CN109135974B - Bee venom beauty handmade soap and preparation method thereof - Google Patents
Bee venom beauty handmade soap and preparation method thereof Download PDFInfo
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- CN109135974B CN109135974B CN201810956421.XA CN201810956421A CN109135974B CN 109135974 B CN109135974 B CN 109135974B CN 201810956421 A CN201810956421 A CN 201810956421A CN 109135974 B CN109135974 B CN 109135974B
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses bee venom beauty handmade soap and a preparation method thereof. The handmade soap comprises the following components in parts by weight: 8-20 parts of olive oil, 24-38 parts of palm oil, 15-20 parts of coconut oil, 5-18 parts of glycerol, 1-4 parts of honey, 8-20 parts of propolis, 2-5 parts of royal jelly, 0.5-4 parts of bee venom, 5-10 parts of calendula extract, 0.2-3 parts of soybean lecithin, 0.5-3 parts of grape seed oil and 1-3 parts of tea seed protein hydrolysate. The coconut oil and palm oil cleansing cream is reasonable in compatibility, exerts a remarkable synergistic effect, solves the problems that the coconut oil and palm oil are selected as base oil in the traditional method, and is easy to cause excessive cleaning, and skin is dry, itchy and irritated, has the advantages of being strong in cleaning power, not tight after being used, not dry, mild and not irritated, and capable of dredging pores and reducing allergy, and simultaneously well exerts the effects of active ingredients, so that the coconut oil cleansing cream has good functions of resisting bacteria, preserving moisture, controlling oil and brightening skin color, and has a good application prospect.
Description
Technical Field
The invention belongs to the technical field of biological medicines. More particularly, relates to a bee venom beauty handmade soap and a preparation method thereof.
Background
A more popular handmade soap has emerged in recent years. The handmade soap is the soap made by DIY, the shape is colorful, an infinite imagination space and an originality space are provided for people, the personality of people can be fully played, and the enjoyment of DIY is enjoyed, so the handmade soap is gradually loved by people in recent years. However, the handmade soap products are as many as possible, effective and ineffective at present, the price is high or low, the difference is very large, and the technical breakthrough, especially the breakthrough in the use effect, is pursued by manufacturers and consumers.
The traditional handmade soap is good in cleaning power, generally has a tight phenomenon after being used and causes discomfort to skin after being analyzed from the aspect of use; after the cleaning liquid is used, the cleaning liquid is not tight, the cleaning force is not good, and certain contradiction exists. It is more difficult to achieve other effects of sterilization, moisture retention, oil control, skin color brightening, mildness, no irritation and the like. In addition, the defects of poor appearance, poor fine and smooth foam, and the like exist. In terms of selection of oil, coconut oil and palm oil are usually selected as base oil, the coconut oil can generate abundant foam, has strong degreasing capability, but is easy to cause excessive cleaning, and the skin has symptoms of dryness, pruritus, irritation and the like, and is easy to cause damage to sensitive skin; palm oil is a commonly used extender oil in soap, can increase the hardness of the finished product, but has low content of nutrient components and is not beneficial to the skin care effect of the product.
Therefore, how to reasonably prepare a scientific formula of the handmade soap and develop the handmade soap which has strong cleaning power, is not tense after use, is not dry, is mild and not irritant, has better skin care effect and high use safety becomes a research and development hotspot in the field of soap manufacture.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides the bee venom beauty handmade soap. The bee venom beauty handmade soap milk has strong cleaning power, is not tight after being used, is not dry, is mild and not irritated, reduces allergy, and also has the effects of dredging pores, resisting bacteria, keeping moisture, brightening skin color and controlling oil.
The invention aims to provide bee venom beauty handmade soap.
The invention also aims to provide a preparation method of the bee venom beauty handmade soap.
The above purpose of the invention is realized by the following technical scheme:
the bee venom beauty handmade soap comprises the following components in parts by weight: 8-20 parts of olive oil, 24-38 parts of palm oil, 15-20 parts of coconut oil, 5-18 parts of glycerol, 1-4 parts of honey, 8-20 parts of propolis, 2-5 parts of royal jelly, 0.5-4 parts of bee venom, 5-10 parts of calendula extract, 0.2-3 parts of soybean lecithin, 0.5-3 parts of grape seed oil and 1-3 parts of tea seed protein hydrolysate.
The Propolis (Propolis) which is a raw material in the active ingredients of the bee venom beauty handmade soap is a colloidal solid with aromatic smell, contains various inorganic salts, vitamins, organic acids, fructose, glucose, reductase and the like, has strong antibacterial and anti-inflammatory capabilities, has strong inhibiting and killing effects on fungi, germs and the like, has the effects of moistening and beautifying, diminishing inflammation and relieving pain, and can be used for treating burns and scalds, skin cracking pain or preventing radiation. Bee venom is a transparent yellowish liquid in a natural state, is bitter in taste, has viscosity and has a special aromatic smell; can promote metabolism, enhance disease resistance, and act as in vivo immunizing agent, and a small number (about 2%) of people can cause anaphylaxis to bee venom. The soybean lecithin forms a protective film on the surface of skin, so that the stimulation and the damage of the skin can be effectively relieved, the allergy occurrence is reduced, meanwhile, the effective components can quickly permeate into the skin bottom, the moisture can be quickly absorbed, and the problem of deep water shortage of the skin bottom is solved; meanwhile, calendula extract, grape seed oil and tea seed protein hydrolysate are added, so that the skin-care and beauty-care effects can be more effectively exerted; the raw materials are used together, and can reduce anaphylaxis caused by bee venom.
Preferably, the bee venom beauty handmade soap comprises the following components in parts by weight: 10-16 parts of olive oil, 25-30 parts of palm oil, 17-19 parts of coconut oil, 10-15 parts of glycerol, 2-3 parts of honey, 10-15 parts of propolis, 3-4 parts of royal jelly, 1-2 parts of bee venom, 6-8 parts of calendula extract, 0.5-2 parts of soybean lecithin, 1-2.5 parts of grape seed oil and 1.5-2.5 parts of tea seed protein hydrolysate.
More preferably, the bee venom beauty handmade soap comprises the following components in parts by weight: 12 parts of olive oil, 27 parts of palm oil, 18 parts of coconut oil, 12 parts of glycerol, 2.5 parts of honey, 13 parts of propolis, 3.5 parts of royal jelly, 1.5 parts of bee venom, 7 parts of calendula extract, 1.8 parts of soybean lecithin, 1.8 parts of grape seed oil and 2 parts of tea seed protein hydrolysate.
Preferably, the bee venom beauty handmade soap further comprises an emulsifier, a surfactant, an alkali and a solvent.
More preferably, the bee venom beauty handmade soap further comprises 1.5-3.5 parts by weight of an emulsifier, 1-2 parts by weight of a surfactant, 3-8 parts by weight of an alkali and 20-45 parts by weight of a solvent.
Still more preferably, the bee venom beauty handmade soap further comprises 2 parts by weight of an emulsifier, 1.5 parts by weight of a surfactant, 7 parts by weight of an alkali and 35 parts by weight of a solvent.
Most preferably, the bee venom beauty handmade soap comprises the following components in parts by weight: 12 parts of olive oil, 27 parts of palm oil, 18 parts of coconut oil, 12 parts of glycerol, 2.5 parts of honey, 13 parts of propolis, 3.5 parts of royal jelly, 1.5 parts of bee venom, 7 parts of calendula extract, 1.8 parts of soybean lecithin, 1.8 parts of grape seed oil, 2 parts of tea seed protein hydrolysate, 2 parts of emulsifier, 1.5 parts of surfactant, 7 parts of alkali and 35 parts of solvent.
Preferably, the emulsifier is Tween-80 or Triton-100; the surfactant is one or more of stearic acid, lauric acid, myristic acid, sodium lauroyl glutamate and sodium methyl cocoyl taurate; the alkali is sodium hydroxide or potassium hydroxide; the solvent is deionized water.
Preferably, the calendula extract is obtained by adding water into calendula to squeeze juice, adding an ethanol solution which is 5-8 times of the weight of the water into the juice, leaching for 10-30 min at the temperature of 60-70 ℃, filtering, centrifuging and concentrating.
More preferably, the calendula extract is obtained by adding water to calendula and squeezing to obtain juice, adding ethanol solution 6.5 times of the weight of the water to the juice, leaching for 20min at 65 ℃, filtering, centrifuging and concentrating.
Preferably, the mass concentration of the ethanol solution is 60-75%.
Preferably, the tea seed protein hydrolysate is prepared by the following method: mixing the crushed tea seed cake and deionized water according to the proportion of 1: 9-11, leaching for 1.8-2.5 h at 35-45 ℃, centrifuging to obtain supernatant, and adjusting the pH value to 4.8-6.2 to obtain the tea seed protein hydrolysate.
More preferably, the weight ratio of the tea seed meal to the deionized water is 1: 10.
more preferably, the leaching conditions are 40 ℃ leaching for 2.2 h.
More preferably, the pH is adjusted to 5.2.
The preparation method of the bee venom beauty handmade soap comprises the following steps:
s1, weighing olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, an emulsifier and a surfactant, uniformly mixing, and heating at 50-60 ℃ to melt;
s2, dissolving alkali in a solvent to obtain an alkali solution, adding the alkali solution into the solution melted in the step S1, and stirring for 3-7 min;
s3, adding the glycerol, the calendula extract, the grape seed oil and the tea seed protein hydrolysate into the mixture at the temperature of 45-60 ℃ under stirring, and then continuously stirring for 7-15 min to obtain a completely mixed semi-finished product; pouring the semi-finished product into a mould, solidifying and forming, and demoulding to obtain the bee venom handmade soap.
Preferably, in step S1, the mixture is melted by heating at 55 ℃.
Preferably, in step S3, glycerin, calendula extract, grape seed oil and tea seed protein hydrolysate are added with stirring at 55 ℃.
Preferably, in step S3, after adding glycerin, calendula extract, grape seed oil and tea seed protein hydrolysate, alcohol is sprayed for defoaming.
The operations of squeezing, filtering, centrifuging, concentrating and the like involved in the invention are all performed according to the conventional method in the field, and the operation parameters of squeezing, filtering, centrifuging and concentrating can be adjusted by a person skilled in the art according to the actual needs.
Compared with the prior art, the invention has the following beneficial effects:
according to the invention, active ingredients such as honey, propolis, royal jelly, bee venom, calendula extract, soybean lecithin, grape seed oil and tea seed protein hydrolysate are added into the handmade soap, the compatibility of the whole formula is reasonable, the remarkable synergistic effect is exerted, the problems that the skin is easy to be excessively cleaned and the skin is dry, itchy and irritated due to the fact that coconut oil and palm oil are selected as base oil in the traditional method are solved, and the handmade soap has the advantages of strong cleaning force, no tightness after use, no dryness, mildness, no irritation, pore dredging and allergy reduction, and simultaneously the effects of the active ingredients are well exerted, so that the handmade soap has the better functions of resisting bacteria, preserving moisture, controlling oil and brightening skin color.
Detailed Description
The present invention is further illustrated by the following specific examples, which are not intended to limit the invention in any way. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Unless otherwise indicated, reagents and materials used in the following examples are commercially available.
Example 1 bee venom handmade soap for beauty treatment and preparation method thereof
1. Formulation of
The formulation of the bee venom beauty handmade soap of this example is shown in table 1.
TABLE 1 formula of bee venom beauty handmade soap
2. The preparation method of the bee venom beauty handmade soap comprises the following steps:
(1) weighing olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, Tween-80 and stearic acid, mixing, and heating at 55 deg.C to melt;
(2) dissolving sodium hydroxide in deionized water to obtain an alkali solution, adding the alkali solution into the solution melted in the step (1), and stirring for 6 min;
(3) adding glycerol, herba Sidae Rhombifoliae extract, grape seed oil and tea seed protein hydrolysate at 55 deg.C under stirring, and stirring for 11min to obtain completely mixed semi-finished product; pouring the semi-finished product into a mould, solidifying and forming, and demoulding to obtain the bee venom beauty handmade soap;
wherein the calendula extract is prepared by the following method: adding water into herba Sidae Rhombifoliae, squeezing to obtain juice, adding 65% ethanol solution 6.5 times of water, leaching at 65 deg.C for 20min, filtering, centrifuging, and concentrating to obtain herba Sidae Rhombifoliae extract;
the tea seed protein hydrolysate is prepared by the following method: mixing the crushed tea seed cake and deionized water according to the proportion of 1: 10, leaching for 2.2h at 40 ℃, centrifuging to obtain supernatant, and adjusting the pH value to 5.2 to obtain the tea seed protein hydrolysate.
Example 2 bee venom handmade soap for beauty treatment and preparation method thereof
1. Formulation of
The formulation of the bee venom beauty handmade soap of this example is shown in table 2.
TABLE 2 formula of bee venom handmade soap for beauty treatment
2. The preparation method of the bee venom beauty handmade soap comprises the following steps:
(1) weighing oleum Olivarum, palm oil, oleum Cocois, Mel, propolis, Lac Regis Apis, venenum Apis, soybean lecithin, Triton-100 and lauric acid, mixing, and heating at 50 deg.C to melt;
(2) dissolving potassium hydroxide in deionized water to obtain an alkali solution, adding the alkali solution into the solution melted in the step (1), and stirring for 3 min;
(3) adding glycerol, herba Sidae Rhombifoliae extract, grape seed oil and tea seed protein hydrolysate at 45 deg.C under stirring, and stirring for 7min to obtain completely mixed semi-finished product; pouring the semi-finished product into a mould, solidifying and forming, and demoulding to obtain the bee venom beauty handmade soap;
wherein the calendula extract is prepared by the following method: adding water into herba Sidae Rhombifoliae, squeezing to obtain juice, adding 60% ethanol solution 5 times of water, leaching at 60 deg.C for 10min, filtering, centrifuging, and concentrating to obtain herba Sidae Rhombifoliae extract;
the tea seed protein hydrolysate is prepared by the following method: mixing the crushed tea seed cake and deionized water according to the proportion of 1: 9, leaching for 1.8h at 35 ℃, centrifuging to obtain supernatant, and adjusting the pH value to 4.8 to obtain the tea seed protein hydrolysate.
Example 3 bee venom handmade soap for beauty treatment and preparation method thereof
1. Formulation of
The formulation of the bee venom beauty handmade soap of this example is shown in table 3.
TABLE 3 formula of bee venom handmade soap for beauty treatment
| Raw material number | Name (R) | Parts by weight (parts) | Purpose of use |
| 1 | Olive oil | 16 | Base oil |
| 2 | Palm oil | 25 | Base oil |
| 3 | Coconut oil | 19 | Base oil |
| 4 | Glycerol | 10 | Moisture-retaining agent |
| 5 | Honey | 3 | Active ingredient |
| 6 | Propolis (propolis) | 10 | Active ingredient |
| 7 | Royal jelly | 4 | Active ingredient |
| 8 | Bee venom | 2 | Active ingredient |
| 9 | Calendula extract | 6 | Active ingredient |
| 10 | Soybean lecithin | 2 | Active ingredient |
| 11 | Grape seed oil | 1 | Active ingredient |
| 12 | Tea seed protein hydrolysate | 2.5 | Active ingredient |
| 13 | Tween-80 | 3.5 | Emulsifier |
| 14 | Myristic acid | 1 | Surface active agent |
| 15 | Sodium hydroxide | 8 | Alkali |
| 16 | Deionized water | 20 | Solvent(s) |
2. The preparation method of the bee venom beauty handmade soap comprises the following steps:
(1) weighing olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, Tween-80 and myristic acid, mixing uniformly, and heating at 60 deg.C to melt;
(2) dissolving sodium hydroxide in deionized water to obtain an alkali solution, adding the alkali solution into the solution melted in the step (1), and stirring for 7 min;
(3) adding glycerol, herba Sidae Rhombifoliae extract, grape seed oil and tea seed protein hydrolysate at 60 deg.C under stirring, and stirring for 15min to obtain completely mixed semi-finished product; pouring the semi-finished product into a mould, solidifying and forming, and demoulding to obtain the bee venom beauty handmade soap;
wherein the calendula extract is prepared by the following method: adding water into herba Sidae Rhombifoliae, squeezing to obtain juice, adding 75% ethanol solution 8 times of water, leaching at 70 deg.C for 30min, filtering, centrifuging, and concentrating to obtain herba Sidae Rhombifoliae extract;
the tea seed protein hydrolysate is prepared by the following method: mixing the crushed tea seed cake and deionized water according to the proportion of 1: 11, leaching for 2.5h at 45 ℃, centrifuging to obtain supernatant, and adjusting the pH value to 6.2 to obtain tea seed protein hydrolysate.
Example 4 bee venom handmade soap for beauty treatment and preparation method thereof
1. Formulation of
The formulation of the bee venom beauty handmade soap of this example is shown in table 4.
TABLE 4 formula of bee venom handmade soap for beauty treatment
| Raw material number | Name (R) | Parts by weight (parts) | Purpose of use |
| 1 | Olive oil | 8 | Base oil |
| 2 | Palm oil | 38 | Base oil |
| 3 | Coconut oil | 15 | Base oil |
| 4 | Glycerol | 18 | Moisture-retaining agent |
| 5 | Honey | 1 | Active ingredient |
| 6 | Propolis (propolis) | 20 | Active ingredient |
| 7 | Royal jelly | 2 | Active ingredient |
| 8 | Bee venom | 0.5 | Active ingredient |
| 9 | Calendula extract | 10 | Active ingredient |
| 10 | Soybean lecithin | 0.2 | Active ingredient |
| 11 | Grape seed oil | 3 | Active ingredient |
| 12 | Tea seed protein hydrolysate | 1 | Active ingredient |
| 13 | Triton-100 | 1.5 | Emulsifier |
| 14 | Sodium lauroyl glutamate | 2 | Surface active agent |
| 15 | Potassium hydroxide | 3 | Alkali |
| 16 | Deionized water | 45 | Solvent(s) |
2. The bee venom beauty handmade soap of this example was prepared in the same manner as in example 1.
Example 5 bee venom handmade soap for beauty treatment and preparation method thereof
1. Formulation of
The formulation of the bee venom beauty handmade soap of this example is shown in table 5.
TABLE 5 formula of bee venom handmade soap for beauty treatment
2. The bee venom beauty handmade soap of this example was prepared in the same manner as in example 1.
Example 6 formulation evaluation
1. Examples 1-5 results of physical and chemical tests of bee venom beauty handmade soap
(1) Traits
The bee venom beauty handmade soap is a milky beauty soap which is good in stability, fragrant in smell, fine and uniform.
(2) Examination of pH value
The bee venom beauty handmade soap of the embodiment 1-5 is wetted by distilled water and then measured by a pH test paper, and the measured pH value is 7.0-7.6.
2. Examples 1 to 5 results of microbial detection of bee venom beauty handmade soap
TABLE 6 results of microbial detection
3. Irritation test and allergy test
The skin of a Kunming white mouse was cut off, and the bee venom hand soap wetted with distilled water prepared in examples 1 to 5 was applied to the cut-off part, and compared with the non-applied part, no irritation or allergic reaction was observed.
Example 7
1. Experiment for inhibiting bacteria
Propionibacterium acnes, Staphylococcus epidermidis and Staphylococcus aureus are the main pathogenic bacteria causing acne. The bacteriostatic and acne-removing effects of different products can be evaluated through bacteriostatic experiments on the three bacteria. The invention adopts a paper diffusion method to evaluate the bacteriostatic effect of different products.
(1) The formulations of the bee venom cosmetic handmade soaps of comparative examples 1 to 6 (see table 7) were changed based on the active ingredient of example 1, and the others were the same as those of example 1; the preparation method is the same as that of example 1.
TABLE 7 formulation of active ingredients for bee venom beauty handmade soap of comparative examples 1-6
(2) Weighing 5g of each of the bee venom beauty handmade soap products of examples 1-5, the comparative examples 1-6 and the commercially available oil-controlling acne-removing beauty soap product, adding 50mL of deionized water, dissolving, filtering, taking the filtrate for standby (ready for use), clamping and soaking a sterilized filter paper sheet with the diameter of 6mm in a sample solution by using a sterile forceps, taking out, airing, placing in a sterile culture dish, and taking the sterilized normal saline as negative control. Transferring 200 mu L of propionibacterium acnes, staphylococcus epidermidis and staphylococcus aureus bacterial suspensions to a solid culture dish, uniformly coating, pasting a prepared filter paper piece on the culture dish, culturing at 37 ℃ for 18-24 h, observing results, measuring the size of a bacteriostatic zone, setting 3 samples in parallel, and taking an average value of the results. The results are shown in Table 8.
(3) Results of the experiment
TABLE 8 results of bacteriostatic experiments
The results show that compared with comparative examples 1-6, the five bee venom beauty handmade soap products in examples 1-5 have good inhibition effects on three bacteria such as propionibacterium acnes, staphylococcus epidermidis and staphylococcus aureus, the diameters of inhibition zones are all more than 15cm, and the effects are superior to those of commercial products. The embodiment of the invention has good antibacterial effect, and the combination of honey, propolis, royal jelly, bee venom, calendula extract, soybean lecithin, grape seed oil and tea seed protein hydrolysate shows obvious synergistic effect, so that the antibacterial effect is greatly improved, and the tea seed protein hydrolysate can be used for removing acne and beautifying.
2. Evaluation of oil control Effect
100 volunteer subjects (50 men, 50 women, age 18-25) are selected, and are all oily skin, normal in physical condition and free of cosmetic allergy history. Volunteers were divided into 5 groups of 20 persons each, with half the male and female proportions. First, trial the product of example 1; second, trial example 5 product; third group, trial of comparative example 6 product; fourthly, a commercial oil-control acne-removing soap product is tried; the fifth group, blank control, was washed with fresh water only. Before the experiment, the oil content of the eyebrow part of each group is respectively tested, then the sample is sent to a volunteer, the volunteer is respectively used for 1 time in the morning and evening, the oil content of the eyebrow part of the volunteer is respectively tested when the sample is used for 30min, 2 weeks and 4 weeks, and the result is shown in a table 9.
TABLE 9 change in skin oil content after use of the product
| Group of | Before use | 30min | 2 weeks | 4 weeks |
| Blank control group | 78.45 | 38.64 | 76.27 | 80.13 |
| Commercially available product | 79.06 | 25.85 | 65.48 | 67.62 |
| Example 1 | 80.15 | 21.26 | 53.72 | 55.35 |
| Example 5 | 80.32 | 23.47 | 58.29 | 65.80 |
| Comparative example 6 | 78.63 | 36.09 | 73.16 | 75.47 |
The results show that after 2 weeks of use of the product of example 1 according to the invention, the oil content of the skin of the 2 test examples was significantly reduced compared to the blank control group and was significantly reduced compared to the commercial product group, whereas the oil content of the skin of the comparative example 6 was also reduced but was not significantly different from the blank control group.
3. Comprehensive use effect
(1) Skin classification
The cosmetic industry generally classifies human skin into seven broad categories, respectively: neutral skin (normal skin), oily skin, dry skin, sensitive skin, combination skin, aged skin, and problem skin. The method comprises the following steps:
skin neutral: namely normal skin, the pH value of the skin is between 5 and 5.6, the skin is healthy and ideal, is not greasy, not dry, rich in elasticity, ruddy and glossy, has small pores, and is not easy to age.
② oily skin: the skin has dark skin color, large pores, vigorous sebum secretion, greasy skin, difficulty in generating wrinkles, easiness in growing acne and pimples, and the pH value is 5.5-6.6.
Dry skin: the skin has less secretion, no greasy feeling, easy growth of fine wrinkles, sensitivity to external stimulation, dull and lusterless skin, easy cracking, scurf and long spots, and can be divided into two types of oil deficiency and water deficiency, and the pH value of the skin is between 4 and 4.5.
(iv) sensitive skin: sensitive to the stimulation of the boundary, thin skin lipid film, weak self-protection capability of the skin, and easy red, swollen, prickled, itchy, painful, peeled and dehydrated phenomena of the skin.
Mixed skin: a skin has two or more appearances (both oily and dry skin characteristics). Most of the cases show that the T area of the face is easy to produce oil, the rest parts are dry, acne sometimes happens, and 80% of adult men are mixed skin. Mixed skin usually occurs between 20 and 39 years of age.
Sixthly, the aging skin: it is common to the middle aged and the elderly or women with a feeling of being sensitive, and the skin is loose, dry and dull, and has less sebum secretion, often causing wrinkles.
Seventh, problematic skin: the symptomatic skin with problems is generally called problem skin. Mainly comprises pigmented spots, acne, tinea, red blood, folliculitis, eczema, rash, desquamation, pustule, various dermatitis, etc.
(2) Study object
The groups with the seven skin attributes are selected as test persons and divided into seven groups, wherein 50 cases in each group are as follows: 50 cases of neutral groups; ② 50 cases of oily group; ③ 50 cases of the dry group; 50 sensitive groups; mixed group 50 cases; sixthly, 50 cases of aging group; seventhly, 50 cases of problem groups.
(3) Test conditions
Subjects washed each day, morning and evening, with the handmade soaps of example 1 and comparative example 1 for a total of 30 days.
(4) Test results
The product effect was examined from several aspects: firstly, allergy is caused; cleaning power; thirdly, brightening the skin color; tension; the whole skin care condition.
The examination results of the bee venom cosmetic handmade soap of example 1 are shown in table 10, and the examination results of the handmade soap of comparative example 1 are shown in table 11.
TABLE 10 Effect of using bee venom cosmetic handmade soap of example 1
TABLE 11 Effect of use of handmade soap of comparative example 1
The results in tables 10 and 11 show that the handmade soap of comparative example 1 is far less effective than the handmade soap of example 1 in cleaning power, allergy, lightening skin color, tension, skin care integrity, etc. According to the handmade soap disclosed by the embodiment 1 of the invention, honey, propolis, royal jelly, bee venom, a calendula extract, soybean lecithin, grape seed oil and tea seed protein hydrolysate are added, and through trial tests of people with different skin types, the handmade soap is found to have the effects of strong cleaning power, no tightness after use, no dryness, antibiosis, acne removal, water and moisture supplement, no tightness, oil control, mildness, no irritation, allergy reduction, skin color brightening and the like.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (3)
1. The bee venom beauty handmade soap is characterized by being prepared from the following components in parts by weight: 12 parts of olive oil, 27 parts of palm oil, 18 parts of coconut oil, 12 parts of glycerol, 2.5 parts of honey, 13 parts of propolis, 3.5 parts of royal jelly and 1.5 parts of bee venom
The components comprise 7 parts of calendula extract, 1.8 parts of soybean lecithin, 1.8 parts of grape seed oil, 2 parts of tea seed protein hydrolysate, 2 parts of emulsifier, 1.5 parts of surfactant, 7 parts of alkali and 35 parts of solvent;
the emulsifier is Tween-80 or triton-100; the surfactant is one or more of stearic acid, lauric acid, myristic acid, sodium lauroyl glutamate and sodium methyl cocoyl taurate; the alkali is sodium hydroxide or potassium hydroxide; the solvent is deionized water;
the calendula extract is obtained by adding water into calendula and juicing, adding an ethanol solution which is 5-8 times of the weight of the water into the juice, leaching for 10-30 min at the temperature of 60-70 ℃, filtering, centrifuging and concentrating;
the tea seed protein hydrolysate is prepared by the following method: mixing the crushed tea seed cake and deionized water according to the proportion of 1: 9-11, leaching for 1.8-2.5 h at 35-45 ℃, centrifuging to obtain supernatant, and adjusting the pH value to 4.8-6.2 to obtain the tea seed protein hydrolysate.
2. The bee venom beauty handmade soap according to claim 1, which is prepared by the method comprising the steps of:
s1, weighing olive oil, palm oil, coconut oil, honey, propolis, royal jelly, bee venom, soybean lecithin, an emulsifier and a surfactant, uniformly mixing, and heating at 50-60 ℃ to melt;
s2, dissolving alkali in a solvent to obtain an alkali solution, adding the alkali solution into the solution melted in the step S1, and stirring for 3-7 min;
s3, adding the glycerol, the calendula extract, the grape seed oil and the tea seed protein hydrolysate into the mixture at the temperature of 45-60 ℃ under stirring, and then continuously stirring for 7-15 min to obtain a completely mixed semi-finished product; pouring the semi-finished product into a mould, solidifying and forming, and demoulding to obtain the bee venom handmade soap.
3. The bee venom beauty handmade soap according to claim 2, wherein in step S3, after adding glycerin, calendula extract, grape seed oil and tea seed protein hydrolysate, alcohol is sprayed for defoaming.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1268348A (en) * | 1999-03-30 | 2000-10-04 | 佟玉杰 | Skin-care prepns. for fair-skinned face |
| CN104371864A (en) * | 2014-11-29 | 2015-02-25 | 山东省农业科学院农产品研究所 | Grape seed polyphenol handmade soap and preparation method thereof |
| CN104546610A (en) * | 2015-01-09 | 2015-04-29 | 湖南新金浩茶油股份有限公司 | Anti-aging facial cleanser and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1268348A (en) * | 1999-03-30 | 2000-10-04 | 佟玉杰 | Skin-care prepns. for fair-skinned face |
| CN104371864A (en) * | 2014-11-29 | 2015-02-25 | 山东省农业科学院农产品研究所 | Grape seed polyphenol handmade soap and preparation method thereof |
| CN104546610A (en) * | 2015-01-09 | 2015-04-29 | 湖南新金浩茶油股份有限公司 | Anti-aging facial cleanser and preparation method thereof |
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