CN101444464A - Emulsified elastin composition - Google Patents
Emulsified elastin composition Download PDFInfo
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- CN101444464A CN101444464A CNA2008102205161A CN200810220516A CN101444464A CN 101444464 A CN101444464 A CN 101444464A CN A2008102205161 A CNA2008102205161 A CN A2008102205161A CN 200810220516 A CN200810220516 A CN 200810220516A CN 101444464 A CN101444464 A CN 101444464A
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Abstract
An emulsified elastin composition comprises: (A) a setting agent which accounts for 0.02%-15.0% of the weight of the composition; (B) a cation polymer which accounts for 0.01%-0.5% of the weight of the composition; (C) an emulsifier which accounts for 0.5%-5.0% of the weight of the composition; (D) a moisturizer composition which consists of (i) nonvolatile dimethyl silicone polymer which accounts for 0.5%-5.0% of the weight of the composition; (ii) volatile dimethyl silicone polymer which accounts for 0.5%-6.0% of the weight of the composition; (iii) grease which accounts for 0.05%-6.0% of the weight of the composition; and (E) water.
Description
Technical field
The present invention relates to a kind of hair setting composition, particularly a kind of elastin composition.
Background technology
Hair styling product in the market mainly is to see curry water and gel cream, this series products mainly is based on molding resin, be aided with a spot of composition of preserving moisture, have the oils and fats that nourishes composition and then be difficult to add its formula system, though, be difficult to reach simultaneously the purpose of nourishing healthy hair so products such as gel water, gel cream have the effect of finalizing the design preferably.Elastin is the novel approved product of a class, except molding resin, also contains compositions such as a large amount of silicone oil, oils and fats in its formula system, can correct be initiated to good moisturizing effect.Existing elastin mainly contains two kinds of suspension system and emulsification systems on the market, patent application 200830215848.1 disclosed powerful elements are suspension system, and product is easily smeared, good dispersion, but the fine and smooth degree of its product appearance is not good enough, also has the slight white phenomenon that rises in addition.The present invention adopts emulsification system, makes product appearance fine and smooth more, and moisture feeling was more outstanding when product used, and had successfully solved a white problem simultaneously, and the adding of volatile polydimethylsiloxaneand can also improve the gloss of hair, brings glittering effect.
Summary of the invention
The purpose of this invention is to provide a kind of emulsified elastin composition, not only contain molding resin in its formula system, also contain moist compositions such as non-volatile polydimethylsiloxane, volatile polydimethylsiloxaneand, oils and fats, can provide excellent conditioning effect, improve the gloss of hair for healthy hair.
Elastin composition of the present invention comprises:
(A) account for the setting agent of composition weight 0.02% to 15.0%;
(B) account for the cationic polymer of composition weight 0.01% to 0.5%;
(C) account for the emulsifying agent of composition weight 0.5% to 5.0%;
(D) moisturizing agent compositions composed of the following components: (i) account for the non-volatile polydimethylsiloxane of composition weight 0.5% to 5.0%; (ii) account for the volatile polydimethylsiloxaneand of composition weight 0.5% to 6.0%; (iii) account for the oils and fats of composition weight 0.05% to 6.0%; With
(E) surplus is a water.
Elastin composition of the present invention, wherein said setting agent are one or both in polyvinylpyrrolidone and derivant, acrylate derivative or the amphoteric resin.
Elastin composition of the present invention, one or both in wherein said setting agent vinylpyrrolidone/vinyl acetate copolymer, vinylpyrrolidone/quaternized dimethylaminoethyl methacrylate copolymer, caprolactam/vinylpyrrolidone/dimethylaminoethyl methacrylate copolymer, polyacrylate-2 cross linked polymer, acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer, the third methacryl ethyl betanin/acrylate copolymer.
Elastin composition of the present invention, wherein said cationic polymer is a cationic cellulose polymer.
Elastin composition of the present invention, wherein said emulsifying agent also have the effect of thickening agent simultaneously.
Elastin composition of the present invention, wherein said emulsifying agent are a kind of in the compositions of compositions, sodium acrylate copolymer and the hydrogenated polydecene of compositions, DMAA/ethyl-trimethyl salmiac methacrylic acid salt copolymer and the propylene glycol dicaprylate/dicaprate of polyquaternary ammonium salt-37 and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecane alcohol ether and polypropylene glycol-1 tridecanol ether-6 and C10-C11 isoparaffin and polypropylene glycol-1 tridecane alcohol ether-6.
Elastin composition of the present invention, the viscosity of wherein said non-volatile polydimethylsiloxane are 1000mPa.s～850000mPa.s.
Elastin composition of the present invention, wherein said volatile polydimethylsiloxaneand is at least a in six polydimethylsiloxane of ring five polydimethylsiloxane, ring.
Elastin composition of the present invention, wherein said oils and fats are a kind of in isopropyl palmitate, isopropyl myristate, sad capric acid triglyceride, Polyethylene Glycol-7 glyceryl cocoate.
Elastin composition of the present invention, it also contains the glycerol that accounts for composition weight 0.5% to 6.0%.
Elastin composition of the present invention, it can also contain the brightener that accounts for composition weight 0.0% to 5.0%.
Elastin composition of the present invention, wherein said brightener are the poly-trimethicone of phenyl.
Elastin composition of the present invention, optimization formula is: the polyvinylpyrrolidone or the vinylpyrrolidone/vinyl acetate copolymer that (A) account for composition weight 0.05% to 10.0%;
(B) account for the polyquaternary ammonium salt-10 of composition weight 0.02% to 0.4%;
(C) account for the compositions of polyquaternary ammonium salt-37 and the propylene glycol dicaprylate/dicaprate and the polypropylene glycol-1 tridecane alcohol ether of composition weight 0.8% to 4.0%;
(D) moisturizing agent compositions composed of the following components: (i) account for the non-volatile polydimethylsiloxane of composition weight 0.8% to 4.0%, the viscosity of non-volatile polydimethylsiloxane is 1500mPa.s～800000mPa.s; (ii) account for ring five polydimethylsiloxane of composition weight 0.8% to 5.0%; (iii) account for the isopropyl palmitate of composition weight 0.1% to 5.0%; With
(E) surplus is a water.
To be elaborated to component selection of the present invention and effect below.
In the bright elastin composition of this law, contain and account for compound weight 0.02% to 15.0%, preferred 0.05% to 10.0% setting agent, described setting agent is polyvinylpyrrolidone and derivant or acrylate derivative, and described setting agent is a polyvinylpyrrolidone, vinylpyrrolidone/vinyl acetate copolymer, vinylpyrrolidone/quaternized dimethylaminoethyl methacrylate copolymer, caprolactam/vinylpyrrolidone/dimethylaminoethyl methacrylate copolymer, polyacrylate-2 cross linked polymer, in acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer one or both.Described polyvinylpyrrolidone is called for short PVP, satisfy structural formula (I), PVP is a kind of water miscible polyamide, can be divided into four kinds of viscosity grade: K-15, K-30, K-60, K-90 according to the K value, its number average relative molecular mass is respectively: 10000,40000,160000,360000, and bright preferred K-30 of this law and K-90.
Described vinylpyrrolidone/vinyl acetate copolymer is called for short PVP/VA, satisfies structural formula (II), and to make the averagemolecular wt amount of vinylpyrrolidone/vinyl acetate copolymer be 2000～50000 to the numerical value of m, n in the formula.Vinylpyrrolidone/vinyl acetate copolymer is a kind of water-soluble polymer, the copolymer of forming by different proportion by vinylpyrrolidone and vinyl acetate, have the advantage of vinylpyrrolidone and vinyl acetate two base polymers concurrently, can form hard and glossiness thin film in hair surface, but the more serious white problem that rises is arranged.Ratio according to vinylpyrrolidone and vinyl acetate is different, and product mainly contains PVP/VA:70/30,60/40,50/50,30/70 etc., and preferred PVP/VA is vinylpyrrolidone/vinyl acetate copolymer of 70/30.
Described vinylpyrrolidone/quaternized dimethylaminoethyl methacrylate copolymer is called for short PVP/DMAEMAQ, satisfy structural formula (III), to make the averagemolecular wt amount of vinylpyrrolidone/quaternized dimethylaminoethyl methacrylate copolymer be 80000～1500000 to the numerical value of m, n in the formula, this polymer is cationic water-soluble polymer, hair had affinity interaction preferably, can form transparent, inviscid, successional thin film in hair surface, effect with setting agent can also be given hair gloss simultaneously.
Described caprolactam/vinylpyrrolidone/dimethylaminoethyl methacrylate copolymer is called for short VCL/PVP/DMAEMA, satisfies structural formula (IV).Described caprolactam/vinylpyrrolidone/dimethylaminoethyl methacrylate copolymer is a kind of water-soluble polymer with cationic property, typing intensity is big, and can keep good typing effect under super-humid conditions, be a kind of good setting agent.
Described polyacrylate-2 cross linked polymer is a kind of acrylate copolymer of slight collateralization of novelty, have siloxane chain and hydrophobicity side chain, have good moisture-proof and typing effect, the sheet bits come off low, characteristic such as be not clamminess after doing, typical case's representative of described polyacrylate-2 cross linked polymer is the Fixate Superhold polymer of Lubrizol Corp..Described acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer is an amphoteric resin, comprises with lower unit (V) in its molecular structure and (VI).
In the formula, R is hydrogen or C
1～C
22It is 4000～300000 that alkyl, the numerical value of m, n make the relative mean molecule quantity of acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer.Contain hydrophobicity and hydrophilic two parts group in its molecule, similar to hair structure, good to the affinity of hair, can on hair, form the slick coating of homogeneous, coating is incrust, thereby has not almost had white phenomenon.Existing hard hydrophobic part also has soft hydrophobic part in the molecular structure of described acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer, such structure is given its certain elasticity, have good persistency, but the typing undercapacity.Described acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer is the DIAFORMER Z-631 of Mitsubishi chemical Co., Ltd.Other is applicable to that amphoteric resin of the present invention also has DIAFORMER Z-632, the DIAFORMER Z-651 etc. of Mitsubishi Chemical.Described third methacryl ethyl betanin/acrylate copolymer is an amphoteric resin, mainly is by following three base polymer monomer polymerizations by a certain percentage, carries out bisexual ion purification then and makes.
a、CH
2＝CCH
3-COO-(CH
2)
2-N(CH
3)
2
b、CH
2＝CCH
3-COO-R
1
c、CH
2＝CCH
3-COO-R
2
R wherein
1Be C
1-C
4Alkyl, R
2Be C
10-C
20Alkyl.All kinds of monomeric ratio differences, the character of formed polymer are difference to some extent also, and suitable hair quality and the proportioning in compositions also have difference.In the used polymer of the present invention, the ratio that the addition of a, b, c accounts for a, b, the total addition of c is as follows, a:50%-70%, b:10%-40%, c:8%-20%.
Contain in the bright elastin composition of this law and account for composition weight 0.01% to 0.5%, preferred 0.02% to 0.4% cationic polymer, described cationic polymer is a cationic cellulose polymer.Described cationic cellulose polymer is the copolymer of hydroxyethyl-cellulose and alkyl trimethyl ammonium chloride, difference according to the cation substitution value can be divided into: high-cation substitution value JR, middle-jiao yang, function of the spleen and stomach ionic replacement degree LR and three kinds of models of low cation substitution value LK, the cationic cellulose polymer of preferred high-cation substitution value, be polyquaternary ammonium salt-10, other is suitable for cationic cellulose polymer of the present invention and also has copolymer of hydroxyethyl-cellulose and dialkyl dimethyl ammonium chloride etc.
Contain in the bright elastin composition of this law and account for composition weight 0.5% to 5.0%, preferred 0.8% to 4.0% emulsifying agent, described emulsifying agent also has the effect of thickening agent simultaneously, and described emulsifying agent is the compositions of polyquaternary ammonium salt-37 and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecane alcohol ether, the compositions of DMAA/ethyl-trimethyl salmiac methacrylic acid salt copolymer and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecanol ether-6 and C10-C11 isoparaffin, a kind of in the compositions of sodium acrylate copolymer and hydrogenated polydecene and polypropylene glycol-1 tridecane alcohol ether-6.The compositions of described polyquaternary ammonium salt-37 and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecane alcohol ether is that this white is mobile liquid, its active component is the cationic homopolymer that is scattered in the crude vegetal, the effect that also has conditioning in formula system except that the emulsifying thickening, typical case's representative of the compositions of described polyquaternary ammonium salt-37 and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecane alcohol ether is the Salcare SC96 of Ciba company limited.The compositions of described DMAA/ethyl-trimethyl salmiac methacrylic acid salt copolymer and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecanol ether-6 and C10-C11 isoparaffin is white flowable emulsion, the solid content of its commercially available prod is about 54%, viscosity is 250cPs, the compositions of described DMAA/ethyl-trimethyl salmiac methacrylic acid salt copolymer and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecanol ether-6 and C10-C11 isoparaffin also has the effect of reparation to impaired hair, can effectively improve the plentiful degree and the gloss of hair, its typical case's representative is the TINOVIS CD of Ciba company limited.The compositions of described sodium acrylate copolymer and hydrogenated polydecene and polypropylene glycol-1 tridecane alcohol ether-6 is white flowable emulsions, the solid content of its commercially available prod is about 54%, viscosity is 250cPs, the compositions of described sodium acrylate copolymer and hydrogenated polydecene and polypropylene glycol-1 tridecane alcohol ether-6 can be given good feel of hair and gloss, and its typical case's representative is the TINOVIS ADE of Ciba company limited.
Contain in the bright elastin composition of this law and account for composition weight 0.5% to 5.0%, preferred 0.8% to 4.0% non-volatile polydimethylsiloxane, the viscosity of described non-volatile polydimethylsiloxane is 1000mPa.s～850000mPa.s.Contain in the bright elastin composition of this law and account for composition weight 0.5% to 6.0%, preferred 0.8% to 5.0% volatile polydimethylsiloxaneand, described volatile polydimethylsiloxaneand is at least a in six polydimethylsiloxane of ring five polydimethylsiloxane, ring.Contain in the bright elastin composition of this law and account for composition weight 0.05% to 6.0%, preferred 0.1% to 5.0% oils and fats, described oils and fats are a kind of in isopropyl palmitate, isopropyl myristate, sad capric acid triglyceride, Polyethylene Glycol-7 glyceryl cocoate.
Also contain the glycerol that accounts for composition weight 0.5% to 6.0% in the elastin composition of the present invention, the effect of wetting agent is mainly played in the adding of described glycerol.Elastin composition of the present invention can also contain the brightener that accounts for composition weight 0.0% to 5.0%, and described brightener is the poly-trimethicone of phenyl.The index of refraction of the poly-trimethicone of described phenyl is 1.45～1.47, is water white liquid, and its high index of refraction can make hair present high gloss, for healthy hair brings glittering visual effect.
In the elastin composition of the present invention, also contain an amount of antiseptic, essence, pigment etc.Choosing of described antiseptic, essence, pigment meets the regulation of hygienic standards for cosmetics, selects safe raw material for use.
The specific embodiment
Be the non-limiting example of elastin composition of the present invention below.Providing of these embodiment only is for illustrative purposes, can not be interpreted as limitation of the invention, because without departing from the spirit and scope of the present invention, can carry out many changes to the present invention.In these embodiments, unless stated otherwise, all concentration all is percentage by weight.
Preparation example I-XV
Elastin composition of the present invention can by any known or other effectively be applicable to the technology preparation that hair setting composition is provided, the method for preparing elastin composition of the present invention comprises conventional preparation and hybrid technology.The suitable method for preparing elastin composition described in example I-XV is as follows: suitable quantity of water is joined in the retort, add polyvinylpyrrolidone, vinylpyrrolidone/vinyl acetate copolymer, cationic cellulose polymer, glycerol, emulsifing thickener successively, mix homogeneously, this is a water; In another retort, add non-volatile polydimethylsiloxane, volatile polydimethylsiloxaneand, oils and fats, the poly-trimethicone of phenyl, mix homogeneously, this is an oil phase; Then water is added in the oil phase, the back that stirs adds essence, antiseptic, pigment, stirs to get final product.
Example I-V
Example VI-X
Example VI-XV
Claims (12)
1. elastin composition comprises:
(A) account for the setting agent of composition weight 0.02% to 15.0%;
(B) account for the cationic polymer of composition weight 0.01% to 0.5%;
(C) account for the emulsifying agent of composition weight 0.5% to 5.0%;
(D) moisturizing agent compositions composed of the following components: (i) account for the non-volatile polydimethylsiloxane of composition weight 0.5% to 5.00%; (ii) account for the volatile polydimethylsiloxaneand of composition weight 0.5% to 6.0%; (iii) account for the oils and fats of composition weight 0.05% to 6.0%; With
(E) surplus is a water.
2. elastin composition according to claim 1, wherein said setting agent are one or both in polyvinylpyrrolidone and derivant, acrylate derivative or the amphoteric resin.
3. elastin composition according to claim 2, one or both in wherein said setting agent vinylpyrrolidone/vinyl acetate copolymer, vinylpyrrolidone/quaternized dimethylaminoethyl methacrylate copolymer, caprolactam/vinylpyrrolidone/dimethylaminoethyl methacrylate copolymer, polyacrylate-2 cross linked polymer, acrylate/lauryl alcohol acrylate/stearyl alcohol acrylate/amine oxides methacrylic acid salt copolymer, the third methacryl ethyl betanin/acrylate copolymer.
4. according to the described elastin composition of aforementioned each claim, wherein said cationic polymer is a cationic cellulose polymer.
5. according to the elastin composition of aforementioned each claim, wherein said emulsifying agent is compositions, DMAA/ethyl-trimethyl salmiac methacrylic acid salt copolymer and propylene glycol dicaprylate/dicaprate and the polypropylene glycol-1 tridecanol ether-6 and the C of polyquaternary ammonium salt-37 and propylene glycol dicaprylate/dicaprate and polypropylene glycol-1 tridecane alcohol ether
10-C
11A kind of in the compositions of the compositions of isoparaffin, sodium acrylate copolymer and hydrogenated polydecene and polypropylene glycol-1 tridecane alcohol ether-6.
6. according to the described elastin composition of aforementioned each claim, the viscosity of wherein said non-volatile polydimethylsiloxane is 1000mPa.s～850000mPa.s.
7. according to the described elastin composition of aforementioned each claim, at least a in ring five polydimethylsiloxane, ring six polydimethylsiloxane of wherein said volatile polydimethylsiloxaneand.
8. according to the described elastin composition of aforementioned each claim, wherein said oils and fats is a kind of in isopropyl palmitate, isopropyl myristate, sad capric acid triglyceride, Polyethylene Glycol-7 glyceryl cocoate.
9. according to the described elastin composition of aforementioned each claim, it also contains the glycerol that accounts for composition weight 0.5% to 6.0%.
10. according to the described elastin composition of aforementioned each claim, it can also contain the brightener that accounts for composition weight 0.0% to 5.0%.
11. being phenyl, elastin composition according to claim 10, wherein said brightener gather trimethicone.
12. elastin composition according to claim 1 comprises:
(A) account for the polyvinylpyrrolidone or the vinylpyrrolidone/vinyl acetate copolymer of composition weight 0.05% to 10.0%;
(B) account for the polyquaternary ammonium salt-10 of composition weight 0.02% to 0.4%;
(C) account for composition weight 0.8% to 4.0% polyquaternary ammonium salt-37 (with) propylene glycol dicaprylate/dicaprate (with) polypropylene glycol-1 tridecane alcohol ether;
(D) moisturizing agent compositions composed of the following components: (i) account for the non-volatile polydimethylsiloxane of composition weight 0.8% to 4.0%, the viscosity of non-volatile polydimethylsiloxane is 1500mPa.s～800000mPa.s; (ii) account for ring five polydimethylsiloxane of composition weight 0.8% to 5.0%; (iii) account for the isopropyl palmitate of composition weight 0.1% to 5.0%; (E) surplus is a water.
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| CN2008102205161A CN101444464B (en) | 2008-12-29 | 2008-12-29 | Emulsified elastin composition |
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|---|---|---|---|
| CN2008102205161A CN101444464B (en) | 2008-12-29 | 2008-12-29 | Emulsified elastin composition |
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| CN101444464B CN101444464B (en) | 2011-04-06 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488629A (en) * | 2011-12-21 | 2012-06-13 | 广州好迪集团有限公司 | Hairspray and hair shaping product |
| CN105213223A (en) * | 2015-06-30 | 2016-01-06 | 朱耀灯 | A kind of Oleum Camelliae elastin and preparation method thereof |
| CN107049830A (en) * | 2017-05-04 | 2017-08-18 | 上海章华保健化妆品有限公司 | A kind of high stability hair conditioner and preparation method thereof |
| CN107669510A (en) * | 2017-08-29 | 2018-02-09 | 澳宝化妆品（惠州）有限公司 | A kind of hair shield type composition using novel cation shield type agent |
-
2008
- 2008-12-29 CN CN2008102205161A patent/CN101444464B/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488629A (en) * | 2011-12-21 | 2012-06-13 | 广州好迪集团有限公司 | Hairspray and hair shaping product |
| CN102488629B (en) * | 2011-12-21 | 2012-11-14 | 广州好迪集团有限公司 | Hairspray and hair shaping product |
| CN105213223A (en) * | 2015-06-30 | 2016-01-06 | 朱耀灯 | A kind of Oleum Camelliae elastin and preparation method thereof |
| CN107049830A (en) * | 2017-05-04 | 2017-08-18 | 上海章华保健化妆品有限公司 | A kind of high stability hair conditioner and preparation method thereof |
| CN107669510A (en) * | 2017-08-29 | 2018-02-09 | 澳宝化妆品（惠州）有限公司 | A kind of hair shield type composition using novel cation shield type agent |
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|---|---|
| CN101444464B (en) | 2011-04-06 |
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Owner name: LAFANG CHEMICAL CO., LTD. Free format text: FORMER NAME: GUANGDONG LAFANG DAILY CHEMICALS CO., LTD. |
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Address after: 515144 LaFang industrial town, Xin Qing Road, 324 National Highway, Chaonan District, Guangdong, Shantou Patentee after: LAF International Group Limited Address before: 515000 D building, 16 Longjiang Road, Wan Ji industrial district, Guangdong, Shantou, China Patentee before: Guangdong Lafang Daily Chemicals Co., Ltd. |