CN114224754B - A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair, and shampoo containing the composition - Google Patents
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair, and shampoo containing the composition Download PDFInfo
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- CN114224754B CN114224754B CN202111623279.5A CN202111623279A CN114224754B CN 114224754 B CN114224754 B CN 114224754B CN 202111623279 A CN202111623279 A CN 202111623279A CN 114224754 B CN114224754 B CN 114224754B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a composition containing plant extracts for regulating scalp grease secretion, brightening hair and smoothing hair, which is prepared from hydrolyzed keratin, camellia seeds, biota orientalis leaves, cassia seeds, porous starch and nano antibacterial particles. The composition containing the plant extracts for regulating scalp grease secretion, brightening hair and smoothing hair contains various plant extracts, can improve ordered arrangement of hair and hair scales, inhibit growth of bacterial fungi, regulate water-oil balance of head skin, clean and remove dandruff, supplement nutrition and moisture required by hair and scalp, reduce scalp itch, prevent hair from falling and branching, improve scalp blood circulation, promote metabolism, strengthen hair roots, make hair beautiful and soft, and make hair appear healthy by utilizing the effects of the camellia oleosa seed oil, other plant extracts and hydrolyzed keratin. The composition and the matrix of the shampoo without silicone oil can effectively avoid scalp problems caused by silicone oil accumulation, so that hair is fluffy and natural after washing, and is truly bright, smooth, soft and glossy.
Description
Technical Field
The invention relates to the technical field of daily chemical products, in particular to a composition containing a plant extract for regulating scalp grease secretion, brightening hair and smoothening hair and shampoo containing the composition.
Background
The surface of human scalp and the internal structure of scalp form a complete ecological system, and the surface of the human scalp is provided with secretion of sebaceous glands, dust, dirt, various bacteria and the like. Hair follicles in the scalp are sites where hair is metabolized, providing essential nutrients and moisture for hair growth, and the scalp is much more exposed to sunlight, cold and heat than the skin in other parts of the body.
Sebaceous glands are in the dermis, where they adhere to the hair follicle, but have their own independent function. Sebaceous glands secrete sebum, which is then discharged through a catheter to the skin surface, where it is typically mixed with many lipids resulting from the breakdown of keratinocytes to form what is known as "scalp oil". The factors such as oily skin, androgen influence, high-calorie food and the like can increase sebum secretion, excessive sebum secretion can cause the problems of greasy scalp and hair, soft and fluffy hair, dull hair, dandruff and the like, and can even cause seborrheic dermatitis/seborrheic alopecia, so that the overall appearance of a person is influenced, and more importantly, the health state of the scalp and the hair is influenced.
In addition, the scalp is affected by many physicochemical processes such as hair care, for example, from simple hair washing and care to complex hair waving, dyeing and bleaching. The hair care products currently on the market also tend to focus on conditioning the hair only, but neglecting its effect on the scalp. Silicone oil is a common ingredient in hair conditioners, which, once contacted with hair, fills the interstices between the hair pieces, thus creating a smooth feel as if the hair had been washed out better. Therefore, the silicone oil is often mistaken for the general person to have the effect of nourishing hair, but the silicone oil which is originally coated on the hair cannot be thoroughly cleaned due to the characteristic that the silicone oil is insoluble in water when the hair care product is used next time, and the subsequent hair care product cannot enter the hair. The hair is covered with the outer layer by layer with the number of times of use, so that the hair is thick and loses elasticity gradually, and pores are blocked and cannot breathe. The scalp health is affected as a result of insufficient oxygen permeation, and the scalp is also prone to itching, and may even be complicated with hair loss and hair loss sequelae.
At present, shampoo with various functions sold in the market is generally chemically synthesized and has stronger shampoo and hair-dressing effects, but after long-term use, the hair quality is easy to be damaged, and the hair becomes more and more greasy, dry, hair loss and other phenomena. And some powerful anti-dandruff shampoo has poor foaming performance and excessive degreasing force, so that the problems of hair interference, large wet comb resistance, poor comb property after the hair is dried, serious deposition of various conditioning agents and the like are caused. The chemical components remain on the hair, so that the three balance problems of head oil, itching and scalp with more dandruff are difficult to be fundamentally solved after long-term use.
At present, most of shampoo products for reducing the greasiness of hair in the market are oil-control shampoo and various shampoo soaps, and the products are strong in alkalinity and strong in cleaning effect, but can remove normal sebum together, so that the acid-alkali environment of scalp is changed, and more grease is secreted from sebaceous glands. Many users of oil control hair washes feel that the hair oil-out speed is rather faster and faster. The formula of the current hair conditioner product has the effects of nursing scalp, and the hair conditioner can have the following three ways: 1. and a moisturizing component is added to avoid excessive degreasing. 2. The anti-allergic and anti-inflammatory components are added to avoid inflammatory reaction of scalp. 3. The silicone oil is adopted to replace components, so that the accumulation of high molecular silicone oil on the scalp is avoided.
Disclosure of Invention
The invention aims to overcome the defects of the prior art, and provides a composition which is free of silicone oil and contains plant extracts and can regulate scalp grease secretion, lighten and smooth hair and shampoo containing the composition, and the problems of greasy hair, scalp itching, dandruff and the like caused by excessive damage of chemical preparations to scalp and unbalanced scalp grease are solved.
In order to achieve the above purpose, the technical scheme adopted by the invention is as follows:
the composition containing the plant extract for regulating scalp grease secretion, brightening hair and smoothing hair comprises the following components:
(1) A first component: hydrolyzing keratin;
(2) And a second component: an oil phase active ingredient and a water phase active ingredient in a mass ratio of 5-20:10-40:5-20, and porous starch;
(3) And a third component: nano antibacterial particles;
the mass ratio of the first component to the second component to the third component is 1-10:20-80:0.1-0.5.
Preferably, the hydrolyzed keratin of the first component is obtained by hydrolyzing one or more raw materials of hair, feathers and fibroin.
Preferably, the oil phase active ingredient comprises camellia seed oil, biota leaf oil and cassia seed oil;
the oil tea seed oil is obtained by the following method: squeezing camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and collecting the upper oil phase, the lower camellia seed water phase component and camellia seed filter residue for later use;
the biota orientalis oil and the cassia seed oil are obtained by the following method: placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 30-60 times of pure water, distilling for 60-150min, and separating to obtain oil phase and water phase containing residue of cacumen Platycladi and semen Cassiae, wherein the oil phase is mixture of cacumen Platycladi oil and semen Cassiae oil.
Preferably, the mass ratio of the camellia seeds, the biota orientalis leaves and the cassia seeds is 20-50:10-20:10-20.
Preferably, the aqueous phase active ingredient is obtained by the following method: adding water phase containing residue of folium Platycladi and semen Cassiae into water phase containing residue of lower layer oil tea seed water phase component and residue of oil tea seed, heating to 50-70deg.C under stirring, maintaining for 30-60min, filtering, centrifuging, standing, collecting supernatant, and concentrating at 40-50deg.C to obtain concentrated solution with relative density of 1.05-1.20 to obtain water phase active ingredient.
Preferably, the aqueous phase active ingredient is obtained by the following method: adding lower layer of water phase component of tea seed and tea seed residue into water phase containing residue of folium Platycladi and semen Cassiae, adding 0.1-0.5% of probiotics, sealing and fermenting at 25-30deg.C, stirring for 5-10min every 12-36h, sealing and fermenting again, sealing at 25-30deg.C for 90-120d after 20-25 times, filtering, and collecting filtrate to obtain water phase active ingredient.
Preferably, the probiotics are one or more of bacillus subtilis, lactobacillus and saccharomycetes.
Preferably, the porous starch is obtained by enzymatic treatment of starch obtained from one or more of potato, corn, wheat and rice as raw materials.
Preferably, the porous starch has a pore radius of 3.80-6.00 μm and a pore depth of 1.5-2.5 μm.
Preferably, the nano antibacterial particles are formed by mixing nano silver particles and/or nano titanium dioxide particles with the particle diameters of 10-30nm according to the weight ratio of 1-10:1-10.
The following are sources and effects of the natural plant materials used in the present invention:
tea-oil camellia seed: is seed of Camellia oleifera of Theaceae. Bitter; sweet; leveling; is toxic. Promoting qi circulation; moistening intestines; killing insects. Abdominal pain due to qi stagnation; constipation due to intestinal dryness; roundworms; hookworm; scabies, tinea and pruritus.
Biota orientalis leaf: is dried branch tip and leaf of Platycladus orientalis Platycladus orientalis (L.) Franco belonging to Cupressaceae. Bitter, astringent and cold. Has obvious effects of regulating blood circulation and removing blood heat, and can prevent alopecia and promote hair growth. The Chinese arborvitae twig decoction can obviously shorten bleeding time and coagulation time, and has the effects of stopping bleeding, blackening beard and hair and relieving cough and asthma.
Semen cassiae: is dry mature seed of Cassia tora Cassia obtusifolia L. Or Cassia tora L. Of Leguminosae. Sweet, bitter, salty, slightly cold. Clear heat and improve eyesight, moisten intestines and relieve constipation. Can be used for treating conjunctival congestion, pain, photophobia, lacrimation, headache, dizziness, dim eyesight, constipation.
The invention also provides a preparation method of the composition, which comprises the steps of spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient.
Another object of the present invention is to make use of the above composition with an acceptable silicone oil free shampoo base to make a silicone oil free shampoo capable of improving the lightening, softening, and puffiness of the hair and controlling the secretion of scalp hair oils, in the form of a shampoo, a cream, a shampoo, the composition being used in an amount of 1.0 to 80.0% in the shampoo.
The silicone oil-free matrix includes, but is not limited to, the following adjuvants:
and (2) a surfactant: AES, AESA, K12, K12A, CAB, SHD, APG, amino acids.
Conditioning agent: p-7, P-10, TC-90, cationic guar gum, quaternized proteins, higher alcohols, lanolin, glycerol, spearmint oil.
And (3) a thickening agent: naCl, NH 4 Cl and other salts, CMEA, DOE-120, hydroxyethyl cellulose, hydroxypropyl methylcellulose, acrylic acid, acrylic esters, carbomers.
Foaming agent: sodium xylene sulfonate.
Foam stabilizer: polyethylene oxide, CMEA.
Chelating agent: EDTA.
Shampoo liquid: the composition is prepared with one or more of surfactant, conditioner, foaming agent, foam stabilizer, thickener and chelating agent according to conventional shampoo production process.
Shampoo: the composition is prepared with one or more of surfactant, conditioner, foaming agent, foam stabilizer, thickener and chelating agent according to conventional shampoo production process.
Hair washing cream: the composition is prepared with one or more of surfactant, conditioner, foaming agent, foam stabilizer, thickener and chelating agent according to conventional shampoo production process.
Shampoo cream: the composition is prepared with one or more of surfactant, conditioner, foaming agent, foam stabilizer, thickener and chelating agent according to conventional shampoo production process.
Due to the adoption of the technical scheme, the invention has the following beneficial effects:
1. the camellia seed in the composition is a good natural plant cleaning product, contains tea saponin, tea polyphenol, vitamins B and E and various natural organic components, provides nutrition for skin, can keep hair black and bright, repair damaged hair quality and supplement nutrients for hair. Vitamins B and E are effective for folliculitis, seborrheic dermatitis, and can also be used for preventing scalp itching, tinea, etc. The tea polyphenol has strong antioxidation, anti-inflammatory and bactericidal effects, and is a natural preservative. Tea saponin is a natural nonionic surfactant, and has good emulsifying and decomposing, foaming and foam stabilizing, and wetting and penetrating effects. Unsaturated fatty acid in the tea seed oil is easy to absorb, so that the hair can be washed by the tea seed oil to recover the luster of the dry hair and prevent the hair from being bifurcated, and the hair washing by the tea seed oil has the effects of preventing scalp itching, relieving itching and removing dandruff and regulating the secretion balance of scalp sebaceous glands.
The cacumen Platycladi has effects of treating alopecia, relaxing smooth muscle, partially blocking action of acetylcholine on smooth muscle, improving hair follicle growth, inhibiting Staphylococcus aureus and Staphylococcus albus, removing dandruff, promoting hair regeneration, and enhancing hair follicle metabolism.
Semen Cassiae contains anthraquinone, pyrrolidone, fatty acid, amino acid and inorganic elements. The alcohol extract and the water extract of semen cassiae have different degrees of inhibition effects on dermatophytes and bacteria. The emodin in the semen cassiae has inhibiting effect on staphylococcus aureus, escherichia coli, pseudomonas aeruginosa and the like, can inhibit the activity of microorganisms such as bacteria, viruses and fungi, inhibit the growth of the microorganisms and even kill the microorganisms, and can also inhibit lipid peroxidation and superoxide radical generation, so that the semen cassiae has a certain antioxidant effect. Anthraquinone in semen Cassiae has strong inhibiting effect on Escherichia coli and Penicillium, and water-soluble polysaccharide as main component of semen Cassiae inner shell can promote intestinal beneficial bacteria proliferation, and competitively inhibit pathogenic bacteria or intestinal harmful bacteria proliferation.
The combination of the three can not only resist bacteria and diminish inflammation, but also effectively remove excessive sebum secreted on scalp, wherein the sebum is a warm bed for survival of various bacteria, so that various bacteria, especially malassezia, are killed and inhibited from exogenous sources, the external channels generated by dandruff are fundamentally blocked, the scalp itching, chapping and eczema are obviously improved, the cleaning capability is strong, and the scalp skin is kept fresh, healthy and comfortable.
2. The hydrolyzed keratin contained in the composition is a product obtained by fermenting keratin by microorganisms and carrying out acid-base hydrolysis treatment. The rich cystine, tyrosine, serine and the like are completely dissolved in water in an ionic state, and have certain bonding capability. The composition of amino acid contained in hydrolyzed keratin is the same as that of amino acid in human hair, and various nutrients such as hydrolyzed keratin, amino acid and the like are directly supplied to dry and coarse hair in a physical mode, and the adhesiveness of protein components on the hair is effectively enhanced through a microsphere transmission system, so that the release time of the protein components is prolonged, and the visual effect of thickening the hair is enhanced while the hair is nourished. A layer of protective film is formed on the surface of the hair to repair damaged hair, so that brittle failure, bifurcation and falling of hair are reduced, and meanwhile, an antistatic effect is achieved, and the hair is smooth and luster.
3. The porous starch has stronger adsorption capacity, and the oil phase active ingredient is absorbed by the porous starch, so that the oil phase active ingredient is slowly released to moisten scalp and hair when the porous starch is used, and meanwhile, the porous starch can be used as an abrasive, can adsorb and erase dirt, grease, dander and aged keratinocytes on the surfaces of the scalp and the hair, is mild, does not hurt the scalp and regulates the oil-water balance.
4. The nano antibacterial particles of the composition have the functions of dust removal, bacteriostasis, sterilization and fatigue elimination. The nano silver particles with strong spectrum sterilization effect have lasting antibacterial effect, can kill bacteria, viruses, fungi and other microorganisms, can effectively control stubborn and drug-resistant antibacterial bacterial strain flora, and can kill a large number of pathogenic organisms with a small amount of silver. Therefore, nano particles are added into the shampoo, so that the shampoo can massage scalp and promote blood circulation when in shampoo, and the shampoo is synergistic with camellia seed oil, hydrolyzed keratin, porous starch and the like, so that the anti-dandruff and antipruritic effects are enhanced.
5. The composition and the silicone oil-free shampoo matrix are prepared into the silicone oil-free shampoo which can improve the luster, softness and fluffiness of the hair and control the secretion of scalp hair oil, and the dosage forms such as shampoo, shampoo cream, shampoo and shampoo adopt vegetable oil to replace silicone oil, so that the scalp problem caused by silicone oil accumulation is effectively avoided, and the hair is fluffy, natural, truly bright, smooth, soft and glossy after washing.
In conclusion, the composition containing the plant extracts for regulating scalp grease secretion, brightening hair and smoothing hair contains various plant extracts, can improve ordered arrangement of hair, hair and hair scales, inhibit bacterial and fungus growth, regulate and control water-oil balance of head skin, achieve the effects of cleaning and removing dandruff, supplement nutrition and moisture required by hair and scalp, reduce scalp itching, prevent hair loss, bifurcation and fungus growth, improve scalp blood circulation, promote metabolism, strengthen hair roots, make hair appear thick and smooth, and make hair appear healthy by utilizing the effects of the camellia oleosa seed oil, other plant extracts and hydrolyzed keratin.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail by referring to preferred embodiments. It should be noted, however, that many of the details set forth in the description are merely provided to provide a thorough understanding of one or more aspects of the invention, and that these aspects of the invention may be practiced without these specific details.
Example 1
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair is prepared by the following preparation method:
(1-1) weighing camellia seeds, biota orientalis leaves and cassia seeds according to the mass ratio of 20:10:10, squeezing the camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and taking an upper oil phase, a lower camellia seed water phase component and camellia seed filter residues for later use; placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 30 times of pure water, distilling for 60min, separating to obtain oil phase, and mixing all the oil phases to obtain oil phase active ingredient.
(1-2) taking all materials remained in the step (1-1) except the oil phase, heating to 50 ℃ under stirring, maintaining for 60min, filtering, centrifuging, standing, taking supernatant, and concentrating to a concentrated solution with a relative density of 1.20 at 50 ℃ to obtain an aqueous phase active ingredient.
(1-3) porous starch is obtained from the market, which is prepared from corn starch by enzyme treatment, wherein the radius of the pores is 3.80-6.00 μm, and the depth of the pores is 1.5-2.5 μm.
The oil phase active ingredient, the water phase active ingredient and the porous starch form a first component according to the mass ratio of 5:10:5.
(2) Hydrolyzed keratin having a molecular weight of 10 kilodaltons, which is obtained from the hydrolysis of hair, is commercially available as the second component.
(3) The third component is composed of commercially available nano silver particles having a particle size of 10 nm.
(4) Weighing the raw materials of the first component, the second component and the third component according to the mass ratio of 1:20:0.1, spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient to obtain the composition containing the plant extract for regulating the secretion of scalp grease, brightening hair and smoothening hair.
Example 2
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair is prepared by the following preparation method:
(1-1) weighing camellia seeds, biota orientalis leaves and cassia seeds according to the mass ratio of 50:20:15, squeezing the camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and taking an upper oil phase, a lower camellia seed water phase component and camellia seed filter residues for later use; placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 45 times of pure water, distilling for 80min, separating to obtain oil phase, and mixing all the oil phases to obtain oil phase active ingredient.
(1-2) taking all materials remained in the step (1-1) except the oil phase, heating to 60 ℃ under stirring, maintaining for 40min, filtering, centrifuging, standing, taking supernatant, and concentrating to a concentrated solution with a relative density of 1.10 at 45 ℃ to obtain an aqueous phase active ingredient.
(1-3) porous starch is obtained from the market, which is prepared from wheat starch by enzyme treatment, wherein the radius of the pores is 3.80-6.00 μm, and the depth of the pores is 1.5-2.5 μm.
The oil phase active ingredient, the water phase active ingredient and the porous starch form a first component according to the mass ratio of 15:30:20.
(2) Hydrolyzed keratin having a molecular weight of 15 kilodaltons, obtained from the hydrolysis of hair, feathers, is commercially available and constitutes the second component.
(3) The nano silver particles and nano titanium dioxide particles with the particle size of 15nm are obtained from the market and uniformly mixed with each other by equal mass to form a third component.
(4) Weighing the raw materials of the first component, the second component and the third component according to the mass ratio of 8:80:0.3, spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient to obtain the composition containing the plant extract for regulating the secretion of scalp grease, brightening hair and smoothening hair.
Example 3
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair is prepared by the following preparation method:
weighing camellia seeds, biota orientalis leaves and cassia seeds according to a mass ratio of 35:15:10, squeezing the camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and taking an upper oil phase, a lower camellia seed water phase component and camellia seed filter residues for later use; placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 60 times of pure water, distilling for 150min, separating to obtain oil phase, and mixing all the oil phases to obtain oil phase active ingredient.
(1-2) taking all materials remained in the step (1-1) except the oil phase, heating to 70 ℃ under stirring, maintaining for 30min, filtering, centrifuging, standing, taking supernatant, and concentrating to a concentrated solution with a relative density of 1.05 at 40 ℃ to obtain an aqueous phase active ingredient.
(1-3) porous starch is obtained from the market, which is prepared from wheat starch by enzyme treatment, wherein the radius of the pores is 3.80-6.00 μm, and the depth of the pores is 1.5-2.5 μm.
The oil phase active ingredient, the water phase active ingredient and the porous starch form a first component according to the mass ratio of 20:40:20.
(2) Hydrolyzed keratin having a molecular weight of 15 kilodaltons, obtained from the hydrolysis of hair, feathers, is commercially available and constitutes the second component.
(3) The silver nanoparticles and titanium dioxide nanoparticles with the particle size of 20nm are obtained from the market and are uniformly mixed according to the mass ratio of 2:1 to form a third component.
(4) Weighing the raw materials of the first component, the second component and the third component according to the mass ratio of 10:35:0.5, spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient to obtain the composition containing the plant extract for regulating the secretion of scalp grease, brightening hair and smoothening hair.
Example 4
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair is prepared by the following preparation method:
weighing camellia seeds, biota orientalis leaves and cassia seeds according to a mass ratio of 40:18:12, squeezing the camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and taking an upper oil phase, a lower camellia seed water phase component and camellia seed filter residues for later use; placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 40 times of pure water, distilling for 80min, separating to obtain oil phase, and mixing all the oil phases to obtain oil phase active ingredient.
(1-2) taking all materials which are left except the oil phase in the step (1-1), adding 0.1% of probiotics microbial inoculum into the materials, sealing and fermenting at 25 ℃, opening a cover and stirring for 10min every 12h, sealing and fermenting again, sealing for 120d at 25 ℃ after the operation for 25 times, filtering, and taking filtrate to obtain an aqueous phase active ingredient; the probiotic bacteria agent is a mixture of three bacteria agents of bacillus subtilis, lactobacillus and saccharomycetes.
(1-3) porous starch is obtained from the market, which is prepared from wheat starch by enzyme treatment, wherein the radius of the pores is 3.80-6.00 μm, and the depth of the pores is 1.5-2.5 μm.
The oil phase active ingredient, the water phase active ingredient and the porous starch form a first component according to the mass ratio of 16:35:14.
(2) Hydrolyzed keratin having a molecular weight of 20 kilodaltons, obtained from the hydrolysis of feathers, is commercially available as the second component.
(3) The silver nanoparticles and titanium dioxide nanoparticles with the particle size of 15nm are obtained from the market and are uniformly mixed according to the mass ratio of 3:5 to form a third component.
(4) Weighing the raw materials of the first component, the second component and the third component according to the mass ratio of 5:20:0.4, spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient to obtain the composition containing the plant extract for regulating the secretion of scalp grease, brightening hair and smoothening hair.
Example 5
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair is prepared by the following preparation method:
weighing camellia seeds, biota orientalis leaves and cassia seeds according to the mass ratio of 30:12:10, squeezing the camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and taking an upper oil phase, a lower camellia seed water phase component and camellia seed filter residues for later use; placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 50 times of pure water, distilling for 100min, separating to obtain oil phase, and mixing all the oil phases to obtain oil phase active ingredient.
(1-2) taking all materials which are left except the oil phase in the step (1-1), adding 0.2% of probiotics microbial inoculum into the materials, sealing and fermenting at 28 ℃, opening a cover every 24 hours, stirring for 8min, sealing and fermenting again, sealing for 100d at 28 ℃ after 20 times of operation, filtering, and taking filtrate to obtain water phase active ingredients; the probiotic bacteria agent is a mixture of three bacteria agents of bacillus subtilis, lactobacillus and saccharomycetes.
(1-3) porous starch is obtained from the market, which is prepared from corn starch by enzyme treatment, wherein the radius of the pores is 3.80-6.00 μm, and the depth of the pores is 1.5-2.5 μm.
The oil phase active ingredient, the water phase active ingredient and the porous starch form a first component according to the mass ratio of 10:40:12.
(2) Hydrolyzed keratin having a molecular weight of 25 kilodaltons, which is obtained from the hydrolysis of fibroin, hair, is commercially available as the second component.
(3) The third component is composed of silver nanoparticles and titanium dioxide nanoparticles with particle diameters of 30nm obtained from the market and uniformly mixed in equal amounts.
(4) Weighing the raw materials of the first component, the second component and the third component according to the mass ratio of 6:30:0.5, spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient to obtain the composition containing the plant extract for regulating the secretion of scalp grease, brightening hair and smoothening hair.
Example 6
A composition containing plant extract for regulating scalp oil secretion, brightening hair and smoothing hair is prepared by the following preparation method:
weighing camellia seeds, biota orientalis leaves and cassia seeds according to the mass ratio of 48:16:12, squeezing the camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and taking an upper oil phase, a lower camellia seed water phase component and camellia seed filter residues for later use; placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 55 times of pure water, distilling for 120min, separating to obtain oil phase, and mixing all the oil phases to obtain oil phase active ingredient.
(1-2) taking all materials which are left except the oil phase in the step (1-1), adding 0.5% of probiotics microbial inoculum into the materials, sealing and fermenting at 30 ℃, opening a cover and stirring for 10min at intervals of 36h, sealing and fermenting again, sealing for 90d at 30 ℃ after 20 times of operation, filtering, and taking filtrate to obtain water phase active ingredients; the probiotic bacteria agent is a mixture of three bacteria agents of bacillus subtilis, lactobacillus and saccharomycetes.
(1-3) porous starch is obtained from the market, which is prepared from corn starch by enzyme treatment, wherein the radius of the pores is 3.80-6.00 μm, and the depth of the pores is 1.5-2.5 μm.
The oil phase active ingredient, the water phase active ingredient and the porous starch form a first component according to the mass ratio of 6:25:8.
(2) Hydrolyzed keratin having a molecular weight of 30 kilodaltons, which is obtained from the hydrolysis of hair, is commercially available as the second component.
(3) The third component is composed of nano titanium dioxide particles with the particle size of 20nm which are obtained from the market.
(4) Weighing the raw materials of the first component, the second component and the third component according to the mass ratio of 10:50:0.4, spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing the porous starch with other raw materials after the porous starch completely absorbs the oil phase active ingredient to obtain the composition containing the plant extract for regulating the secretion of scalp grease, brightening hair and smoothening hair.
Example 7
A shampoo containing plant extract for regulating scalp oil secretion is prepared from composition of example 1, and APG surfactant, glycerol, carbomer, sodium xylene sulfonate, and CMEA according to conventional production process of shampoo, wherein the content of composition of example 1 is 1.0%
Example 8
A shampoo containing plant extract for regulating scalp oil secretion is prepared from the composition of example 2, and K12 surfactant, K12A surfactant, higher alcohol, hydroxyethyl cellulose, sodium xylene sulfonate, polyethylene oxide, EDTA, wherein the content of the composition of example 2 is 1.0% according to conventional production process of shampoo.
Example 9
A shampoo containing plant extract for regulating scalp oil secretion is prepared from the composition of example 3, and CAB surfactant, SHD surfactant, cationic guar gum, hydroxypropyl methylcellulose, sodium xylene sulfonate, polyethylene oxide, EDTA, wherein the content of the composition of example 3 is 1.0% according to conventional production process of shampoo.
Example 10
A shampoo containing plant extract for regulating scalp oil secretion is prepared from the composition of example 4, and AESA surfactant, higher alcohol, lanolin, hydroxyethyl cellulose, sodium xylene sulfonate, polyethylene oxide, EDTA according to conventional production process of shampoo, wherein the content of the composition of example 4 is 3.0%.
Example 11
A shampoo containing plant extract for regulating scalp oil secretion is prepared from the composition of example 5 and amino acid surfactant, spearmint oil, carbomer, acrylic acid, sodium xylene sulfonate, polyethylene oxide, EDTA according to conventional production process of shampoo, wherein the content of the composition of example 5 is 4.0%.
Example 12
A shampoo containing plant extract for regulating scalp oil secretion is prepared from the composition of example 6, and APG surfactant, amino acid surfactant, cationic guar gum, CMEA thickener, DOE-120 thickener, sodium xylene sulfonate, CMEA, EDTA according to conventional production process of shampoo, wherein the content of the composition of example 5 is 5.0%.
The composition containing the plant extract for regulating scalp grease secretion, brightening hair and smoothing hair can be applied to other hair care products such as hair conditioner, gel water and the like besides the application of the embodiment.
The hydrolyzed keratins used in the present invention have a molecular weight of 10 to 30 kilodaltons and are obtainable by hydrolysis or are commercially available.
Investigation of the Using Effect
120 subjects in the age range of 16-60 years are selected, wherein 66 men and 54 women have head parts with flaky white scales and the like which conform to excessive dandruff, and the head parts have greasy and itching. All anti-dandruff hair care products were stopped at 2 weeks prior to the test.
In the test, shampoo of examples 7 to 9 was used as test groups 1 to 3, and control group 1 and control group 2 were provided, wherein the control group 1 and the test group 1 were different in that only shampoo base was contained, and the control group 2 and the control group 1 were different in that ZPT was also contained at 1%. Control 3 differs from control 1 in that it also contains 1% silicone oil. The shampoo products of examples 7-9 and controls 1-3 were used 3 times per week for 8 weeks, randomly divided into 3 groups. And the improvement of the hair and scalp was scored for 10 points each and 100 points total, with the results as set forth in the following table.
Table 1 comprehensive Effect investigation
As shown in the table above, after the shampoo is used for 8 weeks, the shampoo prepared by the invention has remarkable effects on removing dandruff and controlling oil, and the hydrolyzed keratin content of the embodiment 9 is higher, so that the shampoo has a better effect of improving the brightness of the hair. And 3 examples are the formula without silicone oil, compared with the control group, especially the control group 3, the bulk of the hair is improved obviously. The shampoo has rich foam, good decontamination and degreasing performance, smooth wet comb, fresh and cool feeling when in use, good hair elasticity after use, and the effects of degreasing and removing dandruff, brightening hair, softening, relieving itching and preventing hair loss, etc.
The control group 1 used a shampoo base, and after shampooing, the symptoms of excessive hair oil secretion, dandruff and itching were not improved at all, and the symptoms were gradually aggravated with the use time. The shampoo used in the group 2 contains ZPT antibacterial components, has obvious use effect in the first 4 weeks, but gradually reduces the use effect after 5 weeks, which indicates that the shampoo of the group has no obvious effects of removing dandruff and relieving itching and has the phenomenon of repeated attack. The shampoo matrix of the control group 3 contains silicone oil, has good wet comb property and flexibility when washing hair, but has poor fluffiness after the hair is dried, and is accompanied with itching and dandruff aggravation phenomenon.
The inventor finds that the shampoo product is added with 0.5 to 10.0 percent of the composition according to the invention, and the more obvious the effect of improving dull, greasy and collapsed hair quality is along with the increase of the addition amount, the scalp becomes fresh and free of itching, the hair is bright, soft and fluffy and natural, the scalp is mild and free of irritation, the sebaceous gland secretion balance of the scalp can be adjusted, the head oil, the dandruff and the itching are reduced, and the freshness of the scalp and the hair is improved.
Claims (6)
1. A composition containing plant extracts for regulating scalp grease secretion, brightening hair and smoothening hair is characterized by comprising the following components:
(1) A first component: hydrolyzing keratin;
(2) And a second component: an oil phase active ingredient and a water phase active ingredient in a mass ratio of 5-20:10-40:5-20, and porous starch;
(3) And a third component: nano antibacterial particles;
the mass ratio of the first component to the second component to the third component is 1-10:20-80:0.1-0.5;
the oil phase active ingredients comprise camellia seed oil, biota orientalis oil and cassia seed oil;
the oil tea seed oil is obtained by the following method: squeezing camellia seeds at normal temperature, filtering, centrifuging the filtrate, standing for layering, and collecting the upper oil phase, the lower camellia seed water phase component and camellia seed filter residue for later use;
the biota orientalis oil and the cassia seed oil are obtained by the following method: placing cacumen Platycladi and semen Cassiae together into volatile oil extractor, adding 30-60 times of pure water, distilling for 60-150min, and separating to obtain oil phase and water phase containing residue of cacumen Platycladi and semen Cassiae, wherein the oil phase is mixture of cacumen Platycladi oil and semen Cassiae oil;
the mass ratio of the camellia seeds to the biota orientalis leaves to the cassia seeds is 20-50:10-20:10-20;
the aqueous phase active ingredient is obtained by the following method: adding lower layer of water phase component of semen Camelliae sinensis and residue of semen Camelliae sinensis into water phase containing residue of folium Platycladi and semen Cassiae, heating to 50-70deg.C under stirring, maintaining for 30-60min, filtering, centrifuging, standing, collecting supernatant, concentrating at 40-50deg.C to obtain concentrated solution with relative density of 1.05-1.20 to obtain water phase active ingredient;
or alternatively, the process may be performed,
adding lower layer tea seed water phase component and tea seed residue into water phase containing residue of folium Platycladi and semen Cassiae, adding 0.1-0.5% of probiotics, sealing and fermenting at 25-30deg.C, stirring for 5-10min every 12-36 hr under cover opening, sealing and fermenting again, sealing at 25-30deg.C for 90-120d after 20-25 times, filtering, and collecting filtrate to obtain water phase active ingredient;
the nano antibacterial particles are formed by mixing nano silver particles with the particle size of 10-30nm and nano titanium dioxide particles according to the weight ratio of 1-10:1-10.
2. The composition for regulating scalp lipid secretion, brightening hair and smoothing hair comprising a plant extract as claimed in claim 1, wherein the hydrolyzed keratin of the first component is obtained by hydrolyzing one or more raw materials of hair, feathers and fibroin.
3. The composition for regulating scalp fat secretion, brightening hair and smoothing hair comprising the plant extract according to claim 1, wherein the porous starch is obtained by enzymatic treatment of starch obtained from one or more of potato, corn, wheat and rice as raw materials.
4. The composition for regulating scalp oil secretion, brightening and smoothing hair comprising a plant extract according to claim 1, wherein the porous starch has a pore radius of 3.80-6.00 μm and a pore depth of 1.5-2.5 μm.
5. The composition for regulating scalp fat secretion, brightening hair and smoothing hair comprising the plant extract as claimed in claim 1, which is prepared by the following steps: spraying the oil phase active ingredient into the porous starch through an atomization nozzle, and uniformly mixing with other raw materials after the porous starch completely absorbs the oil phase active ingredient.
6. A shampoo prepared from a composition for regulating scalp fat secretion, lightening and smoothing hair comprising the plant extract of any one of claims 1 to 5 and an acceptable silicone oil free shampoo base, wherein the composition is present in the shampoo in an amount of 1.0 to 80.0%.
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| CN1280487A (en) * | 1997-10-24 | 2001-01-17 | 普罗克特和甘保尔公司 | Cleaning and conditioning article for skin or hair having improved fragrance delivery |
| WO2010004553A1 (en) * | 2008-07-06 | 2010-01-14 | Lice Up Ltd. | Anti-phthiraptera treatment compositions |
| CN111617197A (en) * | 2020-06-23 | 2020-09-04 | 杨玲 | Traditional Chinese medicine composition for hair growth and hair nourishing, and preparation method and application thereof |
| CN111658580A (en) * | 2020-06-23 | 2020-09-15 | 广西和桂集团有限公司 | Hair growth and/or hair blackening essence containing various peptides and plant extracts and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1280487A (en) * | 1997-10-24 | 2001-01-17 | 普罗克特和甘保尔公司 | Cleaning and conditioning article for skin or hair having improved fragrance delivery |
| WO2010004553A1 (en) * | 2008-07-06 | 2010-01-14 | Lice Up Ltd. | Anti-phthiraptera treatment compositions |
| CN111617197A (en) * | 2020-06-23 | 2020-09-04 | 杨玲 | Traditional Chinese medicine composition for hair growth and hair nourishing, and preparation method and application thereof |
| CN111658580A (en) * | 2020-06-23 | 2020-09-15 | 广西和桂集团有限公司 | Hair growth and/or hair blackening essence containing various peptides and plant extracts and preparation method thereof |
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