CN107049830A - A kind of high stability hair conditioner and preparation method thereof - Google Patents
A kind of high stability hair conditioner and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
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Abstract
The invention discloses a kind of high stability hair conditioner, include per 100kg raw materials：NMF, cationic surfactant, amphoteric resin, assistant for emulsifying agent, oil, silicone oil, silicone oil emulsion, preservative, essence, acidity regulator and water.Present invention simultaneously discloses its preparation method.In hair conditioner formula of the present invention, due to mutual compatibility between each component, cooperate, cause amphoteric resin to can effectively ensure that the stability of whole hair conditioner system, especially low-temperature stability is good.
Description
Technical field
The present invention relates to a kind of hair conditioner and preparation method thereof, and in particular to a kind of high stability shield containing amphoteric resin
Element and preparation method thereof is sent out, belongs to household chemicals technical field.
Background technology
The impaired situation of the hair of modern is increasingly serious, and shampoo is difficult to meet to repair all required for damaged hair
Composition.Therefore consumer is more likely to select some quick-acting products, the reparation liquid for special nursing.Therefore hair conditioner produce
, it can close the epidermis scales of hair, make the smooth easy comb of healthy hair, and health is submissive, more can effectively be given than shampoo
Hair supplements the nutrients, and repairs damaged hair.
But, the stability problem of current hair conditioner product storage annoying always user, especially temperature less than
Subzero 18 DEG C, then be returned to after normal temperature, material, which is known from experience, after 12 hours there is coarse or water outlet phenomenon, i.e. traditional hair conditioner is put
In subzero 18 DEG C, no more than 12 hours, recover normal temperature material body just coarse；Place 24 hours, when recovering normal temperature, meeting in material body
There is a small amount of elutriation to go out, i.e. water outlet phenomenon, influence the total quality of product.
The content of the invention
To solve the deficiencies in the prior art, it is an object of the invention to provide a kind of good high stability shield of low-temperature stability
Send out element and preparation method thereof.
In order to realize above-mentioned target, the present invention is adopted the following technical scheme that：
A kind of high stability hair conditioner, includes per 100kg raw materials：
NMF：1-5kg；
Cationic surfactant：1-3kg；
Amphoteric resin：0.2-0.6kg；
Assistant for emulsifying agent：3-7kg；
Oil：1-3kg；
Silicone oil：1-3kg；
Silicone oil emulsion：1-3kg；
Preservative：0.05-0.1kg；
Essence：0.05-0.1kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
Form A phases after described humectant, cationic surfactant, amphoteric resin and water mixing, described assistant for emulsifying agent, oil
B phases are formed with after silicone oil mixing, and described silicone oil emulsion, preservative, essence and acidity regulator is classified as C phases.
Further preferably, above-mentioned high stability hair conditioner, includes per 100kg raw materials：
NMF：3kg；
Cationic surfactant：2kg；
Amphoteric resin：0.4kg；
Assistant for emulsifying agent：5kg；
Oil：2kg；
Silicone oil：2kg；
Silicone oil emulsion：2kg；
Preservative：0.1kg；
Essence：0.1kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
Form A phases after described NMF, cationic surfactant, amphoteric resin and water mixing, described assistant for emulsifying agent, oil
Divide and form B phases with after silicone oil mixing, and described silicone oil emulsion, preservative, essence and acidity regulator is classified as C phases.
Further, above-mentioned NMF be glycerine, propane diols, butanediol, panthenol, D-sorbite, dipropylene glycol, oneself two
At least one of alcohol, isopropanol, xylitol, trimethylglycine, polyethylene glycol.
Above-mentioned cationic surfactant is lauryl trimethyl ammonium chloride, cocotrimonium chloride, soya-bean oil fat
Base trimethyl ammonium chloride, hexadecyltrimethylammonium chloride, OTAC, behenyl base trimethyl ammonium chloride,
Butter aliphatic radical trimethyl ammonium chloride, octadecyl trimethyl sulfate methyl ammonium, cetearyl trimethyl ammonium chloride, cetearyl alcohol
Base alkyl dimethyl ammonium chloride, Varisoft 432PPG, h-tallow aliphatic radical octyldimethyl ammonium chloride, h-tallow fat
Base octyldimethyl Methylsulfate ammonium salt, stearic yl pyridines ammonium chloride, hard amide diallyidimethylammonium chloride, hard amide third
Base dimethylamine, PEG-5 stearyls ammonium chloride, lanolinamide ethyl trimethyl ethyl-sulfate ammonium salt, double h-tallow fat
Base alkyl dimethyl ammonium chloride, stearmide alcohol, stearylbenzyidimethylammonium ammonium chloride, acetamide propyltrimethylammonium chloride
At least one of ammonium.
Above-mentioned amphoteric resin is both sexes Hairstyling Resin, preferably VP/DMAPA acrylic acid（Ester）Analog copolymer, propylene
Acid or propylene/laruyl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylate copolymer, acrylic acid
Or at least one in propylene/laruyl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylate copolymer
Kind.
Above-mentioned assistant for emulsifying agent is：At least one of fatty alcohol, wax, stearate, and the described preferred 16- of fatty alcohol
18 alcohol.
Above-mentioned oil is：In vegetable oil, glyceryl ester, branched fatty alcohol, branched chain fatty acid, dimethicone at least
One kind, and the described preferred ethoxylated vegetable oil of vegetable oil.
Above-mentioned preservative is parabens, Kathon CG, Sensiva SC50, Phenoxyethanol, IPBC, benzoic acid
At least one of sodium, phenmethylol.
Above-mentioned essence is odorant.
And above-mentioned acidity regulator is then citric acid or lactic acid.
In addition, the preparation method of above-mentioned high stability hair conditioner, comprises the following steps：
S1：A phases each component is added into kettle according to quality proportioning first, B phases each component is added into oil cauldron point according to quality proportioning
Not Hun Hejunyun, and be heated separately to 80-85 DEG C；
S2：The 15-20% of A phases in kettle is drawn into emulsification pot, then the B phases in oil cauldron are sucked into emulsification pot, is then carried out
5-10min's homogenizes, in Homogenization, the clout for the A phases that substep is added in kettle, then keeps being stirred under vacuum 20min；
S3：Mixture after step S2 is stirred under vacuum is cooled to less than 40 DEG C, and C phases are then sequentially added in the state of stirring
In silicone oil emulsion, preservative, essence and acidity regulator, after being uniformly mixed, be cooled to room temperature, detect it is qualified after discharge
High stability hair conditioner is obtained, and the pH value of high stability hair conditioner is measured as 4.5-7.0 at 25 DEG C using dilution method.
The present invention is advantageous in that：In hair conditioner formula of the present invention, due to mutual compatibility, phase between each component
Mutually cooperation, causes amphoteric resin to can effectively ensure that the stability of whole hair conditioner system, especially low-temperature stability is good.
Embodiment
Make specific introduce to the present invention below in conjunction with specific embodiment.
In the present invention, the formula of high stability hair conditioner is as shown in the table：
Wherein, NMF selects glycerine, and cationic surfactant selects OTAC, and amphoteric resin is selected
VP/DMAPA acrylic acid（Ester）Analog copolymer, assistant for emulsifying agent selects 16-18 alcohol, and oil is odorant from 2EHP, essence.
Certainly, NMF is alternatively selection propane diols, butanediol, panthenol, D-sorbite, dipropylene glycol, hexylene glycol, isopropyl
At least one of alcohol, xylitol, trimethylglycine, polyethylene glycol.
Cationic surfactant is alternatively lauryl trimethyl ammonium chloride, cocotrimonium chloride, soya-bean oil aliphatic radical
Trimethyl ammonium chloride, hexadecyltrimethylammonium chloride, behenyl base trimethyl ammonium chloride, butter aliphatic radical trimethyl ammonium chloride, ten
Eight alkyl trimethyl sulfate methyl ammoniums, cetearyl trimethyl ammonium chloride, cetearyl alkyl dimethyl ammonium chloride, double hexadecanes
Base alkyl dimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl sulfate methyl ammonium
Salt, stearic yl pyridines ammonium chloride, hard amide diallyidimethylammonium chloride, hard amide diemethylamine, PEG-5 stearyl chlorides
Change ammonium, lanolinamide ethyl trimethyl ethyl-sulfate ammonium salt, double h-tallow aliphatic radical alkyl dimethyl ammonium chlorides, stearmide
At least one of alcohol, stearylbenzyidimethylammonium ammonium chloride, acetamide hydroxypropyltrimonium chloride.
Amphoteric resin can also be acrylic acid or propylene/laruyl alcohol acrylate/stearyl alcohol acrylate/ethamine oxidation
Thing methacrylate copolymer, acrylic acid or propylene/laruyl alcohol acrylate/stearyl alcohol acrylate/amine oxides
Methacrylate copolymer etc., and it is several to be not limited to the above.
Assistant for emulsifying agent can also be other fatty alcohols, wax, stearate etc..
And oil can also be then other plant oil, glyceryl ester, branched fatty alcohol, branched chain fatty acid, dimethicone
Deng.
Preservative is parabens, Kathon CG, Sensiva SC50, Phenoxyethanol, IPBC, sodium benzoate, phenmethylol
At least one of.
Acidity regulator can also be lactic acid.In the present invention, the pH value of the protein hydrolysate hair conditioner finally adjusted is
4.5-7.0。
A phases are formed after described NMF, cationic surfactant, amphoteric resin and water mixing, described helps emulsification
B phases are formed after agent, oil and silicone oil mixing, and described silicone oil emulsion, preservative, essence and acidity regulator is classified as C phases.
。
Above-mentioned 16-18 alcohol is cetostearyl alcohol.
The preparation method of hair conditioner described in above example is：
A phases are formed after glycerine, OTAC, amphoteric resin and water mixing, 16-18 alcohol, 2EHP, silicone oil are mixed
B phases are formed after conjunction, and silicone oil emulsion, preservative, essence and citric acid are referred to C phases.
Concretely comprise the following steps：
S1：A phases each component is added into kettle according to quality proportioning first, B phases each component is added into oil cauldron according to quality proportioning mixes
Close uniform, and be heated separately to 80-85 DEG C；
S2：The 15-20% of A phases in kettle is drawn into emulsification pot, then the B phases in oil cauldron are sucked into emulsification pot, is then carried out
5-10min's homogenizes, in Homogenization, the clout for the A phases that substep is added in kettle, then keeps being stirred under vacuum 20min；
S3：Mixture after step S2 is stirred under vacuum is cooled to less than 40 DEG C, and silicon is then sequentially added in the state of stirring
Fat liquor, preservative, essence and citric acid, after being uniformly mixed, are cooled to room temperature, detect that qualified rear discharging obtains high stable
Property hair conditioner.
Cold cycling test is carried out for the high stability hair conditioner that embodiment 1-4 and comparative example are prepared, it is tied
Fruit is as shown in table 1.
Table 1：The cold cycling result of different proportion amphoteric resin
。
As can be seen from Table 1：In the case of containing a small amount of amphoteric resin, 3 cold cyclings are all what is passed through, behind two
Defective material body is just varied from, and 5 cold cyclings of material body more than the amphoteric resin of 0.2 percentage composition all have no problem, and are free of
Cold cycling of formula of amphoteric resin is not all by.Therefore it can be said that the addition of amphoteric resin, substantially increases formula
Stability, is very helpful to the security and stability of product.
The basic principles, principal features and advantages of the present invention have been shown and described above.The technical staff of the industry should
Understand, the invention is not limited in any way for above-described embodiment, it is all to be obtained by the way of equivalent substitution or equivalent transformation
Technical scheme, all falls within protection scope of the present invention.
Claims (10)
1. a kind of high stability hair conditioner, it is characterised in that include per 100kg raw materials：
NMF：1-5kg；
Cationic surfactant：1-3kg；
Amphoteric resin：0.2-0.6kg；
Assistant for emulsifying agent：3-7kg；
Oil：1-3kg；
Silicone oil：1-3kg；
Silicone oil emulsion：1-3kg；
Preservative：0.05-0.1kg；
Essence：0.05-0.1kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
Form A phases after described humectant, cationic surfactant, amphoteric resin and water mixing, described assistant for emulsifying agent, oil
B phases are formed with after silicone oil mixing, and described silicone oil emulsion, preservative, essence and acidity regulator is classified as C phases.
2. a kind of high stability hair conditioner according to claim 1, it is characterised in that include per 100kg raw materials：
NMF：3kg；
Cationic surfactant：2kg；
Amphoteric resin：0.5kg；
Assistant for emulsifying agent：5kg；
Oil：2kg；
Silicone oil：2kg；
Silicone oil emulsion：2kg；
Preservative：0.1kg；
Essence：0.1kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
Form A phases after described NMF, cationic surfactant, amphoteric resin and water mixing, described assistant for emulsifying agent, oil
Divide and form B phases with after silicone oil mixing, and described silicone oil emulsion, preservative, essence and acidity regulator is classified as C phases.
3. a kind of described high stability hair conditioner according to claim 1 or 2, it is characterised in that described NMF
For glycerine, propane diols, butanediol, panthenol, D-sorbite, dipropylene glycol, hexylene glycol, isopropanol, xylitol, the sweet ammonia of trimethyl
At least one of acid, polyethylene glycol.
4. a kind of described high stability hair conditioner according to claim 1 or 2, it is characterised in that described cation
Surfactant is lauryl trimethyl ammonium chloride, cocotrimonium chloride, soya-bean oil aliphatic radical trimethyl ammonium chloride, hexadecane
Base trimethyl ammonium chloride, OTAC, behenyl base trimethyl ammonium chloride, butter aliphatic radical trimethyl ammonium chloride,
Octadecyl trimethyl sulfate methyl ammonium, cetearyl trimethyl ammonium chloride, cetearyl alkyl dimethyl ammonium chloride, double 16
Alkyl dimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl Methylsulfate
Ammonium salt, stearic yl pyridines ammonium chloride, hard amide diallyidimethylammonium chloride, hard amide diemethylamine, PEG-5 stearyls
Ammonium chloride, lanolinamide ethyl trimethyl ethyl-sulfate ammonium salt, double h-tallow aliphatic radical alkyl dimethyl ammonium chlorides, stearoyl
At least one of amine alcohol, stearylbenzyidimethylammonium ammonium chloride, acetamide hydroxypropyltrimonium chloride.
5. a kind of described high stability hair conditioner according to claim 1 or 2, it is characterised in that described both sexes tree
Fat is both sexes Hairstyling Resin, preferably VP/DMAPA acrylic acid（Ester）Analog copolymer, acrylic acid or propylene/laruyl alcohol third
Olefin(e) acid ester/stearyl alcohol acrylate/amine oxides methacrylate copolymer, acrylic acid or propylene/laruyl alcohol propylene
At least one of acid esters/stearyl alcohol acrylate/amine oxides methacrylate copolymer.
6. described a kind of high stability hair conditioner according to claim 1 or 2, it is characterised in that described helps emulsification
Agent is：At least one of fatty alcohol, wax, stearate, and the described preferred 16-18 alcohol of fatty alcohol.
7. described a kind of high stability hair conditioner according to claim 1 or 2, it is characterised in that described oil is：
At least one of vegetable oil, glyceryl ester, branched fatty alcohol, branched chain fatty acid, dimethicone, and described vegetable oil is excellent
Select ethoxylated vegetable oil.
8. a kind of described high stability hair conditioner according to claim 1 or 2, it is characterised in that described preservative
For at least one in parabens, Kathon CG, Sensiva SC50, Phenoxyethanol, IPBC, sodium benzoate, phenmethylol
Kind.
9. described a kind of high stability hair conditioner according to claim 1 or 2, it is characterised in that described essence is
Odorant, described acidity regulator is citric acid or lactic acid.
10. the preparation method of the high stability hair conditioner described in a kind of claim 1 or 2, it is characterised in that including following step
Suddenly：
S1：A phases each component is added into kettle according to quality proportioning first, B phases each component is added into oil cauldron point according to quality proportioning
Not Hun Hejunyun, and be heated separately to 80-85 DEG C；
S2：The 15-20% of A phases in kettle is drawn into emulsification pot, then the B phases in oil cauldron are sucked into emulsification pot, is then carried out
5-10min's homogenizes, in Homogenization, the clout for the A phases that substep is added in kettle, then keeps being stirred under vacuum 20min；
S3：Mixture after step S2 is stirred under vacuum is cooled to less than 40 DEG C, and C phases are then sequentially added in the state of stirring
In silicone oil emulsion, preservative, essence and acidity regulator, after being uniformly mixed, be cooled to room temperature, detect it is qualified after discharge
High stability hair conditioner is obtained, and the pH value of high stability hair conditioner is measured as 4.5-7.0 at 25 DEG C using dilution method.
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| CN107898653A (en) * | 2017-12-30 | 2018-04-13 | 杭州高烯科技有限公司 | A kind of graphene hair conditioner and preparation method thereof |
| CN108478461A (en) * | 2018-03-22 | 2018-09-04 | 东莞市椰乡小镇实业发展有限公司 | A kind of hair conditioner formula and its application method |
| CN108578259A (en) * | 2018-06-06 | 2018-09-28 | 张小伏 | A kind of antibacterial anti-aging black hair conditioner and preparation method thereof |
| CN109846736A (en) * | 2019-01-04 | 2019-06-07 | 澳宝化妆品（惠州）有限公司 | A kind of transparent liquid hair conditioner and preparation method thereof |
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| CN107898653A (en) * | 2017-12-30 | 2018-04-13 | 杭州高烯科技有限公司 | A kind of graphene hair conditioner and preparation method thereof |
| CN108478461A (en) * | 2018-03-22 | 2018-09-04 | 东莞市椰乡小镇实业发展有限公司 | A kind of hair conditioner formula and its application method |
| CN108578259A (en) * | 2018-06-06 | 2018-09-28 | 张小伏 | A kind of antibacterial anti-aging black hair conditioner and preparation method thereof |
| CN109846736A (en) * | 2019-01-04 | 2019-06-07 | 澳宝化妆品（惠州）有限公司 | A kind of transparent liquid hair conditioner and preparation method thereof |
| CN109846736B (en) * | 2019-01-04 | 2021-05-28 | 澳宝化妆品（惠州）有限公司 | Transparent liquid hair conditioner and preparation method thereof |
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