CN107012031A - A kind of snake gourd fruit pulp cold process soap with white-skinned face function and preparation method thereof - Google Patents

A kind of snake gourd fruit pulp cold process soap with white-skinned face function and preparation method thereof Download PDF

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Publication number
CN107012031A
CN107012031A CN201710362631.1A CN201710362631A CN107012031A CN 107012031 A CN107012031 A CN 107012031A CN 201710362631 A CN201710362631 A CN 201710362631A CN 107012031 A CN107012031 A CN 107012031A
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China
Prior art keywords
parts
fruit pulp
snake gourd
gourd fruit
soap
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Pending
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CN201710362631.1A
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Chinese (zh)
Inventor
王玲娜
张永清
刘星劼
姜秋
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Shandong University of Traditional Chinese Medicine
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Shandong University of Traditional Chinese Medicine
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Priority to CN201710362631.1A priority Critical patent/CN107012031A/en
Publication of CN107012031A publication Critical patent/CN107012031A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

Abstract

The invention discloses a kind of snake gourd fruit pulp cold process soap with white-skinned face function, it is characterised in that is made up of the component of following parts by weight:80~100 parts of 220~240 parts of pure water, sodium hydroxide or potassium hydroxide, 100~120 parts of coconut oil, 40~60 parts of brush-cherry seed oil, 120~140 parts of shea butter, 320~360 parts of olive oil, 50~80 parts of palm oil, 50~80 parts of snake gourd fruit pulp.Snake gourd fruit pulp is added in the vegetable oil with basic skin effect and snake gourd fruit pulp cold process soap is made by the present invention as functional raw material.The present invention has no side effect without any chemical composition.

Description

A kind of snake gourd fruit pulp cold process soap with white-skinned face function and preparation method thereof
Technical field
The present invention relates to a kind of snake gourd fruit pulp cold process soap, and in particular to a kind of snake gourd fruit pulp cold process soap with white-skinned face function and its Preparation method.Belong to commodity technical field.
Background technology
With the progress and the improvement of people's living standards of human civilization, the quality of both effectiveness cosmetics is increasingly by people Attention, wherein natural plants or Chinese herbal medicine skin-lightening cosmetic are also increasingly favored by people.
Snakegourd Fruit, is in use for a long time as traditional Chinese medicine in China, ancient times《Mingyi Bielu》It is middle to have recorded " the main obstruction of qi in the chest, happy people from pool Face ", illustrates that Snakegourd Fruit has certain whitening function.Research shows the accessory substance snake gourd fruit pulp in Snakegourd Fruit production process, with suppression The effect of B16 cell key enzyme tyrosinase, is a kind of natural whitening agent in skin care item.Almond, Snakegourd Fruit described in book on Chinese herbal medicine The face white side of black order of flesh and the medicine of pork tripe three composition, the effect brightened with moisturizing is obvious, wherein the sweet matter profit of snake gourd fruit pulp, in the side of being Main ingredient, can Glycerin, decontamination contaminant releasing, dispersing swelling and dissipating binds, acne for face, it is red it is swollen have therapeutic action, almond is gentle, is rich in Grease, the work(for having nourishing is longer than and controlled " blister sore on face ", and pork tripe is apt to qi-restoratives and moisturized, and being applied to face makes skin exquisiteness delicate, is imbued with bullet Property.Three medicines, which are shared, can then receive the cosmetic result of " the black order in face is white, makes us smooth, the eleventh month of the lunar calendar is not chapped ".Therefore snake gourd fruit pulp is very suitable for In the skin-protection products such as anti-aging, whitening, it is combined with handmade soap, its moist, whitening value can be preferably played.
Traditional perfumed soap is mostly mixed at high temperature using all kinds of animal tallows and alkali as raw material, addition exhibiting high surface activity Agent, antiseptic, stabilizer, synthetic perfume etc. are made, and are a kind of cleaning agents of chemical synthesis.Handmade soap is just to have flowed in recent years A kind of intention articles for washing that row gets up, main point regenerates soap, hot soapmaking and cold process soap.
Regeneration soap is to buy soap base from market, heating dissolve after through toning and moulding, cooling and demolding, except profile feature Different outer with commercially available perfumed soap, in composition and functionally not too big difference belongs to semi-hand perfumed soap;Hot soapmaking is to use natural oil Saponification is carried out until complete under continuous heating environment with highly basic, and advantage is the saving time, but it is a large amount of under continuous high temperature Nutriment can be destroyed;Cold process soap is that for hot soapmaking, its whole temperature in manufacturing process is no more than 40 DEG C, The denaturalization phenomenon of the nutrient being lost in by high temperature and grease is avoided, while cold process soap is by produced in saponification process 25% skin The optimal NMF glycerine of skin being retained in soap completely, forms one layer of natural diaphragm on skin, when using more than Hot soapmaking is moistened.
The content of the invention
The purpose of the present invention is that there is provided a kind of snake gourd fruit pulp with white-skinned face function is cold to overcome above-mentioned the deficiencies in the prior art Soapmaking.
Present invention also offers the preparation method of above-mentioned snake gourd fruit pulp cold process soap.
To achieve the above object, the present invention uses following technical proposals:
A kind of snake gourd fruit pulp cold process soap with white-skinned face function, is made up of the component of following parts by weight:Pure water 220~ 240 parts, 80~100 parts of sodium hydroxide or potassium hydroxide, 100~120 parts of coconut oil, 40~60 parts of brush-cherry seed oil, shea butter 120~140 parts, 320~360 parts of olive oil, 50~80 parts of palm oil, 50~80 parts of snake gourd fruit pulp.
As one of preferred technical scheme, it is made up of the component of following parts by weight:230 parts of pure water, hydroxide 90 parts of sodium, 110 parts of coconut oil, 50 parts of brush-cherry seed oil, 130 parts of shea butter, 340 parts of olive oil, 60 parts of palm oil, snake gourd fruit pulp 70 Part.
As one of preferred technical scheme, the snake gourd fruit pulp is directly taken out and obtained after fresh Snakegourd Fruit is splitted.
The preparation method of above-mentioned snake gourd fruit pulp cold process soap, is comprised the following steps that:
(1) alkali lye is prepared:The sodium hydroxide or potassium hydroxide of formula ratio are dissolved in pure water, standing is cooled to 40~45 DEG C, alkali lye is obtained, heating maintains temperature, standby;
(2) grease is prepared:The coconut oil of formula ratio, brush-cherry seed oil, shea butter, palm oil and olive oil are mixed and stirred evenly And continuous heating is to 40~45 DEG C, compound lard is obtained, it is standby;
(3) soap lye is prepared:Alkali lye obtained by step (1) is slowly added to compound lard obtained by step (2), it is lasting to stir, directly To in it is faint yellow thick and occur filiform be saponification complete, obtain soap lye, it is standby;
(4) prepared by snake gourd fruit pulp:The fresh snake gourd fruit pulp of formula ratio is weighed, is blended, filters, takes filtrate, it is standby;
(5) filtrate obtained by step (4) is added in the soap lye in step (3), stirring is mixed to uniform, mould molding, Sterilization, packaging, is produced.
As one of preferred technical scheme, the temperature of alkali lye is maintained at 40 by step (1) by way of heating water bath ~45 DEG C.
As one of preferred technical scheme, the specific method of step (1) is:By the sodium hydroxide or hydroxide of formula ratio Potassium is added in pure water, is stirred 10~15 minutes, and standing is cooled to 40~45 DEG C, and heats the maintenance temperature, obtains alkali lye.
As one of preferred technical scheme, the temperature phase of compound lard obtained by alkali lye obtained by step (1) and step (2) Together.
As one of preferred technical scheme, snake gourd fruit pulp is blended using juice extractor in step (4), filtered through gauze.
As one of preferred technical scheme, formed in mould specific method is in step (5):Soap lye note after stirring evenly Enter in mould, reverse mould is molded after cooling and standings 2~3 days at the aeration-drying, then through maturation in 10~20 days.
As one of preferred technical scheme, the method for disinfection in step (5) is vacreation.
Beneficial effects of the present invention:
Snake gourd fruit pulp is added in the vegetable oil with basic skin effect and snake gourd fruit pulp is made by the present invention as functional raw material Cold process soap.The present invention has no side effect without any chemical composition.
Snake gourd fruit pulp can Glycerin, decontamination contaminant releasing, dispersing swelling and dissipating binds, while having suppression B16 cell key enzyme junket ammonia again The effect of sour enzyme, the present invention is perfectly combined it with handmade soap, can preferably play its skin care value.Meanwhile, using pure day Right vegetable oil and Conventional cryogenic cold process soap method, it is complete to retain grease and the various nutritional ingredients in snake gourd fruit pulp, handmade soap is existed While gentle cleaning, also have Whitening, spot effect.The vegetable oil combination of the present invention includes coconut oil, brush-cherry seed oil, breast wood fruit Oil, olive oil and palm oil, they act synergistically, and promote absorption of the skin to snake gourd fruit pulp composition, so as to be effectively improved skin shape Condition, plays a part of Whitening, spot, while alleviating excitant of the snake gourd fruit pulp to skin.
Embodiment
With reference to embodiment, the present invention will be further elaborated, it should explanation, the description below merely to The present invention is explained, its content is not defined.
It is biological that coconut oil of the present invention, brush-cherry seed oil, shea butter, olive oil and palm oil are purchased from the Xi'an four seasons Science and Technology Ltd..
Embodiment 1:
A kind of snake gourd fruit pulp cold process soap with white-skinned face function, is made up of the component of following parts by weight:Pure water 220 Part, 80 parts of sodium hydroxide, 100 parts of coconut oil, 40 parts of brush-cherry seed oil, 120 parts of shea butter, 320 parts of olive oil, palm oil 50 Part, 50 parts of snake gourd fruit pulp.
The preparation method of above-mentioned snake gourd fruit pulp cold process soap, is comprised the following steps that:
(1) alkali lye is prepared:The sodium hydroxide of formula ratio is added in pure water, stirred 10 minutes, standing is cooled to 40 DEG C, Alkali lye is obtained, and maintains temperature to be 40 DEG C by way of heating water bath, it is standby;
(2) grease is prepared:The coconut oil of formula ratio, brush-cherry seed oil, shea butter, palm oil and olive oil are mixed and stirred evenly And continuous heating is to 40 DEG C, compound lard is obtained, it is standby;
(3) soap lye is prepared:Alkali lye obtained by step (1) is slowly added to compound lard obtained by step (2), it is lasting to stir, directly To in it is faint yellow thick and occur filiform be saponification complete, obtain soap lye, it is standby;
(4) prepared by snake gourd fruit pulp:The fresh snake gourd fruit pulp of formula ratio is weighed, is blended using juice extractor, filtered through gauze takes filtrate, It is standby;
(5) filtrate obtained by step (4) is added in the soap lye in step (3), stirring is mixed to uniform, after stirring evenly In soap lye injection mould, reverse mould is molded after cooling and standings 2 days at the aeration-drying, then through maturation in 10 days, vacreation, packaging, Produce.
Embodiment 2:
A kind of snake gourd fruit pulp cold process soap with white-skinned face function, is made up of the component of following parts by weight:Pure water 240 Part, 100 parts of potassium hydroxide, 120 parts of coconut oil, 60 parts of brush-cherry seed oil, 140 parts of shea butter, 360 parts of olive oil, palm oil 80 Part, 80 parts of snake gourd fruit pulp.
The preparation method of above-mentioned snake gourd fruit pulp cold process soap, is comprised the following steps that:
(1) alkali lye is prepared:The potassium hydroxide of formula ratio is added in pure water, stirred 15 minutes, standing is cooled to 45 DEG C, Alkali lye is obtained, and maintains temperature to be 45 DEG C by way of heating water bath, it is standby;
(2) grease is prepared:The coconut oil of formula ratio, brush-cherry seed oil, shea butter, palm oil and olive oil are mixed and stirred evenly And continuous heating is to 45 DEG C, compound lard is obtained, it is standby;
(3) soap lye is prepared:Alkali lye obtained by step (1) is slowly added to compound lard obtained by step (2), it is lasting to stir, directly To in it is faint yellow thick and occur filiform be saponification complete, obtain soap lye, it is standby;
(4) prepared by snake gourd fruit pulp:The fresh snake gourd fruit pulp of formula ratio is weighed, is blended using juice extractor, filtered through gauze takes filtrate, It is standby;
(5) filtrate obtained by step (4) is added in the soap lye in step (3), stirring is mixed to uniform, after stirring evenly In soap lye injection mould, reverse mould is molded after cooling and standings 3 days at the aeration-drying, then through maturation in 20 days, vacreation, packaging, Produce.
Embodiment 3:
A kind of snake gourd fruit pulp cold process soap with white-skinned face function, is made up of the component of following parts by weight:Pure water 230 Part, 90 parts of sodium hydroxide, 110 parts of coconut oil, 50 parts of brush-cherry seed oil, 130 parts of shea butter, 340 parts of olive oil, palm oil 60 Part, 70 parts of snake gourd fruit pulp.
The preparation method of above-mentioned snake gourd fruit pulp cold process soap, is comprised the following steps that:
(1) alkali lye is prepared:The sodium hydroxide of formula ratio is added in pure water, stirred 12 minutes, standing is cooled to 42 DEG C, Alkali lye is obtained, and maintains temperature to be 42 DEG C by way of heating water bath, it is standby;
(2) grease is prepared:The coconut oil of formula ratio, brush-cherry seed oil, shea butter, palm oil and olive oil are mixed and stirred evenly And continuous heating is to 42 DEG C, compound lard is obtained, it is standby;
(3) soap lye is prepared:Alkali lye obtained by step (1) is slowly added to compound lard obtained by step (2), it is lasting to stir, directly To in it is faint yellow thick and occur filiform be saponification complete, obtain soap lye, it is standby;
(4) prepared by snake gourd fruit pulp:The fresh snake gourd fruit pulp of formula ratio is weighed, is blended using juice extractor, filtered through gauze takes filtrate, It is standby;
(5) filtrate obtained by step (4) is added in the soap lye in step (3), stirring is mixed to uniform, after stirring evenly In soap lye injection mould, reverse mould is molded after cooling and standings 2 days at the aeration-drying, then through maturation in 15 days, vacreation, packaging, Produce.
Comparative example 1
A kind of snake gourd fruit pulp cold process soap, omits brush-cherry seed oil, remaining be the same as Example 5.
Comparative example 2
A kind of snake gourd fruit pulp cold process soap, omits shea butter, remaining be the same as Example 5.
Comparative example 3
A kind of snake gourd fruit pulp cold process soap, snake gourd fruit pulp is 40 parts, remaining be the same as Example 5.
Comparative example 4
A kind of snake gourd fruit pulp cold process soap, snake gourd fruit pulp is 90 parts, remaining be the same as Example 5.
Test example
The snake gourd fruit pulp cold process soap prepared using embodiment 1~3 and comparative example 1~4 has carried out the test of pesticide effectiveness, through the Shandong traditional Chinese medical science Medicine University Medical institute organizes and implements checking.
1st, skin irritation test
Study subject:350 volunteers, are divided into 7 groups, and every group includes man 25,20~30 years old age;Woman 25, 20~35 years old age;
Experimental method:After warm water profit ear, make the abundant diastole of pore, the embodiment of the present invention 1~3 is uniformly smeared at hard of hearing place It is appropriate with the product of comparative example 1~4,2, after 4,8,12 hours, observe and record the hard of hearing dermoreaction of subject.Experimental result is shown in Table 1.
The skin irritation test result of table 1.
Minimal irritation reaction in table 1 is slight tingling sensation, and serious stimulate the reaction is for the red point of appearance and with serious itch Sense.Result of the test shows, by 2, is observed after hard of hearing use within 4,8,12 hours, uses embodiment 1~3 and the (Snakegourd Fruit of comparative example 3 Flesh content is relatively low) cold process soap, volunteer do not occur any irritative response, and nonresponder's ratio reaches 100%, as a result shown The Product Safety is good.Comparative example 1 omits brush-cherry seed oil, and comparative example 2 omits shea butter, the snake gourd fruit pulp of comparative example 4 Content is higher, and volunteer occurs in that different degrees of irritative response after, illustrates that each vegetable oil composition collaboration plays slow The irritating effect of snake gourd fruit pulp is solved, snake gourd fruit pulp content is higher also can be to skin irritant.
2nd, the evaluation of white-skinned face function
Study subject:700 volunteers, are divided into 7 groups, and every group includes:Oily person, 30 people;Dry person, 30 People;Neutral skin person, 40.All volunteers have carried out skin irritation test, do not occur irritative response.
Test method:With warm water wetting, face makes the abundant diastole of pore, and Example 1~3 and comparative example 1~4 are made respectively Standby snake gourd fruit pulp cold process soap plays foam in the palm of the hand in right amount, is uniformly applied to face, with hand face gently loop massage 1~ 2min, then uses warm water cleaning.
Evaluation criterion:Experimental period is one month.Effectively represent that skin water profit is glossy, whitening is flexible, hence it is evident that desalination color Spot;Invalid representation skin texture is with testing preceding and not being any change;Skin quality is typicallyed represent to make moderate progress, but effect is not very aobvious Write, between it is above-mentioned between the two.
Result of the test:Significantly, crowd's whitening to various skin quality is light for the product Whitening, spot effect of the embodiment of the present invention 1~3 Spot is efficient all higher.The snake gourd fruit pulp content of comparative example 3 is relatively low, Whitening, spot it is efficient significant lower;Comparative example 1 is omitted Brush-cherry seed oil, comparative example 2 omits shea butter, and safety in utilization is not ensured, the effective percentage of Whitening, spot is also significant lower; The snake gourd fruit pulp content of comparative example 4 is higher, on the premise of security is not ensured, the effective percentage of Whitening, spot is not improved. It the results are shown in Table 2.
The white-skinned face function result of the test of table 2.
Although the above-mentioned embodiment to the present invention is described, not to the limit of the scope of the present invention System, on the basis of technical scheme, it is each that those skilled in the art need not pay that creative work can make Plant modification or deform still within protection scope of the present invention.

Claims (6)

1. a kind of snake gourd fruit pulp cold process soap with white-skinned face function, it is characterised in that be made up of the component of following parts by weight:It is pure 80~100 parts of 220~240 parts of water purification, sodium hydroxide or potassium hydroxide, 100~120 parts of coconut oil, 40~60 parts of brush-cherry seed oil, 120~140 parts of shea butter, 320~360 parts of olive oil, 50~80 parts of palm oil, 50~80 parts of snake gourd fruit pulp.
2. the preparation method of snake gourd fruit pulp cold process soap described in claim 1, it is characterised in that comprise the following steps that:
(1)Prepare alkali lye:The sodium hydroxide or potassium hydroxide of formula ratio are dissolved in pure water, standing is cooled to 40~45 DEG C, Alkali lye is obtained, heating maintains temperature, standby;
(2)Prepare grease:The coconut oil of formula ratio, brush-cherry seed oil, shea butter, palm oil and olive oil are mixed and stirs evenly and holds It is continuous to be heated to 40 DEG C, compound lard is obtained, it is standby;
(3)Prepare soap lye:By step(1)Gained alkali lye is slowly added to step(2)Gained compound lard, lasting stirring, until being in Faint yellow sticky silk liquid is that saponification is completed, and obtains soap lye, standby;
(4)It is prepared by snake gourd fruit pulp:The fresh snake gourd fruit pulp of formula ratio is weighed, is blended, filters, takes filtrate, it is standby;
(5)By step(4)Gained filtrate is added to step(3)In soap lye in, stirring is mixed to uniform, mould molding, sterilization, Packaging, is produced.
3. preparation method according to claim 2, it is characterised in that step(1)Specific method be:By the hydrogen of formula ratio Sodium oxide molybdena or potassium hydroxide are added in pure water, are stirred 10~15 minutes, and standing is cooled to 40~45 DEG C, obtain alkali lye, heating dimension Hold temperature.
4. preparation method according to claim 2, it is characterised in that step(4)Middle snake gourd fruit pulp is blended using juice extractor, Filtered through gauze.
5. preparation method according to claim 2, it is characterised in that step(5)In formed in mould specific method be:Will In soap lye injection mould after stirring evenly, reverse mould is molded after cooling and standings 2~3 days at the aeration-drying, then through maturation in 10~20 days .
6. preparation method according to claim 2, it is characterised in that step(5)In method for disinfection be vacreation.
CN201710362631.1A 2017-05-22 2017-05-22 A kind of snake gourd fruit pulp cold process soap with white-skinned face function and preparation method thereof Pending CN107012031A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107674789A (en) * 2017-11-07 2018-02-09 山东中医药大学 A kind of cold process soap with skin-active effect and preparation method thereof
CN108721196A (en) * 2018-08-08 2018-11-02 界首市王集镇顺义家庭农场 A kind of snake gourd fruit pulp skin whitener and preparation method thereof
CN109055055A (en) * 2018-10-12 2018-12-21 合肥师范学院 Environmental protection ferment soap and preparation method thereof
CN111317691A (en) * 2020-02-12 2020-06-23 南京中医药大学 Trichosanthes kirilowii flesh total yellow pigment with whitening effect and preparation method and application thereof

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CN103666868A (en) * 2013-12-18 2014-03-26 田英才 Antiseptic and anti-inflammation moisturizing soap containing functional component
CN104130888A (en) * 2014-08-07 2014-11-05 张萍 Special formula of cold-process handmade soap as well as preparation method and application thereof
CN104263557A (en) * 2014-09-05 2015-01-07 杨珍 Spirulina/propolis soap for removing acne marks
CN106010831A (en) * 2016-05-24 2016-10-12 江苏耐雀生物工程技术有限公司 Handmade soap and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN1388234A (en) * 2001-05-30 2003-01-01 孙甫永 Washing and skin care product series of Chinese trichosanthes
CN101649262A (en) * 2009-09-03 2010-02-17 王硕 Natural cooling-making soap and low-temperature soap-making process
CN103666868A (en) * 2013-12-18 2014-03-26 田英才 Antiseptic and anti-inflammation moisturizing soap containing functional component
CN104130888A (en) * 2014-08-07 2014-11-05 张萍 Special formula of cold-process handmade soap as well as preparation method and application thereof
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107674789A (en) * 2017-11-07 2018-02-09 山东中医药大学 A kind of cold process soap with skin-active effect and preparation method thereof
CN108721196A (en) * 2018-08-08 2018-11-02 界首市王集镇顺义家庭农场 A kind of snake gourd fruit pulp skin whitener and preparation method thereof
CN109055055A (en) * 2018-10-12 2018-12-21 合肥师范学院 Environmental protection ferment soap and preparation method thereof
CN111317691A (en) * 2020-02-12 2020-06-23 南京中医药大学 Trichosanthes kirilowii flesh total yellow pigment with whitening effect and preparation method and application thereof

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Application publication date: 20170804