CN111358726B - Agilawood face cleanser and preparation method thereof - Google Patents
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Abstract
The invention provides agilawood face cleansing milk and a preparation method thereof. The agilawood face cleanser disclosed by the invention has the advantages of small skin irritation, fresh and cool skin feeling after use, no tightness, no greasiness, good foamability, rich, fine and stable foam, good cleaning force and good face cleaning effect.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to agilawood face cleanser and a preparation method thereof.
Background
The amino acid facial cleanser is a non-soap base type facial cleanser mainly comprising amino acid surfactants, is usually weakly acidic, is close to the pH value of human skin, has little irritation to the skin, has the effects of moisturizing, moistening and the like, and is popular among consumers in recent years. The amino acid facial cleanser sold on the market at present generally has the problems of poor foaming property, insufficient cleaning strength and the like. Since the improvement of the foaming property of the amino acid facial cleanser is likely to increase the irritation of the amino acid facial cleanser, the preparation of the amino acid facial cleanser with good foaming property and low irritation is a difficult problem to overcome.
Researches show that the agilawood extract can effectively inhibit the decomposition of hyaluronic acid and has a moisturizing effect on skin, and in addition, the antibacterial and antibacterial effects and the special fragrance of the agilawood extract make the agilawood extract especially suitable for face cleaning products. At present, the agilawood face cleaning milk on the market is few, and the agilawood face cleaning milk is researched and developed, maintains the low irritation of amino acid face cleaning milk, has good foamability and high cleaning force, and is particularly suitable for popularization and use on the market.
Disclosure of Invention
In view of the defects of the prior art, the invention provides agilawood face cleanser and a preparation method thereof.
The scheme of the invention comprises the following aspects:
the agilawood face cleanser comprises the following raw materials in percentage by mass:
the cleansing milk also contains 0.8-1.0% of at least one of centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract; and 0.3 to 0.5% of at least one of bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate; the balance being water.
Preferably, the agilawood face cleanser comprises the following raw materials in percentage by mass:
| raw materials | Content/% |
| Sodium lauroyl glutamate | 20.00 |
| Glycerol | 15.00 |
| Sodium lauroyl isethionate | 10.00 |
| PEG-5 lauryl alcohol citrate disodium sulfosuccinate | 5.00 |
| Decyl glucoside | 3.00 |
| Coconut oil acyl methyl taurine sodium taurate | 2.50 |
| Sodium hydroxide | 0.10 |
| Sodium chloride | 0.80 |
| PEG-150 distearate | 0.20 |
| Guar hydroxypropyl trimethyl ammonium chloride | 0.15 |
| Hydroxy phenyl methyl ester | 0.10 |
| Agilawood extract | 0.50 |
| Yeast extract | 0.80 |
| S. Ming-Shaw/radish root fermentation product filtrate | 0.80 |
| Stephania tetrandra extract | 0.80 |
The facial cleanser also contains 0.8% of herba Centellae root extract, rhizoma Polygoni Cuspidati root extract, Scutellariae radix root extract, folium Camelliae sinensis extract, radix Glycytthizae root extract, flos Matricariae Chamomillae extract and herba Rosmarini officinalis leaf extract; and 0.3% bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, and iodopropynyl butylcarbamate; the balance being water.
Preferably, the mass ratio of the asiatic centella root extract, the giant knotweed rhizome extract, the baical skullcap root extract, the tea leaf extract, the glabrous licorice root extract, the chamomile flower extract and the rosemary leaf extract is 7:1:1:3:4:1: 1.
Preferably, the mass ratio of the bis (hydroxymethyl) imidazolidinyl urea to the propylene glycol to the iodopropynyl butylcarbamate is 3:1: 2.
The invention also provides a preparation method of the agilawood face cleanser, which comprises the following steps:
1) dividing the raw materials into a material A, a material B, a material C and a material D;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, PEG-150 distearate, guar gum hydroxypropyl trimethyl ammonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, filtrate of fermentation product of Leuconostoc/radix Raphani, and radix Stephaniae Japonicae extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring and dissolving at 200-300 rpm for 20-25 minutes;
3) slowly cooling the product obtained in the step 2) to 45 +/-2 ℃, sequentially adding the material B, the material C and the material D, mixing and stirring at 200-300 rpm for 20-25 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Aiming at the stability problem of active ingredients, the invention provides a preparation method of an optimized agilawood face cleanser, which comprises the following steps:
1) dividing the raw materials into a material A, a material B, a material C, a material D and a material F;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, guar hydroxypropyl trimonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, tetrandra root extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
f, material: PEG-150 distearate, a filtrate of a fermentation product of Leuconostoc/radish root, a tea extract and a Glycyrrhiza glabra root extract; the mass ratio of the PEG-150 distearate to the water is 1 (5-7); heating water to 45 +/-2 ℃, adding PEG-150 distearate, stirring at 50-100 rpm for dissolving for 20-25 minutes, adjusting pH, adding a glycyrrhiza glabra root extract, uniformly mixing, adjusting pH, adding a leuconostoc/radish root fermentation product filtrate and a tea extract, uniformly mixing at 200-300 rpm, and keeping the temperature for later use;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring and dissolving at 200-300 rpm for 20-25 minutes;
3) slowly cooling the product obtained in the step 2) to 40-75 ℃, adding the material F, mixing uniformly, then sequentially adding the material B, the material C and the material D, mixing and stirring at 200-300 rpm for 20-25 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Preferably, the material F is added with the extract of the glycyrrhiza glabra root after the pH value is adjusted to 7.7-7.9, the mixture is uniformly mixed, the pH value is adjusted to 7.3-7.5, and the filtrate of the fermentation product of the leuconostoc/radish root and the extract of the tea are added.
Compared with the prior art, the invention has the beneficial effects that:
the agilawood face cleanser disclosed by the invention has the advantages of small skin irritation, fresh and cool skin feeling after use, no tightness, no greasiness, good foamability, rich, fine and stable foam, good cleaning force and good face cleaning effect.
The invention also improves the preparation method, firstly, the glycyrrhiza glabra root extract, PEG-150 distearate, the filtrate of the fermentation product of the staphylococcus aureus/radish root and the tea extract form a stable structure, and then the glycyrrhiza glabra root extract with the stable structure is mixed with other surfactants, plant extracts, preservatives and the like according to the colloid theory, so that the glycyrrhiza glabra root extract can be processed in a larger temperature range, the condition limitation of product processing is reduced, and the product stability is good.
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FIG. 1: and (5) a statistical graph of the detection result of the foaming performance.
Detailed Description
In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.
The raw materials used by the facial cleanser are all materials which are commercially available and meet the standards of raw materials of cosmetics.
Examples 1 to 3
The agilawood face cleanser comprises the following raw materials:
the mass ratio of the asiatic centella root extract to the giant knotweed rhizome extract to the baical skullcap root extract to the tea leaf extract to the glabrous root extract to the chamomile flower extract to the rosemary leaf extract is 7:1:1:3:4:1: 1.
The mass ratio of the bis (hydroxymethyl) imidazolidinyl urea to the propylene glycol to the iodopropynyl butylcarbamate is 3:1: 2.
Examples 1-3 methods of making facial cleansers:
1) dividing the raw materials into a material A, a material B, a material C and a material D;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, PEG-150 distearate, guar gum hydroxypropyl trimethyl ammonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, filtrate of fermentation product of Leuconostoc/radix Raphani, and radix Stephaniae Japonicae extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring at 200rpm for dissolving for 25 minutes;
3) slowly cooling the product obtained in the step 2) to 45 +/-2 ℃, sequentially adding the material B, the material C and the material D, mixing and stirring at 200rpm for 25 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Example 4
The main differences between example 4 and example 1 are:
the preparation method of the facial cleanser comprises the following steps:
1) dividing the raw materials into a material A, a material B, a material C and a material D;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, PEG-150 distearate, guar gum hydroxypropyl trimethyl ammonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, filtrate of fermentation product of Leuconostoc/radix Raphani, and radix Stephaniae Japonicae extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring at 300rpm for dissolving for 20 minutes;
3) slowly cooling the product obtained in the step 2) to 45 +/-2 ℃, sequentially adding the material B, the material C and the material D, mixing and stirring at 300rpm for 20 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Example 5
The difference between this example and example 1 is:
the preparation method of the agilawood face cleanser comprises the following steps:
1) dividing the raw materials into a material A, a material B, a material C, a material D and a material F;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, guar hydroxypropyl trimonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, tetrandra root extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
f, material: PEG-150 distearate, a filtrate of a fermentation product of Leuconostoc/radish root, a tea extract and a Glycyrrhiza glabra root extract; the mass ratio of the PEG-150 distearate to the water is 1: 7; heating water to 45 + -2 deg.C, adding PEG-150 distearate, stirring at 100rpm for 20 min to dissolve, adjusting pH to 7.7, adding Glycyrrhrizae radix extract, mixing, adjusting pH to 7.3, adding filtrate of fermentation product of Leuconostoc/radix Raphani and folium Camelliae sinensis extract, mixing at 300rpm, and keeping the temperature;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring at 300rpm for dissolving for 20 minutes;
3) slowly cooling the product obtained in the step 2) to 75 ℃, firstly adding the material F, uniformly mixing, then sequentially adding the material B, the material C and the material D, mixing and stirring at 300rpm for 20 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Example 6
The difference between this example and example 5 is:
the preparation method of the agilawood face cleanser comprises the following steps:
1) dividing the raw materials into a material A, a material B, a material C, a material D and a material F;
a material: water, sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, guar hydroxypropyl trimonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, tetrandra root extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
f, material: PEG-150 distearate, a filtrate of a fermentation product of Leuconostoc/radish root, a tea extract and a Glycyrrhiza glabra root extract; the mass ratio of the PEG-150 distearate to the water is 1: 5; heating water to 45 + -2 deg.C, dissolving PEG-150 distearate at 50rpm for 25 min, adjusting pH to 7.9, adding Glycyrrhrizae radix extract, mixing, adjusting pH to 7.5, adding filtrate of fermentation product of Leuconostoc/radix Raphani and folium Camelliae sinensis extract, mixing at 200rpm, and keeping the temperature;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring at 200rpm for dissolving for 25 minutes;
3) slowly cooling the product obtained in the step 2) to 40 ℃, firstly adding the material F, uniformly mixing, then sequentially adding the material B, the material C and the material D, mixing and stirring at 200rpm for 25 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Example 7
The agilawood face cleanser comprises the following raw materials:
the preparation method of the facial cleanser comprises the following steps:
1) dividing the raw materials into a material A, a material B, a material C and a material D;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, PEG-150 distearate, guar gum hydroxypropyl trimethyl ammonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, lignum Aquilariae Resinatum extract, and radix Glycytthizae extract;
c, material C: yeast extract, filtrate of fermentation product of Leuconostoc/radix Raphani, and radix Stephaniae Japonicae extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring at 200rpm for dissolving for 25 minutes;
3) slowly cooling the product obtained in the step 2) to 45 +/-2 ℃, sequentially adding the material B, the material C and the material D, mixing and stirring at 200rpm for 25 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
Comparative example 1
The main differences between this comparative example and example 7 are:
PEG-5 lauryl alcohol citrate disodium sulfosuccinate was replaced with: cocoamidopropyl Betaine (Cocoamidopropyl Betaine)
The coconut oil acyl methyl taurine sodium taurate is replaced by: DISODIUM COCOAMPHODIACETATE (DISODIUM COCOAMPHODIACETATE)
Comparative example 2
The difference between this comparative example and example 7 is:
experimental example 1 measurement of foaming Properties
The foam testing method refers to GB/T29679 and 2013 shampoo and paste shampoo 6.2.6. The results are shown in Table 1 and FIG. 1.
TABLE 1
The results show that:
the cleansing milk obtained in examples 1 to 7 has a foam height of more than 60mm, good foamability, and a foam reduction rate of not more than 6.7% after foaming for 5min, which indicates that the foam stability is good. From the test results of example 7, it is found that the addition of plant extracts such as centella asiatica extract and tea extract is also advantageous for improving the foam stability of the face cleanser. The pH value of the amino acid facial cleanser in the comparative examples and the examples is 6.5-6.8, the product is mild, and the irritation to skin is low. In addition, all indexes of the facial cleanser in the embodiment meet the requirements of the national standard GB/T29680-2013.
Experimental example 2 facial cleanser glabridin detection
The method is slightly improved by referring to the existing high performance liquid chromatography determination.
A sample to be tested: taking 0.5g of sample to be tested, adding about 7mL of 50% methanol aqueous solution into a 20mL centrifuge tube with a plug, shaking up, ultrasonically extracting for 15min, fixing the volume to 10mL, centrifuging at 8000rpm, taking supernatant, filtering with a filter membrane, and taking filtrate for later use. The sample to be tested is ready for use.
Blank: the samples to which no glabrous greenbrier rhizome extract was added in each example and comparative example were prepared in the same manner as the test samples.
Comparison: taking the extract of the raw material glycyrrhiza glabra root, and preparing the extract into a solution with the same glabridin concentration according to the preparation method of a test sample.
Chromatographic conditions are as follows: agilent Eclipse chromatography column (100 mm. times.2.1 mm, 1.8 μm); the flow rate is 0.3 mL/min; the column temperature is 30 ℃; the sample volume is 50 mu L; mobile phase: 60% by volume aqueous methanol solution (containing 0.1% by volume of phosphoric acid); the detection wavelength is 280 nm.
3 batches were produced for each sample, and the mean value was taken 3 times for each batch. If the blank peak appears, the area of the blank peak is firstly corrected by the area of the blank peak. The relative decomposition rate was calculated from the peak areas of the test sample and the control. The results are shown in Table 2.
The relative decomposition rate of glabridin is (peak area of glabridin in control-area of glabridin peak in test sample)/area of glabridin peak in control.
TABLE 2
The results show that:
the relative decomposition rate of glabridin is low in examples 1 to 7, and particularly when the preparation methods of example 5 and example 6 are adopted, the relative decomposition rate of glabridin is obviously reduced, which shows that the method is favorable for improving the stability of glabridin.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (3)
1. The agilawood face cleanser is characterized by comprising the following raw materials in percentage by mass:
Also contains 0.8 wt% of centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract; and 0.3% by mass of bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, and iodopropynyl butylcarbamate; the balance being water;
the mass ratio of the asiatic centella root extract to the giant knotweed rhizome extract to the baical skullcap root extract to the tea leaf extract to the glabrous root extract to the chamomile flower extract to the rosemary leaf extract is 7:1:1:3:4:1: 1;
the mass ratio of the bis (hydroxymethyl) imidazolidinyl urea to the propylene glycol to the iodopropynyl butylcarbamate is 3:1: 2.
2. The preparation method of the agilawood face cleanser of claim 1, which is characterized by comprising the following steps of:
1) dividing the raw materials into a material A, a material B, a material C, a material D and a material F;
a material: sodium lauroyl glutamate, glycerol, sodium lauroyl isethionate, disodium PEG-5 lauryl citrate sulfosuccinate, decyl glucoside, sodium cocoyl methyl taurate, guar hydroxypropyl trimonium chloride, and methylparaben;
b, material B: sodium hydroxide, sodium chloride, agilawood extract, centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, chamomile flower extract and rosemary leaf extract;
c, material C: yeast extract, tetrandra root extract;
d, material: bis (hydroxymethyl) imidazolidinyl urea, propylene glycol, iodopropynyl butylcarbamate;
f, material: PEG-150 distearate, a filtrate of a fermentation product of Leuconostoc/radish root, a tea extract and a Glycyrrhiza glabra root extract; the mass ratio of the PEG-150 distearate to the water is 1 (5-7); heating water to 45 +/-2 ℃, adding PEG-150 distearate, stirring at 50-100 rpm for dissolving for 20-25 minutes, adjusting pH, adding a glycyrrhiza glabra root extract, uniformly mixing, adjusting pH, adding a leuconostoc/radish root fermentation product filtrate and a tea extract, uniformly mixing at 200-300 rpm, and keeping the temperature for later use;
2) heating water to 85 +/-5 ℃, adding the material A, and stirring and dissolving at 200-300 rpm for 20-25 minutes;
3) cooling the product obtained in the step 2) to 40-75 ℃, adding the material F, mixing uniformly, then adding the material B, the material C and the material D in sequence, mixing and stirring at 200-300 rpm for 20-25 minutes, filtering, inspecting, filling, packaging, inspecting and warehousing.
3. The preparation method of the agilawood face wash according to claim 2, wherein the material F is added with the extract of the glycyrrhiza glabra root after the pH is adjusted to 7.7-7.9, the mixture is uniformly mixed and adjusted to have the pH of 7.3-7.5, and the filtrate of the fermentation product of the leuconostoc/radish root and the extract of the tea leaves are added.
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Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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