CN104546615A - Lotion containing moringa-oleifera-leaf plant extract and preparation method thereof - Google Patents
Lotion containing moringa-oleifera-leaf plant extract and preparation method thereof Download PDFInfo
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- CN104546615A CN104546615A CN201510035119.7A CN201510035119A CN104546615A CN 104546615 A CN104546615 A CN 104546615A CN 201510035119 A CN201510035119 A CN 201510035119A CN 104546615 A CN104546615 A CN 104546615A
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Abstract
The invention discloses lotion containing moringa-oleifera-leaf plant extract and a preparation method thereof and belongs to the technical field of cosmetics. The lotion comprises the following components by weight percent: 5%-8% of moisturizing-agent glycerinum, 0.03%-0.06% of transparent sodium hyaluronate, 0.1%-0.3% of allantoin, 0.1%-0.3% of water-soluble vitamin E, 0.05%-0.1% of carbomer 940, 0.02%-0.08% of EDTA-2NA, 0.01%-15% of moringa-oleifera-leaf plant extract, 0.005%-0.02% of essence and the balance of water. The prepared lotion disclosed by the invention is full in effective components, good in moisturizing effect and strong in wrinkle essence; and due to pure-natural extraction, the lotion is suitable for use of various skin types.
Description
Technical field
The present invention relates to cosmetic technical field, particularly relate to a kind of astringent containing leaf of Moringa plant extract and preparation method thereof.
Background technology
Moringa (Moringa oleifera Lam.), be also called drumstick tree, Capparales Moringaceae plant, originates in India, is perennial tropical deciduous tree.Moringa taste is like Herba Spinaciae, and delicate fragrance is good to eat, is one of edible vegetable in India local people daily life.Leaf and the tender fruit pod of Moringa contain abundant nutritional labeling, gross protein value 25-29g in 100g leaf of Moringa dry powder, and crude fat content is about 8-9g, dietary fiber content 21-25g; Be rich in and enrich trace element, wherein calcium content 1800-2600mg, potassium content 1500-1800mg, iron content 200-500mg; Be rich in abundant vitamin, wherein VA content 34mg, VC content 54mg.The data display that FAO provides, as long as the leaf of Moringa dry powder of three soupspoons (about 25g) just containing needed for child every day 270% VA, the protein of 42%, the calcium of 125%, the ferrum of 70% and the Vc of 22%, being equivalent to calcareous is four times of milk, protein is two times of milk, and potassium is three times of Fructus Musae, and ferrum is three times of Herba Spinaciae, vitamin C is seven times of Citrus, and vitamin A (bata-carotene) is four times of Radix Dauci Sativae.For the women in conceived and suckling, leaf of Moringa can help me and fetus or baby to remain healthy, supplies a large amount of protein, minerals and vitamins.Its nutritive value is suitable with spirulina to have scholar to think.In addition, Moringa is also containing various bioactivators, and wherein antioxidative material just reaches kind more than 40, has augment nutritional as vegetable and food, the function of Dietotherapy health; Also be widely used in the aspect such as medicine, health care, be described as " Tree of Life ", " diamond in plant ".Moringa eats the best raw, but very short as fresh vegetables storage time; The biosynthesis amount of Moringa is high, is badly in need of carrying out deep processed product exploitation.
At present, the research of the converted productss such as leaf of Moringa powder, Pterigospermin capsules, Moringa cookies, Moringa noodles, Moringa Yoghourt, Moringa tea of domestic and international patent and reported in literature, but the utilization of leaf of Moringa in cosmetics water is uncommon, especially lack the astringent correlation technique with leaf of Moringa composition.
Astringent also claims firming lotion, cosmetic water, and its effect is just the pH-value again cleaning to recover skin surface, and nurses one's health horny layer, makes skin absorb nutrition better, and prepares for application maintenance product.So after people's washed, use cosmetic water, moisture content can be supplemented rapidly.In concrete kind, in general oily skin uses firming lotion, and healthy skin uses cosmetic water, and dry skin uses toner/smoothing toner, and mixing skin uses firming lotion.Although current astringent is on the market a feast for the eyes, of a great variety, but great majority all contain the chemical substances such as salicylic acid to play clean-keeping function, the nutrient substance that certain stimulation and skin can be caused to absorb to skin is like this few and single, special for hebetic people, because hormone secretion own is vigorous, oils and fats is more, skin is comparatively responsive, the symptoms such as container acne, stimulate the stimulation of composition that skin can be caused more to worsen if be subject to salicylic acid in astringent etc. again; Also containing antiseptic such as Kazon class, parabens, Bronopol classes in many astringent, these antiseptic may cause potential injury to human body, and long-time use can cause skin intensely dark, also likely damage skin surface; In addition, the nourishing composition in existing astringent is mostly not enough.Therefore be badly in need of one and not only can supplement moisture content, Yellow Gentian Extract, aging resistance, and without the leaf of Moringa astringent and preparation method thereof of any stimulation.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of astringent containing leaf of Moringa plant extract and preparation method thereof, the astringent manufacture method that should contain leaf of Moringa is simple, obtained astringent effective ingredient is sufficient, moistening effect is good, crease-resistant power is strong, and pure natural extracts, and is applicable to various skin quality and uses.
The technical solution used in the present invention is as follows:
A kind of astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 5%-8%, hyaluronate sodium 0.03%-0.06%, allantoin 0.1%-0.3%, water soluble vitamin E0.1%-0.3%, carbopol 940 0.05%-0.1%, EDTA-2NA 0.02%-0.08%, moringa oleifera leaf extractive 0.01%-15%, essence 0.005%-0.02%, surplus adds water.
Further, preferably pigment and antiseptic is also comprised.Wherein the addition of pigment and antiseptic meets state quality standard, without too much requirement.
Further, preferably described antiseptic is one or more combination in imidazolidinyl urea, methyl hydroxybenzoate and propyl hydroxybenzoate.Concrete ratio does not do requirement.
The present invention also provides a kind of preparation method of the astringent containing leaf of Moringa plant extract, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940 EDTA-2NA being joined together with water in emulsifying pot and to be heated to 84-86 DEG C, insulation 9-11 minute, stirs, obtains premix material;
C. the premix material that step B obtains is cooled to 58-62 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 37-40 DEG C, add essence, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
The present invention provides a kind of preparation method of the astringent containing leaf of Moringa plant extract in addition, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940 EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 85 DEG C, being incubated 10 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 60 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 38 DEG C, add essence, pigment and antiseptic, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
In technique scheme, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade frangible to blade drying, for subsequent use;
Step (2), is crushed to 250 ~ 350 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 65-75% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, backflow 2-3 hour, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:17-19(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 9-11%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:9-11(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Further, preferably described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade frangible to blade drying, for subsequent use;
Step (2), is crushed to 250 ~ 350 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 70% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, backflow 2-3 hour, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:18(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 10%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 110m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
compared with prior art, its beneficial effect is in the present invention:
(1) the invention provides a kind of astringent containing leaf of Moringa plant extract, this astringent effective ingredient is sufficient, and moistening effect is good, and crease-resistant power is strong, and pure natural extracts, and without any stimulation, is applicable to various skin quality and uses;
(2) extraction process of leaf of Moringa plant extract of the present invention is simple and reliable, fully extracts to the beneficiating ingredient of skin, goes grain to deposit the dregs of rice, is applicable to people to the demand of astringent;
(3) preparation method of astringent of the present invention is simple, and mild condition is applicable to commercial production, is easy to apply.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention.Unreceipted concrete technology or condition person in embodiment, according to the technology described by the document in this area or condition or carry out according to product description.Agents useful for same or the unreceipted production firm person of instrument, being can by buying the conventional products obtained.
Embodiment 1
Astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 5%, hyaluronate sodium 0.03%, allantoin 0.1%, water soluble vitamin E0.1%, carbopol 940 0.05%, EDTA-2NA 0.02%, moringa oleifera leaf extractive 0.01%, essence 0.005%, surplus adds water.
The preparation method of the astringent containing leaf of Moringa plant extract comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 84 DEG C, being incubated 9 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 58 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 37 DEG C, add essence, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
Astringent containing leaf of Moringa plant extract, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 250 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 65% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, refluxes 2 hours, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:17(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 9%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:9(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Embodiment 2
Astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 8%, hyaluronate sodium 0.06%, allantoin 0.3%, water soluble vitamin E0.3%, carbopol 940 0.1%, EDTA-2NA 0.08%, moringa oleifera leaf extractive 15%, essence 0.02%, surplus adds water.
The preparation method of the astringent containing leaf of Moringa plant extract, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 86 DEG C, being incubated 11 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 62 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 40 DEG C, add essence, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
Containing in the astringent of leaf of Moringa plant extract according to of the present invention, moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 350 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 75% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, refluxes 3 hours, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:19(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 11%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:11(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Embodiment 3
Astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 6.5%, hyaluronate sodium 0.04%, allantoin 0.2%, water soluble vitamin E0.2%, carbopol 940 0.08%, EDTA-2NA 0.06%, moringa oleifera leaf extractive 7%, essence 0.01%, surplus adds water.
The preparation method of the astringent containing leaf of Moringa plant extract, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 85 DEG C, being incubated 10 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 60 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 39 DEG C, add essence, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
Astringent containing leaf of Moringa plant extract, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 300 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 70% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, refluxes 2.5 hours, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:18(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 10%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:10(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Embodiment 4
Astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 6.5%, hyaluronate sodium 0.04%, allantoin 0.2%, water soluble vitamin E0.2%, carbopol 940 0.08%, EDTA-2NA 0.06%, moringa oleifera leaf extractive 7%, essence 0.01%, surplus adds water.
Astringent containing leaf of Moringa plant extract, comprises pigment and antiseptic, and the addition of pigment and antiseptic meets GB.
Astringent containing leaf of Moringa plant extract, described antiseptic is imidazolidinyl urea.
The preparation method of the astringent containing leaf of Moringa plant extract, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 85 DEG C, being incubated 10 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 60 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 39 DEG C, add essence, pigment and antiseptic, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
Astringent containing leaf of Moringa plant extract, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 300 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 70% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, refluxes 2.8 hours, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:17(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 10%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:11(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Embodiment 5
Astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 6.5%, hyaluronate sodium 0.04%, allantoin 0.2%, water soluble vitamin E0.2%, carbopol 940 0.08%, EDTA-2NA 0.06%, moringa oleifera leaf extractive 7%, essence 0.01%, surplus adds water.
Astringent containing leaf of Moringa plant extract, comprises pigment and antiseptic, and the addition of pigment and antiseptic meets GB.
Astringent containing leaf of Moringa plant extract, described antiseptic is methyl hydroxybenzoate and imidazolidinyl urea, and ratio is 1:1.
The preparation method of the astringent containing leaf of Moringa plant extract, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 85 DEG C, being incubated 10 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 60 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 39 DEG C, add essence, pigment and antiseptic, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
Astringent containing leaf of Moringa plant extract, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 300 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 70% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, refluxes 2.2 hours, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:19(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 10%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:9(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Embodiment 6
Astringent containing leaf of Moringa plant extract, comprise the following component according to mass percent: wetting agent glycerol 6.5%, hyaluronate sodium 0.04%, allantoin 0.2%, water soluble vitamin E0.2%, carbopol 940 0.08%, EDTA-2NA 0.06%, moringa oleifera leaf extractive 7%, essence 0.01%, surplus adds water.
Astringent containing leaf of Moringa plant extract, comprises pigment and antiseptic, and the addition of pigment and antiseptic meets GB.
Astringent containing leaf of Moringa plant extract, described antiseptic is imidazolidinyl urea, methyl hydroxybenzoate and propyl hydroxybenzoate, the not requirement of concrete ratio.
The preparation method of the astringent containing leaf of Moringa plant extract, comprises the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 85 DEG C, being incubated 10 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 60 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 38 DEG C, add essence, pigment and antiseptic, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
Astringent containing leaf of Moringa plant extract, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 300 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 70% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, refluxes 2.5 hours, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:18(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 10%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:10(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
Skin skin quality measures:
The astringent adopting the embodiment of the present invention 1 ~ 3 to prepare respectively is that example carries out skin skin quality mensuration.
First, select women's testee of 30 skin healths, it is experimental group that left half face of testee smears astringent prepared by the present invention, and it is blank group that right half face does not smear any material.Test 8 weeks by a definite date, the detection analysis of testee skin is carried out by every instrument respectively at the 4th week and the 8th week, assessment astringent for improvement effect of skin moisture content, skin elasticity, crease-resistant, skin coarseness, sebum secretion amount and enlarged pores number, the 1st week, the 4th week and the 8th Wednesday secondary meansigma methods of testing in table 1.
Table 1 skin skin quality improves effect
Table 1 result shows, crease-resistant, roughness, sebum secretion amount, the enlarged pores number of astringent of the present invention to skin all have minimizing in various degree, and to the effect that skin moisture content and skin elasticity are significantly increased, show product of the present invention and there is the effect improving skin skin quality.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof
.
Claims (7)
1. the astringent containing leaf of Moringa plant extract, it is characterized in that comprising the following component according to mass percent: wetting agent glycerol 5%-8%, hyaluronate sodium 0.03%-0.06%, allantoin 0.1%-0.3%, water soluble vitamin E0.1%-0.3%, carbopol 940 0.05%-0.1%, EDTA-2NA 0.02%-0.08%, moringa oleifera leaf extractive 0.01-15%, essence 0.005%-0.02%, surplus adds water.
2. the astringent containing leaf of Moringa plant extract according to claim 1, characterized by further comprising pigment and antiseptic.
3. the astringent containing leaf of Moringa plant extract according to claim 2, is characterized in that described antiseptic is one or more combination in imidazolidinyl urea, methyl hydroxybenzoate and propyl hydroxybenzoate.
4. the preparation method of the astringent containing leaf of Moringa plant extract according to claim 1, is characterized in that, comprise the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940, EDTA-2NA being joined together with water in emulsifying pot and to be heated to 84-86 DEG C, insulation 9-11 minute, stirs, obtains premix material;
C. the premix material that step B obtains is cooled to 58-62 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 37-40 DEG C, add essence, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
5. the preparation method of the astringent containing leaf of Moringa plant extract according to claim 2, is characterized in that, comprise the steps:
A. clean and disinfect emulsifying pot;
B. wetting agent glycerol, hyaluronate sodium, allantoin, water soluble vitamin E, carbopol 940 EDTA-2NA to be joined together with water in emulsifying pot and to be heated to 85 DEG C, being incubated 10 minutes, stirring, obtain premix material;
C. the premix material that step B obtains is cooled to 60 DEG C, add moringa oleifera leaf extractive and pH adjusting agent successively, after stirring, continue cooling, obtain mixed material;
D. after the mixed material that step C obtains being cooled to 38 DEG C, add essence, pigment and antiseptic, after mix homogeneously, obtain thick product;
F. the thick product that step D obtains is tested, after the assay was approved, filter, get filtrate, be the astringent containing leaf of Moringa plant extract.
6. the astringent containing leaf of Moringa plant extract according to any one of claims 1 to 3, it is characterized in that, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade to blade drying is frangible, for subsequent use;
Step (2), is crushed to 250 ~ 350 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 65-75% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, backflow 2-3 hour, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:17-19(m/v);
Step (4), filtrate concentrate drying powdered step (3) obtained, adds the 1,3 butylene glycol aqueous dissolution that concentration expressed in percentage by volume is 9%-11%, is uniformly dispersed, obtains dispersion liquid; Described powder quality and the volume ratio of 1,3 butylene glycol are 1:9-11(m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
7. the astringent containing leaf of Moringa plant extract according to claim 6, it is characterized in that, described moringa oleifera leaf extractive obtains in accordance with the following steps:
Step (1), preferably fresh tender leaf of Moringa, dries in the shade frangible to blade drying, for subsequent use;
Step (2), is crushed to 250 ~ 350 orders by the leaf of Moringa dried in the shade that step (1) obtains, obtains leaf of Moringa fine powder, for subsequent use;
Step (3), it is 70% ethanol that the leaf of Moringa fine powder obtained to step (2) adds concentration expressed in percentage by volume, backflow 2-3 hour, and filter, filtrate is for subsequent use; Described leaf of Moringa fine powder quality and the volume ratio of ethanol are 1:18(m/v);
Step (4), the filtrate concentrate drying powdered that step (3) is obtained, add that concentration expressed in percentage by volume is 10% 1,3-butanediol aqueous dissolution, is uniformly dispersed, obtains dispersion liquid, wherein be dried to powder quality and the volume ratio of 1,3 butylene glycol are 1:10 (m/v);
Step (5), dispersion liquid step (4) obtained filters, and collects filtrate, is leaf of Moringa plant extract.
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| CN105287290A (en) * | 2015-11-18 | 2016-02-03 | 关美玲 | Whitening and anti-aging face cleaner, and preparation method thereof |
| CN105380897A (en) * | 2015-08-20 | 2016-03-09 | 杨曼生 | Moringa oleifera SP water-soluble extraction golden particles |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104887577A (en) * | 2015-06-03 | 2015-09-09 | 桂林电子科技大学 | Preparation method of momordica grosvenori compound gel |
| CN104887577B (en) * | 2015-06-03 | 2017-09-15 | 桂林电子科技大学 | A kind of preparation method of Momordica grosvenori compound gel |
| CN105380897A (en) * | 2015-08-20 | 2016-03-09 | 杨曼生 | Moringa oleifera SP water-soluble extraction golden particles |
| CN105287290A (en) * | 2015-11-18 | 2016-02-03 | 关美玲 | Whitening and anti-aging face cleaner, and preparation method thereof |
| CN105287290B (en) * | 2015-11-18 | 2018-10-12 | 杭州施莱生物科技有限公司 | A kind of whitening anti-aging mildy wash and preparation method thereof |
| CN105963172A (en) * | 2016-04-29 | 2016-09-28 | 安徽恋尚你食品有限公司 | Moringa smoothing toner and preparation method thereof |
| CN106265456A (en) * | 2016-09-30 | 2017-01-04 | 中国热带农业科学院农产品加工研究所 | A kind of Moringa facial film and preparation method thereof |
| CN106902007A (en) * | 2017-02-17 | 2017-06-30 | 德宏州春雪化妆品销售有限公司 | A kind of Moringa elite, Moringa water and preparation method thereof |
| CN107080725A (en) * | 2017-04-19 | 2017-08-22 | 云南宁泽生物科技有限公司 | Moringa Chinese medicine epithelium maintenance liquid and its processing method |
| CN107281079A (en) * | 2017-06-17 | 2017-10-24 | 严贇华 | A kind of condensation frost |
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