CN113262178A - Moistened satin gloss lip glaze and preparation method thereof - Google Patents

Abstract

The invention discloses moist satin gloss lip glaze and a preparation method thereof. The lip glaze formulations which are mainstream in the market at present are matte lip glaze and water-luster lip glaze. The matte lip glaze has good spreadability and high color rendering degree but is not moist enough and is easy to pull dry, while the water-luster lip glaze is moist and glossy but is sticky and is easy to leave color and difficult to remove makeup. The lip glaze prepared by the invention makes up for the defects of the two lip glazes on the basis of keeping the advantages of the two lip glazes. The silicone and the cross-linked polymer (silicon elastomer) thereof have the lip-covering effect while thickening, and simultaneously provide a pleasant silky feeling for the product, so that the product has good spreadability. The introduction of a proper amount of water and the humectant ensures that the product has long-acting moisture retention and is not easy to pull dry, and the product presents a certain gloss after being smeared.

Description

Moistened satin gloss lip glaze and preparation method thereof

Technical Field

The invention relates to the field of daily cosmetics, in particular to moist satin gloss lip glaze and a preparation method thereof.

Background

In recent years, the development of color cosmetic products is more and more diversified, and lip glaze belongs to an emerging lip color cosmetic unit, is derived from lipstick and lip gloss, and nowadays, different systems such as water dispersion, oil-in-water, water-in-oil and the like are extended. Compared with lipstick, lip gloss and lip gloss, the lip glaze has the advantages of good spreadability, high color rendering degree and the like, and can show different cosmetic effects such as matte (including extraordinary matte and velvet fog surfaces), water gloss (namely mirror surfaces) and the like which cannot be achieved by other formulations.

The matte lip glaze belongs to an oil dispersion system, only oil-soluble raw materials can be added, and a large amount of volatile grease and powder are even added to achieve the matte effect, so that the matte lip glaze has the advantages of good color development degree and light skin feel, but the moisturizing effect is limited, so that lips are easy to pull dry and peel after the lips are put on the mouth for a period of time; the water gloss lip glaze belongs to an oil-in-water emulsion system, is generally added with a large amount of film forming agent and thickening agent, and has the advantages of high glossiness and water texture, but has heavy stickiness after being put on the mouth, and simultaneously has the problems of serious color retention and difficult makeup removal. Therefore, there is a need to develop a lip glaze which has light skin feel, is not sticky, and has a longer moisturizing effect.

Disclosure of Invention

The inventor of the application researches through long-term experiments, combines a silicon elastomer with water, and invents a lip glaze of a water-in-silicon elastomer preparation. The silicon elastomer is silicone and a cross-linked polymer thereof. Proper water and humectant are introduced to improve the water content of the horny layer of the lips, and meanwhile, the silicon elastomer and the emollient are combined to form a soft film to slow down the loss of water in the lips, so that the effects of light skin feel, no stickiness and longer moisturizing effect are achieved.

The invention provides the following technical scheme for achieving the purpose:

a moist satin gloss lip glaze comprises phase A, phase B and phase C components. The phase A comprises 0-14 parts of a softening agent, 5-7 parts of an emulsifier, 0.5-4 parts of an adhesive, 40-70 parts of silicone and a cross-linked polymer (silicon elastomer) thereof, the phase B comprises 5-11 parts of a coloring agent, and the phase C comprises 9-25 parts of water, 2-8 parts of a humectant and 0.5-0.8 part of a preservative.

Further, the moist satin gloss lip glaze comprises phase A, phase B and phase C components. The phase A comprises 4-10 parts of a softening agent, 5-6 parts of an emulsifier, 1-3 parts of an adhesive, 50-60 parts of silicone and a cross-linked polymer (silicon elastomer) thereof, the phase B comprises 7-10 parts of color paste, and the phase C comprises 13-21 parts of water, 4-6 parts of a humectant and 0.6-0.75 part of a preservative.

Further, the emollient is selected from any one of polydimethylsiloxane, cyclopentadimethylsiloxane, diphenylsiloxyphenyltrimethicone, pentaerythritol (ethyl hexanoate), hydrogenated polyisobutene, caprylic/capric triglyceride, dipentaerythritol tetrahydroxystearate/tetraisostearate, dicaprylyl carbonate, pentaerythritol tetraisostearate, phenyl trimethicone, isododecane or a combination of at least two thereof.

Further, the emulsifier is selected from one or a combination of at least two of cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone, PEG-10 polydimethylsiloxane, sorbitan isostearate, sorbitan olivate, glycerol tri (ethylhexanoate) and the like.

Further, the binder is selected from one or a combination of at least two of diisostearyl malate, dimethylsilylated silica, propylene carbonate, distearyldimethylammonium hectorite, VP/hexadecene copolymer, isononyl isononanoate, tridecyl alcohol trimellitate.

Further, the silicone and the cross-linked polymer thereof are selected from one or a combination of at least two of polydimethylsiloxane, cyclopentadidimethylsiloxane, polydimethylsiloxane cross-linked polymer, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, octyl methicone, PEG-12 methicone/PPG-20 cross-linked polymer.

Further, the colorant is selected from one or a combination of at least two of CI 45410, CI77491, CI 77891, CI 15850, CI 15985, CI19140, CI 45380, CI 17200, CI 42090, CI 77492, CI 77499, CI 47005, CI 16035, CI 73360.

Further, the humectant is one or a combination of at least two of cosmetic common polyhydric alcohols such as glycerin, diglycerin, propylene glycol, dipropylene glycol, butylene glycol, pentanediol, isoprene glycol, and hexanediol.

Further, the preservative is selected from one or a combination of at least two of phenoxyethanol, potassium sorbate, sodium benzoate, ethylhexyl glycerol, caprylic hydroxamic acid and glyceryl caprylate.

The preparation method of the moistened satin brilliant lip glaze comprises the following steps:

weighing the components of the phase A in parts by weight, heating to 50-55 ℃, mixing and stirring for 5-10 min to be completely uniform;

weighing the components of the phase B according to parts by weight, adding the components of the phase A into the phase A, and keeping the temperature at 50-55 ℃, mixing and stirring for 5-10 min until the components are completely uniform;

weighing the components of the phase C in parts by weight, heating to 50-55 ℃, mixing and stirring for 5-10 min, and uniformly supplementing water by 3%;

step four, keeping the temperature at 50-55 ℃, slowly adding the phase C into the mixture of the phase A and the phase B at a constant speed, and homogenizing at a speed of about 3000-6000 rpm for 15-20 min;

and step five, cooling to 25-30 ℃, discharging, and filling to obtain a finished product.

The invention innovatively combines a silicon elastomer with water and invents a water-in-silicon elastomer dosage form. The silicon elastomer has the lip wrinkle covering effect while thickening, and provides a pleasant silky feeling for the product, so that the product has good spreadability. The introduction of a proper amount of water and the humectant ensures that the product has long-acting moisture retention and is not easy to pull dry, and the product presents a certain gloss after being smeared.

Drawings

FIG. 1 is a graph showing the stickiness test of the sample of example 4.

Fig. 2 is a graph showing a sticky feeling test experiment of the sample of comparative example 1.

Fig. 3 is a graph showing a sticky feeling test experiment of the sample of comparative example 2.

Detailed Description

Embodiments of the present application will be described in detail by examples, so that how to apply technical means to solve technical problems and achieve technical effects of the present application can be fully understood and implemented.

The raw materials and equipment used in the present application are all common raw materials and equipment in the field, and are all from commercially available products, unless otherwise specified. The methods used in this application are conventional in the art unless otherwise indicated.

There are many other possible embodiments of the present invention, which are not listed here, and the embodiments claimed in the claims of the present invention can be implemented.

In some embodiments, a moist satin gloss lip glaze comprises phase a, phase B, and phase C components. The phase A comprises 0-14 parts of a softening agent, 5-7 parts of an emulsifier, 0.5-4 parts of an adhesive, 40-70 parts of silicone and a cross-linked polymer (namely a silicone elastomer), the phase B comprises 5-11 parts of a coloring agent, and the phase C comprises 9-25 parts of water, 2-8 parts of a humectant and 0.5-0.8 part of a preservative.

Wherein the emollient imparts a silky, soft feel to the skin. Cyclopenta dimethyl silicone is a volatile silicone oil which is colorless, tasteless, non-irritating, compatible with most cosmetic ingredients, while having good spreadability and a soft, smooth texture, and is capable of reducing surface tension and assisting in dispersion of solid pigments. Isododecane is also an irritant low-molecular-weight isoparaffin, has strong volatility, dry and smooth skin feel and can effectively offset the greasy skin feel of other raw materials.

The emulsifier can reduce the interfacial tension and form an oriented adsorption layer at the interface between the dispersed phase droplets and the dispersion medium, thereby improving the stability of the emulsion. The cetyl PEG/PPG-10/1 polydimethylsiloxane is a W/O emulsifier modified by silicone oil, has good compatibility with various organic components, low requirement on emulsification temperature and good thermal stability, and has no greasy feeling and heavy feeling of a typical water-in-oil system after emulsification. Lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone is a nonionic silicone emulsifier, can form a low-viscosity water-in-oil emulsion, has good emulsifiability to both silicone oil and organic grease, and can improve the dispersibility of pigments and fine particles in silicone oil and organic oil. The two components can form a high-strength composite film at the interface, thereby enhancing the stability of the composition.

The binder may provide a more intimate and uniform combination of the colorant and the other components. Isododecane (and) disteardimonium hectorite (and) propylene carbonate enable better suspension of the pigment while stabilizing the emulsion.

The silicone and the cross-linked polymer thereof have special silky feeling and powdery feeling, have obvious soft-focus effect, can cover lip wrinkles when being used for lips, and bring distinctive makeup effect.

Moisturizers prevent water loss from the skin and at the same time absorb water from moist air. 1, 2-pentanediol, butanediol and glycerol are common polyols, wherein the 1, 2-pentanediol and the butanediol have the functions of moisturizing and inhibiting bacteria.

The compositions obtained in the above examples were subjected to sensory evaluation test, 4h moisturizing test, lip mark covering test, sticky feeling test, and gloss test.

Examples

The satin bright lip glaze is prepared according to the following preparation method:

weighing the components of the phase A in parts by weight, heating to 50-55 ℃, mixing and stirring for 5-10 min to be completely uniform;

weighing the components of the phase B according to parts by weight, adding the components of the phase A into the phase A, and keeping the temperature at 50-55 ℃, mixing and stirring for 5-10 min until the components are completely uniform;

weighing the components of the phase C in parts by weight, heating to 50-55 ℃, mixing and stirring for 5-10 min, and uniformly supplementing water by 3%;

step four, keeping the temperature at 50-55 ℃, slowly adding the phase C into the mixture of the phase A and the phase B at a constant speed, and homogenizing at a speed of about 3000-6000 rpm for 15-20 min;

and step five, cooling to 25-30 ℃, discharging, defoaming and filling to obtain a finished product.

The proportional compositions of the components are shown in tables 1 and 2, wherein the fractions are parts by weight.

Wherein A1 is cetyl PEG/PPG-10/1 polydimethylsiloxane, A2 is a mixture of lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone and tocopherol (vitamin E) (tocopherol content less than 100ppm), A3 is cyclopentadecyldimethylsiloxane, A4 is a mixture of isododecane and distearyldimethylammonium hectorite and propylene carbonate, A5 is a mixture of polydimethylsiloxane and a polydimethylsiloxane crosspolymer;

b1 is CI 15850:1 color paste, B2 is CI 17200 color paste, and B3 is CI 15985 color paste;

c1 is water, C2 is 1, 2-pentanediol, C3 is a mixture of phenoxyethanol and ethylhexylglycerin, C4 is butanediol, and C5 is glycerin.

TABLE 1

Examples 1 to 5, 6 to 10, and 11 to 15 are different in that the mass percentages of the emulsifiers are 5%, 6%, and 7%, respectively. The differences between examples 1 to 5, examples 6 to 10, and examples 11 to 15 are that the mass percentages of silicone and its crosslinked polymer (silicone elastomer) and the binder gradually increase, and the mass percentages of the emollient, water, humectant, and preservative gradually decrease.

Example 16: the difference from example 1 is that equal amounts of polydimethylsiloxane were used instead of cyclopentademethicone.

Example 17: the difference from example 1 is that cetyl PEG/PPG-10/1 dimethicone was replaced with an equivalent amount of PEG-10 dimethicone, and lauryl PEG-10 tris (trimethylsiloxy) silylethyl methicone was replaced with an equivalent amount of sorbitan isostearate.

Example 18: the difference from example 1 is that diisostearyl malate is used in equal amounts instead of a mixture of isododecane and disteardimonium hectorite and propylene carbonate.

Example 19: the difference from example 1 is that the mixture of dimethicone and dimethicone crosspolymer was replaced by an equal amount of cyclopentadimethicone and dimethicone/vinyl dimethicone crosspolymer mixture.

Example 20: the difference from example 1 is that diglycerol is used in place of glycerol in equal amounts, 1, 3-propanediol is used in place of butanediol in equal amounts, and isoprene glycol is used in place of 1, 2-pentanediol in equal amounts.

Example 21: the difference from example 1 is that the mixture of phenoxyethanol and ethylhexyl glycerol is replaced by an equal amount of glyceryl caprylate.

COMPARATIVE EXAMPLE 1 (Matt velvet lip glaze)

TABLE 2

The matte velvet lip glaze of example 2 was synthesized in the proportions of table 2 with reference to the following method.

Weighing the phase A components in parts by weight, heating to 85-90 ℃, melting the solid, and uniformly mixing;

step two, weighing the phase B according to the parts by weight, adding the phase A into the phase B, and mixing and stirring the mixture for 20min at the temperature of 65-75 ℃ until the mixture is completely and uniformly dispersed;

weighing the components of the phase C according to parts by weight, adding the components into the mixture of the phase A and the phase B, and keeping the temperature at 65-75 ℃ and stirring for 10min until the components are uniformly mixed;

step four, weighing the components of the phase D according to the parts by weight, adding the components into the mixture of the A, B, C phase, and keeping the temperature at 60-65 ℃ and stirring for 10min until the components are uniformly mixed;

and fifthly, keeping the temperature at 60-65 ℃, discharging, and controlling the filling temperature to be 55-60 ℃.

Comparative example 2 (lip glaze mirror surface)

TABLE 3

The water-polished mirror lip glaze of example 3 was synthesized in the proportions shown in Table 3 by the following method.

Step one, weighing the phase A components in parts by weight, heating the phase A components to 75-80 ℃ to melt the solid, uniformly stirring and mixing the components, and keeping the temperature at 60-65 ℃;

weighing the components of the phase B according to parts by weight, heating to 70-75 ℃ to melt the solid, and mixing and stirring for 5min until the solid is completely and uniformly dispersed;

weighing the components of the phase C according to parts by weight, adding the phase B, and stirring for 5min at the temperature of 60-65 ℃ until the components are uniformly mixed;

step four, keeping the temperature at 60-65 ℃, slowly adding the mixture of the phase B and the phase C into the phase A at a constant speed, and homogenizing at a speed of about 3000-6000 rpm for 15 min; (ii) a

Step five, cooling to below 45 ℃, and adding the phase D to homogenize at a speed of about 4500-5000 rpm for 5 min;

step six, adding the phase E, and homogenizing for 5min at a speed of 4500-5000 rpm;

and seventhly, discharging, defoaming and filling.

Experimental example 1: sensory evaluation test

And selecting 10 volunteers for carrying out sensory evaluation on the examples 1-21, wherein the score is 1-10, the higher the score is, the more satisfied the evaluation is, after scoring, the average score of the 10 volunteers is taken for each evaluation item, and the scoring result is shown in table 4.

TABLE 4

	Degree of water wettability	Degree of dryness	Degree of smoothness	Degree of spreading	Composite score
						Example 1	8.3	6.0	7.6	7.3	29.2
Example 2	8.0	6.8	7.8	7.4	30.0
						Example 3	7.6	7.2	8.4	8.6	31.8
Example 4	7.4	7.8	9.6	9.2	34.0
						Example 5	6.4	8.6	9.0	8.3	32.3
Example 6	8.4	5.7	7.5	7.4	29.0
						Example 7	8.1	6.5	7.7	7.5	29.8
Example 8	8.0	7.0	8.3	8.7	32.0
						Example 9	7.6	7.5	9.5	9.1	33.7
Example 10	6.2	8.3	9.1	8.5	32.1
						Example 11	8.0	5.5	7.8	7.5	28.8
Example 12	7.8	5.9	7.9	7.8	29.4
						Example 13	7.5	6.9	8.5	8.6	31.5
Example 14	7.1	7.5	9.6	9.0	33.2
						Example 15	6.1	8.2	9.1	8.8	32.2
Example 16	8.4	5.8	7.7	7.5	29.4
						Example 17	8.2	6.0	7.5	7.4	29.1
Example 18	8.0	5.5	7.4	7.2	28.1
						Example 19	8.6	5.4	7.7	7.3	29.0
Example 20	8.2	6.1	7.6	7.3	29.2
						Example 21	8.3	5.9	7.6	7.3	29.1

It can be seen from the evaluation results that the change in the content of the emulsifier had little effect on the sensory evaluation of the samples. The higher the water, humectant and emollient content, the more water wet the sample. The higher the silicone elastomer and binder content, the drier the sample. The smoothness and spreadability of the samples also increased with increasing levels of silicone elastomer and binder, but conversely decreased when the levels of silicone elastomer and binder exceeded certain levels.

Experimental example 2: 4h moisture test

Test samples: examples 1 to 5, examples 16 to 21 and comparative examples 1 and 2

Testing an instrument: corneometer MPA580 skin epidermis tester

Test objects: female volunteers between the ages of 20-40 years, 5 persons per group

The test method comprises the following steps: 1. selecting the forearm curve side measuring area of the subject as 2x2cm²Uniformly coating the product on an area to be detected;

2. measurements were performed using a Corneometer at 0h and 2h and 4h before and after use, respectively;

3. the same spot was measured 5 times, and 3 average values were recorded excluding the maximum and minimum values.

(2h, 4h) horny layer water loss rate after use ═ (horny layer water loss rate after use-anterior horny layer water content before use)/anterior horny layer water content before use × 100%

The results are shown in tables 5 and 6

TABLE 5

TABLE 6

According to the test data of the embodiment 1-5, the higher the moisture content and the humectant content is, the better the instant water replenishing effect is; the higher the silicon elastomer content is, the better the lasting moisturizing effect is, but when the silicon elastomer content exceeds a certain amount, the viscosity of the sample is too high, the film cannot be well formed during smearing, and the moisturizing effect is reduced. The test data of examples 16-21 are slightly different from those of example 1, but all have good moisturizing effect.

Although the oil-in-water lip glaze prepared in comparative example 2 has the best instant water replenishing effect, the water content is reduced more rapidly and the moisture retaining effect is slightly poor compared with the lip glaze prepared in examples 1 to 5 and 16 to 21, which indicates that the volatilization speed of water as the inner phase is reduced after being wrapped by the silicon elastomer. Whereas the matte velvet lip glaze prepared by comparative example 1 does not contain moisture and humectant, so long-term use causes the lips to dry.

Experimental example 3: lip mark hiding test

Test samples: example 4, comparative examples 1 and 2 were selected as test samples

Testing an instrument: antera 3D (Miravex, Ireland)

Test objects: artificial leather

The test method comprises the following steps: 1. cleaning artificial leather with wet tissue, and defining a fixed area of 2cm × 2cm at 10 positions on the artificial leather;

2. measuring the texture condition of the fixed area by using an Antera 3D, recording Ra and Rq values, and taking an average value;

2. uniformly smearing 0.3g of a test sample on a fixed area;

3. the texture of the fixed area after application of the product was measured using an Antera 3D, and the Ra, Rq values were recorded and averaged, with the results shown in Table 7.

Parameter interpretation:

ra: average roughness, an average of all deviations from a straight line within the evaluation length, irrespective of the vertical direction;

rq: root mean square roughness is the root mean square average of the roughness ordinate.

TABLE 7

As can be seen from the test data of the embodiments 1 to 5, the lip covering effect is improved along with the increase of the content of the silicon elastomer, but when the content of the silicon elastomer is increased to a certain amount, the lip covering effect is reduced due to the decrease of the spreading degree, and the lip covering effect is not greatly influenced by replacing other raw materials. In addition, the oil-dispersed lip glaze prepared in comparative example 1 contains silica in addition to the silicon elastomer, and thus the lip gloss covering effect is more excellent than that of the lip glaze prepared in example 4 having a similar content of the silicon elastomer. The oil-in-water lip glaze prepared in comparative example 2 did not have a significant lip-masking effect.

Experimental example 4: sticky feeling test

Test samples: example 4, comparative examples 1 and 2

Testing an instrument: high definition camera

Test objects: artificial leather

The test method comprises the following steps: : the product is evenly smeared on the inner side of the forearm of 2cm x2cm, fine sand is sprinkled on the forearm, and the residual quantity of the fine sand is observed after the arm is turned over.

The tests are shown in fig. 1,2, 3.

FIG. 1 a: after using the example 4 sample, fig. 1 b: after covering the fine sand with the sample of example 4, fig. 1 c: after inversion with the sample cover of example 4.

FIG. 2 a: after using the comparative example 1 sample, fig. 2 b: after covering fine sand with the comparative example 1 sample, fig. 2 c: after the flip was covered with the comparative example 1 sample.

FIG. 3 a: after using the comparative example 2 sample, fig. 3 b: after covering fine sand with the comparative example 2 sample, fig. 3 c: after the flip was covered with the comparative example 2 sample.

As can be seen from the test pictures, the residual amount of fine sand in the region coated with the oil-in-water type water gloss lip glaze prepared in comparative example 2 is the largest, the residual amount of fine sand in the region coated with the matte surface lip glaze prepared in comparative example 1 is the smallest, and the residual amount of fine sand in the satin gloss lip glaze prepared in example 4 is intermediate between the two residual amounts. The greasy feeling of the water gloss lip glaze is the strongest, the satin gloss lip glaze is the second, and the matte lip glaze is the weakest in sticky feeling.

Experimental example 5: gloss measurement

Test samples: examples 1 to 5, examples 16 to 21, comparative examples 1 and 2

Testing an instrument: multi-angle glossometer (BYK, Germany)

Test objects: artificial leather

The test method comprises the following steps: : 1. cleaning artificial leather with wet tissue, and defining a fixed area of 2cm × 2cm at 10 positions on the artificial leather;

2. measuring the glossiness value of the fixed area by using a multi-angle glossmeter;

3. uniformly smearing 0.3g of a test sample on a fixed area;

4. and measuring the gloss value of the fixed area after the product is coated by using a multi-angle gloss meter.

The results are shown in Table 8.

TABLE 8

From the test data of the examples 1-5, it can be known that the higher the contents of water, humectant and emollient, the higher the glossiness after smearing, and the less influence on the glossiness of the sample by replacing other raw materials. Although the glossiness of the moistened satin gloss lip glaze prepared in example 1 is not as good as that of the oil-in-water type water gloss lip glaze prepared in comparative example 2, the gloss of the lips after use is still obviously improved.

The details not described in the specification of the present application belong to the common general knowledge of those skilled in the art.

In the following description and in the claims, the terms "include" and "comprise" are used in an open-ended fashion, and thus should be interpreted to mean "include, but not limited to. "substantially" means within an acceptable error range, and a person skilled in the art can solve the technical problem within a certain error range to substantially achieve the technical effect.

It is also noted that the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a good or system that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such good or system. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other like elements in a commodity or system that includes the element.

The foregoing description shows and describes several preferred embodiments of the present application, but as aforementioned, it is to be understood that the application is not limited to the forms disclosed herein, but is not to be construed as excluding other embodiments and is capable of use in various other combinations, modifications, and environments and is capable of changes within the scope of the inventive concept as expressed herein, commensurate with the above teachings, or the skill or knowledge of the relevant art. And that modifications and variations may be effected by those skilled in the art without departing from the spirit and scope of the application, which is to be protected by the claims appended hereto.

Claims (10)

1. A moist satin gloss lip glaze is characterized by comprising phase A, phase B and phase C components;

the phase A comprises 0-14 parts of a softening agent, 5-7 parts of an emulsifier, 0.5-4 parts of a binder, and 40-70 parts of silicone and a cross-linked polymer thereof;

the phase B comprises 5-11 parts of a coloring agent;

the phase C comprises 9-25 parts of water, 2-8 parts of a humectant and 0.5-0.8 part of a preservative;

all in parts by weight.

2. The lip glaze according to claim 1, comprising phase A, phase B, phase C components;

the phase A comprises 4-10 parts of a softening agent, 5-6 parts of an emulsifier, 1-3 parts of an adhesive, 50-60 parts of silicone and a cross-linked polymer thereof;

the phase B comprises 7-10 parts of a colorant;

the phase C comprises 13-21 parts of water, 4-6 parts of a humectant and 0.6-0.75 part of a preservative;

all in parts by weight.

3. The lip glaze of claim 1, wherein:

the emollient is selected from any one of polydimethylsiloxane, cyclopentadimethylsiloxane, diphenylsiloxyphenyltrimethicone, pentaerythritol (ethyl hexanoate), hydrogenated polyisobutene, caprylic/capric triglyceride, dipentaerythritol tetrahydroxystearate/tetraisostearate, dicaprylyl carbonate, pentaerythritol tetraisostearate, phenyl trimethicone, isododecane or a combination of at least two of the foregoing.

4. The lip glaze of claim 1, wherein:

the emulsifier is selected from one or more of cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG-10 tris (trimethylsiloxy) silicon ethyl methicone, PEG-10 polydimethylsiloxane, sorbitan isostearate, sorbitan olivate oleate, glycerol tri (ethyl hexanoate) and the like.

5. The lip glaze of claim 1, wherein:

the adhesive is selected from one or a combination of at least two of diisostearyl malate, dimethylsilylated silica, propylene carbonate, disteardimonium hectorite, VP/hexadecene copolymer, isononyl isononanoate, tridecyl alcohol trimellitate.

6. The lip glaze of claim 1, wherein:

the silicone and the cross-linked polymer thereof are selected from one or the combination of at least two of polydimethylsiloxane, cyclopentadecyldimethylsiloxane, polydimethylsiloxane cross-linked polymer, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, octyl polymethylsiloxane and PEG-12 polymethylsiloxane/PPG-20 cross-linked polymer.

7. The lip glaze of claim 1, wherein: the colorant is selected from one or a combination of at least two of CI 45410, CI77491, CI 77891, CI 15850, CI 15985, CI19140, CI 45380, CI 17200, CI 42090, CI 77492, CI 77499, CI 47005, CI 16035, and CI 73360.

8. The lip glaze of claim 1, wherein: the humectant is one or a combination of at least two of glycerin, diglycerin, propylene glycol, dipropylene glycol, butanediol, pentanediol, isoprene glycol and hexanediol.

9. The lip glaze of claim 1, wherein: the preservative is selected from one or a combination of at least two of phenoxyethanol, potassium sorbate, sodium benzoate, ethylhexyl glycerol, caprylic hydroxamic acid and glycerol caprylate.

10. A method for preparing lip glaze according to claim 1, which comprises the following steps:

weighing the components of the phase A in parts by weight, heating to 50-55 ℃, mixing and stirring for 5-10 min to be completely uniform;

weighing the components of the phase B according to parts by weight, adding the components of the phase A into the phase A, and keeping the temperature at 50-55 ℃, mixing and stirring for 5-10 min until the components are completely uniform;

weighing the components of the phase C in parts by weight, heating to 50-55 ℃, mixing and stirring for 5-10 min, and adding 3% of water in parts by weight;

step four, keeping the temperature at 50-55 ℃, slowly adding the phase C into the mixture of the phase A and the phase B at a constant speed, and homogenizing at a speed of about 3000-6000 rpm for 15-20 min;

and step five, cooling to 25-30 ℃, discharging, and filling to obtain a finished product.

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