CN108815020A - A kind of disposable nutrition profit hair-cream preparation method of water conservation - Google Patents
A kind of disposable nutrition profit hair-cream preparation method of water conservation Download PDFInfo
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- CN108815020A CN108815020A CN201810676001.6A CN201810676001A CN108815020A CN 108815020 A CN108815020 A CN 108815020A CN 201810676001 A CN201810676001 A CN 201810676001A CN 108815020 A CN108815020 A CN 108815020A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- General Health & Medical Sciences (AREA)
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- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of disposable nutrition of water conservation to moisten hair-cream preparation method, includes the following steps：Gelatin, dimethyl dodecyl base tertiary amine, water are stirred evenly, regulation system pH value is 6.4-6.8, and glutamic acid stirring is added, acetone is added, temperature stirring is adjusted, epoxychloropropane is added under stirring, continues to stir, it is cooling, it stands, regulation system continues to stir in alkalinity, it filters, vacuum drying obtains gelatin glutamic acid compound；Olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearate, glycerol are mixed, heating stirring obtains premix a to dissolving completely；Extract solution from aloe, passion fruit extracting solution, collagen polypeptide, hexadecyltrimethylammonium chloride, preservative, pearling agent, deionized water are mixed, heating stirs evenly, and obtains premix b；Premix a, premix b are stirred, homogeneous processing obtains being retained disposable nutrition profit hair-cream.
Description
Technical field
The present invention relates to profit hair-cream technical fields more particularly to a kind of disposable nutrition of water conservation to moisten hair-cream preparation method.
Background technique
Common hair conditioner is all washing-off type, in washing process a large amount of nutriment be not by hair absorption but by
Washing is gone, so not only waste of resource, but also pollution environment.The disposable nutrition profit hair-cream biggest advantage of collagen polypeptide is leave
, hair surface can be rested on and absorbed at leisure by hair by moistening nutriment collagen polypeptide in hair-cream in use process.Collagen is more
Peptide can be absorbed by organisms rapidly in vivo, therefore can prevent hair from drying up, jaundice, bifurcated, bleach, fall off, but there is also antibacterial
The shortcomings that effect is poor, Water-saving effect can not meet demand, unstable product quality.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of disposable nutrition of water conservation to moisten hair-cream preparation side
Method, nutrition needed for can supplementing for hair, Water-saving effect is good, has and makes hair submissiveer, more beautiful and other effects, and bactericidal
Effect is good, is not easy to breed dandruff, does not block hair follicle.
Hair-cream preparation method is moistened in a kind of disposable nutrition of water conservation proposed by the present invention, is included the following steps：
S1, gelatin, dimethyl dodecyl base tertiary amine, water are stirred evenly, regulation system pH value is 6.4-6.8, and paddy is added
Propylhomoserin stirring, is added acetone, adjusts temperature stirring, epoxychloropropane is added under stirring, continues to stir, cooling, stands, adjusts
Section system continues to stir in alkalinity, filters, and vacuum drying obtains gelatin glutamic acid compound；
S2, olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearate, glycerol are mixed
It closes, heating stirring obtains premix a to dissolving completely；
S3, by extract solution from aloe, passion fruit extracting solution, collagen polypeptide, hexadecyltrimethylammonium chloride, preservative, pearl
Photo etching, deionized water mixing, heating stir evenly, and obtain premix b；
S4, premix a, premix b are stirred, homogeneous processing obtains being retained disposable nutrition profit hair-cream.
Preferably, in S1, the weight ratio of gelatin, dimethyl dodecyl base tertiary amine, water, glutamic acid, acetone, epoxychloropropane
For 10-20：4-8：60-100：8-16：60-100：2-6.
Preferably, in S1, gelatin, dimethyl dodecyl base tertiary amine, water are stirred evenly, using hydrochloric acid regulation system pH value
For 6.4-6.8, glutamic acid is added and stirs 3-5h, whipping temp is 45-55 DEG C, and acetone is added, adjusts the temperature to 55-65 DEG C of stirring
Epoxychloropropane is added under stirring in 10-20min, continues to stir 4-8h, cooling, stands 14-20h, and regulation system is in alkali
Property, continue to stir 10-20min, filter, vacuum drying obtains gelatin glutamic acid compound.
Preferably, in S2, olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearic acid
Ester, glycerol weight ratio be 8-16：15-25：2-4：2-4：2-4.
Preferably, in S2, by olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearic acid
Ester, glycerol mixing are warming up to 80-90 DEG C of stirring to dissolving completely, obtain premix a.
Preferably, in S3, extract solution from aloe, collagen polypeptide, hexadecyltrimethylammonium chloride, is prevented passion fruit extracting solution
Rotten agent, pearling agent, deionized water weight ratio be 4-8：3-5：2-4：2-4：2-4：2-4：120-160.
Preferably, in S3, by extract solution from aloe, passion fruit extracting solution, collagen polypeptide, hexadecyltrimethylammonium chloride,
Preservative, pearling agent, deionized water mixing, are warming up to 60-80 DEG C and stir evenly, obtain premix b.
Preferably, in S4, premix a, premix b weight ratio be 25-35：10-20.
Preferably, in S4, premix a, premix b are stirred into 2-5min, mixing speed 40-100r/min, homogeneous place
1-3min is managed, homogeneous speed is 2300-3400r/min, obtains being retained disposable nutrition profit hair-cream.
In S1 of the present invention, dimethyl dodecyl base tertiary amine promotes gelatin that self-crosslinking occurs, and the amino of glutamic acid, carboxyl can
It being crosslinked with the gelatin after crosslinking, water-absorbing-retaining effect is good, quaternary ammonium salt containing long alkyl chain further is formed with epichlorohydrin reaction,
Bactericidal property is good；In S2, gelatin glutamic acid compound is compounded with olive oil, good to the solute effect of nutriment, on hair
Face slow release is simultaneously gradually absorbed and utilized by hair, and help solves the problems, such as that hair is withered, jaundice, bifurcated, bleaches, falls off.
Low in raw material price of the invention, each index meet《QB/T1975-2013》Hair conditioner and《Cosmetics health
Specification》The requirement of version specification in 2007, nutrition needed for can supplementing for hair, Water-saving effect is good, has and makes hair submissiveer, more beautiful
It is beautiful and other effects, and bactericidal and bacteriostatic effect is good, is not easy to breed dandruff, does not block hair follicle.
The dry bacterium of excrement large intestine, staphylococcus aureus, deformable stem bacterium, green dense dry bacterium, total number of bacteria, black mould are carried out to the present invention
Aspergillus, pityrosporum furfur test, bacteriostasis rate of the invention are greater than 94%.
Specific embodiment
In the following, technical solution of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of disposable nutrition profit hair-cream preparation method of water conservation, includes the following steps：
S1,10kg gelatin, 8kg dimethyl dodecyl base tertiary amine, 60kg water are stirred evenly, using hydrochloric acid regulation system pH
Value is 6.4-6.8, and 16kg glutamic acid is added and stirs 3h, and whipping temp is 55 DEG C, and 60kg acetone is added, adjusts the temperature to 65 DEG C and stirs
10min is mixed, 6kg epoxychloropropane is added under stirring, continues to stir 4h, it is cooling, 20h is stood, regulation system is in alkalinity, after
Continuous stirring 10min, filters, vacuum drying obtains gelatin glutamic acid compound；
S2, by 16kg olive oil, 15kg gelatin glutamic acid compound, 4kg acetulan, 2kg cetostearyl alcohol
Stearate, the mixing of 4kg glycerol are warming up to 80 DEG C of stirrings to dissolving completely, obtain premix a；
S3, by 8kg extract solution from aloe, 3kg passion fruit extracting solution, 4kg collagen polypeptide, 2kg cetyl trimethyl chlorination
Ammonium, 4kg preservative, 2kg pearling agent, the mixing of 160kg deionized water, are warming up to 60 DEG C and stir evenly, obtain premix b；
S4,35kg premix a, 10kg premix b is stirred into 5min, mixing speed 40r/min, homogeneous processing 3min,
Homogeneous speed is 2300r/min, obtains being retained disposable nutrition profit hair-cream.
Embodiment 2
A kind of disposable nutrition profit hair-cream preparation method of water conservation, includes the following steps：
S1,20kg gelatin, 4kg dimethyl dodecyl base tertiary amine, 100kg water are stirred evenly, using hydrochloric acid regulation system
PH value is 6.4-6.8, and 8kg glutamic acid is added and stirs 5h, and whipping temp is 45 DEG C, and 100kg acetone is added, adjusts the temperature to 55 DEG C
Stir 20min, 2kg epoxychloropropane be added under stirring, continue to stir 8h, it is cooling, stand 14h, regulation system in alkalinity,
Continue to stir 20min, filter, vacuum drying obtains gelatin glutamic acid compound；
It is S2,8kg olive oil, 25kg gelatin glutamic acid compound, 2kg acetulan, 4kg cetostearyl alcohol is hard
Resin acid ester, the mixing of 2kg glycerol are warming up to 90 DEG C of stirrings to dissolving completely, obtain premix a；
S3, by 4kg extract solution from aloe, 5kg passion fruit extracting solution, 2kg collagen polypeptide, 4kg cetyl trimethyl chlorination
Ammonium, 2kg preservative, 4kg pearling agent, the mixing of 120kg deionized water, are warming up to 80 DEG C and stir evenly, obtain premix b；
S4,25kg premix a, 20kg premix b is stirred into 2min, mixing speed 100r/min, homogeneous processing 1min,
Homogeneous speed is 3400r/min, obtains being retained disposable nutrition profit hair-cream.
Embodiment 3
A kind of disposable nutrition profit hair-cream preparation method of water conservation, includes the following steps：
S1,12kg gelatin, 7kg dimethyl dodecyl base tertiary amine, 70kg water are stirred evenly, using hydrochloric acid regulation system pH
Value is 6.4-6.8, and 14kg glutamic acid is added and stirs 3.5h, and whipping temp is 52 DEG C, and 70kg acetone is added, adjusts the temperature to 62 DEG C
Stir 12min, 5kg epoxychloropropane be added under stirring, continue to stir 5h, it is cooling, stand 18h, regulation system in alkalinity,
Continue to stir 12min, filter, vacuum drying obtains gelatin glutamic acid compound；
It is S2,14kg olive oil, 18kg gelatin glutamic acid compound, 3.5kg acetulan, 2.5kg spermaceti is hard
Lipidol stearate, the mixing of 3.5kg glycerol are warming up to 82 DEG C of stirrings to dissolving completely, obtain premix a；
S3, by 7kg extract solution from aloe, 3.5kg passion fruit extracting solution, 3.5kg collagen polypeptide, 2.5kg cetyl front three
Ammonium chloride, 3.5kg preservative, 2.5kg pearling agent, the mixing of 150kg deionized water, are warming up to 65 DEG C and stir evenly, obtain pre-
Mixing b；
S4,32kg premix a, 12kg premix b is stirred into 3-4min, mixing speed 80r/min, homogeneous processing
1.5min, homogeneous speed are 3200r/min, obtain being retained disposable nutrition profit hair-cream.
Embodiment 4
A kind of disposable nutrition profit hair-cream preparation method of water conservation, includes the following steps：
S1,18kg gelatin, 5kg dimethyl dodecyl base tertiary amine, 90kg water are stirred evenly, using hydrochloric acid regulation system pH
Value is 6.4-6.8, and 10kg glutamic acid is added and stirs 4.5h, and whipping temp is 48 DEG C, and 90kg acetone is added, adjusts the temperature to 58 DEG C
Stir 18min, 3kg epoxychloropropane be added under stirring, continue to stir 7h, it is cooling, stand 16h, regulation system in alkalinity,
Continue to stir 18min, filter, vacuum drying obtains gelatin glutamic acid compound；
It is S2,10kg olive oil, 22kg gelatin glutamic acid compound, 2.5kg acetulan, 3.5kg spermaceti is hard
Lipidol stearate, the mixing of 2.5kg glycerol are warming up to 88 DEG C of stirrings to dissolving completely, obtain premix a；
S3, by 5kg extract solution from aloe, 4.5kg passion fruit extracting solution, 2.5kg collagen polypeptide, 3.5kg cetyl front three
Ammonium chloride, 2.5kg preservative, 3.5kg pearling agent, the mixing of 130kg deionized water, are warming up to 75 DEG C and stir evenly, obtain pre-
Mixing b；
S4,28kg premix a, 18kg premix b is stirred into 3min, mixing speed 80r/min, homogeneous processing
1.5min, homogeneous speed are 3200r/min, obtain being retained disposable nutrition profit hair-cream.
Embodiment 5
A kind of disposable nutrition profit hair-cream preparation method of water conservation, includes the following steps：
S1,15kg gelatin, 6kg dimethyl dodecyl base tertiary amine, 80kg water are stirred evenly, using hydrochloric acid regulation system pH
Value is 6.4-6.8, and 12kg glutamic acid is added and stirs 4h, and whipping temp is 50 DEG C, and 80kg acetone is added, adjusts the temperature to 60 DEG C and stirs
15min is mixed, 4kg epoxychloropropane is added under stirring, continues to stir 6h, it is cooling, 17h is stood, regulation system is in alkalinity, after
Continuous stirring 15min, filters, vacuum drying obtains gelatin glutamic acid compound；
It is S2,12kg olive oil, 2kg gelatin glutamic acid compound, 3kg acetulan, 3kg cetostearyl alcohol is hard
Resin acid ester, the mixing of 3kg glycerol are warming up to 85 DEG C of stirrings to dissolving completely, obtain premix a；
S3, by 6kg extract solution from aloe, 4kg passion fruit extracting solution, 3kg collagen polypeptide, 3kg cetyl trimethyl chlorination
Ammonium, 3kg preservative, 3kg pearling agent, the mixing of 140kg deionized water, are warming up to 70 DEG C and stir evenly, obtain premix b；
S4,30kg premix a, 15kg premix b is stirred into 3.5min, mixing speed 70r/min, homogeneous processing
2min, homogeneous speed are 3000r/min, obtain being retained disposable nutrition profit hair-cream.
Choose 200 have dandruff is more, itching of the scalp, hair dries up, jaundice, bifurcated, bleaches, fall off patient, wherein
Men and women each 100, the age is 20-60 years old.Moisten hair-cream using the disposable nutrition of water conservation obtained by an embodiment 5 every three days, continuously makes
With 5 weeks.
Experimental result shows that property of the present invention is mild, not only has the effect of hair washing, more can reduce itching of the scalp, reduces head
Scurf, the patient more than some dandruffs must wash a hair with similar product in the market daily, and after a week with this product,
Can be reduced to need to only wash weekly secondary hair, while water retaining function is also significant, and easily combing after washing, hair is glossy, submissive, prevent
Alopecia-stopping, disconnected hair effect are also relatively satisfactory.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. hair-cream preparation method is moistened in a kind of disposable nutrition of water conservation, which is characterized in that include the following steps：
S1, gelatin, dimethyl dodecyl base tertiary amine, water are stirred evenly, regulation system pH value is 6.4-6.8, and glutamic acid is added
Acetone is added in stirring, adjusts temperature stirring, epoxychloropropane is added under stirring, continues to stir, cooling, stands, adjusts body
System continues to stir in alkalinity, filters, and vacuum drying obtains gelatin glutamic acid compound；
S2, olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearate, glycerol are mixed,
Heating stirring obtains premix a to dissolving completely；
S3, by extract solution from aloe, passion fruit extracting solution, collagen polypeptide, hexadecyltrimethylammonium chloride, preservative, pearling agent,
Deionized water mixing, heating stir evenly, and obtain premix b；
S4, premix a, premix b are stirred, homogeneous processing obtains being retained disposable nutrition profit hair-cream.
2. being retained disposable nutrition profit hair-cream preparation method according to claim 1, which is characterized in that in S1, gelatin, dimethyl
Dodecyl tertiary amine, water, glutamic acid, acetone, epoxychloropropane weight ratio be 10-20：4-8：60-100：8-16：60-100：
2-6。
3. hair-cream preparation method is moistened in the disposable nutrition of water conservation according to claim 1 or claim 2, which is characterized in that in S1, by gelatin,
Dimethyl dodecyl base tertiary amine, water stir evenly, and use hydrochloric acid regulation system pH value for 6.4-6.8, and glutamic acid is added and stirs 3-
5h, whipping temp are 45-55 DEG C, and acetone is added, adjusts the temperature to 55-65 DEG C of stirring 10-20min, ring is added under stirring
Oxygen chloropropane continues to stir 4-8h, cooling, stands 14-20h, and regulation system continues to stir 10-20min, filter, very in alkalinity
Sky is dried to obtain gelatin glutamic acid compound.
4. hair-cream preparation method is moistened in any one of -3 disposable nutrition of water conservation according to claim 1, which is characterized in that in S2, olive
Olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearate, glycerol weight ratio be 8-16：
15-25：2-4：2-4：2-4.
5. hair-cream preparation method is moistened in any one of -4 disposable nutrition of water conservation according to claim 1, which is characterized in that, will in S2
Olive oil, gelatin glutamic acid compound, acetulan, cetostearyl alcohol stearate, glycerol mixing, are warming up to 80-
90 DEG C of stirrings obtain premix a to dissolving completely.
6. hair-cream preparation method is moistened in any one of -5 disposable nutrition of water conservation according to claim 1, which is characterized in that in S3, reed
Luxuriant growth extracting solution, passion fruit extracting solution, collagen polypeptide, hexadecyltrimethylammonium chloride, preservative, pearling agent, deionized water
Weight ratio is 4-8：3-5：2-4：2-4：2-4：2-4：120-160.
7. hair-cream preparation method is moistened in any one of -6 disposable nutrition of water conservation according to claim 1, which is characterized in that, will in S3
Extract solution from aloe, passion fruit extracting solution, collagen polypeptide, hexadecyltrimethylammonium chloride, preservative, pearling agent, deionized water
Mixing, is warming up to 60-80 DEG C and stirs evenly, obtain premix b.
8. hair-cream preparation method is moistened in any one of -7 disposable nutrition of water conservation according to claim 1, which is characterized in that in S4, in advance
Mixing a, premix b weight ratio be 25-35：10-20.
9. hair-cream preparation method is moistened in any one of -8 disposable nutrition of water conservation according to claim 1, which is characterized in that, will in S4
Premix a, premix b stir 2-5min, mixing speed 40-100r/min, homogeneous processing 1-3min, and homogeneous speed is
2300-3400r/min obtains being retained disposable nutrition profit hair-cream.
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| CN201810676001.6A CN108815020A (en) | 2018-06-27 | 2018-06-27 | A kind of disposable nutrition profit hair-cream preparation method of water conservation |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102283789A (en) * | 2010-06-21 | 2011-12-21 | 金奇集团金奇日化有限公司 | Method for preparing collagen polypeptide nutrition washing-free conditioner composition and product thereof |
| CN104546582A (en) * | 2013-10-22 | 2015-04-29 | 罗鹏程 | Method for preparing skin-friendly health-care hair conditioner |
| CN105832610A (en) * | 2016-05-13 | 2016-08-10 | 马鞍山纽盟知识产权管理服务有限公司 | Novel efficient smoothing hair conditioner |
| CN106832035A (en) * | 2017-02-21 | 2017-06-13 | 山东大学 | A kind of preparation method of hydrophobic associating cationic xanthans |
-
2018
- 2018-06-27 CN CN201810676001.6A patent/CN108815020A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102283789A (en) * | 2010-06-21 | 2011-12-21 | 金奇集团金奇日化有限公司 | Method for preparing collagen polypeptide nutrition washing-free conditioner composition and product thereof |
| CN104546582A (en) * | 2013-10-22 | 2015-04-29 | 罗鹏程 | Method for preparing skin-friendly health-care hair conditioner |
| CN105832610A (en) * | 2016-05-13 | 2016-08-10 | 马鞍山纽盟知识产权管理服务有限公司 | Novel efficient smoothing hair conditioner |
| CN106832035A (en) * | 2017-02-21 | 2017-06-13 | 山东大学 | A kind of preparation method of hydrophobic associating cationic xanthans |
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