CN110063900A - A kind of hair dry-washing composition and preparation method thereof - Google Patents
A kind of hair dry-washing composition and preparation method thereof Download PDFInfo
- Publication number
- CN110063900A CN110063900A CN201910371345.0A CN201910371345A CN110063900A CN 110063900 A CN110063900 A CN 110063900A CN 201910371345 A CN201910371345 A CN 201910371345A CN 110063900 A CN110063900 A CN 110063900A
- Authority
- CN
- China
- Prior art keywords
- parts
- hair
- washing composition
- dry
- hair dry
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/31—Anhydrous
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The present invention provides a kind of hair dry-washing composition, the component including following mass parts: propane and butane are 60-80 parts total, and 15-30 parts of dehydrated alcohol, 2-15 parts of starch granules, 0.2-2 parts of deflocculant.The present invention also provides the methods of above-mentioned hair dry-washing composition preparation dry method shampoo.Compsition for dry washing of the invention removes hair and scalp grease effect is good, saves water resource, reduces the use of shampoo, reduces the damage to hair, scalp, convenient for quickly nursing.Compsition for dry washing of the invention has good homogeneity and stability good by adding distinctive deflocculant, can save for a long time with it is practical.Compsition for dry washing performance of the present invention is mildly non-stimulated, will not cause hair, scalp are dry to itch, and noresidue does not generate the feeling of dandruff, does not generate electrostatic, and use feeling is good.
Description
Technical field
The present invention relates to a kind of hair care compositions, more particularly, to hair dry-washing composition and preparation method thereof.
Background technique
Aerosol products are born in the beginning of the forties, by development in more than 80 years, developed country have become one it is perfect
Industrial system.For whole world aerosol yield in 1996 up to 10,100,000,000 tanks, product variety class is more than 4000 kinds.Aerosol Industry exists
China is an emerging industry, and China starts that a small amount of production section is medicinal and industrial flaw detection aerosol the beginning of the sixties, but
Production development stagnates always for many years, just starts the new stage into people's fast development until the eighties.
Investigate and show according to Euromonitor International: the hair nursing market sales revenue in the U.S. in 2017 is
126.6 hundred million dollars, the sales volume in global hair nursing market is 75,100,000,000 dollars, and the U.S. in 2017 shares 2.82 hundred million tank aerosols
Hair products and nearly 68,200,000 tank aerosol mousse, it was demonstrated that hair products still received an acclaim as in the past, wherein dry-cleaning
Shampoo product is evolved so far by single category before, in color, quality, without increasing more selections above fragrant, effect.
The extra grease of scalp can be absorbed in hair dry-washing shampoo, or hair provides quality and hair amount.Traditionally
For removing grease excessive on hair and scalp, washing-off type shampoo is generally used, the wave of great lot of water resources is on the one hand caused
Take, frequent use of shampoo can also damage hair or even scalp, while washing-off type shampoo is directed in " the seat moon
Son ", the specific groups such as travel and emergency crowd are unable to get the nursing of short time.
Summary of the invention
The present invention is in view of the deficienciess of the prior art, provide a kind of hair dry-washing composition and the hair dry-washing composition
Preparation method, to solve the problem of using existing washing-off type hair washing water waste great lot of water resources and injury hair and scalp.
The technical scheme to solve the above technical problems is that
A kind of hair dry-washing composition, the component including following mass parts: propane and butane are 60-80 parts total, dehydrated alcohol
15-30 parts, 2-15 parts of starch granules, 0.2-2 parts of deflocculant；Wherein, the particle size of the starch granules is 3-20 microns.
In the present invention, starch granules is crossed after many greases of sauce on absorbing hair, and dehydrated alcohol can quickly volatilize its oil
Rouge is taken away, and pays attention to that aqueous alcohol cannot be used, if introducing water in formula, it will cause the water swelling of starch, formula is generated
Flocculation, spray do not come out, and block valve, and effect weakens significantly.
The present invention is further arranged to, and the deflocculant is magnesium stearate, aluminum magnesium silicate, starch ocentyl succinic aluminium
One of or it is a variety of.
Preferably, the deflocculant includes magnesium stearate 0.1-1 mass parts and aluminum magnesium silicate 0.1-1 mass parts.
The present invention is further arranged to, the starch granules be one of rice starch, cornstarch, tapioca or
It is a variety of.When rice starch and cornstarch exist jointly, magnesium stearate and aluminum magnesium silicate are compounded by different proportion, are resisted
Flocculating effect is best.
Preferably, the particle size of rice starch is 10-20 microns, and the particle size of cornstarch is 10-20 microns, wood
The particle size of sweet potato starch is 3-8 microns.After being finally packaged into tank, starch granules partial size is small to facilitate powder not blocking valve
Door, is conducive to starch and can smoothly be pushed into agent to take tank body out of, acts on hair.
Preferably, the anti-starch granules includes rice starch 1-10 mass parts and cornstarch 1-5 mass parts.
The present invention is further arranged to, and further includes the cetrimonium chloride of 0.01-0.2 mass parts.In order to increase use it is comfortable
Degree, prevents electrostatic from generating, and introduces antistatic agent, can be the cetrimonium chloride in composition, or other antistatic agents, but
Must be the cationic polymer of liquid, and additive amount cannot be excessively high, it is excessively high will lead to starch absorb hair excess oil after,
Dehydrated alcohol volatile zone is not walked, and is attracted by antistatic agent, is adsorbed on hair, is caused a kind of illusion of dandruff.
The present invention is further arranged to, and further includes the silica of 0.001-0.02 mass parts, and the particle size of the silica is
6-8 microns.Silica mainly plays the role of smooth, improves dry cardability, and addition is less and significant effect.
The present invention is further arranged to, and further includes the Radix Gentianae extract of 0.01-0.1 mass parts, and Radix Gentianae extract is mainly
The stimulation of scalp bring is given for reducing other substances in dehydrated alcohol and composition, this substance is natural origin.Wherein, imperial
Gall extract the preparation method comprises the following steps: expansion bed-pulse reinforcing proposes+medium temperature extractive technique, specific extracting method can refer to Shanghai
201710183506.4, the 201710184049.0 and ZL of patent 2,016 2 0115699.0 of Jia Yu Biotechnology Co., Ltd.
The present invention is further arranged to, and further includes hydroxy phenylpropionyl amine benzoic acid, the 0.0001- of 0.01-0.05 mass parts
1, the 2- pentanediol of 0.05 mass parts and the butanediol of 0.0001-0.5 mass parts, hydroxy phenylpropionyl amine benzoic acid, 1,2- penta 2
These three substances of alcohol, butanediol compounding, effect are the stimulations for reducing composition in terms of other mechanism and generating to scalp.
The present invention is further arranged to, the essence including 0.1-0.5 mass parts.
Preferably, hair dry-washing composition of the present invention, the component including following mass parts: propane and the total 60-80 of butane
Part, 15-30 parts of dehydrated alcohol, 2-15 parts of starch granules, 0.2-2 parts of deflocculant, 0.01-0.2 parts of cetrimonium chloride, silica
0.001-0.02 parts, 0.01-0.1 parts of Radix Gentianae extract, 0.01-0.05 parts of hydroxy phenylpropionyl amine benzoic acid, 1,2- pentanediol
0.0001-0.05 parts, 0.0001-0.5 parts of butanediol.
The present invention also provides a kind of preparation methods using above-mentioned hair dry-washing composition, comprising the following steps:
(1) various raw materials are weighed according to hair dry-washing composite formula；
(2) starch granules of weighing, deflocculant, silica are added in the container for placing dehydrated alcohol, Bian Tianjia, side
It is stirred with 50-100 revs/min, obtains mixture one；
(3) said mixture after mixing evenly, by the Radix Gentianae extract of weighing, hydroxy phenylpropionyl amine benzoic acid, 1.2- penta
Glycol, butanediol, cetrimonium chloride are added in said mixture one, and the stirring of the side Bian Tianjia, obtains by 50-100 revs/min of mixing speed
To mixture two；
(4) essence is added in said mixture two, continues to stir with 50-100 revs/min, obtains hair dry-washing composition.
The above-mentioned preparation method overall process room temperature of the present invention is stirred at 10-20 DEG C, pays attention to dust-proof, alcohol protection.
In conclusion the embodiment of the present invention has the advantages that
Compsition for dry washing of the invention can remove grease excessive on hair and scalp, while saving water resource, can subtract
Shampoo is frequent less, and then reduces and damage to hair or even scalp, while being in " being confined in childbirth ", travel and emergency people
Qun Deng specific group is convenient for the quick nursing of short time.
Hair dry-washing composition of the invention does not add hydrous matter actively, the addition of hydrous matter is reduced to the greatest extent, water
It is preferably minimized, water content in control composition, it is therefore an objective to prevent starch water-swellable, be gelatinized, condensation is unfavorable for compsition for dry washing
Smoothly spray, influence using.
Compsition for dry washing of the invention, to the different oil absorption capacities of hair, scalp, uses suction according to different modified starches
Oil mass is maximum, and the preferable starch of skin sense, and ability of deoiling is good, and cleaning effect is good.
Further, in order to solve the problems, such as that aerosol valve is blocked, one aspect of the present invention finds the very small shallow lake of partial size
Powder is blocked to solve valve, and another party's compsition for dry washing of the invention, which provides, adds distinctive deflocculant, and solves valve
The key factor blocked, so that compsition for dry washing has good homogeneity and stability good, even if placing for a long time,
It is not easy generating flocculation, can continues to spray to use, existing dry washing shampoo can be substantially improved because being long placed in the bad shadow that can not sprayed
It rings.Preferably, aluminum magnesium silicate is inorganic polymer flocculant, while having charge neutrality effect and adsorption bridging effect, is had good
Good treatment effect, only there is pertinent literature report in sewage treatment at present, and not yet discovery is used for hair dry-washing composition, this hair
It is bright to apply aluminum magnesium silicate in compsition for dry washing, good deflocculation effect is obtained, the new opplication of aluminum magnesium silicate and new is belonged to
It attempts, is mainly charge adsorption effect in this mechanism of action.The present invention not only improves use feeling by addition deflocculant,
Valve, which is also improved, from side is easy the problem of being plugged.
Using hair dry-washing composition of the invention, performance is mildly non-stimulated, act on hair, on scalp after, Bu Huiyin
Rise it is dry itch, and will not remain on hair, not have the feeling that similar dandruff thing generates, use feeling is good.Traditional conditioning
Agent thinks to be exactly cationic surfactant, and special conditioner is added in hair dry-washing composition of the present invention, i.e. the bent chlorine in west
Ammonium, alcohol and silica interaction, after starch absorbs the excess oil on hair, extra starch has been taken away in the volatilization of alcohol
With grease, hair can generate electrostatic and jerky sense later, and cetrimonium chloride improves electrostatic, and silica improves jerky, keep its suitable
It is sliding.Hair conditioning is good after dry-cleaning, does not generate electrostatic, and wherein for cetrimonium chloride as cation opsonizing agent, additive amount is critically important, no
It can add excessively, addition is more, is easy starch adsorption on hair, causes the illusion of " dandruff ", be difficult to clean up, suitably
Amount will not just remain and cause dandruff illusion on hair.
Detailed description of the invention
It to describe the technical solutions in the embodiments of the present invention more clearly, below will be to needed in the embodiment
Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for this field
For those of ordinary skill, without creative efforts, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is the micro-structure diagram of three sections of starch granules；
Fig. 2 is different starch oil absorption test charts；
Fig. 3 different starch flocculation tests after being 1h；
Different starch flocculation tests are toppled over for 90 degree after Fig. 4 is 1h；
Fig. 5 be for 24 hours after 90 degree topple over the flocculation of different starch and test.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
A kind of hair dry-washing composition, the component including following mass parts: propane and totally 60 parts of butane, dehydrated alcohol 30
Part, 6 parts of tapioca, 0.1 part of magnesium stearate, 1 part of aluminum magnesium silicate；Wherein, the particle size of tapioca is 3 microns.
The above-mentioned hair dry-washing composition of the present embodiment, is prepared by the following method:
(1) various raw materials in formula are weighed, are held with vessel that are clean and disinfecting；Pay attention to all utensils held not
It must get wet；Precise dehydrated alcohol pays attention to the protection for carrying out alcohol；
(2) pay attention to logical in precise tapioca, magnesium stearate, the aluminum magnesium silicate extremely beaker containing dehydrated alcohol again
Wind carries out dust-proof protection, Bian Tianjia, while being stirred with 100 revs/min.
Embodiment 2
A kind of hair dry-washing composition, the component including following mass parts: propane and totally 65 parts of butane, dehydrated alcohol 18
Part, 1 part of cornstarch, 1 part of tapioca, 0.7 part of magnesium stearate, 0.1 part of aluminum magnesium silicate, 0.01 part of cetrimonium chloride；Wherein, beautiful
The particle size of rice starch is 16 microns, and the particle size of tapioca is 8 microns.
The above-mentioned hair dry-washing composition of the present embodiment, is prepared by the following method:
(1) various raw materials in formula are weighed, are held with vessel that are clean and disinfecting；Pay attention to all utensils held not
It must get wet；Precise dehydrated alcohol pays attention to the protection for carrying out alcohol；
(2) again precise cornstarch, tapioca, magnesium stearate, aluminum magnesium silicate to the beaker containing dehydrated alcohol
In, pay attention to ventilation, carry out dust-proof protection, Bian Tianjia, while stirring with 50 revs/min, it is abundant to add cetrimonium chloride stirring；
(3) overall process room temperature or 12 DEG C stir, pays attention to it is dust-proof, alcohol protect.
Embodiment 3
A kind of hair dry-washing composition, the component including following mass parts: propane and totally 70 parts of butane, dehydrated alcohol 15
Part, 15 parts of rice starch, 1 part of magnesium stearate, 0.5 part of aluminum magnesium silicate, 0.09 part of cetrimonium chloride, 0.001 part of silica；Rice starch
Particle size be 12 microns, the particle size of silica is 6 microns.
The above-mentioned hair dry-washing composition of the present embodiment, is prepared by the following method:
(1) various raw materials in formula are weighed, are held with vessel that are clean and disinfecting；Pay attention to all utensils held not
It must get wet；Precise dehydrated alcohol pays attention to the protection for carrying out alcohol；
(2) again in precise rice starch, magnesium stearate, aluminum magnesium silicate, the silica extremely beaker containing dehydrated alcohol, note
Dust-proof protection, Bian Tianjia are carried out in meaning ventilation, while being stirred with 70 revs/min；
(3) after mixing evenly, precise cetrimonium chloride, 1.2- pentanediol, butanediol are added to above-mentioned said mixture
In composition, the stirring of the side Bian Tianjia, 60 revs/min of mixing speed；
(4) overall process room temperature or 17 DEG C stir, pays attention to it is dust-proof, alcohol protect.
Embodiment 4
A kind of hair dry-washing composition, the component including following mass parts: propane and totally 80 parts of butane, dehydrated alcohol 25
Part, 1 part of rice starch, 5 parts of cornstarch, 0.2 part of magnesium stearate, 0.007 part of silica, 0.08 part of Radix Gentianae extract, hydroxyphenyl
0.01 part of propionamide benzoic acid, 1,2- 0.0001 part of pentanediol, 0.006 part of butanediol；Wherein, the particle size of rice starch is
15 microns, the particle size of cornstarch is 20 microns, and the particle size of silica is 7 microns.
The above-mentioned hair dry-washing composition of the present embodiment, is prepared by the following method:
(1) various raw materials in formula are weighed, are held with vessel that are clean and disinfecting；Pay attention to all utensils held not
It must get wet；Precise dehydrated alcohol pays attention to the protection for carrying out alcohol；
(2) again in precise cornstarch, rice starch, magnesium stearate, the silica extremely beaker containing dehydrated alcohol, note
Dust-proof protection, Bian Tianjia are carried out in meaning ventilation, while being stirred with 90 revs/min；
(3) said mixture after mixing evenly, precise Radix Gentianae extract, hydroxy phenylpropionyl amine benzoic acid, 1.2- penta
Glycol, butanediol, are added in above-mentioned composition, the stirring of the side Bian Tianjia, and 50 revs/min of mixing speed；
(4) overall process room temperature or 20 DEG C stir, pays attention to it is dust-proof, alcohol protect.
Embodiment 5
A kind of hair dry-washing composition, the component including following mass parts: propane and totally 65 parts of butane, dehydrated alcohol 18
Part, 10 parts of rice starch, 1 part of cornstarch, 2 parts of aluminum magnesium silicate, 0.2 part of cetrimonium chloride, 0.02 part of silica, Radix Gentianae extract
0.01 part, 0.05 part of hydroxy phenylpropionyl amine benzoic acid, 1,2- 0.008 part of pentanediol and 0.0001 part of butanediol；Wherein, rice forms sediment
The particle size of powder is 20 microns, and the particle size of cornstarch is 10 microns, and the particle size of silica is 8 microns.
The above-mentioned hair dry-washing composition of the present embodiment, is prepared by the following method:
(1) various raw materials in formula are weighed, are held with vessel that are clean and disinfecting；Pay attention to all utensils held not
It must get wet；Precise dehydrated alcohol pays attention to the protection for carrying out alcohol；
(2) again in precise cornstarch, rice starch, aluminum magnesium silicate, the silica extremely beaker containing dehydrated alcohol, note
Dust-proof protection, Bian Tianjia are carried out in meaning ventilation, while being stirred with 60 revs/min；
(3) said mixture after mixing evenly, precise cetrimonium chloride, Radix Gentianae extract, hydroxy phenylpropionyl amine benzene first
Acid, 1.2- pentanediol, butanediol, are added in above-mentioned composition, the stirring of the side Bian Tianjia, and 100 revs/min of mixing speed；
(4) overall process room temperature or 15 DEG C stir, pays attention to it is dust-proof, alcohol protect.
Embodiment 6
A kind of hair dry-washing composition, the component including following mass parts: propane and totally 64 parts of butane, dehydrated alcohol 26
Part, 8 parts of rice starch, 4 parts of cornstarch, 1 part of starch ocentyl succinic aluminium, 0.12 part of cetrimonium chloride, Radix Gentianae extract 0.1
Part, 0.04 part of hydroxy phenylpropionyl amine benzoic acid, 1,2- 0.0005 part of pentanediol and 0.5 part of butanediol, 0.3 part of essence；Wherein, rice
The particle size of rice starch is 10 microns, and the particle size of cornstarch is 15 microns.
The above-mentioned hair dry-washing composition of the present embodiment, is prepared by the following method:
(1) various raw materials in formula are weighed, are held with vessel that are clean and disinfecting；Pay attention to all utensils held not
It must get wet；Precise dehydrated alcohol pays attention to the protection for carrying out alcohol；
(2) again precise cornstarch, rice starch, starch ocentyl succinic aluminium to the beaker containing dehydrated alcohol
In, pay attention to ventilation, carry out dust-proof protection, Bian Tianjia, while being stirred with 70 revs/min；
(3) said mixture after mixing evenly, precise cetrimonium chloride, hydroxy phenylpropionyl amine benzoic acid, 1.2- penta 2
Alcohol, butanediol, are added in above-mentioned composition, the stirring of the side Bian Tianjia, and 90 revs/min of mixing speed；
(4) essence is finally added, continues to stir with 50 revs/min；
The present embodiment preparation method overall process is stirred in room temperature or at 10 DEG C, pays attention to dust-proof, alcohol protection.
In hair dry-washing composition, the natural origin starch for being usually used in oil-control is mostly cornstarch, tapioca and rice
Rice starch, since the valve of aerosol and aperture have higher requirement for the granular size of starch, particle is larger to be easy to block up
Obturator valve causes product unqualified.Secondly, being also dependent upon the excellent of dry washing shampoo product efficacy for the oil absorption of different starch
It is bad.Primarily look at 3 sections of starch oil absorption and production formulation procedures in, the flocculation resistance of integral formula, this result of study
The product formula exploitation tool of correct hair shaft cleaning composition has very important significance.Cornstarch, the rice used in the present invention forms sediment
The granular size of powder and tapioca is followed successively by 10-20 microns, and 10-20 microns, 3-8 microns, shape under the microscope is with this
For circle/polygon, circle, circle, referring to Fig. 1.Flocculation is also a factor for causing valve to be blocked, and the present invention passes through addition
Deflocculant not only improves use feeling, also improves valve from side and is easy the problem of being plugged.
Experimental section is as follows:
The test of 1.1 oil absorptions
The beaker peeling weighing of centrifuge tube will be placed with.4 grams of rice starch, cornstarch, para arrowroot are accurately weighed respectively
Powder sample is added in centrifuge tube, records centrifuge tube and starch sample gross weight.The white oil for accurately weighing 20g respectively again is added containing shallow lake
In the centrifuge tube of powder, covers plug and place in centrifuge, 15000rpm centrifugal oil slurry material 15 minutes.Liquid is fallen off to going
In the beaker of skin, and record weight (weight for pouring out oil) when going out in 30 seconds without oil droplet.Oil absorption test value=(practical to add
The weight-for entering oil pours out the weight of oil)/amyloid actual weight.
1.2 flocculation tests
The rice starch, cornstarch, tapioca ethanol solution of 20 mass fractions is respectively configured, 100rpm shakes
Shake 5 minutes, after mixing well, by observation static 1 hour, 1 hour 90 degree topple over and it is static for 24 hours later again 90 degree topple over,
Solution mixes situation under three state, judges the flocculation situation of 3 kinds of starch ethanol solution.
1.3, which suspend, tests
Prepare 3 kinds of solution to be measured:
Solution one is 76 parts of denatured ethyl alcohol, 20 parts of rice starch, 4 parts of magnesium stearate including weight percentage；
Solution two is 76 parts of denatured ethyl alcohol, 20 parts of rice starch, 4 parts of aluminum magnesium silicate including weight percentage；
Solution three is 76 parts of denatured ethyl alcohol, 20 parts of rice starch, 4 parts of bentonite including weight percentage；
After 3 kinds of solution to be measured are prepared, it is static for 24 hours, 3 kinds of solution to be measured are fixed in same plane, by simply rocking
Number observes solution in bottle and forms uniform solution system after rocking how many times, records experimental result.
2 results and discussion
2.1 oil absorption test results
The oil absorption effect of rice starch is most to be shown to rice starch, cornstarch, tapioca oil absorption test result
Good, oil absorption test value is 116.5 parts, oil suction weight be close to 1.2 times, i.e. 4.66g of its rice starch own wt, it is beautiful
The oil suction test value of rice starch and tapioca is 75 parts, and oil suction weight is 3g, referring to fig. 2.
2.2 flocculation test results
From the flocculation test result of 3 kinds of starch can be seen that by rock uniformly after, static 1h, the ethyl alcohol of 3 kinds of starch
Solution is layered, but 20 rice starch show slightly more fluffy, i.e., except bottom, top section is more muddy for flocculation
It is turbid, and cornstarch and tapioca interface are more visible, side reflect rice starch in alcohol system compared to other two
The swelling rate of kind starch is than very fast, reference can be made to Fig. 3.
After 3 samples are still in 1h, 90 degree are toppled over, as shown in figure 4, mobility of the cornstarch with ethanol solution
Be it is best among three, that is, do not need in the case where additionally adding deflocculant, itself deflocculation effect is best, secondly for wood
Sweet potato starch, it is worst for rice starch, there is flocculation situation in body bottom, it, cannot be fine within the short time as body is toppled over
It is miscible.
90 degree of three modified starch samples after being still in for 24 hours were fallen, as shown in figure 5, observation sample is in immediately
Reveal the state come, as a result topples over different from 90 degree after static 1h.The results show that it is static for 24 hours after again 90 degree topple over, corn form sediment
Powder is still best with the mobility of ethyl alcohol, but the flowing of rice starch improves maximum, i.e., itself deflocculation effect changes
Kind maximum, tapioca mobility is among 3, and not as good as rice starch and cornstarch, therefore its own deflocculation effect is
Cornstarch > rice starch > tapioca.But from the point of view of time comparison, it is static for 24 hours after, the overall flow of three kinds of starch
It increases, i.e. deflocculation effect makes moderate progress, and the starch weight of deposited bottom is reduced, and deflocculation situation is past to improve
Direction is developed.
2.3 suspension test results
It is the key factor for solving valve and blocking in addition to finding the very small starch of partial size, suitable deflocculation need to be looked for
Agent is also that the key factor for solving valve and blocking not only improves use feeling, also change from side by adding deflocculant
It has been apt to valve and has been easy the problem of being plugged.By magnesium stearate test formulations, aluminum magnesium silicate test formulations and starch octenyl amber
Amber acid aluminum test formula is fixed on shaking table, is rocked with the speed of 50rpm, is observed in real time, by rocking number, observation material
Body can achieve homogeneous system solution in which time situation, the results showed that the survey containing magnesium stearate and aluminum magnesium silicate
Trial side after rocking 2 times, is just easier to be formed uniform system under the shaking speed of identical frequency, and starch octene
Base butanedioic acid aluminium is compared, it is more difficult to and uniform system is formed, when rocking to the 8th time, just forms preferable uniform system, from
And react, in disposable shampoo by spraying, the deflocculation effect of deflocculant is successively are as follows: magnesium stearate=aluminum magnesium silicate > starch octene
Base butanedioic acid aluminium.
It can be seen that the hair dry-washing composition removing hair and scalp grease effect of the above embodiment of the present invention are good, section
About water resource reduces the use of shampoo, reduces the damage to hair, scalp, convenient for quickly nursing；It is distinctive anti-by adding
Flocculant, have good homogeneity and stability it is good, can save for a long time with it is practical；The mild nothing of hair dry-washing composition properties
Stimulation, will not cause hair, scalp are dry to itch, noresidue does not generate the feeling of dandruff, does not generate electrostatic, and use feeling is good；Hair
Compsition for dry washing is preferably minimized water, water content in control composition.
The foregoing is merely a prefered embodiment of the invention, is not intended to limit the invention, all in the spirit and principles in the present invention
Within, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of hair dry-washing composition, which is characterized in that the component including following mass parts: propane and butane are 60-80 parts total,
15-30 parts of dehydrated alcohol, 2-15 parts of starch granules, 0.2-2 parts of deflocculant.
2. hair dry-washing composition according to claim 1, which is characterized in that the particle size of the starch granules is 3-
20 microns.
3. hair dry-washing composition according to claim 1, which is characterized in that the deflocculant is magnesium stearate, silicon
One of sour magnalium, starch ocentyl succinic aluminium are a variety of.
4. hair dry-washing composition according to claim 1, which is characterized in that the starch granules is rice starch, jade
One of rice starch, tapioca are a variety of.
5. hair dry-washing composition according to claim 1, which is characterized in that further include the west song of 0.01-0.2 mass parts
Oronain.
6. hair dry-washing composition according to claim 1, which is characterized in that further include the silicon of 0.001-0.02 mass parts
Stone；The particle size of the silica is 6-8 microns.
7. hair dry-washing composition according to claim 1, which is characterized in that further include the rough gentian of 0.01-0.1 mass parts
Extract.
8. hair dry-washing composition according to claim 1-7, which is characterized in that further include 0.01-0.05 matter
Measure the hydroxy phenylpropionyl amine benzoic acid of part, 1, the 2- pentanediol of 0.0001-0.05 mass parts, 0.0001-0.5 mass parts fourth two
Alcohol.
9. hair dry-washing composition according to claim 1, which is characterized in that the component including following mass parts: propane
It is 60-80 parts total with butane, 15-30 parts of dehydrated alcohol, 2-15 parts of starch granules, 0.2-2 parts of deflocculant, cetrimonium chloride 0.01-
0.2 part, 0.001-0.02 parts of silica, 0.01-0.1 parts of Radix Gentianae extract, 0.01-0.05 parts of hydroxy phenylpropionyl amine benzoic acid, 1,
0.0001-0.05 parts of 2- pentanediol, 0.0001-0.5 parts of butanediol.
10. a kind of preparation method of hair dry-washing composition as claimed in claim 9, which comprises the following steps:
(1) various raw materials are weighed according to hair dry-washing composite formula；
(2) starch granules of weighing, deflocculant, silica are added in the container for placing dehydrated alcohol, Bian Tianjia, while with
50-100 revs/min of stirring, obtains mixture one；
(3) said mixture after mixing evenly, by the Radix Gentianae extract of weighing, hydroxy phenylpropionyl amine benzoic acid, 1.2- pentanediol,
Butanediol, cetrimonium chloride are added in said mixture one, and the stirring of the side Bian Tianjia, is mixed by 50-100 revs/min of mixing speed
Close object two；
(4) essence is added in said mixture two, continues to stir with 50-100 revs/min, obtains hair dry-washing composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910371345.0A CN110063900A (en) | 2019-05-06 | 2019-05-06 | A kind of hair dry-washing composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910371345.0A CN110063900A (en) | 2019-05-06 | 2019-05-06 | A kind of hair dry-washing composition and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110063900A true CN110063900A (en) | 2019-07-30 |
Family
ID=67370212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910371345.0A Pending CN110063900A (en) | 2019-05-06 | 2019-05-06 | A kind of hair dry-washing composition and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110063900A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111329819A (en) * | 2020-03-02 | 2020-06-26 | 惠州市多美日用品有限公司 | Pet dry-cleaning mousse and preparation method thereof |
| CN112156041A (en) * | 2020-10-16 | 2021-01-01 | 花安堂生物科技集团有限公司 | Dry-cleaning spray composition for hair and preparation method thereof |
| CN112842980A (en) * | 2021-01-21 | 2021-05-28 | 邱璟 | Deoiling powder for hair and preparation method thereof |
| CN115192474A (en) * | 2022-07-12 | 2022-10-18 | 诺斯贝尔化妆品股份有限公司 | Composition with multiple effects of body cooling, cleaning and moisturizing and preparation method and application thereof |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102319189A (en) * | 2011-09-05 | 2012-01-18 | 台州绿岛化妆品有限公司 | Dry aerosol shampoo |
| CN104470586A (en) * | 2012-06-27 | 2015-03-25 | 宝洁公司 | Aerosol composition comprising a particulate tapioca starch |
| CN104510629A (en) * | 2014-12-22 | 2015-04-15 | 东莞市泰赛特汽车用品科技有限公司 | Hair dry-cleaning aerosol and preparation method thereof |
| CN106619183A (en) * | 2017-03-14 | 2017-05-10 | 广东龙湖科技股份有限公司 | Washing-free powdery shampoo and preparation method thereof |
| CN107137261A (en) * | 2017-03-24 | 2017-09-08 | 上海伽誉生物科技有限公司 | Preparation method, purposes and the plant extract device of the rough gentian anti-irritant factor |
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
| CN108721141A (en) * | 2018-08-02 | 2018-11-02 | 广州艾蓓生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
| CN109512686A (en) * | 2018-12-26 | 2019-03-26 | 广州蜜妆生物科技有限公司 | A kind of disposable shampoo and preparation method thereof |
-
2019
- 2019-05-06 CN CN201910371345.0A patent/CN110063900A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102319189A (en) * | 2011-09-05 | 2012-01-18 | 台州绿岛化妆品有限公司 | Dry aerosol shampoo |
| CN104470586A (en) * | 2012-06-27 | 2015-03-25 | 宝洁公司 | Aerosol composition comprising a particulate tapioca starch |
| CN104510629A (en) * | 2014-12-22 | 2015-04-15 | 东莞市泰赛特汽车用品科技有限公司 | Hair dry-cleaning aerosol and preparation method thereof |
| CN106619183A (en) * | 2017-03-14 | 2017-05-10 | 广东龙湖科技股份有限公司 | Washing-free powdery shampoo and preparation method thereof |
| CN107137261A (en) * | 2017-03-24 | 2017-09-08 | 上海伽誉生物科技有限公司 | Preparation method, purposes and the plant extract device of the rough gentian anti-irritant factor |
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
| CN108721141A (en) * | 2018-08-02 | 2018-11-02 | 广州艾蓓生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
| CN109512686A (en) * | 2018-12-26 | 2019-03-26 | 广州蜜妆生物科技有限公司 | A kind of disposable shampoo and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 中国食品添加剂和配料协会: "《食品添加剂手册》", 30 September 2012, 中国轻工业出版社 * |
| 黄可龙: "《精细化学品技术手册》", 30 June 1994, 中南工业大学出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111329819A (en) * | 2020-03-02 | 2020-06-26 | 惠州市多美日用品有限公司 | Pet dry-cleaning mousse and preparation method thereof |
| CN112156041A (en) * | 2020-10-16 | 2021-01-01 | 花安堂生物科技集团有限公司 | Dry-cleaning spray composition for hair and preparation method thereof |
| CN112842980A (en) * | 2021-01-21 | 2021-05-28 | 邱璟 | Deoiling powder for hair and preparation method thereof |
| CN115192474A (en) * | 2022-07-12 | 2022-10-18 | 诺斯贝尔化妆品股份有限公司 | Composition with multiple effects of body cooling, cleaning and moisturizing and preparation method and application thereof |
| CN115192474B (en) * | 2022-07-12 | 2023-09-26 | 诺斯贝尔化妆品股份有限公司 | Composition with multiple effects of refreshing, cleaning and moisturizing as well as preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110063900A (en) | A kind of hair dry-washing composition and preparation method thereof | |
| US10583071B2 (en) | Personal cleansing compositions comprising expanded perlite microspheres | |
| CN1925837B (en) | Mild, viscous cleansing composition with versatile compatibility and enhanced conditioning | |
| CN107709534A (en) | In the flavor compositions of encapsulating or associated improvement | |
| RU2446788C2 (en) | Skin cleanser | |
| US20020193256A1 (en) | Suspensions of particles in non-aqueous solvents | |
| WO2001019946A1 (en) | Suspending clear cleansing formulation | |
| CN101690697B (en) | Anti-dandruff shampoo composition | |
| CN109316439A (en) | A kind of suspension maintenance Essence containing Crithmum maritimum stem cell | |
| CN106619183A (en) | Washing-free powdery shampoo and preparation method thereof | |
| CN103261102A (en) | Water clarification composition and process | |
| CN108135799A (en) | Composition of skin cleanser | |
| BR112019018944A2 (en) | consumer product compositions comprising microcapsules | |
| WO2021033742A1 (en) | Particles containing starch, method for producing same, and cosmetic preparation | |
| JP2015529213A (en) | Powerful skin cleanser free from surfactants and solvents | |
| JPS6132050B2 (en) | ||
| CN102319189B (en) | Dry aerosol shampoo | |
| US5380356A (en) | Quartz-free powdered magmatic nepheline rock material for the surface treatment of dental parts, especially grinding, polishing and/or blasting material | |
| BR112019022020B1 (en) | AEROSOL COMPOSITION FOR HAIR AND AEROSOL PRODUCT FOR HAIR | |
| JPH01268604A (en) | Suspended agricultural chemical composition | |
| CN105473128A (en) | Deodorant or refreshing cosmetic material, and non-aerosol type spray product | |
| JP2003081811A (en) | Bathing agent for thickening bath water | |
| JPH07304651A (en) | Liquid detergent for scrubbing | |
| JPWO2018216242A1 (en) | Aerosol composition for hair and aerosol product for hair | |
| JPH06239735A (en) | Enzyme-included gelatin capsule |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190730 |