CN111557865A - Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof - Google Patents
Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof Download PDFInfo
- Publication number
- CN111557865A CN111557865A CN202010465848.7A CN202010465848A CN111557865A CN 111557865 A CN111557865 A CN 111557865A CN 202010465848 A CN202010465848 A CN 202010465848A CN 111557865 A CN111557865 A CN 111557865A
- Authority
- CN
- China
- Prior art keywords
- powder
- salicylic acid
- oil
- dandruff
- hair
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a hair oil-controlling and dandruff-removing fluffy powder containing salicylic acid microcapsules for slowly releasing fragrance, which is characterized by comprising a powder part, a water phase part, a hydroxypropyl cellulose aqueous solution, essence microcapsules and salicylic acid microcapsules, wherein the powder part comprises corn starch, beta-cyclodextrin and sodium benzoate, and the water phase part comprises glycerol, emulsified silicone oil and an ethanol aqueous solution. The preparation method comprises respectively preparing powder and water phase; dispersing a hydroxypropyl cellulose aqueous solution into a water phase, then adding powder, and stirring to paste; drying, pulverizing, and sieving; adding essence microcapsule and salicylic acid microcapsule. The corn starch serving as the powdery raw material is natural and safe, has a good oil absorption effect, is added with the salicylic acid microcapsule, so that the effective dandruff removing and itching relieving effects are improved, the fragrance is kept for a long time, and the application range of dry-cleaning hair cleaning products is expanded.
Description
Technical Field
The invention relates to a cosmetic, in particular to an oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and a preparation method thereof.
Background
According to research, the daily hair washing can cause excessive grease loss on the scalp, so that the scalp and the hair lose natural protective barriers and are harmful to the health of the scalp and the hair quality; and office workers and student parties often do not have energy to wash and care hair due to time work problems. However, if the hair is too greasy or electrically neutral, collapse may occur. At present, oil-absorbing powder products for hair appear in the cosmetic market, the effects of the oil-absorbing powder products mainly comprise oil control, hair filling and the like, great concern is obtained, but some problems still exist. The invention aims to improve the product, and increase the functions of slow release and fragrance retention, effective oil removal, bacteriostasis and dandruff removal and the like.
The successful application of the microcapsule technology in the scientific research of cosmetics brings revolutionary changes to the cosmetic industry. The invention relates to a cosmetic, which is characterized in that an additive in the cosmetic is coated by microcapsules, so that the reactivity, the durability (prolonging the storage time of volatile substances), the sub-sensitivity, the heat sensitivity and the photosensitivity of encapsulated substances, the odor control release and the like of the encapsulated substances are improved, and the product performance is more excellent.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: the cosmetics in the prior art have the technical problems of short fragrance retention time, excessive grease, dandruff breeding, scalp itching and influence on the effect of the cosmetics.
In order to solve the technical problems, the invention provides an oil-controlling and dandruff-removing fluffy powder containing salicylic acid microcapsule slow-release fragrance for hair, which is characterized by comprising a powder part, a water phase part, a hydroxypropyl cellulose aqueous solution with the mass concentration of 0.5-5%, an essence microcapsule and a salicylic acid microcapsule, wherein the powder part comprises corn starch, beta-cyclodextrin and sodium benzoate, and the water phase part comprises glycerol, emulsified silicone oil and an ethanol aqueous solution.
Preferably, the powder part comprises 35 parts by weight of corn starch, 64.99 parts by weight of beta-cyclodextrin and 0.01 part by weight of sodium benzoate; the water phase part comprises 5 parts by weight of glycerol, 3 parts by weight of silicone emulsion and 102 parts by weight of ethanol aqueous solution; the addition amount of the hydroxypropyl cellulose aqueous solution is 0.5 to 3 percent of the total mass of all the raw materials; the adding amount of the essence microcapsule is 5-10% of the total mass of all the raw materials; the addition amount of the salicylic acid microcapsules is 3-6% of the total mass of all the raw materials.
Preferably, the mass concentration of the ethanol water solution is 50-60%.
The invention also provides a preparation method of the oil-controlling and dandruff-removing fluffy powder for hair containing the salicylic acid microcapsule slow-release fragrance, which is characterized by comprising the following steps:
step 1): preparing corn starch, beta-cyclodextrin and sodium benzoate into powder; preparing water phase from glycerol, emulsified silicone oil, ethanol and pure water;
step 2): dispersing the hydroxypropyl cellulose aqueous solution into the water phase, uniformly stirring, then adding the mixture into the powder, and fully and uniformly stirring the mixture to be pasty;
step 3): drying the mixture obtained in the step 2), crushing and sieving;
step 4): adding the essence microcapsules and the salicylic acid microcapsules into the powder obtained in the step 3), and uniformly mixing.
Preferably, the stirring speed in the step 2) is 100-500r/min, and the stirring time is 5-10 min.
Preferably, the drying temperature in the step 3) is 30-35 ℃.
Preferably, the step 3) is performed by 200-300 mesh sieve.
The essence and the functional raw materials are coated and sealed by adopting a microcapsule granulation technology, so that the essence and the functional raw materials are powdered, the stability of the essence is improved, and the problems of short aroma retention time, poor solubility, strong liquid volatility and the like of the product are solved: most essence is liquid substance, which can not be added into the fluffy powder or is influenced by phototoxicity and stability, so that the performance of other products is limited, and the prepared emulsion or liquid has the problems of quick volatilization, inconvenience, cool feeling and the like.
Polysaccharide polymers (such as corn starch and modified starch) are mainly used for absorbing hair-coat grease, keeping hair fresh and fluffy, and increasing the safety and the anti-sensitivity of products: modified starch is mainly used as a main substrate, and powder post-treatment technologies such as dispersion treatment, appearance treatment and the like are adopted to ensure that the product powder is fine and smooth and has good stability;
the antibacterial substance raw material and the dandruff-removing and itching-relieving raw material, namely the salicylic acid microcapsule are added, the salicylic acid has a bidirectional cutin regulating effect, and on one hand, the cutin is loosened, the hyperkeratotic cutin metabolism can be promoted, and the medicine absorption can be promoted; on the other hand, the expression of filaggrin can be promoted, the barrier function repair is promoted, so that the dandruff generation is effectively inhibited, the problems of dandruff increase and scalp itching of similar products in the market are solved, the growth and the propagation of malassezia are inhibited, grease is adsorbed, and the problems are solved in the dandruff generation process; compared with the prior art, the invention has remarkable technical progress. The powder raw material is natural and safe, and the microcapsule coating technology is added, so that the fluffy powder has excellent performance, is convenient to use, greatly reduces the consumption of the preservative, enlarges the types of novel products free from washing off the head oil, and provides reference for the application of the microcapsule technology in cosmetics.
Drawings
FIG. 1 shows the results of a 72 hour unwashed hair oil test on 4 subjects.
Detailed Description
In order to make the invention more comprehensible, preferred embodiments are described in detail below with reference to the accompanying drawings.
The specification of the raw materials used in the examples of the present invention and information on the manufacturer are shown in table 1.
TABLE 1
Raw materials | Reagent specification | Manufacturer of the product |
Corn starch | Analytical purity | Shanghai Weimeisi Condiments Co.,Ltd. |
Glycerol | Analytical purity | SINOPHARM CHEMICAL REAGENT Co.,Ltd. |
β Cyclodextrin | Analytical purity | Temple of Jinshang Guo town of Mengzhou city, Henan province |
Emulsified silicone oil | Analytical purity | SINOPHARM CHEMICAL REAGENT Co.,Ltd. |
Hydroxypropyl cellulose | Analytical purity | SINOPHARM CHEMICAL REAGENT Co.,Ltd. |
Ethanol | Analytical purity | SINOPHARM CHEMICAL REAGENT Co.,Ltd. |
Sodium benzoate | Analytical purity | SINOPHARM CHEMICAL REAGENT Co.,Ltd. |
Salicylic acid microcapsule | - | Self-made |
Microcapsule essence | - | Self-made |
The model of the equipment and the information of the manufacturer used in the preparation process of each embodiment of the invention are as follows:
electronic balance, PL403, mettler-toledo instruments ltd;
constant temperature magnetic stirrer, 524G, shanghai meipu instruments manufacturing ltd;
digital display constant temperature water bath, HH-2, changzhou guohua electrical appliances limited;
an air-blowing constant-temperature drying box, a GZX-9023MBE electric heating air-blowing drying box.
Example 1
Preparing 20g of hydroxypropyl cellulose aqueous solution with the mass concentration of 5% by using deionized water, and stirring the solution at room temperature until the solution is completely dissolved; preparing required powder raw materials: 15.12g of corn starch and 22.7g of beta-cyclodextrin; 30g of an ethanol solution was prepared.
Adding 2.5g of glycerol and 1.5g of emulsified silicone oil into the prepared powder raw material, and adding a hydroxypropyl cellulose solution; adding ethanol solution rapidly while stirring, stirring thoroughly and rapidly to obtain uniform paste, and oven drying at 35 deg.C for 48 hr in a constant temperature oven until water is completely evaporated to obtain powder cake.
And (3) fully grinding the powder cake into a grinding dish until the powder cake is dispersed into a powder shape, filtering the powder cake by using a 120-mesh sieve to obtain a powder sample, adding microcapsule essence accounting for 5 percent of the total mass of the raw materials and salicylic acid microcapsules accounting for 6 percent of the total mass of the raw materials into the powder sample, and uniformly mixing the powder sample and the essence to obtain the fluffy powder of the powder sample.
Example 2
Firstly weighing 20.0g of pure water, preparing a hydroxypropyl cellulose solution with the mass concentration of 1%, stirring until the pure water is completely dissolved, then adding 0.5g of glycerol and 0.3g of emulsified silicone oil into the solution, adding 30g of ethanol, and stirring uniformly.
Adding 35.0g corn starch, 65.0g beta-cyclodextrin and appropriate amount of sodium benzoate into the solution rapidly, stirring into paste, stirring at normal temperature for 10min, and drying the resultant paste suspension at constant temperature of 35 deg.C for 48 hr to completely volatilize water and alcohol into cake.
Taking out the cake, grinding and filtering the cake by a ball mill to control the granularity of the cake to be about 180 meshes, finally adding salicylic acid microcapsules accounting for 6 percent of the total mass of the raw materials and essence microcapsules accounting for 5 percent of the total mass of the raw materials, and uniformly mixing to obtain the white powdery fluffy powder.
Example 3
Preparing 20.0g of hydroxypropyl cellulose aqueous solution with the mass concentration of 0.5%, stirring until the hydroxypropyl cellulose aqueous solution is completely dissolved, and standing for later use; preparing mixed powder of 30.0g of corn starch and 50.0g of beta-cyclodextrin, pouring all the powder into a hydroxypropyl cellulose solution, adding 4.0g of glycerol and 3.0g of emulsified silicone oil into the hydroxypropyl cellulose solution, adding an ethanol solution into the mixture to adjust the mixture to a proper consistency, forming pasty suspension, and stirring the mixture at a low speed for 20min until the mixture is uniformly stirred.
And (3) putting the suspension into a blast constant-temperature drying oven, and drying at the constant temperature of 35 ℃ to volatilize all water and alcohol to form blocky solid. And crushing and scattering the solid in a grinding mode, sieving by a 100-mesh sieve, and finally adding 4.0g of essence microcapsules and 4.8g of salicylic acid microcapsules according to the mass of the powder.
And (3) testing results:
1. oil absorption and oil control effect test:
the results are shown in FIG. 1 by detecting the change in oil content of hair without hair washing for 72 hours in the daily routine of 4 testers, and with and without the use of the powder. The used test method is that the testers are required to be not cleaned by the conventional method within 72 hours under the daily condition, the hair is kept in a natural state, whether the fluffy powder is used or not is tested for the oil content, and the test sample paper is as follows: the Clean Clear oil absorbent paper (Clean Clear oil absorbent film) is tested by utilizing the principle that a film colloid material is easy to combine with oil and the color becomes dark after oil absorption, and the Clean Clear oil absorbent paper is tested by shooting the effect of the Clean Clear oil absorbent paper after fully absorbing oil with hair under the same contact mode, force and position conditions.
The test result shows that the area of the shadow part after using the awning powder and the area of the shadow part before using the awning powder are obviously reduced, the area is distributed from large area to large area, and is dispersed and distributed individually, and the whole color of the oil absorption paper after being used integrally is obviously lighter. The fluffy powder has better effects of cleaning, removing and conditioning grease.
2. Testing the fragrance retention effect and fragrance stability:
under the condition of normal use of the awning powder, 10 volunteer testers are subjected to lighter training and then subjected to sensory evaluation, and after one-time normal use, the volunteers are subjected to olfactory sensory evaluation respectively after 6 hours, 12 hours and 24 hours, so that the aroma concentration change of the volunteer testers is described, and the aroma concentration change is divided into five grades of heavy, thick, common, lighter and very light.
TABLE 2
Numbering | Fragrance intensity of 6 hours | Fragrance intensity for 12 hours | Fragrance intensity for 24 |
1 | Is thicker | In general | Is relatively light |
2 | Concentration of heavy metal | In general | Is very light |
3 | Is thicker | Is relatively light | Is very light |
4 | Concentration of heavy metal | In general | Is very light |
5 | Is thicker | In general | Is relatively light |
6 | Is thicker | In general | Is very light |
7 | Is thicker | Is relatively light | Is very light |
8 | Concentration of heavy metal | Is thicker | Is relatively light |
9 | Is thicker | In general | Is very light |
10 | Is thicker | In general | Is very light |
The essence microcapsule has good durability, can basically maintain more than 24 hours in daily life, and can play a significant role in slowly releasing the fragrance.
3. And (3) testing bacteriostatic, anti-dandruff and itching-relieving effects:
dandruff is produced because scalp is constantly metabolized, and if metabolism is abnormal, excessive scalp cells are exfoliated and become anucleate and inanimate cuticle, thereby causing dandruff problems. At the latest world dermatological congress in paris, scientists of the american treasure company declared that this dandruff is caused by the lipid metabolic waste of 2 fungi, malassezia restricta and malassezia globosa. Malassezia restricta and Malassezia globosa are characterized by lipophilicity, and they take the fatty substances secreted in the hair follicle of human scalp as food, leaving some of the digested fat on the scalp as a stimulus to cause dandruff.
The antibacterial effect of the sample is detected by sampling the sample and carrying out antibacterial experiments, and then the problems of dandruff generation, scalp itching and the like are reduced through the antibacterial effect. Preparing the sample into stock solution, and performing drug effect sterilization effect and toxicity test according to the requirements of disinfection technical specifications to obtain the salicylic acid-containing microcapsule capable of killing more than or equal to 99.0% of bacteria.
TABLE 3
Numbering | Fragrance intensity of 6 hours | Fragrance intensity for 12 hours | Fragrance intensity for 24 |
1 | Is thicker | In general | Is relatively light |
2 | Concentration of heavy metal | In general | Is very light |
3 | Is thicker | Is relatively light | Is very light |
4 | Concentration of heavy metal | In general | Is very light |
5 | Is thicker | In general | Is relatively light |
6 | Is thicker | In general | Is very light |
7 | Is thicker | Is relatively light | Is very light |
8 | Concentration of heavy metal | Is thicker | Is relatively light |
9 | Is thicker | In general | Is very light |
10 | Is thicker | In general | Is very light |
In conclusion, the oil-controlling and dandruff-removing fluffy powder for the hair with the microcapsule slow-release fragrance is suitable for cleaning the oil on the surface of the hair, conditioning the oil balance, keeping fluffy and refreshing, controlling dandruff bacteriostasis and slowly releasing the fragrance; the main raw materials of the invention are from natural and edible grade, without side effect, the microcapsule technology reduces the usage of the antiseptic and the salicylic acid antibacterial antipruritic, greatly reduces the irritation, does not hurt the scalp, has high stability, is suitable for various people, and is convenient to use in a dry cleaning mode, more meets the use requirement of consumers and enhances the convenience.
Claims (7)
1. The oil-controlling and dandruff-removing fluffy powder containing the salicylic acid microcapsule slow-release fragrance for the hair is characterized by comprising a powder part, a water phase part, a hydroxypropyl cellulose water solution with the mass concentration of 0.5% -5%, an essence microcapsule and a salicylic acid microcapsule, wherein the powder part comprises corn starch, beta-cyclodextrin and sodium benzoate, and the water phase part comprises glycerol, emulsified silicone oil and an ethanol water solution.
2. The oil-controlling and dandruff-removing powder containing salicylic acid microcapsule slow-release fragrance for hair of claim 1, wherein the powder part comprises 35 parts by weight of corn starch, 64.99 parts by weight of beta-cyclodextrin and 0.01 part by weight of sodium benzoate; the water phase part comprises 5 parts by weight of glycerol, 3 parts by weight of silicone emulsion and 102 parts by weight of ethanol aqueous solution; the addition amount of the hydroxypropyl cellulose aqueous solution is 0.5 to 3 percent of the total mass of all the raw materials; the adding amount of the essence microcapsule is 5-10% of the total mass of all the raw materials; the addition amount of the salicylic acid microcapsules is 3-6% of the total mass of all the raw materials.
3. The oil-controlling and dandruff-removing awning powder for hair of slow-release fragrance containing salicylic acid microcapsules of claim 1, wherein the mass concentration of the ethanol aqueous solution is 50-60%.
4. The method for preparing the oil-controlling and dandruff-removing awning powder for hair of the slow-release fragrance of the salicylic acid-containing microcapsules as claimed in any one of claims 1 to 3, which is characterized by comprising the following steps:
step 1): preparing corn starch, beta-cyclodextrin and sodium benzoate into powder; preparing water phase from glycerol, emulsified silicone oil, ethanol and pure water;
step 2): dispersing the hydroxypropyl cellulose aqueous solution into the water phase, uniformly stirring, then adding the mixture into the powder, and fully and uniformly stirring the mixture to be pasty;
step 3): drying the mixture obtained in the step 2), crushing and sieving;
step 4): adding the essence microcapsules and the salicylic acid microcapsules into the powder obtained in the step 3), and uniformly mixing.
5. The method for preparing the oil-controlling and anti-dandruff fluffy powder for the hair with the salicylic acid-containing microcapsule slow-release fragrance as claimed in claim 4, wherein the stirring speed in the step 2) is 100-500r/min and the stirring time is 5-10 min.
6. The method for preparing the oil-controlling and dandruff-removing awning powder for hair containing salicylic acid microcapsule slow-release fragrance as claimed in claim 4, wherein the drying temperature in the step 3) is 30-35 ℃.
7. The method for preparing the oil-controlling and dandruff-removing powder for the hair with the salicylic acid-containing microcapsule slow-release fragrance as claimed in claim 4, wherein the step 3) is carried out by sieving with a 200-300 mesh sieve.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010465848.7A CN111557865A (en) | 2020-05-28 | 2020-05-28 | Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010465848.7A CN111557865A (en) | 2020-05-28 | 2020-05-28 | Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN111557865A true CN111557865A (en) | 2020-08-21 |
Family
ID=72068652
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202010465848.7A Pending CN111557865A (en) | 2020-05-28 | 2020-05-28 | Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN111557865A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112089650A (en) * | 2020-09-22 | 2020-12-18 | 广州花出见生物科技有限公司 | Deoiling composition and application thereof |
CN114099386A (en) * | 2021-11-29 | 2022-03-01 | 广州温雅日用化妆品有限公司 | Bacteriostatic and fragrance-releasing foam shampoo |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1996000563A1 (en) * | 1994-06-28 | 1996-01-11 | Pierre Fabre Dermo-Cosmetique | Phytogenic dry shampoo |
CN106619183A (en) * | 2017-03-14 | 2017-05-10 | 广东龙湖科技股份有限公司 | Washing-free powdery shampoo and preparation method thereof |
CN107362062A (en) * | 2017-08-16 | 2017-11-21 | 佛山市三水区嘉华化学研究院(普通合伙) | A kind of disposable spraying of scalp care |
CN108125799A (en) * | 2017-12-29 | 2018-06-08 | 上海应用技术大学 | A kind of composite slow release essence microcapsule and preparation method thereof |
CN108210346A (en) * | 2018-01-10 | 2018-06-29 | 上海应用技术大学 | It is a kind of to load salicylic compound wall materials microcapsules and preparation method thereof |
EP3586818A1 (en) * | 2017-05-23 | 2020-01-01 | Toyo Aerosol Industry Co., Ltd. | Aerosol composition for hair and aerosol product for hair |
-
2020
- 2020-05-28 CN CN202010465848.7A patent/CN111557865A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1996000563A1 (en) * | 1994-06-28 | 1996-01-11 | Pierre Fabre Dermo-Cosmetique | Phytogenic dry shampoo |
CN106619183A (en) * | 2017-03-14 | 2017-05-10 | 广东龙湖科技股份有限公司 | Washing-free powdery shampoo and preparation method thereof |
EP3586818A1 (en) * | 2017-05-23 | 2020-01-01 | Toyo Aerosol Industry Co., Ltd. | Aerosol composition for hair and aerosol product for hair |
CN107362062A (en) * | 2017-08-16 | 2017-11-21 | 佛山市三水区嘉华化学研究院(普通合伙) | A kind of disposable spraying of scalp care |
CN108125799A (en) * | 2017-12-29 | 2018-06-08 | 上海应用技术大学 | A kind of composite slow release essence microcapsule and preparation method thereof |
CN108210346A (en) * | 2018-01-10 | 2018-06-29 | 上海应用技术大学 | It is a kind of to load salicylic compound wall materials microcapsules and preparation method thereof |
Non-Patent Citations (4)
Title |
---|
佚名: "不洗头也不怕出油•fujiko蓬蓬粉", 《HTTPS://WWW.SOHU.COM/A/249925361_649860?_F=INDEX_PAGERECOM_7,2018-08-25》 * |
倪青等: "《常用临床药物手册》", 30 September 1999, 中国医药科技出版社 * |
张菊芳: "《现代毛发移植技术》", 31 May 2018, 浙江科学技术出版 * |
黄仲华: "《中国调味食品技术实用手册》", 28 February 1991, 中国标准出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112089650A (en) * | 2020-09-22 | 2020-12-18 | 广州花出见生物科技有限公司 | Deoiling composition and application thereof |
CN114099386A (en) * | 2021-11-29 | 2022-03-01 | 广州温雅日用化妆品有限公司 | Bacteriostatic and fragrance-releasing foam shampoo |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN110025658A (en) | A kind of hair-loss preventing and hair-restoring liquid and preparation method thereof | |
CN111557865A (en) | Oil-controlling and dandruff-removing awning powder containing salicylic acid microcapsule slow-release fragrance for hair and preparation thereof | |
KR101565778B1 (en) | Manufacturing Method of Antibiosis Soap Containing Xinc Oxide of Nano Size and Antibiosis Soap Thereof | |
CN101416928A (en) | Matcha anti-senescence face mask added with superoxide dismutase and preparation method thereof | |
CN109528755A (en) | One kind composition containing nano-sulfur and its application | |
CN108451858A (en) | A kind of shampoo powder and its preparation method and application | |
DE69934307T2 (en) | USE OF A TOPICAL COMPOSITION | |
CN109922785A (en) | Ivory nut powder and mannosan from ivory nut | |
CN114652884A (en) | Camellia soothing essence disposable hygienic product nursing base material, preparation method and application | |
CN108939913A (en) | A kind of paste composition and preparation method thereof removing formaldehyde | |
Ginting et al. | Preparation of Moisturizing Lotion from Combination Extract of Clitoria ternatea Flower and Dragon Fruit Peels | |
CN109431842B (en) | Eczema cream for children | |
CN107137306A (en) | A kind of Nano Silver purification, which is washed, unloads two-in-one solution | |
CN106591011A (en) | Antibacterial soap and preparation method thereof | |
CN108904307A (en) | A kind of face cleaning beans and preparation method thereof with mild makeup removing effect | |
CN110227050A (en) | A kind of anti-aging maintenance sustained release Essence and the anti-aging Face-protecting mask using its preparation | |
CN109528619A (en) | A kind of deodorizing type shower cream | |
Lestari et al. | Physical properties test peel off gel mask based of date palm seeds powder (phoenix dactylifera) and olive oil | |
CN108261379A (en) | A kind of facial mask and preparation method thereof | |
CN108030707A (en) | A kind of composition and its application with moistening effect | |
CN107789285A (en) | A kind of anti-oxidant and lightening compositions and the skin care item containing said composition | |
CN1125055A (en) | Method for preparing chewing gum using wheat protein as gumming base | |
RU2696879C1 (en) | Cosmetic face mask for skin care | |
CN106420537A (en) | Rose flower residue exfoliating massaging bathing cream and preparing method thereof | |
CN111803415A (en) | Plant essential oil nano emulsion, preparation method thereof and application thereof in lip products |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200821 |