CN104146931A - Natural nourishment and maintenance type hair conditioner and preparation method thereof - Google Patents

Abstract

The invention discloses a natural nourishment and maintenance type hair conditioner and a preparation method thereof. The hair conditioner comprises the following substances: self-emulsifying monoglycerides, cetostearyl alcohol, polyoxyl (40) stearate, camellia seed oil, lanolin, dimethyl siloxane, EG-1(ethylene glycol-1), LUXE, water, propylene glycol, alum, sorbitol, amino acid for moisturizing and resisting allergies, APG, Glydant, QM, sodium alginates, cationic guar gum, a saponin extracting solution, a soapberry extracting solution and essences. Compared with existing products in the market, the hair conditioner prepared by the invention has the advantages that the property is mild, and the security is high; a method that active substances of natural plants are combined with mild surface active agents is adopted, so that the living environments of hair roots are improved, and the hair roots are nourished; meanwhile, through the particular and balanced nourishment and maintenance functions of the saponin, damaged hair follicles are repaired, and the hair is urged to develop and grow once again, so that the hair is thicker and firmer.

Description

A kind of natural nourishing maintenance type hair conditioner and preparation method thereof

Technical field

The present invention relates to a kind of hair conditioner, particularly a kind of natural nourishing maintenance type hair conditioner and preparation method thereof.

Background technology

Modern's operating pressure is large, study is nervous, brain overwork, and easily happiness is easily sad, and these usually can cause alopecia.People's brain overwork, or be often laden with anxiety, unhappiness, spirit is too nervous, makes brain be subject to very large stimulation, sometimes also can have influence on supply and the growth of hair nutrition.Environmental pollution also can bring certain injury to our hair, the particle existing in air, various pollutant are easy to be attached on our hair and scalp, so not only on hair, be full of unclean material, also can cause pore to block, hair is tarnished.The injury maximum of environmental pollution to dryness hair quality, is easy to cause hair fluffy withered, intense darkness without light, so that is difficult to combing, and easily curling, fracture.Hair is again " video-tape of heavy metal to man body pollution ", and the metaphor of this image also can illustrate that environmental pollution meeting causes subtle impact to hair.

Our hair is the same with health can be subject to extraneous climatic influences.Interim when summer, in general, the moisture of our hair is also many, at this time must note the clean of hair.Scalp pore is perspired more, if carry out not in time cleaning, is easy to block pore, and dandruff and dry situation of itching will occur, and easy breed bacteria, affects aesthetic feeling and health.Dry season on hair to affect meeting larger.Airborne water deficient, human body itself is dry, and hair will lack moisture, so there is the situations such as static.Therefore, we will determine according to ambient conditions the care method of hair, and make in time various adjustment, and the external world is dropped to minimum on the impact of hair.

Healthy hair top layer is made up of the protecting film of hair the oils and fats of one group of complete hair scale sheet and secretion naturally, too much wash reason, boiling hotly dye, exposure in sunshine all can destroy this layer of natural protecting film, causes cortex water loss, and hair is dried up, and follows the string and flexibility.Only have frequent use hair conditioner, could form lastingly the protecting film of hair, hair is escaped injury.Chinese medicine elite is dissolved in hair products, is the scientific and technological Development Trend of modern hair care.Utilize sophisticated technologies, the elite composition in extraction Chinese medicine, makes effective ingredient fully contact with hair, brings into play better effect.

Summary of the invention

For solving the problems of the technologies described above, the invention provides a kind of natural nourishing maintenance type hair conditioner, solve withered, impaired problem that hair brings because of hydropenia.

The present invention also provides a kind of preparation method of natural nourishing maintenance type hair conditioner.

The natural nourishing maintenance of one provided by the invention type hair conditioner, contains following material in 300g hair conditioner:

Described Fructus Sapindi Mukouossi extract is to prepare by the following method:

Take Fructus Sapindi Mukouossi appropriate, after pulverizing, soak 0.2-0.8h, heating decocts extracts 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of Fructus Sapindi Mukouossi weight, filters and get final product.

Described Fructus Gleditsia extracting solution is prepared by the following method:

Take Fructus Gleditsia appropriate, after pulverizing, soak 0.2-0.8h, heating decocts extracts 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of Fructus Gleditsia weight, filters and get final product.

Described essence is: flavoring pineapple essence, osmanthus flower fragrance, Fructus Citri Limoniae essence, rose essence, peach flavor, green cucumber essence or jasmin essence.

The preparation method of a kind of natural nourishing maintenance type hair conditioner provided by the invention, is characterized in that its preparation method comprises the following steps:

A) take cation melon glue 0.1-4g, join in the distilled water of 50-100ml, 60-80 DEG C of heating in water bath, heats while stirring, to be mixed evenly after, leave standstill and make it fully swelling, obtain conditioner 1;

B) take sodium alginate 0.5-5g, join in 50-100ml distilled water, 60-80 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtains thickening agent 1;

C) take the crosslinked 0.5-5g of Copolymer of Methyl Vinyl Ether/Maleic Anhydride and decadinene, add in 50-100ml distilled water, 60-80 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtains thickening agent 2;

D) take respectively self emulsifying monoglyceride 3-8g, cetostearyl alcohol 3-8g, polyoxyethylene stearate (40) ester 6-10g, lanoline 0.5-3g, camellia seed oil 1-10ml, dimethyl siloxane 3-8g, PEG-26 glycerin ether 3-8g, Lipomulse Luxe 5-10g in beaker 1, be placed in 60-90 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as oil phase;

E) take respectively Alumen 5-10g, sorbitol 5-10g, aminoacid moisturizing anti-sensitizer 5-10g, distilled water 30ml-200ml, propylene glycol 1-5ml to beaker 2, be placed in 60-90 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as water;

F) when water, oil phase temperature equate by the time, become thread shape to pour in water oil phase, limit edged stirs, constantly stir and continuous heating, add essence 0.05-0.25g, Fructus Gleditsia extracting solution 0.1-5g, Fructus Sapindi Mukouossi extracting solution 0.1-5g, alkyl polyglucoside APG 0.1-1g, dihydroxymethyl dimethyl hydantoin 0.2-0.5g stir, and obtain emulsion bases;

G) in emulsion bases, add thickening agent 1, thickening agent 2, conditioner 1, be uniformly mixed, obtain natural nourishing maintenance type hair conditioner.

Various compositions in the present invention are as follows:

Fructus Sapindi Mukouossi foam is abundant, feel exquisiteness, and strong detergency, makes hair be rich in gloss, elasticity.The effect such as antibacterial, antiinflammatory in addition, antioxidation, removing free radical simultaneously.Can prevent the dandruff, have anti-dandruff, antipruritic, anticreep effect for hair washing, its pH value, between 5～7, is nature acidity, is the surfactant of pure natural, do not hurt sb.'s feelings body, not polluted source.

Fructus Gleditsia is the natural material of articles for washing.Fructus Gleditsia, can removing scurf and relieving itching containing triterpene saponin, saponin etc.Life-time service can thoroughly solve dandruff head pruritus, the problem easily broken, turn to be yellow bifurcated, greasy alopecia that dries up, and also can promote hair restoration.Major function is to help improve impaired hair quality and scalp problems.If hair does not have any problem, use Fructus Gleditsia liquid also can play the effect of maintenance hair.

Camellia seed oil contains unsaturated fatty acid, and it has the title of " beauty treatment acid ".Unsaturated fatty acid is in liberal supply, can make hair pitch-black shinny; Otherwise hair will come off.The Main Ingredients and Appearance of camellia seed oil is that oleic acid and linoleic acid are main unsaturated and fatty acid, and its content reaches more than 90%, and oleic acid content exceedes 80%, is very easily absorbed by the body.

Dimethyl siloxane is as submissive conditioner washing in hair products, produces lubriciously without greasy sensation, can form the thin film that one deck breathability is fabulous in hair surface, has antidusting, reduces static, increases hair gloss, improves effect of Hair setting.

Alkyl polyglucoside APG is the organic monomer that utilizes nature the most extensively to exist--the surfactant that glucose is development of raw materials, belong to non-ionic surface active agent, be known as new generation of green surfactant, can totally biodegradable, can use with any type list surface-active agent is collaborative, there is stronger broad spectrum antibiotic activity.

Lanoline is good moistness material.

Aminoacid moisturizing anti-sensitizer is natural moisture preserving agent, and tool height bio-compatibility can improve rapidly for personal care product the moisture hold facility that skin is sent out, activated cell vigor, make skin moist, smooth, prevent dry and obfuscation.This product can reduce the zest of surfactant and other functional raw materials, and dodecylbenzene sodium sulfonate and CAB are had to foam enhancing effect, not obvious on other surfactant foam impacts.This product Surfactant viscosity influence is little, but the water-soluble macromolecule thickener using in formula (card ripple etc.) is had to the effect of thickening and quickening speed of expansion.During for hair care product, can play the damage prevention after moisturizing, conditioning and hair chemical treatment.

Copolymer of Methyl Vinyl Ether/Maleic Anhydride and decadinene are crosslinked can form clear gel substrate, and not viscous leaves smooth soft feel on hair, skin, strengthens guarantor's type ability of hair fixing product, with personal care product's well compatibility of component.

The Alumen external parasite killing that can detoxify, dampness removing to stop itchin, has antibacterial action.Alumen has inhibitory action to multiple Grain-negative, positive coccus and bacillus.

The aqueous dispersions of cation guar gum has cushioning effect, can stable existence between PH4.0-10.5, and continuous heating can reduce the viscosity of dispersion liquid.In skin-protection product, can reduce detergent injury-free to the zest of skin and protection keratoprotein, make hair smooth, reduce the loss of natural lipid in hair, increase the pliability of hair.Mix with anion, nonionic and dual character surfactant.

Sodium alginate hydrophilic is strong, in cold water and warm water, can dissolve, and forms the very uniform solution of thickness.The true solution forming has other analog and is difficult to the flexibility, homogeneity and other good characteristics that obtain, has the effect of very strong protecting colloid.In Shampoo & Conditioner, play good thickening, antistatic and steady bubble effect.In addition, can also improve the moisture retention of hair, make the long-term maintenance of hair submissive, be thickening agent and wetting agent common in hair shampoo article.

In this hair conditioner prescription, add the extraction elite of two kinds of natural Chinese medicinal herb Fructus Sapindi Mukouossis, Fructus Gleditsia, supplied with the necessary moisture of healthy hair follicle and nutrient, improved root of hair living environment, anti-loss, and provide enough energy for the regeneration of hair.The compositions such as the Saponin in Fructus Sapindi Mukouossi are cleaning-nursing scalp and hair well, and the gentle injury skin that is difficult for of quality.Fructus Gleditsia is rich in rich in protein composition and nourishes withered root of hair, makes new living again.Gentle medicine olein China, dredging purifies muddy hair follicle environment, allows newborn hair health regeneration in pure scalp environment.Cation guar gum has good steady bubble, antistatic property, improves wet comb and the dry comb property of hair, makes hair keep for a long time gloss, softness, high resilience.Dimethyl siloxane can increase hair gloss, improves effect of Hair setting.Camellia seed oil can make hair pitch-black shinny, has the moistness of height.

In prescription, composition complements each other, and can nourish hair comprehensively, layer by layer deeply infiltration, solve withered, impaired problem that hair brings because of hydropenia, lasting moisturizing is moist, makes hair be easy to combing, bright to sending out tip water profit jade-like stone from root of hair, healthy hair is a softer and smoother touch, obtains seemingly water and lives newborn.

Detailed description of the invention

Below in conjunction with embodiment, the present invention will be further described.

Camellia seed oil of the present invention is commercially available.

Embodiment 1

The preparation of 1.1 Fructus Sapindi Mukouossi extracting solution

Take Fructus Sapindi Mukouossi 200g, after pulverizing, soak 0.5h, heating decocts extracts 3 times, add 8 times of water gagings the 1st time, extract 2h, add 6 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, filter merging filtrate at every turn with 3 layers of gauze, the volume of filtrate is concentrated into 4 times of g/ml of Fructus Sapindi Mukouossi weight, stand-by.

The preparation of 1.2 Fructus Gleditsia extracting solution

Take Fructus Gleditsia 100g, after pulverizing, soak 0.5h, heating decocts extracts 3 times, adds for the first time 10 times of water gagings, extracts 2.5h, adds 8 times of water gagings the 2nd time, extracts 1.25h, adds 4 times of water gagings the 3rd time, extracts 0.75h.Each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 4 times of g/ml of Fructus Gleditsia weight.

The preparation of 1.3 hair conditioner

A) take cation melon glue 1g, join in the distilled water of 100ml, 80 DEG C of heating in water bath, heat while stirring, to be mixed evenly after, leave standstill and make it fully swelling, obtain conditioner 1;

B) take sodium alginate 1.5g, join in the beaker that 100ml distilled water is housed, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain thickening agent 1.

C) take the crosslinked QM 1g of Copolymer of Methyl Vinyl Ether/Maleic Anhydride and decadinene, join in 100ml distilled water, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain thickening agent 2;

D) take respectively self emulsifying monoglyceride 4g, cetostearyl alcohol 3g, polyoxyethylene stearate (40) ester 7g, lanoline 1g, camellia seed oil 4ml, dimethyl siloxane 3g, PEG-26 glycerin ether 5g, Lipomulse Luxe 7g in beaker 1, be placed in 80 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as oil phase;

E) take respectively Alumen 6g, sorbitol 7g, aminoacid moisturizing anti-sensitizer 6g, water 70ml, propylene glycol 3ml to beaker 2, be placed in 80 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as water;

F) when water, oil phase temperature equate by the time, become thread shape to pour in water oil phase, limit edged stirs.Constantly stir and continuous heating, add essence 0.1g, Fructus Gleditsia extracting solution 0.2g, Fructus Sapindi Mukouossi extracting solution 0.1g, alkyl polyglucoside APG 0.3g, dihydroxymethyl dimethyl hydantoin Glydant 0.2g stir, and obtain emulsion bases;

G) in emulsion bases, add thickening agent 1, thickening agent 2, conditioner 1, be uniformly mixed, obtain natural nourishing maintenance type hair conditioner.

Embodiment 2

The preparation of 2.1 Fructus Sapindi Mukouossi extracting solution

Take Fructus Sapindi Mukouossi 100g, after pulverizing, soak 0.5h, heating decocts extracts 3 times, adds 9 times of water gagings the 1st time, extract 2h, add 7 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 3 times of g/ml of Fructus Sapindi Mukouossi weight.

The preparation of 2.2 Fructus Gleditsia extracting solution

Take Fructus Gleditsia 200g, after pulverizing, soak 1h, heating decocts extracts 3 times, adds for the first time 8 times of water gagings, extracts 2h, adds 6 times of water gagings the 2nd time, extracts 1h, adds 4 times of water gagings the 2nd time, extracts 0.5h.Each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 3 times of g/ml of Fructus Gleditsia weight.

The preparation of 2.3 hair conditioner

A) take cation melon glue 1.5g, add in 100ml distilled water, 75 DEG C of heating in water bath, heat while stirring, to be mixed evenly after, leave standstill and make it fully swelling, obtain conditioner 1;

B) take sodium alginate 1g, add in 100ml distilled water, 75 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain thickening agent 1;

C) take the crosslinked QM 1.5g of Copolymer of Methyl Vinyl Ether/Maleic Anhydride and decadinene, add in 100ml distilled water, 75 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain thickening agent 2;

D) take respectively self emulsifying monoglyceride 5g, cetostearyl alcohol 2g, polyoxyethylene stearate (40) ester 8g, lanoline 1.5g, camellia seed oil 3ml, dimethyl siloxane 3.5g, PEG-26 glycerin ether EG-14g, Lipomulse Luxe 6g in beaker 1, be placed in 75 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as oil phase;

E) take respectively Alumen 5g, sorbitol 6g, aminoacid moisturizing anti-sensitizer 5g, water 80ml, propylene glycol 4ml to beaker 2, be placed in 75 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as oil phase;

F) when water, oil phase temperature equate by the time, become thread shape to pour in water oil phase, limit edged stirs, add essence 0.09g, Fructus Gleditsia extracting solution 0.1g, Fructus Sapindi Mukouossi extracting solution 0.2g, alkyl polyglucoside 0.2g, dihydroxymethyl dimethyl hydantoin Glydant 0.2g stir, and obtain emulsion bases;

G) in emulsion bases, add thickening agent 1, thickening agent 2, conditioner 1, be uniformly mixed, obtain natural nourishing maintenance type hair conditioner.

Embodiment 3

The physical and chemical index of embodiment 1,2 is as follows:

3.1 character

This product is that viscosity is suitable, and foam is abundant, cool and comfortable, and good stability, abnormal smells from the patient fragrance, transparent sparkling and crystal-clear, fine and smooth hair conditioner uniformly.

3.2pH value checks

Get this product, fixed with PH instrumentation, recording pH value is between 6.9-7.0.

3.3 caloric test

Hair conditioner is packaged in transparent dressing product bottle, within one month, observes without lamination in the refrigerator cold-storages of 4 DEG C.Be placed in 24h in the calorstat of 55 DEG C, hair conditioner is without layering, the phenomenon such as spoiled.

3.4 centrifugal test

Hair conditioner is packaged in to 3000r/min in tool plug test tube, and centrifugal 20min, without lamination.

3.5 room temperatures are placed experiment

Embodiment 1,2 made hair conditioner are placed in to bottle for cosmetics, and room temperature leaves standstill investigates 6 months, and without lamination, unchanged with aftersensation, abnormal smells from the patient is unchanged.

3.6 irritation tests, anaphylaxis experiment

White mice back cuts off hair, smears respectively by the hair conditioner of embodiment 1,2 preparation in cutting plucked position, and is not coated with position and compares, and result does not have zest and anaphylaxis.

Get embodiment 1,2 and be applied in right amount in volunteer (25-65 year, 150 people) gesture and facial expression, observe after spending 30 minutes, all do not occur rubescent, dermexanthesis, foaming phenomenon.

Embodiment 4

Hair conditioner resultant effect is investigated

Below utilize effect of feeling to come the hair conditioner that Evaluation operation example 1,2 produces on probation.Adopt public-opinion poll point system, choose people's object on probation of 80 25-65 year age bracket, be divided into arbitrarily two groups, respectively with the hair conditioner hair conditioning of embodiment 1,2 preparations.Nursing twice after hair washing weekly, be two months service time.Every result of use total score is 5 points: five are divided into best result, represents better, very satisfied; 4 be divided into fine; 3 are divided into and can accept; 3 points is bad below, can not accept.Be below every average, the results are shown in Table 1:

Table 1 resultant effect is investigated

Result of use	The every average of embodiment 1	The every average of embodiment 2
			Smoothness	5	5
Wet comb property	5	5
			Dry comb property	5	5
Nourishing property	4.7	4.6
			Moisture retention	4.9	4.8

In sum, this hair conditioner exquisiteness is soft and smooth, has fine nourishing, moisture retention, feels very smooth when use, and wet comb property, dry comb property are all better.

Claims (5)

1. a natural nourishing maintenance type hair conditioner, is characterized in that containing in 300g hair conditioner following material:

2. natural nourishing maintenance type hair conditioner according to claim 1, is characterized in that, described Fructus Sapindi Mukouossi extract is to prepare by the following method:

Take Fructus Sapindi Mukouossi appropriate, after pulverizing, soak 0.2-0.8h, heating decocts extracts 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of Fructus Sapindi Mukouossi weight, filters and get final product.

3. natural nourishing maintenance type hair conditioner according to claim 1, is characterized in that, described Fructus Gleditsia extracting solution is prepared by the following method:

Take Fructus Gleditsia appropriate, after pulverizing, soak 0.2-0.8h, heating decocts extracts 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times of g/ml of Fructus Gleditsia weight, filters and get final product.

4. natural nourishing maintenance type hair conditioner according to claim 1, is characterized in that, described essence is: flavoring pineapple essence, osmanthus flower fragrance, Fructus Citri Limoniae essence, rose essence, peach flavor, green cucumber essence, jasmin essence.

5. a preparation method for natural nourishing maintenance type hair conditioner claimed in claim 1, is characterized in that its preparation method comprises the following steps:

A) take cation melon glue 0.1-4g, join in the distilled water of 50-100ml, 60-80 DEG C of heating in water bath, heats while stirring, to be mixed evenly after, leave standstill and make it fully swelling, obtain conditioner 1;

B) take sodium alginate 0.5-5g, join in 50-100ml distilled water, 60-80 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtains thickening agent 1;

C) take the crosslinked 0.5-5g of Copolymer of Methyl Vinyl Ether/Maleic Anhydride and decadinene, add in 50-100ml distilled water, 60-80 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtains thickening agent 2;

D) take respectively self emulsifying monoglyceride 3-8g, cetostearyl alcohol 3-8g, polyoxyethylene stearate (40) ester 6-10g, lanoline 0.5-3g, camellia seed oil 1-10ml, dimethyl siloxane 3-8g, PEG-26 glycerin ether 3-8g, Lipomulse Luxe 5-10g in beaker 1, be placed in 60-90 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as oil phase;

E) take respectively Alumen 5-10g, sorbitol 5-10g, aminoacid moisturizing anti-sensitizer 5-10g, water 30ml-200ml, propylene glycol 1-5ml to beaker 2, be placed in 60-90 DEG C of thermostat water bath stirring and dissolving, after dissolving completely, as water;

F) when water, oil phase temperature equate by the time, become thread shape to pour in water oil phase, limit edged stirs, constantly stir and continuous heating, add essence 0.05-0.25g, Fructus Gleditsia extracting solution 0.1-5g, Fructus Sapindi Mukouossi extracting solution 0.1-5g, alkyl polyglucoside APG 0.1-1g, dihydroxymethyl dimethyl hydantoin 0.2-0.5g stir, and obtain emulsion bases;

G) in emulsion bases, add thickening agent 1, thickening agent 2, conditioner 1, be uniformly mixed, obtain natural nourishing maintenance type hair conditioner.