CN115192474A - Composition with multiple effects of body cooling, cleaning and moisturizing and preparation method and application thereof - Google Patents
Composition with multiple effects of body cooling, cleaning and moisturizing and preparation method and application thereof Download PDFInfo
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- CN115192474A CN115192474A CN202210818445.5A CN202210818445A CN115192474A CN 115192474 A CN115192474 A CN 115192474A CN 202210818445 A CN202210818445 A CN 202210818445A CN 115192474 A CN115192474 A CN 115192474A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention provides a composition with multiple effects of body cooling, cleaning and moisturizing, a preparation method and application thereof, wherein the composition with multiple effects of body cooling, cleaning and moisturizing comprises a lubricant, a humectant, an emollient, a thickener, an emulsifier and a solvent, and the lubricant comprises rice starch and corn starch; the weight ratio of the rice starch to the corn starch is (1-2) to 1. The composition with multiple effects of body cooling, cleaning and moisturizing provided by the invention has excellent moisturizing and cleaning effects, and is suitable for multiple outdoor scenes; and brings fresh, soft, moist and smooth feeling to people. Meanwhile, the stability and the production feasibility of the composition with multiple effects of body cooling, cleaning and moisture retention can be ensured.
Description
Technical Field
The invention belongs to the technical field of skin care products, and particularly relates to a composition with multiple effects of body cooling, cleaning and moisturizing, and a preparation method and application thereof.
Background
The body refreshing wet tissue is one kind of cleaning wet tissue, and aims at wiping off body secreted oil, sweat and dirt, making skin smooth, refreshing and maintaining normal physiological state of skin. Possesses clean, cool antiperspirant and function of refreshing oneself as an organic whole, and it is convenient to carry, satisfies the demand of consumer to this type product.
Most of the toilet products on the market are traditional toilet powder, toilet milk, toilet spray, toilet wet tissue and the like.
Traditional talcum powder is mostly powdery, causes the dust very easily during the use to fly, thereby inhale the respiratory track passively, have very big potential safety hazard to healthy. Talcum powder is mostly used as talcum powder, the main components of the talcum powder are magnesium tetrachloride, magnesium silicate and the like, wherein the magnesium silicate is unstable in property and has more side effects, and asbestos is a national banned substance which is possibly contained in the talcum powder and is harmful to human health, so that certain potential safety hazard exists.
The problem of dust flying of the toilet powder is solved by the toilet milk product, however, the toilet products generally suspend the solid toilet powder and add a large amount of suspending agent, so that the use feeling is not good. In addition, the cassava starch is also used for replacing the talcum powder, so that the potential safety hazard of the talcum powder is avoided, but the cassava starch is unstable in property and is likely to be gelatinized, so that the product loses consumer attributes such as smooth feeling and powdery feeling which can be provided by the cassava starch, and the adding process has strict requirements.
Most of the body-refreshing spray products on the market use butane, propane and isobutane as propellants, and have toxicity hidden danger to the skin under the liquid state; when the product is used, the content is required to be atomized and sprayed, and certain potential safety hazard of respiratory tract stimulation also exists.
The refreshing wet tissue products in the market are relatively few and contain a few solid refreshing agents, the general solid refreshing agents cannot be well dispersed in essence, and extremely many suspending agents are required to be added for achieving the effects of uniform dispersion and stable suspension, so that the fluidity of the essence cannot meet the requirement of filling.
CN109602616A discloses a non-powdery body refreshing composition, a preparation method thereof and a body refreshing wet tissue containing the composition, and although the prepared product has good fluidity, the two sides of the prepared product are required to be uniformly sprayed on the surface of non-woven fabric during filling, which brings great difficulty on equipment.
Therefore, how to provide a composition having multiple functions of body refreshing, cleaning and moisturizing is a problem to be solved.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a composition with multiple effects of body cooling, cleaning and moisturizing, a preparation method and application thereof. The composition with multiple effects of body cooling, cleaning and moisturizing provided by the invention brings refreshing, soft, moist and smooth feeling to people.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the present invention provides a multi-effect body, cleaning and moisturizing composition comprising a slip agent, a humectant, an emollient, a thickener, an emulsifier, and a solvent, the slip agent comprising rice starch and corn starch; the weight ratio of the rice starch to the corn starch is (1-2): 1 (wherein, the '1-2' can be 1, 1.2, 1.4, 1.6, 1.8, 2, etc.).
In the invention, the grain diameter of the rice starch and the corn starch is 5-30 microns, and the granular solid small particles can be stably suspended in the dispersion liquid with good flowing property, and can not be settled and agglomerated after being observed by a heat resistance test for 48 hours.
In the present invention, rice starch and corn starch can adsorb sweat and oil secreted from the skin, maintain a dry feeling of the body, and provide a "powdery" feeling of touch by their own granular structure.
In the present invention, in the case of the present invention, the composition with multiple effects of body cooling, cleaning and moisturizing comprises 2-5 parts (for example, 2 parts, 3 parts, 4 parts, 5 parts and the like), 3-10 parts (for example, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts and the like) of a slipping agent, 2-8 parts (for example, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts and the like) of an emollient, 0.1-0.5 part (for example, 0.1 part, and the like) of a thickening agent 0.12 part, 0.14 part, 0.16 part, 0.18 part, 0.2 part, 0.22 part, 0.25 part, 0.27 part, 0.3 part, 0.32 part, 0.34 part, 0.36 part, 0.38 part, 0.4 part, 0.42 part, 0.44 part, 0.46 part, 0.48 part, 0.5 part, etc.), an emulsifier 0.1-0.5 part (for example, 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, etc.), and a solvent 70-95 parts (for example, 70 parts, 75 parts, 80 parts, 85 parts, 90 parts, 95 parts, etc.).
In the present application, the slipping agent, humectant and emollient agent in specific contents and components cooperate with each other to synergistically enhance, have excellent moisturizing, cleansing effects, and give a refreshing feeling to people.
In the present invention, the moisturizer includes a polyhydric alcohol moisturizer, an amino acid moisturizer, and a polysaccharide moisturizer.
Preferably, the weight ratio of the polyhydric alcohol-based moisturizer, the amino acid-based moisturizer and the polysaccharide-based moisturizer is (6-8): 1-3): 1 (wherein, "6-8" may be 6, 6.2, 6.5, 6.8, 7, 7.3, 7.5, 7.8, 8, etc., and "1-3" may be 1, 1.2, 1.5, 1.8, 2, 2.3, 2.5, 2.7, 3, etc.).
In the present invention, the polyhydric alcohol humectant includes any one or a combination of at least two of glycerin, butylene glycol, propylene glycol, 1,3-propylene glycol, or dipropylene glycol.
Preferably, the polyol-based humectant comprises a combination of glycerin and 1,3-propylene glycol.
Preferably, the weight ratio of glycerol to 1,3-propanediol is (1.4-1.8): 1 (where "1.4-1.8" can be 1.4, 1.5, 1.6, 1.7, 1.8, etc.).
Preferably, the amino acid based humectant comprises any one or a combination of at least two of glycine, trimethylglycine, dimethylglycine or betaine.
Preferably, the amino acid based moisturizer comprises a combination of betaine and glycine.
Preferably, the weight ratio of betaine to glycine is (1-2): 1 (where "1-2" can be 1, 1.2, 1.4, 1.6, 1.8, 2, etc.).
Preferably, the polysaccharide moisturizer comprises any one or a combination of at least two of trehalose, hyaluronic acid or sodium hyaluronate.
Preferably, the polysaccharide moisturizer comprises a combination of trehalose and sodium hyaluronate.
Preferably, the weight ratio of trehalose to sodium hyaluronate is (8-10): 1 (where "8-10" may be 8, 8.5, 9, 9.5, 10, etc.).
Preferably, the moisturizer comprises a polyhydric alcohol moisturizer, an amino acid moisturizer and a polysaccharide moisturizer in a weight ratio of (6-8): 1-3): 1, the polyhydric alcohol moisturizer comprises a combination of glycerol and 1,3-propylene glycol in a weight ratio of (1.4-1.8): 1, the amino acid moisturizer comprises a combination of betaine and glycine in a weight ratio of (1-2): 1, and the polysaccharide moisturizer comprises a combination of trehalose and sodium hyaluronate in a weight ratio of (8-10): 1.
In the invention, glycerin, 1,3-propylene glycol, betaine, glycine, trehalose and sodium hyaluronate with specific contents are matched with each other to realize synergistic interaction, so that the cleaning and moisturizing effects of the composition can be improved, and refreshing, soft, moist and smooth feelings are brought to people.
In the present invention, the emollient comprises any one or a combination of at least two of caprylic/capric triglyceride, isopropyl palmitate, isononyl isononanoate, polydimethylsiloxane, or hydrogenated polyisobutene.
Preferably, the emollient comprises a combination of polydimethylsiloxane and hydrogenated polyisobutene.
Preferably, the weight ratio of the polydimethylsiloxane to the hydrogenated polyisobutene is (2-2.5): 1, "where 2-2.5" can be 2, 2.1, 2.2, 2.3, 2.4, 2.5, etc.
In the application, polydimethylsiloxane and hydrogenated polyisobutene with specific contents are matched with each other, so that the cleaning and moisturizing effects of the composition can be improved.
In the present invention, the thickener includes any one of or a combination of at least two of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, carbomer, hydroxyethyl cellulose, acrylic copolymer, acrylic acid (ester)/C10-30 alkanol acrylate crosspolymer, or xanthan gum.
Preferably, the emulsifier comprises any one of tween-60, PEG-100 stearate, glyceryl stearate or sorbitan stearate or a combination of at least two thereof.
Preferably, the solvent comprises water.
Preferably, the composition with multiple efficacies of body cooling, cleaning and moisturizing further comprises a pH regulator, and the pH regulator comprises any one of sodium hydroxide, arginine or triethanolamine or a combination of at least two of the sodium hydroxide, the arginine or the triethanolamine.
Preferably, the composition having multiple effects of body cooling, cleansing and moisturizing further comprises an additive.
Preferably, the additive is present in the composition with multiple effects of body cooling, cleaning and moisturizing in an amount of 0.1 to 20 parts by weight (e.g., 0.1, 1, 2, 4, 6, 8, 10, 12, 14, 16, 18, 20, etc.).
Preferably, the additive comprises any one or a combination of at least two of an antioxidant, a preservative, a fragrance, a skin conditioning agent, a chelating agent or a cooling agent.
Preferably, the antioxidant comprises any one or a combination of at least two of squalane, tocopherol acetate, p-hydroxyacetophenone, or bisabolol.
Preferably, the preservative comprises any one or a combination of at least two of methylparaben, phenoxyethanol or ethylparaben.
Preferably, the essence comprises any one of or a combination of at least two of mint essence, jasmine essence, rose essence, vetiver essential oil, lemon essential oil or lavender essential oil.
Preferably, the skin conditioning agent comprises any one of, or a combination of at least two of, ceramide, niacinamide, hydrolyzed yeast protein, ethylhexyl glycerol, carnosine, or a lactobacillus fermentation product.
Preferably, the chelating agent comprises disodium EDTA and/or caprylhydroxamic acid.
Preferably, the cooling agent comprises any one of menthyl lactate, menthyl pyrrolidone carboxylate, menthol, menthyl lactate or menthane carboxamide or a combination of at least two thereof.
In a second aspect, the present invention provides a method for preparing a composition having multiple effects of body cooling, cleansing and moisturizing according to the first aspect, the method comprising the steps of:
(1) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing the emulsifier and the emollient, and stirring to obtain an oil phase;
(2) Mixing the water phase and the oil phase obtained in the step (1), and homogenizing to obtain a second mixture;
(3) And (3) mixing the second mixture obtained in the step (2) with a slipping agent, and homogenizing to obtain the composition with multiple effects of body slipping, cleaning and moisture preservation.
Preferably, in step (1), in the operation of obtaining the first mixture, the rotation speed of the homogenization is 1500-2500r/min (for example, 1500r/min, 1700r/min, 1900r/min, 2100r/min, 2300r/min, 2500r/min, etc.), the temperature of the homogenization is 75-80 ℃ (for example, 75 ℃, 76 ℃, 77 ℃,78 ℃, 79 ℃,80 ℃, etc.), and the time of the homogenization is 5-8min (for example, 5min, 6min, 7min, 8min, etc.).
Preferably, in the step (1), in the operation of obtaining the aqueous phase, the rotation speed of the stirring is 35 to 50r/min (for example, 35r/min, 37r/min, 39r/min, 41r/min, 43r/min, 45r/min, 47r/min, 50r/min, etc.), the temperature of the stirring is 75 to 80 ℃ (for example, 75 ℃, 76 ℃, 77 ℃,78 ℃, 79 ℃,80 ℃, etc.), and the time of the stirring is 5 to 8min (for example, 5min, 6min, 7min, 8min, etc.).
Preferably, in the step (1), the temperature of the stirring in the operation of obtaining the oil phase is 75-80 ℃ (for example, 75 ℃, 76 ℃, 77 ℃,78 ℃, 79 ℃,80 ℃ and the like can be adopted).
Preferably, in step (2), the temperature for homogenization is 75-80 ℃ (for example, 75 ℃, 76 ℃, 77 ℃,78 ℃, 79 ℃,80 ℃ and the like can be achieved), and the time for homogenization is 5-8min (for example, 5min, 6min, 7min, 8min and the like can be achieved).
Preferably, in step (3), the temperature for homogenization is 40-45 deg.C (for example, 40 deg.C, 41 deg.C, 42 deg.C, 43 deg.C, 44 deg.C, 45 deg.C, etc.).
Preferably, in the step (3), before the second mixture and the slipping agent obtained in the step (2) are mixed, the second mixture and the pH regulator are mixed and stirred to obtain a third mixture, and then the third mixture and the slipping agent are mixed.
Preferably, in step (3), the mixing further comprises an additive.
As a preferred technical scheme, the preparation method of the composition with multiple effects of body cooling, cleaning and moisturizing comprises the following steps:
(I) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing emulsifier and emollient, and stirring to obtain oil phase;
wherein, in the operation of obtaining the first mixture, the rotation speed of the homogenization is 1500-2500r/min, the temperature of the homogenization is 75-80 ℃, and the time of the homogenization is 5-8min; in the operation of obtaining the water phase, the rotating speed of stirring is 35-50r/min, the stirring temperature is 75-80 ℃, and the stirring time is 5-8min; in the operation of obtaining the oil phase, the stirring temperature is 75-80 ℃;
(II) mixing the water phase and the oil phase obtained in the step (I), and homogenizing at 75-80 ℃ for 5-8min to obtain a second mixture;
(III) mixing the second mixture obtained in the step (II) with a slipping agent, and homogenizing at 40-45 ℃ to obtain the composition with multiple effects of body cooling, cleaning and moisturizing;
preferably, in the step (III), before mixing the second mixture obtained in the step (II) with the slipping agent, the second mixture and the pH regulator are mixed and stirred to obtain a third mixture, and then the third mixture and the slipping agent are mixed;
preferably, in step (III), the mixing further comprises an additive.
In a third aspect, the present invention provides a use of the composition according to the first aspect for multiple effects of body cooling, cleansing and moisturizing in the preparation of a skin care product.
Specifically, the invention provides application of the composition with multiple effects of body cooling, cleaning and moisturizing according to the first aspect in preparation of wet tissue liquid.
In a fourth aspect, the present invention provides a wet tissue fluid comprising the composition of the first aspect having multiple effects of body cooling, cleansing and moisturizing.
Compared with the prior art, the invention has the following beneficial effects:
the composition with multiple effects of body cooling, cleaning and moisturizing provided by the invention has excellent moisturizing and cleaning effects, and is suitable for multiple outdoor scenes; and brings fresh, soft, moist and smooth feeling to people. Meanwhile, the stability and the production feasibility of the composition with multiple effects of body cooling, cleaning and moisture retention can be ensured.
Detailed Description
The technical solution of the present invention is further described below by way of specific embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
Example 1
The embodiment provides a composition with multiple effects of body cooling, cleaning and moisturizing, which comprises the following components in parts by weight:
the preparation method of the composition with multiple effects of body cooling, cleaning and moisturizing comprises the following steps:
(I) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing the emulsifier and the emollient, and stirring to obtain an oil phase;
wherein, in the operation of obtaining the first mixture, the rotation speed of the homogenization is 1500r/min, the temperature of the homogenization is 80 ℃, and the time of the homogenization is 5min; in the operation of obtaining the water phase, the rotating speed of stirring is 35r/min, the stirring temperature is 80 ℃, and the stirring time is 5min; in the operation of obtaining the oil phase, the stirring temperature is 80 ℃;
(II) mixing the water phase and the oil phase obtained in the step (I), and homogenizing at 80 ℃ for 5min to obtain a second mixture;
(III) mixing the second mixture obtained in the step (II) with a pH regulator, and stirring at 43 ℃ to obtain a third mixture; and then mixing the third mixture, the slipping agent and the additive, and homogenizing at 43 ℃ to obtain the composition with multiple effects of body cooling, cleaning and moisturizing.
Example 2
The embodiment provides a composition with multiple effects of body cooling, cleaning and moisturizing, which comprises the following components in parts by weight:
the preparation method of the composition with multiple effects of body cooling, cleaning and moisturizing comprises the following steps:
(I) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing the emulsifier and the emollient, and stirring to obtain an oil phase;
wherein, in the operation of obtaining the first mixture, the rotation speed of the homogenization is 2500r/min, the temperature of the homogenization is 75 ℃, and the time of the homogenization is 8min; in the operation of obtaining the water phase, the rotating speed of stirring is 50r/min, the stirring temperature is 75 ℃, and the stirring time is 8min; in the operation of obtaining the oil phase, the stirring temperature is 75 ℃;
(II) mixing the water phase and the oil phase obtained in the step (I), and homogenizing at 75 ℃ for 8min to obtain a second mixture;
(III) mixing the second mixture obtained in the step (II) with a pH regulator, and stirring at 40 ℃ to obtain a third mixture; and then mixing the third mixture, the slipping agent and the additive, and homogenizing at 40 ℃ to obtain the composition with multiple effects of body cooling, cleaning and moisturizing.
Example 3
The embodiment provides a composition with multiple effects of body cooling, cleaning and moisturizing, which comprises the following components in parts by weight:
the preparation method of the composition with multiple effects of body cooling, cleaning and moisturizing comprises the following steps:
(I) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing the emulsifier and the emollient, and stirring to obtain an oil phase;
wherein, in the operation of obtaining the first mixture, the rotation speed of the homogenization is 2000r/min, the temperature of the homogenization is 78 ℃, and the time of the homogenization is 7min; in the operation of obtaining the water phase, the rotating speed of stirring is 45r/min, the stirring temperature is 78 ℃, and the stirring time is 7min; in the operation of obtaining the oil phase, the stirring temperature is 77 ℃;
(II) mixing the water phase and the oil phase obtained in the step (I), and homogenizing at 78 ℃ for 7min to obtain a second mixture;
(III) mixing the second mixture obtained in the step (II), a slipping agent and an additive, and homogenizing at 45 ℃ to obtain the composition with multiple effects of body cooling, cleaning and moisturizing.
Example 4
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, differing from example 1 only in that the weight parts of the polyhydric alcohol moisturizers (glycerin and 1,3-propylene glycol) were reduced to 5 parts, and the weight parts of the amino acid moisturizers (betaine and glycine) were increased to 4 parts; the weight ratio of glycerol to 1,3-propanediol is kept constant, the weight ratio of betaine to glycine is kept constant, and other preparation raw materials and preparation methods are the same as those of example 1.
Example 5
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, differing from example 1 only in that the weight parts of the polyhydric alcohol moisturizers (glycerin and 1,3-propanediol) were increased to 8.5 parts, and the weight parts of the amino acid moisturizers (betaine and glycine) were reduced to 0.5 part; the weight ratio of glycerol to 1,3-propanediol is kept constant, the weight ratio of betaine to glycine is kept constant, and other preparation raw materials and preparation methods are the same as those of example 1.
Example 6
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, differing from example 1 only in that the polyhydric alcohol moisturizer is not included, the weight part of the amino acid moisturizers (betaine and glycine) is increased to 6.7 parts, and the weight part of the polysaccharide moisturizers (trehalose and sodium hyaluronate) is increased to 3.3 parts; the weight ratio of betaine to glycine and the weight ratio of trehalose to sodium hyaluronate were kept constant, and the other preparation raw materials and preparation methods were the same as in example 1.
Example 7
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, differing from example 1 only in that, without amino acid moisturizers, the weight parts of polyol moisturizers (glycerin and 1,3-propanediol) were increased to 8.75 parts, and the weight parts of polysaccharide moisturizers (trehalose and sodium hyaluronate) were increased to 1.25 parts; the weight ratio of glycerol to 1,3-propanediol is kept constant, the weight ratio of trehalose to sodium hyaluronate is kept constant, and the other preparation raw materials and preparation methods are the same as those of example 1.
Example 8
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, differing from example 1 only in that, without the polysaccharide moisturizer, the weight parts of the polyol moisturizers (glycerin and 1,3-propanediol) were increased to 7.7 parts, and the weight parts of the amino acid moisturizers (betaine and glycine) were increased to 2.3 parts; the weight ratio of the glycerol to the 1,3-propylene glycol is kept unchanged, the weight ratio of the betaine to the glycine is kept unchanged, and other preparation raw materials and preparation methods are the same as those in example 1.
Example 9
This example provides a composition with multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that 1,3-propanediol is not included, the weight part of glycerin is increased to 7 parts, and other preparation raw materials and preparation methods are the same as example 1.
Example 10
This example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that glycine is not contained, the parts by weight of betaine is increased to 2 parts, and other preparation raw materials and preparation methods are the same as example 1.
Example 11
This example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that sodium hyaluronate is not contained, the weight part of trehalose is increased to 1 part, and other preparation raw materials and preparation methods are the same as example 1.
Example 12
This example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that glycerin is replaced with butylene glycol in an equal weight part, and other preparation raw materials and preparation methods are the same as example 1.
Example 13
This example provides a composition with multiple effects of body refreshing, cleaning and moisturizing, which is different from example 1 only in that betaine is replaced by polyglutamic acid in the same weight part, and other preparation raw materials and preparation methods are the same as example 1.
Example 14
The present example provides a composition with multiple effects of body cooling, cleaning and moisture retention, which is different from example 1 only in that trehalose is replaced by tremella polysaccharide with the same weight parts, and other preparation raw materials and preparation methods are the same as example 1.
Example 15
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, which is different from example 1 only in that polydimethylsiloxane is not included, the weight part of hydrogenated polyisobutene is increased to 6 parts, and other preparation raw materials and preparation methods are the same as example 1.
Example 16
This example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that hydrogenated polyisobutene is not included, the weight part of polydimethylsiloxane is increased to 6 parts, and other preparation raw materials and preparation methods are the same as those of example 1.
Example 17
This example provides a composition with multiple effects of body cooling, cleansing and moisturizing, which differs from example 1 only in that hydrogenated polyisobutene is replaced with an equivalent weight fraction of polyisobutene, and the other preparation raw materials and preparation methods are the same as those of example 1.
Comparative example 1
This comparative example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that rice starch is not contained, the weight part of corn starch is increased to 2.5 parts, and other preparation raw materials and preparation methods are the same as example 1.
Comparative example 2
This comparative example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that corn starch is not included, the weight part of rice starch is increased to 2.5 parts, and other preparation raw materials and preparation methods are the same as example 1.
Comparative example 3
The comparative example provides a composition with multiple effects of body refreshing, cleaning and moisturizing, and is different from the composition in example 1 only in that corn starch is replaced by cassava starch in the same weight part, and other preparation raw materials and preparation methods are the same as those in example 1.
Comparative example 4
This comparative example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that the weight part of rice starch is reduced to 1.1 parts and the weight part of corn starch is increased to 1.4 parts, and other preparation raw materials and preparation methods are the same as example 1.
Comparative example 5
This comparative example provides a composition having multiple effects of body refreshing, cleansing and moisturizing, which is different from example 1 only in that the weight part of rice starch is increased to 1.7 parts and the weight part of corn starch is decreased to 0.8 parts, and other preparation raw materials and preparation methods are the same as example 1.
Test example 1
Sensory evaluation
Testing a sample: examples 1 to 17 and comparative examples 1 to 5 provide compositions having multiple effects of body-building, cleansing and moisturizing.
The test method comprises the following steps: 220 healthy skin people, 20-45 years old, were selected and divided into 22 groups of 5 males and 5 females, and each group was tested with one of the samples of examples 1-17 and comparative examples 1-5, respectively, under an environment of a temperature of 23 + -1 deg.C and a relative humidity of 50 + -5%. The refreshing feeling, the soft feeling, the moistening feeling, the water moistening feeling and the smooth feeling of the skin after use are respectively evaluated, each item is fully divided into 20 points, the higher the score is, the better the experience of the volunteer is shown, the average value of each group is taken as the test result, and the test result is shown in the following table 1:
TABLE 1
As can be seen from the data in Table 1, the moisturizing agent, the emollient and the slipping agent with specific contents and compositions are matched with each other and synergically, and the prepared composition with multiple effects of body cooling, cleaning and moisturizing brings fresh, soft, moisturizing, hydrating and smoothing feelings to people.
Test example 2
Skin moisture content test
Testing a sample: examples 1 to 17 and comparative examples 1 to 5 provide compositions having multiple effects of body-building, cleansing and moisturizing.
Testing an instrument: a skin moisture content Corneometer test probe manufactured by Courage + Khazaka, germany (CK, germany). The capacitance of the stratum corneum of the skin before and after use is measured by the instrument, and the change of the water content of the stratum corneum is measured.
The test method comprises the following steps: 220 healthy skin people aged 20 to 45 years were selected and divided into 22 groups of 5 males and 5 females, and each group was tested with one of the samples of examples 1 to 17 and comparative examples 1 to 5, respectively. Any product (cosmetics or external medicines or internal health care products) cannot be used 15 days before the tested part. Before the test, the subjects were asked to wash their forearms and sit in a constant temperature and humidity room at 22. + -. 1 ℃ and 50. + -. 5% humidity for 30min while maintaining a relaxed state. Then, 3X 3cm was drawn on the left and right forearm sides of the testers 2 The square experiment area of size, with the test area of left arm as the product, the corresponding symmetric region of right arm is blank control, and the moisture content of every experiment position is detected to reuse Corneometer test probe, repeats 5 times respectively, obtains the average value of each test, records data. The calculation formula is as follows:
hydration (%) = (test value-blank value) × 100/blank value.
The test results are shown in table 2 below:
TABLE 2
As can be seen from the data in Table 2, the moisturizer, the emollient and the slipping agent with specific contents and compositions cooperate with each other to realize synergistic interaction, and the prepared composition with multiple effects of body refreshing, cleaning and moisturizing not only provides effective cleaning power, but also achieves the effects of nourishing and moisturizing while cleaning the skin.
As is clear from comparison between examples 1 and 4 to 8, the use of a polyhydric alcohol-based moisturizing agent, an amino acid-based moisturizing agent, and a polysaccharide-based moisturizing agent in a specific mass ratio improves hydration of the skin and promotes skin hydration.
As can be seen from a comparison of examples 1 and 9-14, glycerin, 1,3-propanediol, betaine, glycine, trehalose and sodium hyaluronate cooperate with each other to synergistically maintain skin moisture in the present invention.
As can be seen from the comparison between example 1 and examples 15-17, the polydimethylsiloxane and the hydrogenated polyisobutene cooperate with each other to achieve a synergistic effect, so that the skin has a high hydration rate after use.
Test example 3
Evaluation of physical cleaning Properties
Test samples: examples 1 to 17 and comparative examples 1 to 5 provide compositions having multiple effects of body-building, cleansing and moisturizing.
The test method comprises the following steps: coating 1cm 3M air permeable adhesive tape 3 Weighing color cosmetic, and collecting 1cm 3 After the composition with multiple effects of body cooling, cleaning and moisturizing is loaded and rubbed for 2min, the adhesive tape is washed by clean water and then dried, and then weighed, and the remaining amount of the color cosmetic is calculated.
Cleansing foam cleanliness = (tape weight before use-tape weight after use)/(tape weight before use-tape dry weight); the weight of a 1cm by 3cm size 3M permeable adhesive tape weighed 0.8g.
The test results are shown in table 3:
TABLE 3
As can be seen from the data in Table 3, the humectant, the emollient and the slipping agent with specific contents and compositions cooperate with each other to realize synergistic interaction, and the prepared composition with multiple effects of body cooling, cleaning and moisturizing has excellent cleaning effect.
As is clear from comparison between examples 1 and 4 to 8, the cleansing ability can be improved by using the polyhydric alcohol-based moisturizing agent, the amino acid-based moisturizing agent, and the polysaccharide-based moisturizing agent in a specific mass ratio in combination.
A comparison of examples 1 and 9-14 shows that glycerol, 1,3-propanediol, betaine, glycine, trehalose, and sodium hyaluronate cooperate with each other to provide a synergistic cleaning effect.
As can be seen from comparison of example 1 and examples 15-17, the polydimethylsiloxane and the hydrogenated polyisobutene cooperate with each other to achieve a synergistic effect, and have high cleaning power.
As can be seen from the comparison of example 1 with comparative examples 1 to 5, the rice starch and corn starch of the present invention in a specific mass ratio cooperate with each other to synergistically enhance the cleaning ability.
Test example 4
Mild testing
Test samples: examples 1 to 17 and comparative examples 1 to 5 provide compositions having multiple effects of body-building, cleansing and moisturizing.
The test method comprises the following steps: 220 volunteers between 22 and 25 years old were selected, and the subjects were divided into 22 groups of 10 subjects each using the same test sample. The subjects cleaned both sides of the nose, wiped dry, dropped a drop of water on both sides of the nose, applied a certain amount of the composition having multi-effects of body-building, cleansing and moisturizing provided in examples 1 to 17 and comparative examples 1 to 5, respectively, on both sides of the nose of each group of volunteers, and rubbed and massaged for 2 minutes to clean both sides of the nose.
The test index is the scoring condition of skin pain, burning, allergy or red swelling, a score of 10 is adopted, 0 represents no corresponding feeling, 10 represents obvious feeling, statistical data is averaged, and the larger the number is, the more obvious the feeling is represented.
The test results are shown in table 4:
TABLE 4
As can be seen from the data in Table 4, the composition with multiple effects of body cooling, cleaning and moisturizing provided by the invention has no phenomena of pain, burning, allergy or red swelling during the use process of a tester, and can be used at ease.
The applicant states that the present invention is illustrated by the above examples, but the present invention is not limited to the above examples, i.e. it is not meant to be dependent on the above examples to practice the present invention. It should be understood by those skilled in the art that any modifications of the present invention, equivalent substitutions of the raw materials of the product of the present invention, and the addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (10)
1. A multi-effect composition for body cooling, cleansing and moisturizing, wherein the multi-effect composition for body cooling, cleansing and moisturizing comprises a lubricant, a humectant, an emollient, a thickener, an emulsifier and a solvent, and the lubricant comprises rice starch and corn starch; the weight ratio of the rice starch to the corn starch is (1-2) to 1.
2. The composition with multiple effects of body cooling, cleaning and moisturizing as claimed in claim 1, wherein the composition with multiple effects of body cooling, cleaning and moisturizing comprises, by weight, 2-5 parts of a slipping agent, 3-10 parts of a humectant, 2-8 parts of an emollient, 0.1-0.5 part of a thickener, 0.1-0.5 part of an emulsifier and 70-95 parts of a solvent.
3. The composition with multiple effects of body cooling, cleaning and moisturizing as claimed in claim 1 or 2, wherein the moisturizers comprise polyhydric alcohol moisturizers, amino acid moisturizers and polysaccharide moisturizers;
preferably, the weight ratio of the polyhydric alcohol humectant to the amino acid humectant to the polysaccharide humectant is (6-8): 1-3): 1.
4. The multiple refreshing, cleansing and moisturizing composition according to any one of claims 1 to 3, wherein the polyhydric alcohol moisturizer comprises any one or a combination of at least two of glycerin, butylene glycol, propylene glycol, 1,3-propylene glycol, or dipropylene glycol;
preferably, the polyol humectant comprises a combination of glycerin and 1,3-propanediol;
preferably, the weight ratio of glycerol to 1,3-propanediol is (1.4-1.8): 1;
preferably, the amino acid-based moisturizer comprises any one or a combination of at least two of glycine, trimethylglycine, dimethylglycine, or betaine;
preferably, the amino acid based moisturizer comprises a combination of betaine and glycine;
preferably, the weight ratio of betaine to glycine is (1-2): 1;
preferably, the polysaccharide humectant comprises any one of trehalose, hyaluronic acid or sodium hyaluronate or a combination of at least two thereof;
preferably, the polysaccharide moisturizer comprises a combination of trehalose and sodium hyaluronate;
preferably, the weight ratio of the trehalose to the sodium hyaluronate is (8-10) 1;
preferably, the moisturizer comprises a polyhydric alcohol moisturizer, an amino acid moisturizer and a polysaccharide moisturizer in a weight ratio of (6-8): 1-3): 1, the polyhydric alcohol moisturizer comprises a combination of glycerol and 1,3-propylene glycol in a weight ratio of (1.4-1.8): 1, the amino acid moisturizer comprises a combination of betaine and glycine in a weight ratio of (1-2): 1, and the polysaccharide moisturizer comprises a combination of trehalose and sodium hyaluronate in a weight ratio of (8-10): 1.
5. The multiple refreshing, cleansing and moisturizing composition according to any one of claims 1-4, wherein said emollient comprises any one or a combination of at least two of caprylic/capric triglyceride, isopropyl palmitate, isononyl isononanoate, dimethicone or hydrogenated polyisobutene;
preferably, the emollient comprises a combination of polydimethylsiloxane and hydrogenated polyisobutylene;
preferably, the weight ratio of the polydimethylsiloxane to the hydrogenated polyisobutene is (2-2.5): 1.
6. The multiple refreshing, cleaning and moisturizing composition according to any one of claims 1-5, wherein the thickening agent comprises any one or a combination of at least two of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, carbomer, hydroxyethyl cellulose, acrylic copolymer, acrylic/C10-30 alkanol acrylate crosspolymer or xanthan gum;
preferably, the emulsifier comprises any one or a combination of at least two of tween-60, PEG-100 stearate, glyceryl stearate or sorbitan stearate;
preferably, the solvent comprises water;
preferably, the composition with multiple efficacies of body cooling, cleaning and moisturizing further comprises a pH regulator, wherein the pH regulator comprises any one or a combination of at least two of sodium hydroxide, arginine or triethanolamine;
preferably, the composition with multiple effects of body cooling, cleaning and moisturizing further comprises additives;
preferably, the weight part of the additive in the composition with multiple efficacies of body cooling, cleaning and moisturizing is 0.1-20 parts;
preferably, the additive comprises any one or a combination of at least two of an antioxidant, a preservative, a fragrance, a skin conditioning agent, a chelating agent, or a cooling agent;
preferably, the antioxidant comprises any one or a combination of at least two of squalane, tocopherol acetate, p-hydroxyacetophenone or bisabolol;
preferably, the preservative comprises any one or a combination of at least two of methylparaben, phenoxyethanol or ethylparaben;
preferably, the essence comprises any one or a combination of at least two of mint essence, jasmine essence, rose essence, vetiver essential oil, lemon essential oil or lavender essential oil;
preferably, the skin conditioning agent comprises any one of, or a combination of at least two of, ceramide, niacinamide, hydrolyzed yeast protein, ethylhexyl glycerol, carnosine, or lactobacillus fermentation product;
preferably, the chelating agent comprises disodium EDTA and/or caprylhydroxamic acid;
preferably, the cooling agent comprises any one of menthyl lactate, menthyl pyrrolidone carboxylate, menthol, menthyl lactate or menthane carboxamide or a combination of at least two thereof.
7. A method for preparing the composition with multiple effects of body cooling, cleaning and moisturizing as claimed in any one of claims 1 to 6, characterized in that it comprises the following steps:
(1) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing the emulsifier and the emollient, and stirring to obtain an oil phase;
(2) Mixing the water phase and the oil phase obtained in the step (1), and homogenizing to obtain a second mixture;
(3) Mixing the second mixture obtained in the step (2) with a slipping agent, and homogenizing to obtain the composition with multiple effects of body slipping, cleaning and moisture retention;
preferably, in the step (1), in the operation of obtaining the first mixture, the rotation speed of the homogenizing is 1500-2500r/min, the temperature of the homogenizing is 75-80 ℃, and the time of the homogenizing is 5-8min;
preferably, in the step (1), in the operation of obtaining the water phase, the rotation speed of stirring is 35-50r/min, the stirring temperature is 75-80 ℃, and the stirring time is 5-8min;
preferably, in the step (1), the temperature of the stirring is 75-80 ℃ in the operation of obtaining the oil phase;
preferably, in the step (2), the homogenization temperature is 75-80 ℃, and the homogenization time is 5-8min;
preferably, in the step (3), the homogenization temperature is 40-45 ℃;
preferably, in the step (3), before the second mixture and the slipping agent obtained in the step (2) are mixed, the second mixture and the pH regulator are mixed and stirred to obtain a third mixture, and then the third mixture and the slipping agent are mixed;
preferably, in step (3), the mixing further comprises an additive.
8. The method for preparing the composition with multiple efficacies of body cooling, cleaning and moisturizing as claimed in claim 7 comprises the following steps:
(I) Mixing a thickening agent and a solvent, and homogenizing to obtain a first mixture; mixing the first mixture and the humectant, and stirring to obtain a water phase; mixing the emulsifier and the emollient, and stirring to obtain an oil phase;
wherein, in the operation of obtaining the first mixture, the rotation speed of the homogenization is 1500-2500r/min, the temperature of the homogenization is 75-80 ℃, and the time of the homogenization is 5-8min; in the operation of obtaining the water phase, the rotating speed of stirring is 35-50r/min, the stirring temperature is 75-80 ℃, and the stirring time is 5-8min; in the operation of obtaining the oil phase, the stirring temperature is 75-80 ℃;
(II) mixing the water phase and the oil phase obtained in the step (I), and homogenizing at 75-80 ℃ for 5-8min to obtain a second mixture;
(III) mixing the second mixture obtained in the step (II) with a slipping agent, and homogenizing at 40-45 ℃ to obtain the composition with multiple effects of body cooling, cleaning and moisturizing;
preferably, in the step (III), before mixing the second mixture obtained in the step (II) with the slipping agent, the second mixture and the pH regulator are mixed and stirred to obtain a third mixture, and then the third mixture and the slipping agent are mixed;
preferably, in step (III), the mixing further comprises an additive.
9. Use of a composition according to any one of claims 1 to 6 for multiple effects of body cooling, cleansing and moisturizing in the preparation of a skin care product.
10. A wet wipe solution comprising the multi-effect composition of claims 1-6 for body cooling, cleansing and moisturizing.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107625689A (en) * | 2017-10-18 | 2018-01-26 | 湖南大三湘油茶生态产业有限公司 | Camellia oleifera fruit disposable clean hair agent, preparation method and application method |
| CN109771328A (en) * | 2019-01-24 | 2019-05-21 | 广州雅纯化妆品制造有限公司 | A kind of mild children's skin toner composition and preparation method thereof |
| CN110063900A (en) * | 2019-05-06 | 2019-07-30 | 上海绿瑞生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
| CN111773118A (en) * | 2020-08-06 | 2020-10-16 | 上海市天乐日化厂 | Novel honey powder cake and preparation method thereof |
| CN111870549A (en) * | 2020-08-06 | 2020-11-03 | 上海市天乐日化厂 | Clean energy eye shadow and preparation method thereof |
| CN112569134A (en) * | 2020-12-29 | 2021-03-30 | 广州星际悦动股份有限公司 | Cleaning composition and preparation method thereof |
| CN114376925A (en) * | 2021-12-27 | 2022-04-22 | 广东碧茜生物科技有限公司 | Plant loose powder and preparation method thereof |
-
2022
- 2022-07-12 CN CN202210818445.5A patent/CN115192474B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107625689A (en) * | 2017-10-18 | 2018-01-26 | 湖南大三湘油茶生态产业有限公司 | Camellia oleifera fruit disposable clean hair agent, preparation method and application method |
| CN109771328A (en) * | 2019-01-24 | 2019-05-21 | 广州雅纯化妆品制造有限公司 | A kind of mild children's skin toner composition and preparation method thereof |
| CN110063900A (en) * | 2019-05-06 | 2019-07-30 | 上海绿瑞生物科技有限公司 | A kind of hair dry-washing composition and preparation method thereof |
| CN111773118A (en) * | 2020-08-06 | 2020-10-16 | 上海市天乐日化厂 | Novel honey powder cake and preparation method thereof |
| CN111870549A (en) * | 2020-08-06 | 2020-11-03 | 上海市天乐日化厂 | Clean energy eye shadow and preparation method thereof |
| CN112569134A (en) * | 2020-12-29 | 2021-03-30 | 广州星际悦动股份有限公司 | Cleaning composition and preparation method thereof |
| CN114376925A (en) * | 2021-12-27 | 2022-04-22 | 广东碧茜生物科技有限公司 | Plant loose powder and preparation method thereof |
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