CN107308041A - A kind of gentle nourishing type shampoo and preparation method thereof - Google Patents
A kind of gentle nourishing type shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to daily chemical product technical field, and in particular to a kind of gentle nourishing type shampoo and preparation method thereof.Gentle nourishing type shampoo of the invention includes following components and its mass percent：Amino acid surfactant 20 30%, olive oil 5 10%, Chinese mugwort ash 4 8%, the, of conditioner 2 4% treatment oil composition 1 4%, vitamin E 1 3%, phytosterol 1 3%, Cer EOS 3%, limonene 0.5 1.5%, protein hydrolysate 0.05 0.15%, emulsifying agent 1.2 3%, preservative 0.1 0.3% and water 30.05 63.15%.The technical advantages of the present invention are that：Used cooperatively using amino acid surfactant, Chinese mugwort ash, treatment oil composition etc., obtained product has good cleaning capacity, moisturizing effect good；Hair after washing is bright, submissive, flexible, cardability is good；It is gentleer to skin, it is nontoxic non-stimulated and comfortable soft and moist.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of gentle nourishing type shampoo and preparation method thereof.
Background technology
Dandruff is medically referred to as capitis pityriasis, is skin disease caused by a kind of a kind of chlosma as fungi.Horse
Amount reproduction of the color bacterium on scalp is drawn to cause the hyperplasia of scalp cuticula, so as to promote corneocyte with white or ash
The form of color phosphorus bits comes off extremely, and this phosphorus bits come off are dandruff.Dandruff Producing reason be generally divided into physiological and
Pathologic.The greasy root of hair is that the ecological balance of scalp is destroyed, and when scalp fat secretion is unbalance, scalp will become
It is greasy, if being not added with preventing and treating, can more trigger flora, metabolism it is unbalance, make whole scalp state disorderly, heavy damage scalp it is strong
Health situation；And scalp, as the most important command control center of human body, its fragility and sensitiveness are even more to be only second to eyelid, are
Pull one hair and move the whole body.Scalp problems can't neglect, and need also exist for carrying out health control, only comprehensive to scalp progress, system,
The conditioning maintenance of science, the scalp problems such as hair oil could be eliminated from root, the healthy normality of scalp is kept.
Surfactant, which is played regulatory role, in shampoo minimizes the electrostatic in hair so that hair be easy to comb, easily
In release, and be wet hair and dry hair combing it is easy and smooth.Shampoo requirement simultaneously has high spumescence, low de-
Fat ability, easily low excitant, micelle structure of the higher system viscosity of formation etc., the selection of such Surfactant just has
Certain limitation.The excitant of the cationic surfactant such as cationic polymer such as guar gum quaternary amine, poly-quaternary ammonium salt is big, raw
Thing degradability is poor, and because hair and dirt are general all negatively charged, this will make dirt-removing power be deteriorated, attachment is serious.
Cationic polymer can show the eutrophication to surface water simultaneously, and this is due to their nitrogen content and substantial amounts of every
What the cationic polymer that year uses in the washable composition of cosmetic was caused.Therefore, there is a kind of trend to limit cation to gather
Compound is used in the washable composition of cosmetic.Corresponding people are just seeking the washable composition cationic polymerization of cosmetic
The substitute of thing, specific carbohydrate and polysaccharide are disclosed, such as sucrose, alginates, inulin, guar gum.
Chinese patent CN103655262A discloses a kind of nursing type shampoo, by alkylpolyoxyethylene sulfuric acid
Sodium, coconut acid diethanolamide, small particle silicone emulsion, seaweed extract thing and deionized water composition, a large amount of silicon are contained in the inside
Oil component, silicone oil enables to hair after hair washing to have cardability and smooth feeling, but silicone oil component contacts and be detained scalp meeting
Correct leatherware has certain damage, and the harm of health can be brought to consumer by being used for a long time.
Chinese patent CN104473790A discloses one kind without silicon shampoo, and it includes alkylpolyoxyethylene sulfuric acid
Sodium, Cocoamidopropyl betaine, cocinic acid, diglycollic amide, glycol stearate, cellulose quaternary amine, citric acid,
Sodium chloride, shredding, essence, disodium EDTA and water.Though the shampoo not silicate-containing oil, contains cationic surface
Activating agent cellulose quaternary amine, it is larger to skin irritation.
The content of the invention
To solve problems of the prior art, the present invention provides a kind of gentle nourishing type shampoo and its preparation side
Method.
A kind of gentle nourishing type shampoo of the present invention, including following components and its mass percent：
Amino acid surfactant 20-30%, olive oil 5-10%, Chinese mugwort ash 4-8%, conditioner 2-4%, treatment oil compositions 1-
4%th, vitamin E 1-3%, phytosterol 1-3%, Cer EOS -3%, limonene 0.5-1.5%, protein hydrolysate 0.05-
0.15%th, emulsifying agent 1.2-3%, preservative 0.1-0.3% and water 30.05-63.15%.
It is preferred that, described gentle nourishing type shampoo is made up of following components and its mass percent：
Amino acid surfactant 25%, olive oil 7.5%, Chinese mugwort ash 6%, the, of conditioner 3% treatment oil composition 2.5%, dimension life
Plain E 2%, phytosterol 2%, Cer NS %, limonene 1%, protein hydrolysate 0.1%, emulsifying agent 2.1%, preservative
0.2% and water 46.6%.
It is preferred that, described amino acid surfactant presses quality by sodium lauroyl sarcosine and sodium cocoyl glutamate
Than 1:4 compositions.
It is preferred that, described conditioner is double cocounut oil alkane acyl ethyl-hydroxyethyl ester quats.
It is preferred that, Suo Shu treatment oil composition is silk peptide.
It is preferred that, described emulsifying agent is sucrose stearate.
Further preferably, described preservative is Phenoxyethanol and Sensiva SC50 in mass ratio 3:2 compositions.
In addition, present invention also offers a kind of preparation method of gentle nourishing type shampoo, comprising the following steps：
S1, using high-energy mechanical ball milling method by end ash be prepared into nano powder；
S2, the grey nano powder of the Chinese mugwort that olive oil, step S1 are obtained, conditioner, vitamin E and emulsifying agent are placed in oil phase pot
In, 70-80 DEG C is stirred and heated to, oil phase A is uniformly mixing to obtain；
Water is put into S3, water-bath, and adds amino acid surfactant, phytosterol and limonene, stirs and heats
To 60-70 DEG C, stir to obtain aqueous phase B；
S4, oil phase A and aqueous phase B mixed into obtain material C；
S5, material C is cooled to 30-40 DEG C, adds protein hydrolysate and stir, be down to room temperature Hou Jia Ru treatment oil composition,
Ceramide and preservative are produced.
It is preferred that, 75 DEG C are heated in step S2.
Further preferably, 65 DEG C are heated in step S3.
Sodium lauroyl sarcosine CAS：137-16-6；Sodium cocoyl glutamate CAS：67187-32-6；Olive oil
No. CAS：8001-25-0；Vitamin E CAS：14638-18-7；Phytosterol CAS：83-46-5；Ceramide CAS：
100404-17-3；Limonene CAS：138-86-3；Protein hydrolysate CAS：9015-54-7；Sucrose stearate CAS：
37318-31-3；Phenoxyethanol CAS：122-99-6；Sensiva SC50 CAS：70445-33-9.
Sodium lauroyl sarcosine is a kind of surfactant as mild as a dove, with antibiotic and sterilizing while biological degradability
It is good, it is environmentally safe；Sodium cocoyl glutamate foam is appropriate, and washing force is strong, to hard water strong adaptability, can effectively repair by
Hair quality is damaged, and it is extremely soft to skin, and can be quickly by biological decomposition.
Olive oil is also prevented from alopecia, hair is fuel-displaced and hair is dried and jag in addition to providing nutrition for hair
Occur etc. phenomenon；Double cocounut oil alkane acyl ethyl-hydroxyethyl ester quats are high concentration liquid ester quat, are the cationic conditionings of a new generation
Agent, the shortcomings of it effectively overcomes high excitant, the difficult for biological degradation that conventional quaternary ammonium salts have, can be effectively improved the comb of hair
Rationality and tangling property, minimizing electrostatic, more significantly improve hair quality, increase the glossiness and tensile strength of hair；The structure of silk peptide
With the structure of hair closely, and active ingredient amino acid therein is easy to be absorbed by hair, so as to play nourishing hair
Effect, while the SP of HMW is easy to form transparent film on hair again, thus it has good hair care performance again.
Ceramide is a kind of water-soluble lipid matter, can penetrate into skin and cuticula, be combined to form with water quickly
A kind of network structure simultaneously pins moisture；Limonene is colourless oil liquid, with good bacteriostasis；Phenoxyethanol is a kind of
Conventional preservative, Sensiva SC50 is that a kind of synergy preservative is used for neutralizing Phenoxyethanol to reduce preservative to greatest extent
Harm to skin, plays a protective role.
It can be seen that the present invention using by sodium N-lauroyl sarcosinate and sodium cocoyl glutamate from test example of the present invention
In mass ratio 1:The components such as amino acid surfactant, Chinese mugwort Hui, treatment oil composition, the conditioner of 4 compositions cooperate, synergy
There is good effect to anti-dandruff and itching-relieving, have preferably for improving hair smoothness, cardability, moistness, glossiness etc.
Effect, and product safety is non-stimulated, is particularly suitable for women and infant uses.
Compared with prior art, the technical advantages of the present invention are that：With good cleaning, washability, moisturizing effect
It is good；Hair after washing is bright, submissive, flexible, cardability is good；It is gentleer to skin, it is nontoxic non-stimulated and comfortable soft and moist.
Embodiment
The present invention is described in further details below by specific embodiment, these embodiments are only used for the mesh of illustration
, it is in no way intended to limit protection scope of the present invention.
Double cocounut oil alkane acyl ethyl-hydroxyethyl ester quats are purchased from Dongguan City member of Imperial Academy Chemical Co., Ltd.；Silk peptide is purchased from Anhui Province
Xuancheng Jingrui New Material Co., Ltd..
Embodiment 1-3, comparative example 1-3
Table 1 lists the composition and mass percent of shampoo prepared by 1-3 of the embodiment of the present invention and comparative example 1-3.
The composition and mass percent of the embodiment of table 1 and comparative example shampoo
The difference of comparative example 1 and embodiment 2 is：Amino acid surfactant is by sodium lauroyl sarcosine and cocoyl
Sodium glutamate in mass ratio 1:1 composition.
The difference of comparative example 2 and embodiment 2 is：Without Chinese mugwort ash, increase the content of olive oil.
The difference of comparative example 3 and embodiment 2 is：Bu Han treatment oil compositions, increase the content of conditioner.
The preparation method of the shampoo of embodiment 1：
S1, using high-energy mechanical ball milling method by end ash be prepared into nano powder；
S2, the grey nano powder of the Chinese mugwort that olive oil, step S1 are obtained, conditioner, vitamin E and emulsifying agent are placed in oil phase pot
In, 70 DEG C are stirred and heated to, oil phase A is uniformly mixing to obtain；
Water is put into S3, water-bath, and adds amino acid surfactant, phytosterol and limonene, stirs and heats
To 60 DEG C, stir to obtain aqueous phase B；
S4, oil phase A and aqueous phase B mixed into obtain material C；
S5, material C is cooled to 30 DEG C, adds protein hydrolysate and stir, be down to room temperature Hou Jia Ru treatment oil composition, nerve
Acid amides and preservative are produced.
The preparation method of the shampoo of embodiment 2：
S1, using high-energy mechanical ball milling method by end ash be prepared into nano powder；
S2, the grey nano powder of the Chinese mugwort that olive oil, step S1 are obtained, conditioner, vitamin E and emulsifying agent are placed in oil phase pot
In, 75 DEG C are stirred and heated to, oil phase A is uniformly mixing to obtain；
Water is put into S3, water-bath, and adds amino acid surfactant, phytosterol and limonene, stirs and heats
To 65 DEG C, stir to obtain aqueous phase B；
S4, oil phase A and aqueous phase B mixed into obtain material C；
S5, material C is cooled to 35 DEG C, adds protein hydrolysate and stir, be down to room temperature Hou Jia Ru treatment oil composition, nerve
Acid amides and preservative are produced.
The preparation method of the shampoo of embodiment 3：
S1, using high-energy mechanical ball milling method by end ash be prepared into nano powder；
S2, the grey nano powder of the Chinese mugwort that olive oil, step S1 are obtained, conditioner, vitamin E and emulsifying agent are placed in oil phase pot
In, 80 DEG C are stirred and heated to, oil phase A is uniformly mixing to obtain；
Water is put into S3, water-bath, and adds amino acid surfactant, phytosterol and limonene, stirs and heats
To 70 DEG C, stir to obtain aqueous phase B；
S4, oil phase A and aqueous phase B mixed into obtain material C；
S5, material C is cooled to 40 DEG C, adds protein hydrolysate and stir, be down to room temperature Hou Jia Ru treatment oil composition, nerve
Acid amides and preservative are produced.
The preparation method of comparative example 1-3 shampoos is similar to Example 2.
Properties of product evaluation test
Test example 1：Irritation test
Test material：Shampoo prepared by embodiment 1-3 and comparative example 1-3.
Subjects：Choose healthy rabbit 60, body weight 180-220g male and female half and half.
Content of the test：24h cuts off the hair of experiment white rabbit back backbone both sides before experiment, does not damage epidermis, and unhairing scope is left
Right every 3cm × 3cm.Tested material i.e. embodiment 1-3 and each 0.5g of comparative example 1-3 is taken to be added on 2.5cm × 2.5cm 4 layers of gauze
On, side skin is affixed on, after one layer of oilpaper covering, with immobilization with adhesive tape, opposite side is blank control.Removed after closing 4h tested
Thing, and residual tested material is washed away with clear water, in 1 after removal tested material, 24,48h observation recipient site local skin reactions, press
《Cosmetics health specification》(2007 editions) skin irritation/corrosion test carries out dermoreaction scoring, is integrated with animal subject
Average value carry out overall merit, and observe other toxic side effects in addition to excitant.
Result of the test：Each observing time point top average in experiment<0.5, belong to nonirritant, i.e., skin irritation is tried
It is nonirritant to test result.Therefore the shampoo that 1-3 of the embodiment of the present invention and comparative example 1-3 is provided is gently non-stimulated to skin.
Test example 2：Anti-dandruff effect test
1. test material：Shampoo prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：Horse traction colour standard bacterial strain, is purchased from DSMZ of Wuhan University.
3. content of the test：The shampoo respectively prepared by embodiment 1-3 and comparative example 1-3, is configured to the molten of 0.2g/mL
Liquid.According to《The foundation and application study of the anti-dandruff effect detection evaluation method of shampoo》Disclosed method is to made from embodiment
Shampoo carries out inhibition zone diameter test, and anti-dandruff effect to shampoo product is evaluated.Wherein according to the document (shampoo
The foundation and application study of anti-dandruff effect detection evaluation method, where, Wang Tan, Jia Zebao, Hong Xiaopeng, Peng Jin, silk treasured daily use chemicals have
Research and development department of limit company, household chemicals science, o. 11th in 2009) method, directly will test raw material shampoo change hair washing into
Water is tested.Inhibition zone diameter is bigger, and anti-dandruff effect is better.
4. result of the test：Embodiment 1-3 and the anti-dandruff measure of merit result of comparative example 1-3 shampoos are as shown in table 2.
The anti-dandruff measure of merit of the shampoo of table 2
| Group | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Inhibition zone diameter/mm | 16.4 | 18.5 | 15.6 | 13.0 | 13.3 | 15.2 |
Known by table 2, the anti-dandruff effect of shampoo prepared by 1-3 of the embodiment of the present invention is preferable, and comparative example 1-3 anti-dandruff effect
It is relatively poor, and shampoo inhibition zone diameter prepared by embodiment 2 is maximum, anti-dandruff effect is best, illustrates the present invention using by the moon
Osmanthus acylsarcosine sodium and sodium cocoyl glutamate in mass ratio 1:The component phases such as amino acid surfactant, the Chinese mugwort ash of 4 compositions
Mutually coordinate, synergy has more preferable effect to anti-dandruff and itching-relieving.
Test example 3：Sensory evaluation is tested
1. test material：Shampoo prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：The people of crowd 150 on probation, age distribution is at 20-60 Sui, and wherein male's number is 70 people, Nv Xingren
Number is 80 people.
3. content of the test：Crowd on probation is divided into 6 groups, i.e. embodiment 1-3 groups and comparative example 1-3 groups, every group of 25 people, difference
Carry out sensory evaluation test to shampoo prepared by embodiment 1-3 and comparative example 1-3, each sampling 2 weeks, tester according to
The sensation of oneself is scored.Standards of grading：Ten point system is taken, 1 point worst, 10 points best, and fraction more high effect is better.
4. result of the test：Various shampoo using effect evaluation results are as shown in table 3.
The embodiment of table 3 and comparative example shampoo sensory evaluation effect
Known by table 3, shampoo scoring prepared by 1-3 of the embodiment of the present invention is higher, and common sensation is preferable, and comparative example 1-3
Salubrious property, the foaming abundancy degree of the shampoo of preparation are poorer than the effect of the shampoos prepared of embodiment of the present invention 1-3, illustrate this
Invention is using by sodium lauroyl sarcosine and sodium cocoyl glutamate in mass ratio 1:The amino acid surfactant of 4 compositions,
The components such as Hui, treatment oil composition, conditioner that end cooperate, act synergistically for improve hair smoothness, cardability, moistness,
Glossiness etc. has more preferable effect.
It the above is only the preferred embodiment of the present invention, it is noted that above-mentioned preferred embodiment is not construed as pair
The limitation of the present invention, protection scope of the present invention should be defined by claim limited range.For the art
For those of ordinary skill, without departing from the spirit and scope of the present invention, some improvements and modifications can also be made, these change
Enter and retouch and also should be regarded as protection scope of the present invention.
Claims (10)
1. a kind of gentle nourishing type shampoo, it is characterised in that including following components and its mass percent：
Amino acid surfactant 20-30%, olive oil 5-10%, Chinese mugwort ash 4-8%, conditioner 2-4%, treat with oil composition 1-4%,
Vitamin E 1-3%, phytosterol 1-3%, Cer EOS -3%, limonene 0.5-1.5%, protein hydrolysate 0.05-
0.15%th, emulsifying agent 1.2-3%, preservative 0.1-0.3% and water 30.05-63.15%.
2. gentle nourishing type shampoo according to claim 1, it is characterised in that by following components and its mass percent
Composition：Amino acid surfactant 25%, olive oil 7.5%, Chinese mugwort ash 6%, the, of conditioner 3% treatment oil composition 2.5%, vitamin E
2%th, phytosterol 2%, Cer NS %, limonene 1%, protein hydrolysate 0.1%, emulsifying agent 2.1%, the and of preservative 0.2%
Water 46.6%.
3. gentle nourishing type shampoo according to claim 1 or 2, it is characterised in that described amino acid surface activity
Agent is by sodium lauroyl sarcosine and sodium cocoyl glutamate in mass ratio 1:4 compositions.
4. gentle nourishing type shampoo according to claim 1 or 2, it is characterised in that described conditioner is double cocounut oil
Alkane acyl ethyl-hydroxyethyl ester quat.
5. gentle nourishing type shampoo according to claim 1 or 2, it is characterised in that Suo Shu treatment oil composition is fibroin
Peptide.
6. gentle nourishing type shampoo according to claim 1 or 2, it is characterised in that described emulsifying agent is that sucrose is hard
Resin acid ester.
7. gentle nourishing type shampoo according to claim 1 or 2, it is characterised in that described preservative is benzene oxygen second
Alcohol and Sensiva SC50 in mass ratio 3:2 compositions.
8. the preparation method of the gentle nourishing type shampoo according to claim any one of 1-7, it is characterised in that including with
Lower step：
S1, using high-energy mechanical ball milling method by end ash be prepared into nano powder；
S2, the grey nano powder of the Chinese mugwort that olive oil, step S1 are obtained, conditioner, vitamin E and emulsifying agent are placed in oil phase pot,
70-80 DEG C is stirred and heated to, oil phase A is uniformly mixing to obtain；
Water is put into S3, water-bath, and adds amino acid surfactant, phytosterol and limonene, 60- is stirred and heated to
70 DEG C, stir to obtain aqueous phase B；
S4, oil phase A and aqueous phase B mixed into obtain material C；
S5, material C is cooled to 30-40 DEG C, adds protein hydrolysate and stir, be down to room temperature Hou Jia Ru treatment oil composition, nerve
Acid amides and preservative are produced.
9. the preparation method of gentle nourishing type shampoo according to claim 8, it is characterised in that be heated in step S2
75℃。
10. the preparation method of gentle nourishing type shampoo according to claim 8, it is characterised in that heated in step S3
To 65 DEG C.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176270A (en) * | 2016-08-31 | 2016-12-07 | 威莱(广州)日用品有限公司 | A kind of amino acid shampoo of gentleness and preparation method thereof |
| CN106726761A (en) * | 2016-12-24 | 2017-05-31 | 叶宗瑞 | A kind of salubrious shower cream and preparation method thereof |
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2017
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176270A (en) * | 2016-08-31 | 2016-12-07 | 威莱(广州)日用品有限公司 | A kind of amino acid shampoo of gentleness and preparation method thereof |
| CN106726761A (en) * | 2016-12-24 | 2017-05-31 | 叶宗瑞 | A kind of salubrious shower cream and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 张巧鸣: "《中国化妆品》", 31 August 2004 * |
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