remove the tea dregs of rice after Residual oil, pulverize, cross 70-90 mesh sieve, deionized water is added according to the feed liquid weight ratio of 1:8-12, by alkali (alkali adopted is sodium hydroxide or potassium hydroxide or sodium carbonate or potassium carbonate or other inorganic base) aqueous solution adjust ph to 9-11, then lixiviate 1.5-3h under 30-50 DEG C of condition, centrifugal treating under 3000-5000r/min condition again, get supernatant, and by acid (acid adopted is hydrochloric acid or sulphuric acid or other mineral acid) aqueous solution adjust ph to 4-5, obtain camellia oleosa seed protein hydrolyzate.
Meanwhile, also provide a kind of preparation method of defying age cleansing milk, its preparation process is as follows:
(i), get the raw materials ready: according to said ratio, get each raw material respectively, for subsequent use;
(ii), surface active composition preparation:
First the sodium lauroyl glutamate in surface active composition for subsequent use is joined in deionized water for subsequent use, be stirred to and be uniformly dissolved; Then add cocamido propyl betaine for subsequent use and coconut monoethanol amide, be stirred to dissolving; Regulate its pH value to be 6-7 with the citric acid in aid component for subsequent use again, and add sodium methyl cocoyl taurate, be stirred to dissolving, obtain component A, for subsequent use;
(iii), aqueous components preparation:
By the glycerol in aqueous components for subsequent use, propylene glycol 1-5 and 1,3 butanediol aqueous components mixed dissolutions, obtain B component, for subsequent use;
(iv), component mixing: mixed with B component by component A for subsequent use, stirring 2-10min, obtains blending ingredients, for subsequent use;
(v), homogenizing: by blending ingredients for subsequent use with the ramp of 4-6 DEG C/min to 70-80 DEG C, then, stir under the condition of 10-20r/min and keep this temperature 5-10min, obtaining homogenizing component, for subsequent use;
(vi), mix: the sodium chloride in aid component for subsequent use is joined in homogenizing component for subsequent use, stir under the condition of 20-50r/min, its temperature is made to be down to 50-60 DEG C, then the hyaluronic acid in nutrition composition for subsequent use, squalane, Camellia Leaves extract and camellia oleosa seed protein hydrolyzate is added, and under the condition of 10-20r/min, continue stirring until temperature be down to 40-50 DEG C, add the essence in aid component for subsequent use and antiseptic again, continue stirring until room temperature, defying age cleansing milk.
Defying age cleansing milk of the present invention, the main raw material(s) adopted comprises:
A, sodium lauroyl glutamate: amino acid surfactant;
B, cocamido propyl betaine: be a kind of zwitterionic surfactant, stimulate little, foaming power is strong;
C, coconut monoethanol amide: a kind of quaternary zwitterionic surfactant;
D, sodium methyl cocoyl taurate: the amino acid surfactant of natural origin;
E, propylene glycol: in the present invention with glycerol, 1,3 butanediols form aqueous components together;
F, glycerol: i.e. glycerol, the wetting agent in the present invention;
G, butanediol: have another name called 1,3-dihydroxy butane, the wetting agent in the present invention and solvent;
H, squalane: a kind of active component with good antioxygenic property, good to skin affinity, low stimulation;
I, Camellia Leaves extract: containing multiple flavone compound, have the effect of removing diphenylpicrylhydrazine free radical (DPPH);
J, camellia oleosa seed protein hydrolyzate: the hydrolyzed solution containing tea-seed peptide, has scavenging free radicals, antioxidative effect;
K, citric acid: regulate pH;
L, sodium chloride: regulate viscosity;
M, essence: give the fragrance that product is joyful, as geraniol, lilestralis, ionoionone and JSM-LAC (Z)-7-Decen-5-olide etc.;
N, antiseptic: be the inirritative compound of gentleness, as imidazolidinyl urea, Kazon and compound thereof.
Defying age cleansing milk of the present invention, adopt gentle amino acid surface active component, add the Camellia Leaves extract containing flavone compound, and the natural camellia oleosa seed protein hydrolyzate extracted from the tea dregs of rice, add the nutritional labeling with moistening effect and anti-oxidation efficacy simultaneously, while effectively clean skin, keep moisture of skin, and there is the effect of slowing down skin aging speed.
Defying age cleansing milk of the present invention carried out detecting and test:
Test data:
One, sanitary index and sense organ physical and chemical index
The every sanitary index of cleansing milk of the present invention and organoleptic indicator all meet the standard of GB/T29680-2013 cleansing milk, cleansing cream after testing.
Following table 1 is sanitary index and the sense organ physical and chemical index of defying age cleansing milk of the present invention.
The sanitary index of table 1 defying age cleansing milk of the present invention and sense organ physical and chemical index
Two, compliance test result test
Defying age cleansing milk of the present invention, verifies its effect by the moisture-keeping functions and the experiment of water loss barrier function measuring skin.
The moisture of 1 mensuration keratodermatitis
When the moisture of skin changes, the capacitance of skin changes, and thus can be carried out the change of analyzing skin surface moisture content by the change of Instrument measuring capacitance.
2 measure moisture through skin windage
Moisture is through skin windage (Transepidermal Water Loss, be called for short TEWL) be by the water vapor pressure gradient in the formation of nearly epidermis place test horny layer moisture loss, measure the water quantities through epidermis evaporation, thus investigate the situation of epiderm skin water loss.TEWL value is an important symbol that can be used for evaluating skin barrier quality, and numerical value is lower, and skin barrier effect is better, and vice versa.
3 tests
Test number is 20 people, and the age, between 25-50 year, is the women of skin health.
Test condition: test environment keeps stable temperature and humidity, sit quietly before first time test and to use after 30min moisture of skin measuring instrument and the moisture of skin tester that scatters and disappears to measure skin initial value, use product of the present invention to clean the numerical value of after face 1,3,5 hour.
4 test results
Test result is as shown in table 2:
The change of table 2 moisture content of skin and TEWL value
As shown in Table 2, use defying age cleansing milk of the present invention, can moisture content of skin be increased, and the water content of skin keeps stable after 1h, 3h, 5h of test, and exceed matched group.TEWL value can investigate the situation of epiderm skin water loss, and TEWL value reduction degree is larger, illustrates that moistening effect is better, helps skin barrier moisture loss effect better, can better maintain skin physiology function, delay skin aging.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplified, but protection scope of the present invention is not limited thereto.
Embodiment one:
The defying age cleansing milk of the present embodiment, be prepared from by surface active ingredient, aqueous components, nutrition composition and aid component, its preparation process is as follows:
(i), pretreatment of raw material:
1., Camellia Leaves extract preparation: choose fresh, healthy free of contamination oil tea Lao Ye, dry at 45 DEG C to moisture lower than 10%, then pulverize, 60 mesh sieves, obtain oil tea Lao Ye powder excessively; Thereafter, add according to every 50g oil tea Lao Ye powder the ratio that volumetric concentration is the edible ethanol 400ml of 70%, filter after water-bath reflux, extract, 3h at 85 DEG C; Its filtering residue adds according to former every 50g oil tea Lao Ye powder the ratio that volumetric concentration is the edible ethanol 200ml of 70% again, and filters after water-bath reflux, extract, 1h at 85 DEG C; Merge twice filtrate, obtain Camellia Leaves extracting solution; Again Camellia Leaves extracting solution is evaporated to 35% of original volume, obtains Camellia Leaves extract, under being stored in aseptic condition, for subsequent use.
2., camellia oleosa seed protein hydrolyzate preparation: will remove the tea dregs of rice after Residual oil, pulverize, cross 80 mesh sieves, add deionized water according to the feed liquid weight ratio of 1:10, regulate pH to 10 with sodium hydroxide solution, then lixiviate 2h under 40 DEG C of conditions, centrifugal treating under 4000r/min condition, gets supernatant again, and by hydrochloric acid solution adjust ph to 4.5, obtain camellia oleosa seed protein hydrolyzate, for subsequent use.
(ii), get the raw materials ready: according to weight portion, get following raw materials respectively:
Surface active ingredient: sodium lauroyl glutamate 10 parts, cocamido propyl betaine 1 part, coconut monoethanol amide 1 part, sodium methyl cocoyl taurate 5 parts;
Aqueous components: glycerol 5 parts, propylene glycol 2 parts, 1,3 butanediols 2 parts;
Nutrition composition: hyaluronic acid 0.1 part, squalane 0.1 part, Camellia Leaves extract 3 parts, camellia oleosa seed protein hydrolyzate 3 parts;
Aid component:
Citric acid 0.5 part, 0.5 part, sodium chloride, essence (can adopt geraniol, lilestralis, ionoionone and JSM-LAC (Z)-7-Decen-5-olide etc., the present embodiment adopts geraniol) 0.1 part and antiseptic (can adopt imidazolidinyl urea, Kazon and compound thereof etc., the present embodiment adopts imidazolidinyl urea) 0.3 part, surplus is deionized water, adds up to 100 parts.
(iii), preparation process:
1., surface active composition preparation:
First the sodium lauroyl glutamate in surface active composition for subsequent use is joined in deionized water for subsequent use, be stirred to and be uniformly dissolved; Then add cocamido propyl betaine for subsequent use and coconut monoethanol amide, be stirred to dissolving; Regulate its pH value to be 6.5 with the citric acid in aid component for subsequent use again, and add sodium methyl cocoyl taurate, be stirred to dissolving, obtain component A, for subsequent use;
2., aqueous components preparation:
By the glycerol in aqueous components for subsequent use, propylene glycol 1-5 and 1,3 butanediol aqueous components mixed dissolutions, obtain B component, for subsequent use;
3., component mixing: mixed with B component by component A for subsequent use, stirring 8min, obtains blending ingredients, for subsequent use;
4., homogenizing: by blending ingredients for subsequent use with the ramp to 75 DEG C of 5 DEG C/min, then, stir under the condition of 15r/min and keep this temperature 8min, obtaining homogenizing component, for subsequent use;
5., mix: the sodium chloride in aid component for subsequent use is joined in homogenizing component for subsequent use, stir under the condition of 35r/min, its temperature is made to be down to 55 DEG C, then the hyaluronic acid in nutrition composition for subsequent use, squalane, Camellia Leaves extract and camellia oleosa seed protein hydrolyzate is added, and under the condition of 15r/min, continue stirring until temperature be down to 45 DEG C, add the essence in aid component for subsequent use and antiseptic again, continue stirring until room temperature, defying age cleansing milk.
Defying age cleansing milk of the present invention, using method is: get appropriate cleansing milk, in face clean 3min gently after dense lather of getting blisters out, cleans with proper amount of clear water, is suitable for ripe skin crowd use in age.
Embodiment two:
The present embodiment is substantially identical with embodiment one, is material preparation step difference wherein;
(ii), get the raw materials ready: according to weight portion, get following raw materials respectively:
Surface active ingredient: sodium lauroyl glutamate 8 parts, cocamido propyl betaine 3 parts, coconut monoethanol amide 3 parts, sodium methyl cocoyl taurate 1 part;
Aqueous components: glycerol 1 part, propylene glycol 5 parts, 1,3 butanediols 5 parts;
Nutrition composition: hyaluronic acid 0.5 part, squalane 0.2 part, Camellia Leaves extract 10 parts, camellia oleosa seed protein hydrolyzate 10 parts;
Aid component:
Citric acid 0.3 part, 0.6 part, sodium chloride, lilestralis 0.1 part and Kazon 0.4 part, surplus is deionized water, and add up to 100 parts, other is identical with embodiment one.
Embodiment three:
The present embodiment is substantially identical with embodiment one, is material preparation step difference wherein;
(ii), get the raw materials ready: according to weight portion, get following raw materials respectively:
Surface active ingredient: sodium lauroyl glutamate 5 parts, cocamido propyl betaine 3 parts, coconut monoethanol amide 2 parts, sodium methyl cocoyl taurate 5 parts;
Aqueous components: glycerol 3 parts, propylene glycol 2 parts, 1,3 butanediols 3 parts;
Nutrition composition: hyaluronic acid 0.3 part, squalane 0.5 part, Camellia Leaves extract 8 parts, camellia oleosa seed protein hydrolyzate 6 parts;
Aid component:
Citric acid 0.2 part, 0.5 part, sodium chloride, ionoionone 0.15 part and imidazolidinyl urea 0.3 part, surplus is deionized water, and add up to 100 parts, other is identical with embodiment one.
Embodiment four:
The present embodiment is substantially identical with embodiment one, is material preparation step difference wherein;
(ii), get the raw materials ready: according to weight portion, get following raw materials respectively:
Surface active ingredient: sodium lauroyl glutamate 10 parts, cocamido propyl betaine 5 parts, coconut monoethanol amide 3 parts, sodium methyl cocoyl taurate 10 parts;
Aqueous components: glycerol 5 parts, propylene glycol 5 parts, 1,3 butanediols 4 parts;
Nutrition composition: hyaluronic acid 0.5 part, squalane 1.0 parts, Camellia Leaves extract 10 parts, camellia oleosa seed protein hydrolyzate 10 parts;
Aid component:
Citric acid 0.5 part, 0.9 part, sodium chloride, JSM-LAC (Z)-7-Decen-5-olide 0.15 part and Kazon 0.5 part, surplus is deionized water, and add up to 100 parts, other is identical with embodiment one.
Defying age cleansing milk of the present invention, is suitable for crowd's use of different skin quality, all ages and classes.
Claims (4)
1. a defying age cleansing milk, it is characterized in that being prepared from by following raw material by weight:
Surface active composition:
Sodium lauroyl glutamate 1-10 cocamido propyl betaine 1-5
Coconut monoethanol amide 1-3 sodium methyl cocoyl taurate 1-10;
Aqueous components:
Glycerol 1-5 propylene glycol 1-5 1,3 butanediol 1-5;
Nutrition composition:
Hyaluronic acid 0.1-0.5 squalane 0.1-1
Camellia Leaves extract 1-10 camellia oleosa seed protein hydrolyzate 1-10;
Aid component:
Citric acid 0.1-0.5 sodium chloride 0.1-1 essence 0.05-0.2
Antiseptic 0.1-0.5;
Surplus is deionized water, adds up to 100 parts.
2. defying age cleansing milk according to claim 1, it is characterized in that, described Camellia Leaves extract is prepared from as follows: choose fresh, healthy free of contamination oil tea Lao Ye, dry to moisture lower than 10% at 40-50 DEG C, then pulverize, cross 50-70 mesh sieve, obtain oil tea Lao Ye powder; Thereafter, add according to every 50g oil tea Lao Ye powder the ratio that volumetric concentration is the edible ethanol 350-450ml of 60-80%, filter after water-bath reflux, extract, 2-4h at 80-90 DEG C; Its filtering residue adds according to former every 50g oil tea Lao Ye powder the ratio that volumetric concentration is the edible ethanol 150-250ml of 60-80% again, and filters after water-bath reflux, extract, 0.5-1.5h at 80-90 DEG C; Merge twice filtrate, obtain Camellia Leaves extracting solution; Again Camellia Leaves extracting solution is evaporated to the 20-50% of original volume, obtains Camellia Leaves extract, under being stored in aseptic condition.
3. defying age cleansing milk according to claim 1, it is characterized in that, described camellia oleosa seed protein hydrolyzate is prepared from as follows: will remove the tea dregs of rice after Residual oil, pulverizes, cross 70-90 mesh sieve, deionized water is added according to the feed liquid weight ratio of 1:8-12, by aqueous alkali adjust ph to 9-11, then lixiviate 1.5-3h under 30-50 DEG C of condition, centrifugal treating again, get supernatant, and by aqueous acid adjust ph to 4-5, obtain camellia oleosa seed protein hydrolyzate.
4. the preparation method of defying age cleansing milk according to any one of claim 1-3, is characterized in that preparation process is as follows:
(i), get the raw materials ready: according to said ratio, get each raw material respectively, for subsequent use;
(ii), surface active composition preparation:
First the sodium lauroyl glutamate in surface active composition for subsequent use is joined in deionized water for subsequent use, be stirred to and be uniformly dissolved; Then add cocamido propyl betaine for subsequent use and coconut monoethanol amide, be stirred to dissolving; Regulate its pH value to be 6-7 with the citric acid in aid component for subsequent use again, and add sodium methyl cocoyl taurate, be stirred to dissolving, obtain component A, for subsequent use;
(iii), aqueous components preparation:
By the glycerol in aqueous components for subsequent use, propylene glycol 1-5 and 1,3 butanediol aqueous components mixed dissolutions, obtain B component, for subsequent use;
(iv), component mixing: mixed with B component by component A for subsequent use, stirring 2-10min, obtains blending ingredients, for subsequent use;
(v), homogenizing: by blending ingredients for subsequent use with the ramp of 4-6 DEG C/min to 70-80 DEG C, then, stir and keep this temperature 5-10min, obtaining homogenizing component, for subsequent use;
(vi), mix: the sodium chloride in aid component for subsequent use is joined in homogenizing component for subsequent use, stir, its temperature is made to be down to 50-60 DEG C, then the hyaluronic acid in nutrition composition for subsequent use, squalane, Camellia Leaves extract and camellia oleosa seed protein hydrolyzate is added, and continue stirring until temperature and be down to 40-50 DEG C, add the essence in aid component for subsequent use and antiseptic again, continue stirring until room temperature, defying age cleansing milk.
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| CN108743483A (en) * | 2018-07-26 | 2018-11-06 | 贵州夜郎古国生物科技有限公司 | A kind of camellia oil moisturizing liquid and preparation method |
| CN109135974A (en) * | 2018-08-21 | 2019-01-04 | 广州人为峰生物科技有限公司 | A kind of bee venom beauty handmade soap and preparation method thereof |
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| CN106473992A (en) * | 2016-12-10 | 2017-03-08 | 珍尔姿（广州）化妆品有限公司 | A kind of facial milk cleanser with crease-resistant effect |
| CN106943323A (en) * | 2017-05-09 | 2017-07-14 | 南通千竹电子科技有限公司 | A kind of balance skin pH value mildy wash and preparation method thereof |
| CN108743483A (en) * | 2018-07-26 | 2018-11-06 | 贵州夜郎古国生物科技有限公司 | A kind of camellia oil moisturizing liquid and preparation method |
| CN109135974A (en) * | 2018-08-21 | 2019-01-04 | 广州人为峰生物科技有限公司 | A kind of bee venom beauty handmade soap and preparation method thereof |
| CN109135974B (en) * | 2018-08-21 | 2020-08-11 | 广州人为峰生物科技有限公司 | Bee venom beauty handmade soap and preparation method thereof |
| CN111358726A (en) * | 2020-04-29 | 2020-07-03 | 海口楠脂香业有限公司 | Agilawood face cleanser and preparation method thereof |
| CN111358726B (en) * | 2020-04-29 | 2021-09-21 | 海口楠脂香业有限公司 | Agilawood face cleanser and preparation method thereof |
| CN112120985A (en) * | 2020-10-22 | 2020-12-25 | 广州科盈化妆品有限公司 | Oil-control facial cleanser and preparation method thereof |
| WO2022127421A1 (en) * | 2020-12-15 | 2022-06-23 | 上海家化联合股份有限公司 | Cleaning composition |
| CN115364013A (en) * | 2022-08-31 | 2022-11-22 | 湖南大三湘茶油股份有限公司 | Oil tea extract, preparation method and application in cosmetic raw materials |
| CN115364013B (en) * | 2022-08-31 | 2023-08-29 | 湖南大三湘茶油股份有限公司 | Oil tea leaf extract, preparation method and application thereof in cosmetic raw materials |
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