CN102319189B - Dry aerosol shampoo - Google Patents
Dry aerosol shampoo Download PDFInfo
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- CN102319189B CN102319189B CN 201110259280 CN201110259280A CN102319189B CN 102319189 B CN102319189 B CN 102319189B CN 201110259280 CN201110259280 CN 201110259280 CN 201110259280 A CN201110259280 A CN 201110259280A CN 102319189 B CN102319189 B CN 102319189B
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- dry aerosol
- shampoo
- aerosol shampoo
- corn starch
- butane
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Abstract
The present invention discloses a dry aerosol shampoo. The dry aerosol shampoo comprises the following components, by mass, 14-18% of n-butane, 12-16% of dimethyl ether, 18-22% of isobutene, 10-14% of modified corn starch, 12-16% of propane, 15-19% of dehydrated alcohol, 0.1-0.3% of cyclomethicone, 0.2-0.4% of dioctadecyl dimethyl ammonium chloride and 0.1-0.3% of essence. In the prior art, sodium dodecylsulfate anionic surfactant in the water aqua type aerosol shampoo provides the corrosion effect for the tin plate container and the aluminum container. With the present invention, the problem in the prior art is solved; the use method of the dry aerosol shampoo is easy; the cleaning effect of the dry aerosol shampoo is good.
Description
Technical field
The present invention relates to a kind of dry aerosol shampoo and preparation method thereof.
Background technology
The main effect of shampoo is cleaning hair and scalp, and desirable shampoo must possess following condition:
1, gentle (non-stimulated) cleaning and decontamination;
2, the effective property nursed one's health;
3,, nonirritant nontoxic to skin and eyes;
4, every physical and chemical index and sanitary index meet the requirements of the standard.
When shampoo is solution or white type Emulsion, mainly contains water and Surfactants mixed system and form.It can make on the hair and stick to laying dust, body surface oils and fats and other chip emulsifying on the scalp.Nearly all shampoo all contains anion surfactant, as wishes that the character of product is gentle and select amphoteric surfactant, the pH value of product can make him change negative status into.Non-ionic surface active agent also is used for increasing foam, stable foam and increases cleansing power, has also used increase viscosity simultaneously.
The water aqua type aerial fog shampoo is the sodium lauryl sulphate analog anion surfactants owing to what play main cleaning action in the prescription, and this class surfactant has corrosiveness to tinplate and aluminium vessel, this technical barrier has hindered the development of shampoo aerosol, stores the good result of experiment and can not guarantee that tank body perforation problem can not occur product on market.
The dryness shampoo is not owing to needing to adopt water to make solvent, thus there is not the situation that tank body is produced corrosion failure, and, for specific crowd, in the process of cleaning hair and scalp, can not finish by water.The dryness shampoo that exists on the market owing to adopting plastic bottle packing, by shower nozzle ejection goods, easily causes the generation of spraying the inhomogeneous and product bad phenomenon such as conglomeration in Packaging Bottle.Like this, the shampoo aerosol is known about certainly the approach of difficulty-be mixed with dry aerosol shampoo technically, can satisfy the hair washing demand of some people on market.
Summary of the invention
The purpose of this invention is to provide a kind of dry aerosol shampoo, the present invention adopts inhalator jar to pack, because tank body is full of propellant, by rocking in the situation that have gas to exist well to disperse, simultaneously by injection with pressure, atomize very good, product evenly is sprayed on the hair that needs cleaning.And as the aerosol shampoo, the present invention has solved again sodium lauryl sulphate analog anion surfactants in the water aqua type aerial fog shampoo has corrosiveness to tinplate and aluminium vessel problem.
The technical solution used in the present invention is:
A kind of dry aerosol shampoo is comprised of each component of following mass percent:
Normal butane 14%～18%, dimethyl ether 12～16%, iso-butane 18～22%, modified corn starch 10～14%, propane 12～16%, dehydrated alcohol 15～19%, Cyclomethicone 0.1～0.3%, dioctadecyl dimethyl ammonium chloride 0.2～0.4%, essence 0.1～0.3%.
The DRY-FLO AF modified corn starch that modified corn starch of the present invention provides for AkzoNobel company.
Described modified corn starch is free flowable young fine powder for the natural polymer through degenerative treatments, must feel to have hydrophobicity, water-resistance as user softness, velvet, does not whiten on hair, skin.
Described essence be used for to be regulated the abnormal smells from the patient that improves product, the essence that use can make people feel comfortable all can, the pure white floral perfume of the CF-39941 that provides for Shenzhen BoDun spice Co., Ltd can be provided usually.
Preferably, dry aerosol shampoo of the present invention is comprised of each component of following mass percent:
Normal butane 17%, dimethyl ether 15%, iso-butane 21%, modified corn starch 13%, propane 15%, dehydrated alcohol 18%, Cyclomethicone 0.3%, dioctadecyl dimethyl ammonium chloride 0.4%, essence 0.3%.
The present invention also provides the preparation method of described dry aerosol shampoo:
(1) by formula proportion normal butane, iso-butane, propane, four kinds of gas raw materials of dimethyl ether are mixed in the gas tank, for subsequent use as propellant;
(2) get dehydrated alcohol by prescription, in the process that stirs, add modified corn starch, Cyclomethicone, dioctadecyl dimethyl ammonium chloride, essence, send into filling machine after filtering through 25 micron screen after stirring; Proportional valve is installed in fill amount fill in accordance with regulations additional, after the airtight sealing, is filled with step (1) gained propellant by prescription by inflator, namely makes described dry aerosol shampoo.
The invention provides a kind of dry aerosol shampoo.The present invention adopts inhalator jar to pack, because tank body is full of propellant, in the situation that have gas to exist well to disperse, simultaneously by injection with pressure, atomize very good, product evenly is sprayed on the hair that needs clean by rocking.And as the aerosol shampoo, the present invention has solved again sodium lauryl sulphate analog anion surfactants in the water aqua type aerial fog shampoo has corrosiveness to tinplate and aluminium vessel problem.
Beneficial effect of the present invention is:
(1) using method is simple, during use this product is sprayed on the greasy dried hair, crumples at least with the hair of dry powder 1 minute with hands, then removes all dry powder with dry towel and gets final product.Do not need washing, applicable to the user of cleaning hair or the quick plot hair of specific needs in the situation that does not have water.(2) starch in the prescription can adsorb grease and the pure resin that dissolves of quilt on the hair, can wipe again the resinous polymer (from hair jelly, mousse or gel) that remains on the hair, and cleaning effect is good.Ring first silicone in the prescription bring gloss, beautiful and soft and moist effect can for the hair after the dry-cleaning, and dioctadecyl dimethyl ammonium chloride can effectively be eliminated the static on the hair, and brings submissive effect to hair.
The specific embodiment
Embodiment 1
Total amount 100g, each component prescription consists of:
The pure white floral perfume 0.3% of the CF-39941 that the DRY-FLOAF modified corn starch 13% that normal butane 17%, dimethyl ether 15%, iso-butane 21%, AkzoNobel company provide, propane 15%, dehydrated alcohol 18%, Cyclomethicone 0.3%, dioctadecyl dimethyl ammonium chloride 0.4%, Shenzhen BoDun spice Co., Ltd provide.
Preparation method:
By prescription normal butane, iso-butane, propane, four kinds of gas raw materials of dimethyl ether are mixed in the gas tank, for subsequent use as propellant; Get dehydrated alcohol by prescription, in the process that stirs, add modified corn starch, Cyclomethicone, dioctadecyl dimethyl ammonium chloride, essence, send into filling machine after filtering through 25 micron screen after stirring; Proportional valve is installed in fill amount fill in accordance with regulations additional, after the airtight sealing, is filled with propellant by inflator, namely makes described dry aerosol shampoo.
Products obtained therefrom technical specification: microbiological indicator: total number of bacteria/(CFU/g)≤1000; The yeast and mold sum/(CFU/g)≤100; Excrement colibacillus group must not detect; Staphylococcus aureus must not detect; Bacillus pyocyaneus must not detect; Noxious substance is limited the quantity of: plumbous/(mg/kg)≤40; Hydrargyrum/(mg/kg)≤1; Arsenic/(mg/kg)≤10; Emission rate: % (mass fraction) 〉=96%, internal pressure: in 25 ℃ of waters bath with thermostatic control≤0.8MPa.
The products obtained therefrom assay: total number of bacteria/(CFU/g)＜1000; The yeast and mold sum/(CFU/g)＜100; Excrement colibacillus group does not detect; Staphylococcus aureus does not detect; Bacillus pyocyaneus does not detect; Noxious substance is limited the quantity of: plumbous/(mg/kg)＜40; Hydrargyrum/(mg/kg)＜1; Arsenic/(mg/kg)＜10; Emission rate: % (mass fraction) 98.5%, internal pressure: 0.35MPa in 25 ℃ of waters bath with thermostatic control
Adopt instron tensile strength tester (Diastron Tensile Tester) that products obtained therefrom is carried out performance measurement, be used for measuring the effect of the correct Comb rational faculty of hair washing product.
Concrete assay method is:
1, getting hair lengths is 20cm, and weight is the hair that cleans of 50 grams, is fixed on the instron tensile strength tester, starts the machine and measures, and determination data is transferred to and carries out date processing in the computer, draws corresponding data;
2, the hair of measuring is sprayed 5 gram dry aerosol shampoos, with the hands crumple 50 times, complete shampoo and dirt combing with comb;
3, washed hair is placed on the instron tensile strength tester again, adopts 1 identical method to measure, the transfer of data that obtains is carried out date processing in computer, draw corresponding data.
The resistance opposite with the comb direction of motion that produces during the logical pigtail of continuous record comb.The resistance that to be comb produce in the pigtail length combing effect process of the determination data that obtains reflection.The results are shown in following table 1:
Table 1
| Dry aerosol shampoo | The maintenance level resistance | The maintenance level acting | Maximum resistance | Total work |
| gmf | Joules | gmf | Joules | |
| Before the use | 2.03E+02 | 1.14E-00 | 5.95E+02 | 1.04E-00 |
| After the use | 2.13E+01 | 1.08E-02 | 4.13E+01 | 8.89E-02 |
Embodiment 2
Total amount 100g, each component prescription consists of:
The pure white floral perfume 0.3% of the CF-39941 that the DRY-FLOAF modified corn starch 14% that normal butane 14%, dimethyl ether 16%, iso-butane 22%, AkzoNobel company provide, propane 14%, dehydrated alcohol 19%, Cyclomethicone 0.3%, dioctadecyl dimethyl ammonium chloride 0.4%, Shenzhen BoDun spice Co., Ltd provide.
Preparation method makes the dryness dry aerosol shampoo with embodiment 1.And test acquired results such as following table 2 according to the performance test methods of embodiment 1:
Table 2
| Dry aerosol shampoo | The maintenance level resistance | The maintenance level acting | Maximum resistance | Total work |
| gmf | Joules | gmf | Joules | |
| Before the use | 2.03E+02 | 1.14E-00 | 5.95E+02 | 1.04E-00 |
| After the use | 2.14E+01 | 1.09E-02 | 4.15E+01 | 8.91E-02 |
Embodiment 3
Total amount 100g, each component prescription consists of:
The pure white floral perfume 0.3% of the CF-39941 that the DRY-FLOAF modified corn starch 10% that normal butane 18%, dimethyl ether 15%, iso-butane 21%, AkzoNobel company provide, propane 16%, dehydrated alcohol 19%, Cyclomethicone 0.3%, dioctadecyl dimethyl ammonium chloride 0.4%, Shenzhen BoDun spice Co., Ltd provide.
Preparation method makes the dryness dry aerosol shampoo with embodiment 1.And test acquired results such as following table 3 according to the performance test methods of embodiment 1:
Table 3
| Dry aerosol shampoo | The maintenance level resistance | The maintenance level acting | Maximum resistance | Total work |
| gmf | Joules | gmf | Joules | |
| Before the use | 2.03E+02 | 1.14E-00 | 5.95E+02 | 1.04E-00 |
| After the use | 2.15E+01 | 1.11E-02 | 4.15E+01 | 8.93E-02 |
Embodiment 4
Total amount 100g, each component prescription consists of:
Normal butane 17%, dimethyl ether 12%, iso-butane 22%, modified corn starch 13%, propane 16%, dehydrated alcohol 19%, Cyclomethicone 0.3%, dioctadecyl dimethyl ammonium chloride 0.4%, the pure white floral perfume 0.3% of CF-39941.
Preparation method makes the dryness dry aerosol shampoo with embodiment 1.And test acquired results such as following table 3 according to the performance test methods of embodiment 1:
Table 4
| Dry aerosol shampoo | The maintenance level resistance | The maintenance level acting | Maximum resistance | Total work |
| gmf | Joules | gmf | Joules | |
| Before the use | 2.03E+02 | 1.14E-00 | 5.95E+02 | 1.04E-00 |
| After the use | 2.11E+01 | 1.06E-02 | 4.15E+01 | 8.91E-02 |
Claims (3)
1. dry aerosol shampoo is characterized in that described dry aerosol shampoo is comprised of each component of following mass percent:
Normal butane 14% ~ 18%, dimethyl ether 12 ~ 16%, iso-butane 18 ~ 22%, modified corn starch 10 ~ 14%, propane 12 ~ 16%, dehydrated alcohol 15 ~ 19%, Cyclomethicone 0.1 ~ 0.3%, dioctadecyl dimethyl ammonium chloride 0.2 ~ 0.4%, essence 0.1 ~ 0.3%, the DRY-FLO AF modified corn starch that described modified corn starch provides for AkzoNobel company.
2. dry aerosol shampoo as claimed in claim 1 is characterized in that described dry aerosol shampoo is comprised of each component of following mass percent:
Normal butane 17%, dimethyl ether 15%, iso-butane 21%, modified corn starch 13%, propane 15%, dehydrated alcohol 18%, Cyclomethicone 0.3%, dioctadecyl dimethyl ammonium chloride 0.4%, essence 0.3%.
3. dry aerosol shampoo as claimed in claim 1 is characterized in that described dry aerosol shampoo prepares by the following method:
(1) by formula proportion normal butane, iso-butane, propane, four kinds of gas raw materials of dimethyl ether are mixed in the gas tank, for subsequent use as propellant;
(2) get dehydrated alcohol by prescription, in the process that stirs, add modified corn starch, Cyclomethicone, dioctadecyl dimethyl ammonium chloride, essence, send into filling machine after filtering through 25 micron screen after stirring; Proportional valve is installed in fill amount fill in accordance with regulations additional, after the airtight sealing, is filled with step (1) gained propellant by prescription by inflator, namely makes described dry aerosol shampoo.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110259280 CN102319189B (en) | 2011-09-05 | 2011-09-05 | Dry aerosol shampoo |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110259280 CN102319189B (en) | 2011-09-05 | 2011-09-05 | Dry aerosol shampoo |
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| Publication Number | Publication Date |
|---|---|
| CN102319189A CN102319189A (en) | 2012-01-18 |
| CN102319189B true CN102319189B (en) | 2013-01-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110259280 Active CN102319189B (en) | 2011-09-05 | 2011-09-05 | Dry aerosol shampoo |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104510629B (en) * | 2014-12-22 | 2018-01-05 | 东莞市泰赛特汽车用品科技有限公司 | A kind of hair dry-washing aerosol and preparation method |
| CN108524325A (en) * | 2018-05-29 | 2018-09-14 | 佛山市顺德区香江精细化工实业有限公司 | A kind of Non-water washing hair spray and preparation method thereof |
| CN109512686A (en) * | 2018-12-26 | 2019-03-26 | 广州蜜妆生物科技有限公司 | A kind of disposable shampoo and preparation method thereof |
| CN110063900A (en) * | 2019-05-06 | 2019-07-30 | 上海绿瑞生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1097592A (en) * | 1994-02-09 | 1995-01-25 | 南宁市迪生新技术研究所 | The preparation technology of dry washing shampoo |
| CN101181195A (en) * | 2007-12-06 | 2008-05-21 | 曹月秀 | Multifunctional shampoo |
-
2011
- 2011-09-05 CN CN 201110259280 patent/CN102319189B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1097592A (en) * | 1994-02-09 | 1995-01-25 | 南宁市迪生新技术研究所 | The preparation technology of dry washing shampoo |
| CN101181195A (en) * | 2007-12-06 | 2008-05-21 | 曹月秀 | Multifunctional shampoo |
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| CN102319189A (en) | 2012-01-18 |
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Address after: 317100 No. 5 Industrial Avenue, three industrial park, Taizhou, Zhejiang Applicant after: Zhejiang Ludao Technology Co., Ltd. Address before: 317100 No. 5 Industrial Avenue, three industrial park, Taizhou, Zhejiang Applicant before: Taizhou Green Island Cosmetic Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: TAIZHOU LUDAO COSMETICS CO., LTD. TO: ZHEJIANG LUDAO TECHNOLOGY CO., LTD. |
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