CN109135974A - A kind of bee venom beauty handmade soap and preparation method thereof - Google Patents
A kind of bee venom beauty handmade soap and preparation method thereof Download PDFInfo
- Publication number
- CN109135974A CN109135974A CN201810956421.XA CN201810956421A CN109135974A CN 109135974 A CN109135974 A CN 109135974A CN 201810956421 A CN201810956421 A CN 201810956421A CN 109135974 A CN109135974 A CN 109135974A
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- parts
- bee venom
- oil
- handmade soap
- beauty
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- 239000003659 bee venom Substances 0.000 title claims abstract description 82
- 239000000344 soap Substances 0.000 title claims abstract description 80
- 230000003796 beauty Effects 0.000 title claims abstract description 67
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 54
- 240000001432 Calendula officinalis Species 0.000 claims abstract description 37
- 239000000284 extract Substances 0.000 claims abstract description 29
- 239000003531 protein hydrolysate Substances 0.000 claims abstract description 27
- AJBZENLMTKDAEK-UHFFFAOYSA-N 3a,5a,5b,8,8,11a-hexamethyl-1-prop-1-en-2-yl-1,2,3,4,5,6,7,7a,9,10,11,11b,12,13,13a,13b-hexadecahydrocyclopenta[a]chrysene-4,9-diol Chemical compound CC12CCC(O)C(C)(C)C1CCC(C1(C)CC3O)(C)C2CCC1C1C3(C)CCC1C(=C)C AJBZENLMTKDAEK-UHFFFAOYSA-N 0.000 claims abstract description 25
- 235000003880 Calendula Nutrition 0.000 claims abstract description 25
- 239000008169 grapeseed oil Substances 0.000 claims abstract description 22
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims abstract description 19
- 241000241413 Propolis Species 0.000 claims abstract description 19
- 239000003240 coconut oil Substances 0.000 claims abstract description 19
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 19
- 229940069949 propolis Drugs 0.000 claims abstract description 19
- 229940083466 soybean lecithin Drugs 0.000 claims abstract description 19
- 235000019482 Palm oil Nutrition 0.000 claims abstract description 18
- 235000012907 honey Nutrition 0.000 claims abstract description 18
- 239000002540 palm oil Substances 0.000 claims abstract description 18
- 229940109850 royal jelly Drugs 0.000 claims abstract description 18
- 239000004006 olive oil Substances 0.000 claims abstract description 15
- 235000008390 olive oil Nutrition 0.000 claims abstract description 15
- 244000269722 Thea sinensis Species 0.000 claims abstract 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 22
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 13
- 239000003513 alkali Substances 0.000 claims description 13
- 239000003995 emulsifying agent Substances 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 235000005881 Calendula officinalis Nutrition 0.000 claims description 12
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 12
- 239000011265 semifinished product Substances 0.000 claims description 10
- 239000004094 surface-active agent Substances 0.000 claims description 10
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000005119 centrifugation Methods 0.000 claims description 5
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- 238000005345 coagulation Methods 0.000 claims description 5
- 239000003921 oil Substances 0.000 claims description 5
- 235000019198 oils Nutrition 0.000 claims description 5
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 5
- 229920000053 polysorbate 80 Polymers 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 238000010257 thawing Methods 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 4
- 235000021355 Stearic acid Nutrition 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical group CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 3
- 229940045944 sodium lauroyl glutamate Drugs 0.000 claims description 3
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims description 3
- 239000008117 stearic acid Substances 0.000 claims description 3
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 claims description 3
- 239000005639 Lauric acid Substances 0.000 claims description 2
- 239000000155 melt Substances 0.000 claims description 2
- 240000007817 Olea europaea Species 0.000 claims 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 235000021314 Palmitic acid Nutrition 0.000 claims 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims 1
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- 241000186427 Cutibacterium acnes Species 0.000 description 2
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- 238000001514 detection method Methods 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
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- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 description 1
- 206010027654 Allergic conditions Diseases 0.000 description 1
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- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 244000147568 Laurus nobilis Species 0.000 description 1
- 235000017858 Laurus nobilis Nutrition 0.000 description 1
- 235000021360 Myristic acid Nutrition 0.000 description 1
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 1
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- 125000003118 aryl group Chemical group 0.000 description 1
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- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
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- 235000013336 milk Nutrition 0.000 description 1
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- 235000016709 nutrition Nutrition 0.000 description 1
- 230000037312 oily skin Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- 230000017854 proteolysis Effects 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
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- -1 royal jelly Substances 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
Abstract
The invention discloses a kind of bee venom beauty handmade soaps and preparation method thereof.The handmade soap in parts by weight, including following components: 8~20 parts of olive oil, 24~38 parts of palm oil, 15~20 parts of coconut oil, 5~18 parts of glycerol, 1~4 part of honey, 8~20 parts of propolis, 2~5 parts of royal jelly, 0.5~4 part of bee venom, 5~10 parts of calendula extract, 0.2~3 part of soybean lecithin, 0.5~3 part of grape seed oil, 1~3 part of tea seed protein hydrolyzate.Complete square compatibility 5 of the present invention rationally, has played the effect of significant synergy, solves conventional method and selects coconut oil, palm oil as its base oil, easily causing cleaning, excessively there is the problem of dry and astringent, itch, excitement in skin, has strong cleaning force, it is not tightened after, it does not dry, does not stimulate mildly, dredge pore, the advantages of reducing allergy, the effect of having played active constituent well simultaneously, makes it have the function of preferable antibacterial, moisturizing, oil-control and bright color, application prospect is good.
Description
Technical field
The invention belongs to biomedicine technical fields.More particularly, to a kind of bee venom beauty handmade soap and its preparation side
Method.
Background technique
Occurs a kind of more popular handmade soap in recent years.Handmade soap refers to the perfumed soap that oneself DIY is worked it out, moulding
It is colourful, unlimited imagination space and Creative spaces are provided for people, and people can be allowed to give full play to the individual character of oneself, enjoyed
By the enjoyment of DIY, therefore gradually liked in recent years by people.But handmade soap product goes out to the greatest extent not thoroughly at present, it is effective
, do not have effect, mix the genuine with the fictitious, it is low that price has height to have, and difference is also very big, technical breakthrough, especially in using effect
On breakthrough, be that manufacturer and consumer pursue jointly.
Traditional handmade soap is analyzed from using, and cleaning force is good, will generally occur tight phenomenon, skin after
Skin is uncomfortable；It is not tightened after, general cleaning force is not very well that there are certain paradoxes again.Reach other sterilizations, protect
Wet, oil-control, bright color, mild not stimulus equivalence fruit, it is just more difficult.In addition, that there is also appearances is bad, foam is not thin
Greasy, not abundant etc. defect.From the selection of grease, usually as its base oil, coconut oil can be produced for selection coconut oil, palm oil
Raw foam abundant, degreasing power is strong, but also easily causes cleaning excessively, and the symptoms such as dry and astringent, itch, excitement occurs in skin, right
Damage is easily caused in sensitive skin type；Palm oil is that commonly filling is oily in soap, can increase finished product hardness, but its nutritional ingredient
Content is lower, is unfavorable for product and plays skin care effect.
Therefore, how the handmade soap formula of reasonable disposition science, exploitation and do not stretch tight at not only having strong cleaning force after
Tightly, it does not dry, does not stimulate mildly, there is preferable skin care effect, Manual perfumed soap safe to use to become soap production field
Research and development focus.
Summary of the invention
It is an object of the invention to overcome above-mentioned the deficiencies in the prior art, a kind of bee venom beauty handmade soap is provided.The bee
Malicious beauty handmade soap milk strong cleaning force, does not tighten after, does not dry, do not stimulate mildly, reduces allergy, there are also pore is dredged, resists
The effect of bacterium, moisturizing, bright color, oil-control.
The object of the present invention is to provide a kind of bee venom beauty handmade soaps.
It is a further object of the present invention to provide the preparation methods of above-mentioned bee venom beauty handmade soap.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
A kind of bee venom beauty handmade soap, in parts by weight, including following components: 8~20 parts of olive oil, palm oil 24~38
Part, 15~20 parts of coconut oil, 5~18 parts of glycerol, 1~4 part of honey, 8~20 parts of propolis, 2~5 parts of royal jelly, bee venom 0.5~4
Part, 5~10 parts of calendula extract, 0.2~3 part of soybean lecithin, 0.5~3 part of grape seed oil, tea seed protein hydrolyzate 1~3
Part.
Raw material propolis (Propolis) in the active constituent of bee venom beauty handmade soap of the invention is a kind of with fragrance
The colloidal solid object of smell, containing plurality of inorganic salt, vitamin, organic acid and fructose, glucose, reductase etc., have compared with
Strong antibacterial, anti-inflammatory activity, have very strong inhibition killing effect to fungi and germ etc., there is gentle beauty treatment, anti-inflammatory analgetic
Effect can be used for treating burn and scald, skin Tearing Pain or radiation protection.Bee venom is transparent yellowish liquid under native state
Body, bitter, toughness and special aromatic odor；It can promote body metabolism, enhance the disease resistance of body, play in vivo
The effect of immunizing agent, a few peoples' (accounting for about 2%) can cause allergic reaction to bee venom.Soybean lecithin is formed in skin surface and is protected
Film can effectively slow down skin stimulation and injury, reduce allergy, while effective component can also be made to permeate flesh bottom rapidly, help
Moisture quickly absorbs, and improves flesh bottom deep layer water shortage problem；Calendula extract, grape seed oil and tea seed proteolysis are added simultaneously
Liquid can more effectively play cosmetology effect；Above-mentioned raw materials share, and can be reduced allergic reaction caused by bee venom.
Preferably, the bee venom beauty handmade soap in parts by weight, including following components: 10~16 parts of olive oil, palm
Oil 25~30 parts, 17~19 parts of coconut oil, 10~15 parts of glycerol, 2~3 parts of honey, 10~15 parts of propolis, 3~4 parts of royal jelly,
1~2 part of bee venom, 6~8 parts of calendula extract, 0.5~2 part of soybean lecithin, 1~2.5 part of grape seed oil, tea seed albumen water
1.5~2.5 parts of liquid of solution.
It is highly preferred that the bee venom beauty handmade soap is in parts by weight, including following components: 12 parts of olive oil, palm oil
27 parts, 18 parts of coconut oil, 12 parts of glycerol, 2.5 parts of honey, 13 parts of propolis, 3.5 parts of royal jelly, 1.5 parts of bee venom, pot marigold extraction
7 parts of object, 1.8 parts of soybean lecithin, 1.8 parts of grape seed oil, 2 parts of tea seed protein hydrolyzate.
Preferably, the bee venom beauty handmade soap further includes emulsifier, surfactant, alkali and solvent.
It is highly preferred that by weight, the bee venom beauty handmade soap further includes 1.5~3.5 parts of emulsifier, surface-active
1~2 part of agent, 3~8 parts of alkali, 20~45 parts of solvent.
It is further preferred that by weight, the bee venom beauty handmade soap further includes 2 parts of emulsifier, surface-active
1.5 parts of agent, 7 parts of alkali, 35 parts of solvent.
Most preferably, the bee venom beauty handmade soap in parts by weight, including following components: 12 parts of olive oil, palm oil
27 parts, 18 parts of coconut oil, 12 parts of glycerol, 2.5 parts of honey, 13 parts of propolis, 3.5 parts of royal jelly, 1.5 parts of bee venom, pot marigold extraction
7 parts of object, 1.8 parts of soybean lecithin, 1.8 parts of grape seed oil, 2 parts of tea seed protein hydrolyzate, 2 parts of emulsifier, surfactant 1.5
Part, 7 parts of alkali, 35 parts of solvent.
Preferably, the emulsifier is Tween-80 or Qula logical -100；The surfactant is stearic acid, laurel
One or more of acid, myristic acid, sodium lauroyl glutamate, sodium methyl cocoyl taurate；The alkali is hydroxide
Sodium or potassium hydroxide；The solvent is deionized water.
Preferably, the calendula extract be after adding pot marigold water to squeeze the juice be added in juice used water weight 5~
8 times of ethanol solution extracts 10~30min under the conditions of 60~70 DEG C, filters, and centrifugation obtains after concentration.
It is highly preferred that the calendula extract is that water weight used is added in juice after adding pot marigold water to squeeze the juice
6.5 times of ethanol solution extracts 20min under the conditions of 65 DEG C, filters, and centrifugation obtains after concentration.
Preferably, the mass concentration of the ethanol solution is 60%~75%.
Preferably, the tea seed protein hydrolyzate is prepared by following methods: by smashed tea seed cake and deionized water
It is mixed according to the weight ratio of 1:9~11, in 35~45 DEG C of 1.8~2.5h of extraction, centrifuging and taking supernatant, adjusting pH value to 4.8~
6.2, obtain tea seed protein hydrolyzate.
It is highly preferred that the weight ratio of tea seed cake and deionized water is 1:10.
It is highly preferred that the condition of extraction is 40 DEG C of extraction 2.2h.
It is highly preferred that adjusting pH value to 5.2.
The preparation method of the bee venom beauty handmade soap, comprising the following steps:
S1. weigh olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, emulsifier and
Surfactant makes its thawing after mixing, in 50~60 DEG C of heating；
S2. alkali is dissolved in solvent and obtains aqueous slkali, then the aqueous slkali is added to the solution after step S1 melts
In, stir 3~7min；
S3. glycerol, calendula extract, grape seed oil and tea seed protein hydrolyzate is added in 45~60 DEG C of stirrings, then holds
7~15min of continuous stirring, the semi-finished product being thoroughly mixed；Semi-finished product are poured into mold, after its coagulation forming, demoulding, i.e.,
The bee venom beauty handmade soap can be obtained.
Preferably, in step S1, in 55 DEG C of heating and meltings.
Preferably, in step S3, glycerol, calendula extract, grape seed oil and tea seed albumen water is added in 55 DEG C of stirrings
Solve liquid.
Preferably, in step S3, after glycerol, calendula extract, grape seed oil and tea seed protein hydrolyzate is added, sprinkling
Alcohol defoaming.
Squeezing, filtering, centrifugation and concentration for being related in the present invention etc. operation, be by this field conventional method into
Row, those skilled in the art can according to actual needs be adjusted the operating parameter of squeezing, filtering, centrifugation and concentration.
Compared with prior art, the invention has the following beneficial effects:
The present invention joined in handmade soap honey, propolis, royal jelly, bee venom, calendula extract, soybean lecithin,
Grape seed oil and tea seed protein hydrolyzate isoreactivity ingredient, complete square compatibility 5 rationally, have played the effect of significant synergy, solve
Conventional method of having determined selects coconut oil, palm oil as its base oil, and easily causing cleaning, excessively dry and astringent, itch, thorn occurs in skin
The advantages of the problem of excitation, has strong cleaning force, does not tighten, do not dry after, do not stimulate mildly, dredges pore, reduce allergy,
The effect of having played active constituent well simultaneously, makes it have the function of preferable antibacterial, moisturizing, oil-control and bright color.
Specific embodiment
Further illustrate the present invention below in conjunction with specific embodiment, but embodiment the present invention is not done it is any type of
It limits.Unless stated otherwise, the present invention uses reagent, method and apparatus is the art conventional reagents, method and apparatus.
Unless stated otherwise, following embodiment agents useful for same and material are commercially available.
1 bee venom beauty handmade soap of embodiment and preparation method thereof
1, it is formulated
The formula of the bee venom beauty handmade soap of the present embodiment is as shown in table 1.
The formula of 1 bee venom beauty handmade soap of table
2, the preparation method of the bee venom beauty handmade soap of the present embodiment, comprising the following steps:
(1) olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, Tween-80 are weighed
After mixing with stearic acid, make its thawing in 55 DEG C of heating；
(2) sodium hydroxide is dissolved in deionized water and obtains aqueous slkali, then the aqueous slkali is added to step (1) and is melted
In solution afterwards, 6min is stirred；
(3) glycerol, calendula extract, grape seed oil and tea seed protein hydrolyzate is added in 55 DEG C of stirrings, then persistently stirs
11min is mixed, the semi-finished product being thoroughly mixed；Semi-finished product are poured into mold, after its coagulation forming, demoulding be can be obtained
Bee venom beauty handmade soap；
Wherein, calendula extract is prepared by following methods: after pot marigold plus water juicing, institute being added in juice
With 6.5 times of water weight of 65% ethanol solution, 20min is extracted under the conditions of 65 DEG C, is filtered, is centrifuged, and concentration obtains pot marigold and mentions
Take object；
Tea seed protein hydrolyzate is prepared by following methods: by smashed tea seed cake and deionized water according to the weight of 1:10
Amount is than mixing, and in 40 DEG C of extraction 2.2h, centrifuging and taking supernatant adjusts pH value to 5.2, obtains tea seed protein hydrolyzate.
2 bee venom beauty handmade soap of embodiment and preparation method thereof
1, it is formulated
The formula of the bee venom beauty handmade soap of the present embodiment is as shown in table 2.
The formula of 2 bee venom beauty handmade soap of table
2, the preparation method of the bee venom beauty handmade soap of the present embodiment, comprising the following steps:
(1) weigh olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, Qula it is logical-
100 and lauric acid after mixing, make its thawing in 50 DEG C of heating；
(2) potassium hydroxide is dissolved in deionized water and obtains aqueous slkali, then the aqueous slkali is added to step (1) and is melted
In solution afterwards, 3min is stirred；
(3) glycerol, calendula extract, grape seed oil and tea seed protein hydrolyzate is added in 45 DEG C of stirrings, then persistently stirs
7min is mixed, the semi-finished product being thoroughly mixed；Semi-finished product are poured into mold, after its coagulation forming, bee is can be obtained in demoulding
Malicious beauty handmade soap；
Wherein, calendula extract is prepared by following methods: after pot marigold plus water juicing, institute being added in juice
With 5 times of water weight of 60% ethanol solution, 10min is extracted under the conditions of 60 DEG C, is filtered, is centrifuged, and concentration obtains pot marigold extraction
Object；
Tea seed protein hydrolyzate is prepared by following methods: by smashed tea seed cake and deionized water according to the weight of 1:9
Amount is than mixing, and in 35 DEG C of extraction 1.8h, centrifuging and taking supernatant adjusts pH value to 4.8, obtains tea seed protein hydrolyzate.
3 bee venom beauty handmade soap of embodiment and preparation method thereof
1, it is formulated
The formula of the bee venom beauty handmade soap of the present embodiment is as shown in table 3.
The formula of 3 bee venom beauty handmade soap of table
| Raw material serial number | Title | Parts by weight (part) | Use purpose |
| 1 | Olive oil | 16 | Base oil |
| 2 | Palm oil | 25 | Base oil |
| 3 | Coconut oil | 19 | Base oil |
| 4 | Glycerol | 10 | Moisturizer |
| 5 | Honey | 3 | Active constituent |
| 6 | Propolis | 10 | Active constituent |
| 7 | Royal jelly | 4 | Active constituent |
| 8 | Bee venom | 2 | Active constituent |
| 9 | Calendula extract | 6 | Active constituent |
| 10 | Soybean lecithin | 2 | Active constituent |
| 11 | Grape seed oil | 1 | Active constituent |
| 12 | Tea seed protein hydrolyzate | 2.5 | Active constituent |
| 13 | Tween-80 | 3.5 | Emulsifier |
| 14 | Myristic acid | 1 | Surfactant |
| 15 | Sodium hydroxide | 8 | Alkali |
| 16 | Deionized water | 20 | Solvent |
2, the preparation method of the bee venom beauty handmade soap of the present embodiment, comprising the following steps:
(1) olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, Tween-80 are weighed
After mixing with myristic acid, make its thawing in 60 DEG C of heating；
(2) sodium hydroxide is dissolved in deionized water and obtains aqueous slkali, then the aqueous slkali is added to step (1) and is melted
In solution afterwards, 7min is stirred；
(3) glycerol, calendula extract, grape seed oil and tea seed protein hydrolyzate is added in 60 DEG C of stirrings, then persistently stirs
15min is mixed, the semi-finished product being thoroughly mixed；Semi-finished product are poured into mold, after its coagulation forming, demoulding be can be obtained
Bee venom beauty handmade soap；
Wherein, calendula extract is prepared by following methods: after pot marigold plus water juicing, institute being added in juice
With 8 times of water weight of 75% ethanol solution, 30min is extracted under the conditions of 70 DEG C, is filtered, is centrifuged, and concentration obtains pot marigold extraction
Object；
Tea seed protein hydrolyzate is prepared by following methods: by smashed tea seed cake and deionized water according to the weight of 1:11
Amount is than mixing, and in 45 DEG C of extraction 2.5h, centrifuging and taking supernatant adjusts pH value to 6.2, obtains tea seed protein hydrolyzate.
4 bee venom beauty handmade soap of embodiment and preparation method thereof
1, it is formulated
The formula of the bee venom beauty handmade soap of the present embodiment is as shown in table 4.
The formula of 4 bee venom beauty handmade soap of table
| Raw material serial number | Title | Parts by weight (part) | Use purpose |
| 1 | Olive oil | 8 | Base oil |
| 2 | Palm oil | 38 | Base oil |
| 3 | Coconut oil | 15 | Base oil |
| 4 | Glycerol | 18 | Moisturizer |
| 5 | Honey | 1 | Active constituent |
| 6 | Propolis | 20 | Active constituent |
| 7 | Royal jelly | 2 | Active constituent |
| 8 | Bee venom | 0.5 | Active constituent |
| 9 | Calendula extract | 10 | Active constituent |
| 10 | Soybean lecithin | 0.2 | Active constituent |
| 11 | Grape seed oil | 3 | Active constituent |
| 12 | Tea seed protein hydrolyzate | 1 | Active constituent |
| 13 | Qula logical -100 | 1.5 | Emulsifier |
| 14 | Sodium lauroyl glutamate | 2 | Surfactant |
| 15 | Potassium hydroxide | 3 | Alkali |
| 16 | Deionized water | 45 | Solvent |
2, the preparation method of the bee venom beauty handmade soap of the present embodiment is same as Example 1.
5 bee venom beauty handmade soap of embodiment and preparation method thereof
1, it is formulated
The formula of the bee venom beauty handmade soap of the present embodiment is as shown in table 5.
The formula of 5 bee venom beauty handmade soap of table
2, the preparation method of the bee venom beauty handmade soap of the present embodiment is same as Example 1.
6 Formula Evaluation of embodiment
1, the Physico-chemical tests result of Examples 1 to 5 bee venom beauty handmade soap
(1) character
Bee venom beauty handmade soap of the invention is that stability is good, fragrant, fine and smooth uniform milky beauty soap.
(2) pH value inspection
The bee venom beauty handmade soap of Example 1~5 after being soaked with distilled water, is measured, measuring pH value is with pH test paper
Between 7.0~7.6.
2, the microorganism detection result of Examples 1 to 5 bee venom beauty handmade soap
6 microorganism detection result of table
3, irritation test, anaphylaxis experiment
Kunming small white mouse back is cut off into hair, smear respectively by Examples 1 to 5 preparation soaked with distilled water after bee venom
Beauty handmade soap is in cutting plucked position, and does not apply position and be not compared, as a result without irritation and allergic reaction.
Embodiment 7
1, bacteriostatic experiment
Propionibacterium acnes, staphylococcus epidermis and staphylococcus aureus are to lead acnegenic the main pathogenic fungi.Pass through
To the bacteriostatic experiment of these three bacteriums, the antibacterial anti-acne effect of different product can be evaluated.The present invention is using disk diffusion method to not
Fungistatic effect with product is evaluated.
(1) in the formula (being shown in Table 7) of the bee venom beauty handmade soap of comparative example 1~6 on the basis of 1 active constituent of embodiment
It is changed, other are as the formula of embodiment 1；Preparation method is same as Example 1.
The active constituent formula of the bee venom beauty handmade soap of 7 comparative example 1~6 of table
(2) bee venom beauty handmade soap Examples 1 to 5,1~6 product of comparative example and commercially available oil control and acne removal beauty are weighed respectively
Deionized water 50mL is added in each 5g of soap product, dissolves, and filtering takes filtrate spare (ready-to-use), by the diameter 6mm after sterilizing
Filter paper, with aseptic nipper clamping be immersed in sample liquid, take out, dry, be placed in sterile petri dish, with sterilize after life
Reason salt water makees negative control.200 μ L propionibacterium acnes, staphylococcus epidermis and staphylococcus aureus bacteria suspension are pipetted to admittedly
On body culture dish, uniformly, ready filter paper is affixed on culture dish for coating, and 37 DEG C of cultures 18~for 24 hours, observation is as a result, survey
Determine inhibition zone size, each sample sets 3 in parallel, and results are averaged.It the results are shown in Table 8.
(3) experimental result
8 bacteriostatic experiment result of table
The result shows that five bee venom beauty handmade soap products of Examples 1 to 5 are to acne propionic acid compared with comparative example 1~6
Three kinds of bacteriums such as bacillus, staphylococcus epidermis and staphylococcus aureus have good inhibiting effect, the diameter of inhibition zone
In 15cm or more, effect is superior to commercial product.Illustrating the embodiment of the present invention has good bacteriostasis, honey, bee
Glue, royal jelly, bee venom, calendula extract, soybean lecithin, grape seed oil and tea seed protein hydrolyzate share show it is bright
Aobvious synergistic function, fungistatic effect are increased dramatically, and can be used for acne-removing beauty.
2, oil-control effect assessment
Aspiration 100 people of trier (50 people of male, 50 people of women, 18~25 years old age) is chosen, is oily skin, body
Situation is normal, no cosmetic allergic contact dermatitis history.Volunteer is divided into 5 groups, every group of 20 people, male to female ratio is fifty-fifty.It first group, tries out and implements
1 product of example；Second group, try out 5 product of embodiment；Third group tries out 6 product of comparative example；4th group, try out commercially available oil control and acne removal
Soap product；5th group, blank control group only uses clear water when washing one's face.Before experiment, the grease that each group tests place between the eyebrows position respectively contains
Amount, then sample is issued into volunteer, allow it sooner or later respectively using 1 time, to test aspiration respectively when using 30min, 2 weeks and 4 weeks daily
Trier's place between the eyebrows position fat content, the results are shown in Table 9.
Table 9 uses skin oil and fat changes of contents after product
| Group | Before use | 30min | 2 weeks | 4 weeks |
| Blank control group | 78.45 | 38.64 | 76.27 | 80.13 |
| Commercial product | 79.06 | 25.85 | 65.48 | 67.62 |
| Embodiment 1 | 80.15 | 21.26 | 53.72 | 55.35 |
| Embodiment 5 | 80.32 | 23.47 | 58.29 | 65.80 |
| Comparative example 6 | 78.63 | 36.09 | 73.16 | 75.47 |
The results show that compared with blank control group, after using 1 product of the embodiment of the present invention 2 weeks, 2 embodiment tests
The fat content of group skin is decreased obviously, and declines more obvious than commercial product group, and 6 product group of comparative example, although skin
Skin fat content is also declined, but unobvious with blank group comparing difference.
3, comprehensive using effect
(1) skin classification
The skin of people is generally divided into seven major class by cosmetic industry, is respectively: neutral skin (normal skin), oiliness skin
Skin, dry skin, sensitive, combination, Aging skin, problem skin.Specifically:
1. neutral skin: namely normal skin, pH value is the desired skin of health between 5~5.6, not oily
Greasy not dry, high resilience, ruddy glossy, pore is tiny, it is not easy to aging.
2. Oily: such skin complexion is deeper, and pore is coarse, and sebum secretion is vigorous, and skin greasing is not allowed to be also easy to produce
Wrinkle, is easy that long powder is perverse, dark sore, and pH value is between 5.5~6.6.
3. dry skin: skin secretory volume is few, without greasy feeling, is easy long fine wrinkles, more sensitive to environmental stimuli,
Skin is obscure, lackluster, easily rupturable, play scurf, long spot, can be divided into oil starvation and two kinds water deficient, pH value about 4~
Between 4.5.
4. sensitive: more sensitive to the stimulation of circle of place, sebum film is thin, and skin self supporting capacity is weaker, and skin easily goes out
It is existing it is red, swollen, pierce, itch, pain and decortication, dehydrating phenomena.
5. combination: the appearance that a kind of skin shows two or more (while having oiliness and stemness skin
The feature of skin).Common easily fuel-displaced for the area face T position, rest part is then dried, and when have an acne, 80% adult male
Property is all combination.Combination mostly occurred between 20~39 years old.
6. Aging skin: it is more common in the middle-aged and the old or sentimental women, there is relaxation, dry, tarnish in skin,
Sebum secretion is few, wrinkle often occurs.
7. problem skin: all Symptomatic skin to go wrong is all referred to as problem skin.Mainly include
Color spot skin, powder be perverse, acne, spot tinea, red capillary, epifolliculitis, eczema, fash, decortication, fester, various dermatitis etc..
(2) research object
It chooses and states the crowds of seven class skin attributes as trier, be divided into seven groups, every group 50, are as follows: 1. neutral group 50；
2. oiliness group 50；3. stemness group 50；4. sensibility group 50；5. Combination group 50；6. Aging group 50；7. problem
Property group 50.
(3) test situation
Research object is respectively cleaned once using the handmade soap of embodiment 1 and comparative example 1 sooner or later for each person every day, uses 30 altogether
It.
(4) test result
Product effect: 1. allergy is examined or check from the following aspects respectively；2. cleaning force；3. bright color；4. tight feelings
Condition；5. skin integrally maintains situation.
The results are shown in Table 10 for the examination of the bee venom beauty handmade soap of embodiment 1, the investigation result of the handmade soap of comparative example 1
As shown in table 11.
The using effect of the bee venom beauty handmade soap of 10 embodiment 1 of table
The using effect of the handmade soap of 11 comparative example 1 of table
Table 10 and table 11 the result shows that, the handmade soap of comparative example 1 either cleans dynamics or allergic conditions, bright color
Situation, tight situation, skin integrally maintain the handmade soap that situation effect etc. is all nothing like embodiment 1.The embodiment of the present invention 1
Handmade soap is added to honey, propolis, royal jelly, bee venom, calendula extract, soybean lecithin, grape seed oil and tea seed albumen
Hydrolyzate tries out test by the crowd of different skin type, it is found that it, with strong cleaning force, is not tightened after, do not dry, also
Have not tight antibacterial, anti-acne, replenishing water and preserving moisture, oil-control, mildly do not stimulate, reduce allergy, bright color and other effects.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (10)
1. a kind of bee venom beauty handmade soap, which is characterized in that in parts by weight, including following components: 8~20 parts of olive oil, palm fibre
24~38 parts of palmitic acid oil, 15~20 parts of coconut oil, 5~18 parts of glycerol, 1~4 part of honey, 8~20 parts of propolis, 2~5 parts of royal jelly,
0.5~4 part of bee venom, 5~10 parts of calendula extract, 0.2~3 part of soybean lecithin, 0.5~3 part of grape seed oil, tea seed albumen
1~3 part of hydrolyzate.
2. bee venom beauty handmade soap according to claim 1, which is characterized in that in parts by weight, including following components: olive
10~16 parts of olive oil, 25~30 parts of palm oil, 17~19 parts of coconut oil, 10~15 parts of glycerol, 2~3 parts of honey, propolis 10~15
Part, 3~4 parts of royal jelly, 1~2 part of bee venom, 6~8 parts of calendula extract, 0.5~2 part of soybean lecithin, grape seed oil 1~
2.5 parts, 1.5~2.5 parts of tea seed protein hydrolyzate.
3. bee venom beauty handmade soap according to claim 1 or 2, which is characterized in that further include emulsifier, surface-active
Agent, alkali and solvent.
4. bee venom beauty handmade soap according to claim 3, which is characterized in that further include emulsifier 1.5 in parts by weight
~3.5 parts, 1~2 part of surfactant, 3~8 parts of alkali, 20~45 parts of solvent.
5. bee venom beauty handmade soap according to claim 4, which is characterized in that in parts by weight, including following components: olive
Olive oil 12 parts, 27 parts of palm oil, 18 parts of coconut oil, 12 parts of glycerol, 2.5 parts of honey, 13 parts of propolis, 3.5 parts of royal jelly, bee venom
1.5 parts, 7 parts of calendula extract, 1.8 parts of soybean lecithin, 1.8 parts of grape seed oil, 2 parts of tea seed protein hydrolyzate, emulsifier 2
Part, 1.5 parts of surfactant, 7 parts of alkali, 35 parts of solvent.
6. bee venom beauty handmade soap according to claim 3, which is characterized in that the emulsifier is Tween-80 or Qula
Logical -100；The surfactant is stearic acid, lauric acid, myristic acid, sodium lauroyl glutamate, methyl cocoyl ox sulphur
One or more of sour sodium；The alkali is sodium hydroxide or potassium hydroxide；The solvent is deionized water.
7. bee venom beauty handmade soap according to claim 1, which is characterized in that the calendula extract is by pot marigold
After adding water to squeeze the juice, the ethanol solution of 5~8 times of weight of water used is added in juice, 10~30 are extracted under the conditions of 60~70 DEG C
Min is filtered, and centrifugation obtains after concentration.
8. bee venom beauty handmade soap according to claim 1, which is characterized in that the tea seed protein hydrolyzate is by with lower section
Method is prepared: smashed tea seed cake and deionized water being mixed according to the weight ratio of 1:9~11, extract 1.8 in 35~45 DEG C
~2.5 h, centrifuging and taking supernatant adjust pH value to 4.8~6.2, obtain tea seed protein hydrolyzate.
9. any bee venom beauty handmade soap according to claim 1~8, which is characterized in that preparation method includes following step
It is rapid:
S1. olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, emulsifier and table are weighed
Face activating agent makes its thawing after mixing, in 50~60 DEG C of heating；
S2. alkali is dissolved in solvent and obtains aqueous slkali, then the aqueous slkali is added in the solution after step S1 melts,
Stir 3~7 min；
S3. glycerol, calendula extract, grape seed oil and tea seed protein hydrolyzate is added in 45~60 DEG C of stirrings, then persistently stirs
7~15 min are mixed, the semi-finished product being thoroughly mixed；Semi-finished product are poured into mold, after its coagulation forming, demoulding
Obtain the bee venom beauty handmade soap.
10. bee venom beauty handmade soap according to claim 9, which is characterized in that in step S3, glycerol, pot marigold is added
After extract, grape seed oil and tea seed protein hydrolyzate, sprinkling alcohol defoaming.
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| CN112226304A (en) * | 2020-10-18 | 2021-01-15 | 江西联锴科技有限公司 | Camellia seed oil soap-based material and preparation method thereof |
| WO2022132090A3 (en) * | 2020-12-18 | 2022-09-01 | Sbs Bi̇li̇msel Bi̇o Çözümler Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ | A cream composition with herbal extract and production method thereof |
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| CN112226304A (en) * | 2020-10-18 | 2021-01-15 | 江西联锴科技有限公司 | Camellia seed oil soap-based material and preparation method thereof |
| CN112226304B (en) * | 2020-10-18 | 2024-03-01 | 江西联锴科技有限公司 | Oil tea seed oil soap base material and preparation method thereof |
| WO2022132090A3 (en) * | 2020-12-18 | 2022-09-01 | Sbs Bi̇li̇msel Bi̇o Çözümler Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ | A cream composition with herbal extract and production method thereof |
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