CN108210356A - A kind of whitening emulsion and preparation method thereof - Google Patents
A kind of whitening emulsion and preparation method thereof Download PDFInfo
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- CN108210356A CN108210356A CN201711472794.1A CN201711472794A CN108210356A CN 108210356 A CN108210356 A CN 108210356A CN 201711472794 A CN201711472794 A CN 201711472794A CN 108210356 A CN108210356 A CN 108210356A
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- whitening emulsion
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/14—Liposomes; Vesicles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to cosmetic technical fields, and in particular to a kind of whitening emulsion and its preparation method and application.Whitening emulsion provided by the present invention is made of following component according to weight percent：0.1~10% liposome, 1~30% polyalcohols moisturizer, 1~30% grease, 0.5~5% emulsifier, 0.01~0.5% thickener, 0.01~1% extract, acceptable carrier on 0.1~5% cosmeceutical, surplus is water.Due to containing liposome in the whitening emulsion in the present invention, and the liposome is using the form of Ascorbyl Tetraisopalmitate and tocopherol acetate package lecithin, so that the miscible effect of oil phase and water phase is more preferable in whitening emulsion, be not in the unstable situations such as common whitening product discoloration, thinning, layering.
Description
Technical field
The invention belongs to cosmetic fields, and in particular to a kind of whitening emulsion containing liposome and preparation method thereof.
Background technology
Whitening agent is divided into the types such as water-soluble, the molten and alcohol of oil is molten, but is substantially directly to add in whitening agent in formula and dissolve
Or it is emulsified into product.But water-soluble whitening agent is not good enough to the affine penetrating fluid of skin, although oil-soluble whitening agent with
Skin-friendliness is preferable, but whitening agent is ionic bigger, is easily reduced the viscosity of formula system, and the real energy of skin
The amount of absorption is few, it is difficult to reach the optimum efficiency of whitening agent.
In addition, having, many whitening agents are unstable to light and heat, easily discoloration or inactivation, therefore the required stabilization in market is again
Efficient whitening product makes relative difficulty.
Invention content
The purpose of the present invention is to provide a kind of formulas of the whitening emulsion of high stability, and second is designed to provide this
The preparation method of whitening emulsion.
To achieve these goals, the present invention is implemented by the following technical programs：
The first aspect of the present invention is to provide a kind of whitening emulsion, is made of following component according to weight percent：
Preferably, liposome includes the lecithin, 1~10% glycerine, 1~10% fourth that weight percent is 1~5%
Glycol, 0.01~2% Ascorbyl Tetraisopalmitate, 0.01~2% tocopherol acetate, 0.1~5% cosmetics
Acceptable carrier on, surplus are water.
Preferably, liposome wraps up the form of lecithin for Ascorbyl Tetraisopalmitate and tocopherol acetate.
Preferably, the preparation method of liposome is as follows：The lecithin is dispersed in qs glycerin and butanediol, is stirred
Uniformly, the Ascorbyl Tetraisopalmitate and the tocopherol acetate are added in stirring, is uniformly mixed, is added appropriate
50 DEG C of water, stirs evenly, and is heated to 75 DEG C or so, and aforesaid liquid is added in high speed and high pressure homogenizer by high speed homogenization 5 minutes,
Cycle three times, surveys its grain size, grain size is in 100nm.
Preferably, polyalcohols moisturizer includes one or both of glycerine and butanediol.
Preferably, grease includes pungent caprylic/capric triglyceride, saualane, cetanol ethylhexoate, Jojoba seed
It is one or more in oil, carbonic acid dioctyl ester.
Preferably, emulsifier includes the smooth stearate of sorb, PEG-80 rilanit specials, stearine, stearoyl
It is one or more in sodium glutamate.
Preferably, thickener is one or more in carragheen, xanthan gum, carbomer.
Preferably, extract is carried including glycyrrhiza glabra root extract, jujube berry extract, Artemisia capillaris flower extract, scutellariae,radix
It takes object, mulberry root extract, peony root extractive, aaron's beard extract, hydrolyze the one or more of European Lee.
Further, the present invention also provides a kind of optimization formula of whitening emulsion, by following component according to weight percent
Composition：
The second aspect of the present invention is the provision of the preparation method of above-mentioned whitening emulsion, includes the following steps：
A, water phase is prepared：Water and thickener are added in a suitable vessel, is dispersed with stirring uniformly, is heated to 85 DEG C and persistently stirs
It mixes 20-50 minutes, adds in polyalcohols moisturizer after disperseing completely, stir evenly, heat preservation for standby use；
B, oil phase is prepared：Grease and emulsifier are added in a suitable vessel, are heated to 85 DEG C of persistently 20-50 points of stirring
Clock, for use；
C, oil phase is poured slowly into water phase in stirring, then homogeneous 5-10 minutes, after homogeneous, is cooled to while stirring
40 DEG C hereinafter, add in cosmeceutical on acceptable carrier, continue stirring be cooled to 25-35 DEG C, be slowly homogeneously added into lipid
Body, and after stirring evenly, stop allotment, it is filling after detection is qualified.
Beneficial effects of the present invention are as follows：
Due to containing liposome in the whitening emulsion in the present invention, and the liposome uses four different palmitic acid of ascorbic acid
The form of ester and tocopherol acetate package lecithin, so that the miscible effect of oil phase and water phase is more preferable in whitening emulsion,
Be not in the unstable situations such as common whitening product discoloration, thinning, layering, therefore, whitening emulsion ratio prepared by the present invention
More preferably, the whitening agent with the whitening agent additive amount infiltration skin inner layer of dosage is more, whitening effect for common whitening emulsion whitening effect
Fruit is more prominent.
Description of the drawings
Fig. 1 is the stability change figure of the product of the preparation of the embodiment of the present invention 1 at different conditions；
Fig. 2 is the practical effect figure of the whitening emulsion in 1~embodiment of the embodiment of the present invention 3.
Specific embodiment
With reference to the present invention drawings and examples to the present invention implementation elaborate, following embodiment be with
Implemented under premised on technical solution of the present invention, give detailed embodiment and specific operation process, but the present invention
Protection domain is not limited to following embodiments.
The reagents and materials used in the present invention are commercially available or can be prepared by literature method.Tool is not specified in the following example
The experimental method of concrete conditions in the establishment of a specific crime, usually according to normal condition or according to the normal condition proposed by manufacturer.
Embodiment 1
Whitening emulsion in the present embodiment is made of following component according to weight percent：
The preparation method of whitening emulsion in the present embodiment is as follows：
1. prefabricated liposome：Lecithin is dispersed in the glycerine and butanediol of half, is stirred evenly, is added in stirring anti-
Four different palmitate of bad hematic acid and tocopherol acetate are uniformly mixed, and are added appropriate 50 DEG C of water, are stirred evenly, be heated to
75 DEG C or so, high speed homogenization 5 minutes.Then aforesaid liquid is added in into high speed and high pressure homogenizer, cycle three times, surveys its grain size, grain
Diameter is in 100nm or so, available for facial mask；
2. prepared by water phase：By remaining water and EDTA-2Na, carbomer, xanthans adds in a suitable vessel, is dispersed with stirring
Uniformly, remaining glycerine, butanediol are added in, is heated to 85 DEG C, continues stirring 30 minutes；
4. oil phase：By the smooth stearate of sorb, PEG-80 rilanit specials, caprylic/capric triglyceride, saualane, whale
Ceryl alcohol ethylhexoate adds in a suitable vessel, is heated to 85 DEG C, continues stirring 30 minutes, for use；
5. oil phase is added in water phase in stirring, it is uniformly mixed, opens homogeneous speed 2000-5000rpm/min, homogeneous 3-6
Minute, it is subsequently agitated for being cooled to 45 DEG C hereinafter, adding in preservative, essence, extract, 10-20r/min stirs 10-20 minutes extremely
It is uniformly mixed, cooling；
6. being cooled to 32 DEG C, liposome is added in, is dispersed with stirring uniformly, adds sodium hydroxide, stirs 20-40 minutes and mixes
It closes uniformly, allotment terminates.
Embodiment 2
Whitening emulsion in the present embodiment is made of following component according to weight percent：
The preparation method is the same as that of Example 1.
Embodiment 3
Whitening emulsion in the present embodiment is made of following component according to weight percent：
The preparation method is the same as that of Example 1.
The performance of whitening emulsion prepared according to the formula of above three embodiments and preparation method almost without difference, under
By taking product prepared by embodiment 1 as an example, stability, viscosity and U.S. of product for being prepared to formula according to the present invention and method
White effect illustrates, referring specifically to embodiment 4~7.
Implement 4 stability tests
Fig. 1 is the stability change figure of the product of the preparation of embodiment 1 at different conditions.As shown in Figure 1, the product is distinguished
It is placed in 6 DEG C, 25 DEG C, 37 DEG C, 43 DEG C and 50 DEG C five temperature conditions 3 months, it is seen that beautiful through high and low temperature condition three months
The color of Virgin's milk liquid is substantially unchanged, has good stability.
5 viscosimetric analysis of embodiment is tested
Table 1 is the viscosity data for testing product prepared by embodiment 1 in different time sections, it can be seen that product viscosity is small
In the range of fluctuate, do not occur viscosity decline it is apparent the phenomenon that, have good stability.
Product prepared by 1 embodiment 1 of table is in viscosity test results in different time periods
| Time | 24h | 1 week | 2 weeks | 3 weeks | 4 weeks | 2 months | 3 months |
| Viscosity cps | 3500 | 3601 | 3505 | 3500 | 3498 | 3465 | 3402 |
The variation test of 6 melanin value of embodiment
Table 2 is in six week of whitening emulsion prepared using embodiment 1, is surveyed with skinanalysis apparatus Mexameter MX18
Try melanin value variation table, it can be seen that after this whitening emulsion six weeks, dermal melanin averagely reduces 12.635%, whitening
It is with obvious effects.
2 melanin value of table changes table
7 whitening effect of embodiment is tested
The different volunteer of three plane portion skin conditions is randomly selected, respectively using the whitening emulsion in Examples 1 to 3,
And after product is used 56 days, every volunteer's skin of face variation of actual observation.
As shown in Fig. 2, first volunteer's skin is very yellow, red point is more apparent at circumference of eyes and the bridge of the nose, uses rear red point
It has been completely eliminated that, yellowing is also obviously improved；Second volunteer's skin of face is partially yellow, and the color spot at eye circumference position is apparent, uses
Jaundice state is obviously improved afterwards, and color spot is also apparent thin out, and skin whiteness has very big promotion；The jaundice of third position volunteer's skin
Degree is most light, but there are color spots around eye and the corners of the mouth, are become apparent from using rear whiteness, and color spot is also apparent thin out.
It follows that the whitening effect of the whitening emulsion of three embodiments is clearly, but Integrated comparative, embodiment 2
Whitening effect slightly protrudes a bit.
The preferred embodiment of the invention is illustrated above, but the invention be not limited to it is described
Embodiment, those skilled in the art can also make various equivalent under the premise of without prejudice to the invention spirit
Modification or replacement, these equivalent modifications or replacement are all contained in the application claim limited range.
Claims (10)
1. a kind of whitening emulsion, which is characterized in that be made of following component according to weight percent：
2. whitening emulsion according to claim 1, it is characterised in that：
Wherein, the liposome includes the lecithin, 1~10% glycerine, 1~10% fourth two that weight percent is 1~5%
Alcohol, 0.01~2% Ascorbyl Tetraisopalmitate, 0.01~2% tocopherol acetate, 0.1~5% cosmeceutical
Upper acceptable carrier, surplus is water.
3. whitening emulsion according to claim 2, it is characterised in that：
Wherein, the liposome wraps up the form of lecithin for Ascorbyl Tetraisopalmitate and tocopherol acetate.
4. whitening emulsion according to claim 3, it is characterised in that：
Wherein, the preparation method of the liposome is as follows：The lecithin is dispersed in qs glycerin and butanediol, stirring is equal
It is even, the Ascorbyl Tetraisopalmitate and the tocopherol acetate are added in stirring, is uniformly mixed, adds appropriate 50
DEG C water, stir evenly, be heated to 75 DEG C or so, aforesaid liquid is added in high speed and high pressure homogenizer, followed by high speed homogenization 5 minutes
Ring three times, surveys its grain size, grain size is in 100nm.
5. whitening emulsion according to claim 1, it is characterised in that：
Wherein, the polyalcohols moisturizer includes one or both of glycerine and butanediol；
It is pungent that the grease includes caprylic/capric triglyceride, saualane, cetanol ethylhexoate, jojoba seed oil, carbonic acid two
It is one or more in ester.
6. whitening emulsion according to claim 1, it is characterised in that：
Wherein, the emulsifier includes the smooth stearate of sorb, PEG-80 rilanit specials, stearine, stearoyl paddy
It is one or more in propylhomoserin sodium.
7. whitening emulsion according to claim 1, it is characterised in that：
Wherein, the thickener is one or more in carragheen, xanthan gum, carbomer.
8. whitening emulsion according to claim 5 or 6, it is characterised in that：
Wherein, the extract includes glycyrrhiza glabra root extract, jujube berry extract, Artemisia capillaris flower extract, scutellariae,radix extraction
Object, peony root extractive, aaron's beard extract, hydrolyzes the one or more of European Lee at mulberry root extract.
9. whitening emulsion according to claim 1, which is characterized in that be made of following component according to weight percent：
10. the preparation method of whitening emulsion described in claim 1, which is characterized in that include the following steps：
A, water phase is prepared：Water and thickener are added in a suitable vessel, are dispersed with stirring uniformly, is heated to 85 DEG C of lasting stirrings
20-50 minutes, polyalcohols moisturizer is added in after disperseing completely, is stirred evenly, heat preservation for standby use；
B, oil phase is prepared：Grease and emulsifier are added in a suitable vessel, 85 DEG C is heated to and persistently stirs 20-50 minutes, treat
With；
C, oil phase is poured slowly into water phase in stirring, then homogeneous 5-10 minutes, after homogeneous, is cooled to 40 DEG C while stirring
Hereinafter, adding in acceptable carrier on cosmeceutical, continue stirring and be cooled to 25-35 DEG C, be slowly homogeneously added into the lipid
Body, and after stirring evenly, stop allotment, it is filling after detection is qualified.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711472794.1A CN108210356A (en) | 2017-12-29 | 2017-12-29 | A kind of whitening emulsion and preparation method thereof |
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| CN201711472794.1A CN108210356A (en) | 2017-12-29 | 2017-12-29 | A kind of whitening emulsion and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108836882A (en) * | 2018-08-30 | 2018-11-20 | 广州市美驰化妆品有限公司 | A kind of lipoid plastid and composite skin care product with whitening spot-removing function |
| CN110897988A (en) * | 2019-12-17 | 2020-03-24 | 湖北省麦诗特生物科技有限公司 | Hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and preparation method thereof |
| CN111544343A (en) * | 2020-05-15 | 2020-08-18 | 中国热带农业科学院农产品加工研究所 | Whitening emulsion rich in rosewood essential oil liposome and preparation method and application thereof |
| CN112741781A (en) * | 2021-02-02 | 2021-05-04 | 上海奥利实业有限公司 | Transparent oil solution of water-oil insoluble licoflavone, and its preparation method and application |
| CN112915041A (en) * | 2021-03-19 | 2021-06-08 | 上海奥利实业有限公司 | Oil-insoluble transparent oil solution of dipotassium glycyrrhizinate and its preparation method and application |
| CN114796119A (en) * | 2022-02-21 | 2022-07-29 | 重庆医科大学 | Composite antioxidant co-carried liposome and preparation method thereof |
| CN115778880A (en) * | 2023-02-01 | 2023-03-14 | 卡莱丽化妆品有限公司 | Liposome, preparation method and application thereof |
| CN116098832A (en) * | 2023-02-28 | 2023-05-12 | 上海师范大学 | Ascorbyl tetraisopalmitate lyotropic liquid crystal nanoparticle dispersion, preparation method and application thereof, and toning lotion |
| CN116807928A (en) * | 2023-02-08 | 2023-09-29 | 杭州清潭维艾国际贸易有限公司 | Whitening composition containing plant essential oil and preparation method thereof |
| CN116966106A (en) * | 2023-08-16 | 2023-10-31 | 广州市澳莱化妆品有限公司 | Liposome wrapper, preparation method and application |
| CN117503656A (en) * | 2023-12-04 | 2024-02-06 | 广东科盈科技有限公司 | Composite plant extract whitening and spot-fading composition and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1408338A (en) * | 2001-09-28 | 2003-04-09 | 上海知菲化妆品有限公司 | Liposome beauty cosmetic and its producing method |
| CN106214511A (en) * | 2016-08-22 | 2016-12-14 | 上海乐宝日化股份有限公司 | A kind of whitening lotion containing liposome and preparation method thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1408338A (en) * | 2001-09-28 | 2003-04-09 | 上海知菲化妆品有限公司 | Liposome beauty cosmetic and its producing method |
| CN106214511A (en) * | 2016-08-22 | 2016-12-14 | 上海乐宝日化股份有限公司 | A kind of whitening lotion containing liposome and preparation method thereof |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108836882B (en) * | 2018-08-30 | 2021-03-23 | 广州市美驰化妆品有限公司 | Liposome-like body with whitening and freckle removing functions and skin care product composition |
| CN108836882A (en) * | 2018-08-30 | 2018-11-20 | 广州市美驰化妆品有限公司 | A kind of lipoid plastid and composite skin care product with whitening spot-removing function |
| CN110897988B (en) * | 2019-12-17 | 2022-05-03 | 湖北省麦诗特生物科技有限公司 | Hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and preparation method thereof |
| CN110897988A (en) * | 2019-12-17 | 2020-03-24 | 湖北省麦诗特生物科技有限公司 | Hair-strengthening and hair-nourishing amino acid shampoo containing sturgeon roe extract liposome and preparation method thereof |
| CN111544343A (en) * | 2020-05-15 | 2020-08-18 | 中国热带农业科学院农产品加工研究所 | Whitening emulsion rich in rosewood essential oil liposome and preparation method and application thereof |
| CN111544343B (en) * | 2020-05-15 | 2022-11-11 | 中国热带农业科学院农产品加工研究所 | Whitening emulsion rich in rosewood essential oil liposome and preparation method and application thereof |
| CN112741781A (en) * | 2021-02-02 | 2021-05-04 | 上海奥利实业有限公司 | Transparent oil solution of water-oil insoluble licoflavone, and its preparation method and application |
| CN112915041A (en) * | 2021-03-19 | 2021-06-08 | 上海奥利实业有限公司 | Oil-insoluble transparent oil solution of dipotassium glycyrrhizinate and its preparation method and application |
| CN114796119A (en) * | 2022-02-21 | 2022-07-29 | 重庆医科大学 | Composite antioxidant co-carried liposome and preparation method thereof |
| CN115778880A (en) * | 2023-02-01 | 2023-03-14 | 卡莱丽化妆品有限公司 | Liposome, preparation method and application thereof |
| CN116807928A (en) * | 2023-02-08 | 2023-09-29 | 杭州清潭维艾国际贸易有限公司 | Whitening composition containing plant essential oil and preparation method thereof |
| CN116807928B (en) * | 2023-02-08 | 2024-06-04 | 杭州清潭维艾国际贸易有限公司 | Whitening composition containing plant essential oil and preparation method thereof |
| CN116098832A (en) * | 2023-02-28 | 2023-05-12 | 上海师范大学 | Ascorbyl tetraisopalmitate lyotropic liquid crystal nanoparticle dispersion, preparation method and application thereof, and toning lotion |
| CN116966106A (en) * | 2023-08-16 | 2023-10-31 | 广州市澳莱化妆品有限公司 | Liposome wrapper, preparation method and application |
| CN116966106B (en) * | 2023-08-16 | 2024-04-16 | 广州市澳莱化妆品有限公司 | Liposome wrapper, preparation method and application |
| CN117503656A (en) * | 2023-12-04 | 2024-02-06 | 广东科盈科技有限公司 | Composite plant extract whitening and spot-fading composition and preparation method and application thereof |
| CN117503656B (en) * | 2023-12-04 | 2024-04-05 | 广东科盈科技有限公司 | Composite plant extract whitening and spot-fading composition and preparation method and application thereof |
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Application publication date: 20180629 |