CN114869807A - All-natural water-containing lip glaze and preparation method thereof - Google Patents
All-natural water-containing lip glaze and preparation method thereof Download PDFInfo
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- CN114869807A CN114869807A CN202210639115.XA CN202210639115A CN114869807A CN 114869807 A CN114869807 A CN 114869807A CN 202210639115 A CN202210639115 A CN 202210639115A CN 114869807 A CN114869807 A CN 114869807A
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- oil
- plant
- lip glaze
- natural
- water
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Abstract
The application discloses an all-natural water-containing lip glaze and a preparation method thereof. The all-natural water-containing lip glaze comprises the following components in percentage by weight: vegetable oil and fat: 30% -50%; plant powder: 10% -25%; plant emulsifier: 3% -15%; water phase components: 20% -48%, wherein the water phase component comprises water, a plant humectant, an ion stabilizer, a pH regulator and a plant preservative; natural thickeners: 0.1% -3%; other auxiliary agents: 0.2 to 4 percent. The all-natural water-containing lip enamel provided by the application is fine and smooth, has uniform color, has good moisturizing and moisturizing effects and water locking effects, and is almost nonirritating and high in safety. And secondly, the plant components in the all-natural water-containing lip glaze can be fully degraded, and the lip glaze is environment-friendly. In addition, the preparation method of the all-natural water-containing lip glaze provided by the application is simple in process, short in time consumption, low in equipment requirement, well compatible with the existing process and extremely high in large-scale application potential.
Description
Technical Field
The application belongs to the technical field of daily cosmetics, and particularly relates to a natural water-containing lip glaze and a preparation method thereof.
Background
The lip beautifying product is one of the essential beautifying color cosmetic products for women, and has the functions of making lips ruddy and glossy, moistening and maintaining the lips, giving color to the lips, increasing the aesthetic feeling of the face and correcting the contour of the lips, wherein lip glaze is one of the essential beautifying color cosmetic products for the lips, and is popular and concerned by many consumers.
However, the lip glaze sold in the market at present mainly adopts an unnatural anhydrous pure oil system or a lip glaze containing a small amount of water-soluble components, so that the safety of the lip glaze cannot be guaranteed, and the requirements of consumers on the lip glaze with high moisture retention, moistening and water locking effects cannot be met.
Disclosure of Invention
In view of the above, the application provides an all-natural water-containing lip glaze and a preparation method thereof, aiming at solving the problems of low safety of the lip glaze containing non-natural components and poor moisture-preserving and water-locking performances.
In one aspect, the present application provides an all-natural water-containing lip glaze, which includes, by weight:
vegetable oil and fat: 30% -50%;
plant powder: 10% -25%;
plant emulsifier: 3% -15%;
water phase components: 20% -48%, wherein the water phase component comprises water, a plant humectant, an ion stabilizer, a pH regulator and a plant preservative;
a natural thickener: 0.1% -3%;
other auxiliary agents: 0.2 to 4 percent.
According to an embodiment of one aspect of the application, the aqueous phase component comprises in weight percent:
water: 20% -30%;
plant humectant: 2% -5%;
an ionic stabilizer: 0.2% -1.0%;
pH regulator: 0.3 to 1.5 percent;
plant preservative: 0.1 to 8 percent.
According to an embodiment of one aspect of the application, the plant humectant is selected from one or more of glycerol, propylene glycol and 1,3 butylene glycol.
According to an embodiment of one aspect of the application, the ionic stabilizer is selected from one or more of sodium chloride, magnesium chloride and calcium chloride.
According to an embodiment of one aspect of the application, the pH adjusting agent is selected from one or more of citric acid, malic acid, tartaric acid and gallic acid.
According to an embodiment of one aspect of the application, the plant preservative is selected from one or more of pentanediol, 1,2 hexanediol, glyceryl caprylate, anisic acid and magnolia bark extract.
According to an embodiment of one aspect of the application, the vegetable fat is selected from one or more of jojoba oil, sunflower seed oil, castor oil, coconut oil, grape seed oil, shea butter, meadowfoam seed oil, macadamia nut oil, olive oil, palm oil, squalane, cocoa butter, jojoba fat, glycolipids, octyldodecanol, caprylic/capric triglyceride, coco-caprylic/capric triglyceride, oleic/linoleic/linolenic polyglycerides and dioctyldodecanol dimer linoleate.
According to an embodiment of one aspect of the present application, the plant powder includes a plant toner and a filler; the plant toner is selected from one or more of tomato red, beet red, safflower red, purple sweet potato, elderberry red and radish red; the filler is selected from corn starch and/or rice starch.
According to an embodiment of one aspect of the application, the vegetable emulsifier is selected from one or more of polyglyceryl-3 diisostearate, polyglyceryl 2-dipolyhydroxystearate, polyglyceryl-2 isostearate, polyglyceryl 4-isostearate, polyglyceryl 3-polyricinoleate, polyglyceryl 6-polyricinoleate, glyceryl stearate, sorbitan isostearate, sorbitan oleate and sucrose cocoate.
According to an embodiment of one aspect of the application, the natural thickener is selected from one or more of sunflower seed wax, candelilla wax, behenyl, carnauba wax, cercis green flower wax, tara gum, dextrin palmitate, dextrin isostearate, disteardimonium hectorite, silica gel and bentonite.
According to an embodiment of one aspect of the application, the other adjuvants include a plant antioxidant and a plant essential oil;
the plant antioxidant is selected from one or more of tocopherol, tocopheryl acetate, ascorbyl palmitate, tea polyphenol and rice bran oil;
the plant essential oil is one or more selected from lemon peel oil, citronellol, lavender oil, rosemary essential oil, palmarosa oil and geranium oil.
In another aspect, the present application provides a method for preparing an all-natural water-containing lip glaze, including:
adding the uniformly mixed water phase component into a mixture containing vegetable oil, vegetable powder, a vegetable emulsifier and a natural thickener at the temperature of 60-80 ℃, and reacting to obtain an emulsified mixture;
and cooling the mixture to below 40 ℃, adding other additives, and uniformly stirring to obtain the all-natural water-containing lip glaze.
According to another aspect of the embodiment of the present application, the rotation speed during stirring is 4000-. .
Compared with the prior art, the application has at least the following beneficial effects:
(1) the application provides an all natural moisture type lip glaze, on the one hand possess good moisturizing, moisten and frivolous result of use, the security is high, and the texture is exquisite, the colour is even, also very friendly to the user of pregnant woman, sensitive muscle. On the other hand, the plant components in the all-natural water-containing lip glaze can be degraded and is environment-friendly.
Firstly, the all-natural water-containing lip glaze in the application takes 100% of all-natural materials (plant sources and mineral sources) as raw materials, replaces chemical synthesis or non-natural components in the traditional makeup products, and is safer. Secondly, the stability of the all-natural water-containing lip glaze can be improved by adding the efficient plant emulsifier; meanwhile, the use of the plant preservative can further improve the safety level of the whole-plant anhydrous lip glaze. In addition, the raw materials of the all-natural water-containing lip glaze contain 20-48% of water phase components, so that the use effects of moisture retention, lightness and thinness of the all-natural water-containing lip glaze can be improved to the greatest extent, and the requirements of consumers on the high-moisture-retention water-locking lip glaze are met.
(2) The preparation method of the all-natural water-containing lip glaze is simple in process, short in time consumption, low in equipment requirement, well compatible with the existing process, and extremely high in large-scale application potential.
Detailed Description
In order to make the application purpose, technical solution and beneficial technical effects of the present application clearer, the present application is further described in detail with reference to the following embodiments. It should be understood that the embodiments described in this specification are only for the purpose of explaining the present application and are not intended to limit the present application.
For the sake of brevity, only some numerical ranges are explicitly disclosed herein. However, any lower limit may be combined with any upper limit to form ranges not explicitly recited; and any lower limit may be combined with any other lower limit to form a range not explicitly recited, and similarly any upper limit may be combined with any other upper limit to form a range not explicitly recited. Also, although not explicitly recited, each point or individual value between endpoints of a range is encompassed within the range. Thus, each point or individual value can form a range not explicitly recited as its own lower or upper limit in combination with any other point or individual value or in combination with other lower or upper limits.
In the description of the present application, it is to be noted that, unless otherwise specified, "above" and "below" are inclusive of the present number, and "plural" of "one or more" means two or more.
The above summary of the present application is not intended to describe each disclosed embodiment or every implementation of the present application. The following description more particularly exemplifies illustrative embodiments. At various points throughout this application, guidance is provided through a list of embodiments that can be used in various combinations. In each instance, the list is merely a representative group and should not be construed as exhaustive.
The existing lip glaze has the defects of complex raw material components, poor moisture retention, often containing more chemically synthesized or non-natural components, low safety, easy causing anaphylactic reaction such as lip mucosa chapping, peeling, cheilitis and the like, even containing carcinogenic substances and seriously harming the body health.
Based on the above, the inventor carries out a great deal of research, and finds that the safety performance of the lip glaze can be improved by preparing the all-natural water-containing lip glaze, and the all-natural water-containing lip glaze has excellent effects of moistening, moisturizing, thinning and lightening under the synergistic action of all natural components.
All natural water-containing lip glaze
In one aspect, the embodiment of the present application provides an all-natural water-containing lip glaze, which includes, by weight:
vegetable oil and fat: 30% -50%;
plant powder: 10% -25%;
plant emulsifier: 3% -15%;
water phase components: 20% -48%, wherein the water phase component comprises water, a plant humectant, an ion stabilizer, a pH regulator and a plant preservative;
natural thickeners: 0.1% -3%;
other auxiliary agents: 0.2 to 4 percent.
According to the embodiment of the application, the all-natural water-containing lip glaze takes 100% of all-natural materials as raw materials, chemical synthesis or non-natural ingredients in the traditional makeup product are replaced, the lip glaze is safer, and the requirements of consumers on natural products are met. In addition, the plant components in the all-natural water-containing lip glaze can be degraded, and the lip glaze is environment-friendly.
The all-natural water-containing lip glaze takes vegetable oil as a main body, and can be prepared into the all-natural water-containing lip glaze with fine texture, uniform color, moisture retention and moistening and high safety by adding a certain content of water phase components.
In some embodiments, the aqueous phase components comprise, in weight percent:
water: 20% -30%;
plant humectant: 2% -5%;
an ionic stabilizer: 0.2% -1.0%;
pH regulator: 0.3% -1.5%;
plant preservative: 0.1 to 8 percent.
According to the embodiment of the application, the addition of the water phase component can make the all-natural water-containing lip glaze lighter, thinner, less sticky and better in ductility.
According to the embodiment of the application, the stability of the lip glaze can be enhanced by adding the ionic stabilizer, and the lip glaze is not easy to delaminate and the like by adopting the ionic stabilizer with the weight ratio of 0.2-1.0%. For example, the weight percentage of ionic stabilizer is 0.2%, 0.4%, 0.6%, 0.8%, or 1.0%. The weight percent of the ionic stabilizer can also range between any combination of the above values. In embodiments of the present application, the ionic stabilizer may be selected from one or more of sodium chloride, magnesium chloride and calcium chloride.
According to the embodiment of the application, the pH regulator can regulate the pH of the all-natural water-containing lip glaze to keep the pH within a range (5-7) suitable for skin use. For example, the weight percentage of the pH adjuster is 0.3%, 0.6%, 0.9%, 1.2%, or 1.5%. The weight percent of the pH adjuster can also range from any combination of the above values. In the present embodiment, the pH adjusting agent may be selected from one or more of citric acid, malic acid, tartaric acid and gallic acid.
According to the embodiment of the application, the plant preservative with the weight percentage of 0.1-8% can not only prevent the lip glaze from being polluted by microorganisms in the storage and use processes, but also has no harm to human health. The hydroxybenzene methyl ester preservative which is common in the traditional preservatives is one of the reasons for the high incidence of female diseases such as breast cancer, uterine diseases and the like for women; for men, it can inhibit male hormone induced infertility. For example, the weight percentage of the plant preservative is 0.3%, 1%, 2.5%, 5.5%, or 8%. The weight percent of the plant preservative can also be any combination of the above values.
In some embodiments, the plant preservative may be selected from one or more of pentanediol, 1, 2-hexanediol, glyceryl caprylate, anisic acid, and magnolia bark extract.
According to the embodiment of the application, the plant preservatives are water-soluble preservatives and can be well compatible with other substances in the water-phase component. Wherein, the anisic acid is derived from natural substances of anethole and anise oil, has better antiseptic effect under acidic condition, and has obvious bacteriostatic action on staphylococcus aureus, escherichia coli, bacillus subtilis, aspergillus niger and aspergillus flavus. The pentanediol and the 1, 2-hexanediol can be used as important components of plant preservatives because of the antiseptic and bacteriostatic activity. The glyceryl caprylate has good compatibility with other preservatives and has a synergistic function. The main active ingredient of the magnolia bark extract is magnolol which has good inhibition effect on escherichia coli, staphylococcus aureus, bacillus subtilis and the like.
In some embodiments, the plant humectant may be selected from one or more of glycerin, propylene glycol, and 1,3 butylene glycol.
According to the examples of the present application, glycerin, propylene glycol and 1, 3-butylene glycol are all of vegetable origin, and glycerin of vegetable origin is a compound derived from vegetable oil, usually palm oil or coconut oil, which has strong moisturizing properties. The plant humectant in the lip glaze can absorb moisture from the environment, supplement the moisture to the skin and increase the moisture content of the skin surface, thereby achieving the effect of long-term moisture retention and moistening of the all-natural water-containing lip glaze.
In some embodiments, the vegetable oil or fat may be selected from one or more of jojoba oil, sunflower seed oil, castor oil, coconut oil, grape seed oil, shea butter, meadowfoam seed oil, macadamia nut oil, olive oil, palm oil, squalane, cocoa butter, jojoba fat, glycolipids, octyldodecanol, caprylic/capric triglyceride, coco-caprylic/capric triglyceride, oleic/linoleic/linolenic polyglycerides, and dioctyldodecanol dimer linoleate. For example, the vegetable oil can be jojoba oil, coconut oil, mixture of grape seed oil and olive oil, or mixture of sunflower seed oil, castor oil and coconut oil. The vegetable oil and fat can also be selected from any one of the vegetable oil and fat or a mixture of any more of the vegetable oil and fat.
According to the embodiment of the present application, the oil and fat are essential components in the lip glaze, and the above-listed oil and fat are vegetable oil and fat extracted from plants, and the vegetable oil and fat can ensure the safety, the moisturizing property, the fluidity and the ductility of the all-natural water-containing lip glaze, and ensure the moisturizing effect thereof. The thickness of the skin of the lips is only one third of that of cheeks, and the lips are not provided with sebaceous glands and are the parts most prone to being dried and cracked, and 30% -50% of plant oil for moistening and locking water is added into the lip glaze, so that continuous moistening after the lip glaze is applied is guaranteed. Wherein, the grape seed oil, the coconut oil and the sunflower seed oil also have antioxidant effect, can accelerate the lip crack repair effect and reduce the damage of ultraviolet rays.
In some embodiments, the plant powder may include a plant toner and a filler.
The plant toner may be selected from one or more of lycopene, beet red, safflower red, purple sweet potato, elderberry red and radish red.
The bulking agent may be selected from corn starch and/or rice starch.
According to the embodiment of the application, the plant toner is derived from natural plants, has strong hydrophilicity, has good dispersibility in grease after being subjected to hydrophobic coating modification, and is high in color development chromaticity and not easy to discolor. The hydrophobic modifier of the plant toner may be selected from cyclodextrin, chitosan, liposome, maltodextrin, acacia and hydrophobic starch.
In some embodiments, the vegetable emulsifier is selected from one or more of polyglyceryl-3 diisostearate, polyglyceryl 2-dipolyhydroxystearate, polyglyceryl-2 isostearate, polyglyceryl 4-isostearate, polyglyceryl 3-polyricinoleate, polyglyceryl 6-polyricinoleate, glyceryl stearate, sorbitan isostearate, sorbitan oleate and sucrose cocoate.
According to the embodiment of the application, the plant emulsifier is plant-derived, green and safe, has no stimulation to skin, is suitable for sensitive muscle user groups, and is very suitable for the concept of 'pure makeup'. Wherein, the polyglycerol stearate can form a lamellar liquid crystal type colloid network structure in an emulsification system, and the stability of the emulsification system is improved. The polyglycerol-3 diisostearate and the polyglycerol 2-dipolyhydroxystearate have high emulsifying capacity, can wrap more water phase with less oil phase, has good dispersibility and stability for plant toner, and has good compatibility with various water-in-oil system emulsifiers.
In some embodiments, the natural thickener may be selected from one or more of sunflower seed wax, candelilla wax, behenyl tribehenate, carnauba wax, cercis chinensis wax, tara gum, dextrin palmitate, dextrin isostearate, disteardimonium hectorite, silicone gel, and bentonite.
According to the examples of the present application, candelilla wax, behenyl tribehenate, carnauba wax, cercis chinensis wax, tara gum, dextrin palmitate, and dextrin isostearate are of vegetable origin, and disteardimonium hectorite, silica gel, and bentonite are of mineral origin. The natural thickener has important functions on thickening, stability and rheological property of lip glaze. The natural thickener with the weight percentage of 0.1-3% is adopted, so that the all-natural water-containing lip glaze has good consistency, excellent coating property and ductility.
In some embodiments, other adjuvants may include plant antioxidants and plant essential oils.
The plant antioxidant can be one or more selected from tocopherol, tocopheryl acetate, ascorbyl palmitate, tea polyphenols and rice bran oil.
The plant essential oil can be one or more selected from lemon peel oil, citronellol, lavender oil, rosemary essential oil, palmarosa oil and geranium oil.
According to the embodiment of the application, the plant antioxidant can prevent or delay the oxidation of unsaturated components in the all-natural water-containing lip glaze and prolong the service life of the all-natural water-containing lip glaze. The plant essential oil can enhance the moisturizing and lustering feeling of the all-natural water-containing lip glaze, can timely nourish and relieve the dryness and the peeling condition of skin, has a good repairing effect, can promote the generation of new cells of the skin and stimulate the growth of cells in vivo, and can endow the all-natural water-containing lip glaze with specific fragrance.
According to the embodiment of the application, the all-natural water-containing lip glaze is fine and smooth in texture, uniform in color, good in moisturizing, moistening and light and thin in effect, high in safety and very friendly to a user of sensitive muscles.
Preparation method of all-natural water-containing lip glaze
The application also provides a preparation method of the all-natural water-containing lip glaze, which comprises the following steps:
s10, adding the uniformly mixed water phase component into a mixture containing the vegetable oil and fat, the vegetable powder, the vegetable emulsifier and the natural thickener at the temperature of 60-80 ℃, and reacting to obtain an emulsified mixture;
s20, cooling the mixture to below 40 ℃, adding the other auxiliary agents, and uniformly stirring to obtain the all-natural water-containing lip glaze.
In some embodiments, S10 further includes:
s110, adding vegetable oil, a vegetable emulsifier, vegetable powder and a natural thickener into an emulsifying device, uniformly stirring and heating to 60-80 ℃;
s120, uniformly stirring all the water phase components, and heating to 60-80 ℃;
and S130, slowly adding the uniformly mixed water phase component into the mixture in the S110, and carrying out homogeneous stirring for 15min to obtain an emulsified mixture.
According to the embodiment of the application, the plant emulsifier can effectively reduce the surface tension, form a stable water-in-oil emulsifying system and is beneficial to obtaining the all-natural water-containing lip glaze with uniform and stable texture.
In some embodiments, the stirring speed in steps S110 and S130 can be 4000-.
In some embodiments, the homogeneous stirring in step S130 may be high-pressure homogeneous stirring at 10000-.
The preparation method of the all-natural water-containing lip glaze can be used for preparing the all-natural water-containing lip glaze, the process is simple, the consumed time is short, the requirement on equipment is low, the prepared lip glaze system is stable, the harm to the health of a user can not be caused, and the preparation method has large-scale application potential.
Examples
The present disclosure is more particularly described in the following examples that are intended as illustrative only, since various modifications and changes within the scope of the present disclosure will be apparent to those skilled in the art. Unless otherwise indicated, all parts, percentages, and ratios reported in the following examples are on a weight basis, and all reagents used in the examples are commercially available or synthesized according to conventional methods and can be used directly without further treatment, and the equipment used in the examples is commercially available.
Example 1
An all-natural water-containing lip glaze comprises the following components in percentage by mass:
15% of radish red, 2.5% of rice starch, 4.5% of polyglycerol-3 diisostearate, 1.5% of polyglycerol 2-dipolyhydroxystearate, 4% of jojoba oil, 1% of shea butter, 20% of octyldodecanol, 5% of oleic acid/linoleic acid/linolenic acid polyglycerol esters, 15% of carbohydrate gum, 1% of disteardimonium hectorite, 20% of deionized water, 5% of glycerol, 0.5% of sodium chloride, 0.5% of citric acid, 2% of pentanediol, 1.5% of glyceryl caprylate, 0.5% of magnolia bark extract, 0.4% of tocopherol and 0.1% of lavender oil;
the preparation method of the all-natural water-containing lip glaze comprises the following steps:
(1) uniformly mixing radish red, rice starch, polyglycerol-3 diisostearate, polyglycerol 2-dipolyhydroxystearate, jojoba oil, shea butter, octyldodecanol, coconut oil alcohol-caprylic capric triglyceride, oleic acid/linoleic acid/linolenic acid polyglycerol esters, carbohydrate gum and disteardimonium hectorite, adding into an emulsifying device, heating to 70 ℃, stirring for 10min, wherein the rotating speed is 4500 rpm;
(2) mixing deionized water, glycerol, sodium chloride and citric acid, heating to 70 ℃, and uniformly stirring;
(3) slowly adding the material in the step (2) into the emulsification equipment in the step (1), and homogenizing for 15min at the rotating speed of 6000 rpm;
(4) cooling the mixture in the emulsifying device to below 40 deg.C, adding pre-dissolved pentanediol, glyceryl caprylate, cortex Magnolia officinalis extract, tocopherol and Lavender essential oil, homogenizing, stirring, and mixing to obtain natural water-containing lip glaze.
Example 2
An all-natural water-containing lip glaze comprises the following components in percentage by mass:
elderberry red 18%, rice starch 2%, polyglycerol-3 diisostearate 3%, polyglycerol 2-dipolyhydroxystearate 3%, polyglycerol 4-isostearate 1.5%, polyglycerol 3-polyricinoleate 3%, polyglycerol 6-polyricinoleate 3%, squalane 8%, meadowfoam seed oil 4.5%, coco-caprylic decanoate 15%, dextrin palmitate 1%, disteardimonium hectorite 1%, deionized water 28%, glycerol 2%, sodium chloride 0.5%, citric acid 1%, pentanediol 2.5%, glyceryl caprylate 2%, anisic acid 0.5%, tocopheryl acetate 0.4% and palmarosa oil 0.1%;
the preparation method of the all-natural water-containing lip glaze comprises the following steps:
(1) uniformly mixing elderberry red, rice starch, polyglycerol-3 diisostearate, polyglycerol 2-dipolyhydroxystearate, polyglycerol 4-isostearate, polyglycerol 3-polyricinoleate, polyglycerol 6-polyricinoleate, squalane, chinquapin seed oil, coconut oil alcohol-caprylic acid decanoate, dextrin palmitate and distearyl dimethyl ammonium hectorite, adding into an emulsifying device, heating to 75 ℃, and stirring for 10min at the rotating speed of 4000 rpm;
(2) mixing deionized water, glycerol, sodium chloride and citric acid, heating to 75 ℃, and uniformly stirring;
(3) slowly adding the materials in the step (2) into the emulsification equipment in the step (1), homogenizing for 15min, wherein the rotating speed is 5000 rpm;
(4) cooling the mixture in the emulsifying equipment to below 40 ℃, adding pre-dissolved pentanediol, glyceryl caprylate, anisic acid, tocopheryl acetate and palmarosa oil, homogenizing, stirring and mixing uniformly to obtain the all-natural water-containing lip glaze.
Example 3
An all-natural water-containing lip glaze comprises the following components in percentage by mass:
tomato red 20%, polyglycerol-3 diisostearate 2%, polyglycerol 2-dipolyhydroxystearate 2%, polyglycerol 3-polyricinoleate 2%, jojoba oil 5%, sunflower seed oil 5%, caprylic capric triglyceride 10%, coco-caprylic decanoate 10%, carbohydrate gum 10%, behenyl 1%, dextrin palmitate 1%, distearyl dimethyl ammonium hectorite 1%, deionized water 20%, glycerol 5%, sodium chloride 0.5%, malic acid 1%, hexanediol 2%, glyceryl caprylate 1.5%, magnolia bark extract 0.5%, tocopherol 0.4%, and geranium oil 0.1%;
the preparation method of the all-natural water-containing lip glaze comprises the following steps:
(1) uniformly mixing tomato red, polyglycerol-3 diisostearate, polyglycerol 2-dipolyhydroxystearate, polyglycerol 3-polyricinoleate, jojoba oil, sunflower seed oil, caprylic capric triglyceride, coconut oil alcohol-caprylic decanoate, carbohydrate gum, behenyl trimaran, dextrin palmitate and disteardimonium hectorite, adding into an emulsifying device, heating to 70 ℃, stirring for 10min, and rotating at 5000 rpm;
(2) mixing deionized water, glycerol, sodium chloride and malic acid, heating to 70 deg.C, and stirring;
(3) slowly adding the material in the step (2) into the emulsification equipment in the step (1), and homogenizing for 10min at high pressure at 10000 rpm;
(4) cooling the mixture in the emulsifying device to below 40 deg.C, adding pre-dissolved pentanediol, glyceryl caprylate, cortex Magnolia officinalis extract, tocopherol and geranium sunflower oil, homogenizing, stirring, and mixing to obtain natural water-containing lip glaze.
Example 4
An all-natural water-containing lip glaze comprises the following components in percentage by mass:
20% of purple sweet potato red, 2% of polyglycerol-3 diisostearate, 2% of polyglycerol 2-dipolyhydroxystearate, 1% of sorbitan isostearate, 1% of sucrose cocoate, 8% of castor oil, 6% of coconut oil, 10% of coco alcohol-caprylic decanoate, 10% of caprylic capric triglyceride, 2% of behenyl alcohol, 1% of distearyl dimonium hectorite, 28% of deionized water, 2% of glycerol, 0.5% of sodium chloride, 1% of tartaric acid, 2.5% of hexanediol, 2% of glyceryl caprylate, 0.5% of anisic acid, 0.4% of ascorbyl palmitate and 0.1% of lemon peel oil;
the preparation method of the all-natural water-containing lip glaze comprises the following steps:
(1) uniformly mixing purple sweet potato red, polyglycerol-3 diisostearate, polyglycerol 2-dipolyhydroxystearate, sorbitan isostearate, sucrose cocoate, castor oil, coconut oil alcohol-caprylic decanoate, caprylic capric triglyceride, behenyl sanchinide and distearyl dimethyl ammonium hectorite, adding into an emulsifying device, heating to 75 ℃, and stirring for 10min at the rotation speed of 6500 rpm;
(2) mixing deionized water, glycerol, sodium chloride and tartaric acid, heating to 75 ℃, and uniformly stirring;
(3) slowly adding the material in the step (2) into the emulsification equipment in the step (1), and homogenizing for 10min at high pressure at the rotating speed of 12000 rpm;
(4) when the mixture in the emulsifying equipment is cooled to below 40 ℃, adding pre-dissolved hexanediol, glyceryl caprylate, anisic acid, ascorbyl palmitate and lemon peel oil, and homogenizing, stirring and mixing uniformly to obtain the all-natural water-containing lip glaze.
Test section
1) Test for moisture retention
The Vapometer transdermal water loss meter is a fully portable instrument that can be used to measure TEWL (trans-epidermal water loss) values and evaporation rates. TEWL is a well-known indicator of skin barrier function.
The Vapometer is a battery-driven portable instrument. This provides great convenience and the possibility of difficult area measurements. The joints with different sizes can be replaced, and the possibility of measuring various parts of the human body is realized.
The detection principle is as follows: the core of the Vapometer is a sensitive humidity sensor located in a cylindrical measuring chamber. During the measurement, the chamber is closed by the skin or other measurement surface and is not affected by the ambient air flow. During the measurement, the sensor monitors the indoor Relative Humidity (RH) increase. Evaporation rate value (g/m) 2 h) Is automatically calculated based on the relative humidity increase. Between measurements, the laboratory is ventable, the ventilation time being automatically controlled.
The test method comprises the following steps: selecting 30 test volunteers, smearing samples on a marked area of 5 × 5 square centimeters of the inner area of the arm, standing for 30min in an environment with constant temperature of 20 ℃ and constant humidity of 50%, slightly and vertically pressing the equipment on the inner skin of the arm, and testing for three times to obtain a value by averaging. The calculation formula of the water increase rate is as follows:
moisture growth rate (test data after sample application for 30 min-value before sample application)/value before sample application.
The water content increase rates of 30 volunteers were averaged to obtain a water content average increase rate value.
The all-natural water-containing lip glaze of the above examples 1 to 4 was subjected to the related performance tests, and the test results are shown in table 1 below.
TABLE 1 results of performance test of all-natural water-containing lip glaze of examples 1 to 4
| Sample (I) | Mean rate of increase of water |
| Example 1 | 68.22％ |
| Example 2 | 70.47％ |
| Example 3 | 73.10％ |
| Example 4 | 60.31％ |
From the test results in table 1 above, it can be seen that the average moisture increase rate of the all-natural water-containing lip glaze of examples 1 to 4 is higher than 60.31%, which indicates that the all-natural water-containing lip glaze provided by the present application has good moisture retention performance. Among them, the example 3 has a better moisturizing effect than the other examples because the all-natural water-containing lip glaze of the example 3 is rich in strong moisturizing components such as jojoba oil, hexanediol, and sunflower seed oil.
2) Skin Water Lock Performance test
The skin water locking performance is tested by selecting a MoistureMeter SC stratum corneum hydration measuring instrument and a Finland Delfin MOISTURETERSC skin hydration measuring instrument.
Selecting 30 test volunteers, smearing samples on a marked area of 5 × 5 square centimeters of the inner area of the arm, standing for 30min in an environment with constant temperature of 20 ℃ and constant humidity of 50%, slightly and vertically pressing the equipment on the inner skin of the arm, and testing for three times to obtain a value by averaging. The calculation formula of the water increase rate is as follows:
moisture growth rate (test data after sample application for 30 min-value before sample application)/value before sample application.
The water content increase rates of 30 volunteers were averaged to obtain a water content average increase rate value.
The all-natural water-containing lip glaze of the above examples 1 to 4 was subjected to the related performance tests, and the test results are shown in the following table 2.
TABLE 2 Performance test results of the all-natural water-containing lip glaze of examples 1 to 4
| Sample (I) | Mean rate of increase of water |
| Example 1 | 51.23％ |
| Example 2 | 54.31％ |
| Example 3 | 50.14％ |
| Example 4 | 31.25％ |
From the test results in table 2 above, it is understood that the average increase rate of the moisture in the all-natural water-containing lip glaze of examples 1 to 3 is higher than 50.14%, and the average increase rate of the moisture in the all-natural water-containing lip glaze of example 4 is low because the water-locking component in example 4 is small.
4) Skin irritation test
Healthy adult rabbits and young rabbits from milk are selected to be 4 rabbits each, and the male and female are 2 rabbits respectively. Each animal marked two intact skin areas and two damaged skin areas on the left and right sides of the back, respectively, the damaged skin areas were washed with warm water and sterilized with iodophor, and a well number was drawn in the unhairing area with a sterile needle to cause skin damage. The left sides are coated with deionized water, the right sides are coated with the sample mother liquor in the embodiment, the coating area is 3 x 3 square centimeters, the time lasts for 4-6 hours, the coating is continuously carried out for 7 days, the erythema and the edema are observed and recorded 1 hour after the sample is wiped every day, and the observation is continuously carried out 30-60min, 24 hours, 48 hours and 72 hours after the sample is given last time. And (4) scoring according to the skin irritation response standard, calculating the average score, and judging the irritation strength.
No erythema and edema rated as 0;
mild erythema and edema (barely visible) were rated 1;
moderate edema and erythema (evident) 2 points;
severe edema (1 mm skin swelling, contour clear) and erythema (3 points);
reddish purple erythema to mild eschar formation and severe edema (skin bulge of more than 1mm with enlargement) of 4 points;
the scores of the items are averaged:
0-0.49 has no irritation;
mild irritation of 0.5-2.99;
3-5.99 moderate stimulation;
6-8 severe stimulation.
The all-natural water-containing lip glaze of the above examples 1 to 4 was subjected to the related performance tests, and the test results are shown in the following table 3.
TABLE 3 Performance test results of the all-natural water-containing lip glaze of examples 1 to 4
| Sample (I) | Results of irritation test |
| Example 1 | 4 has no irritation |
| Example 2 | 3 had no irritation, 1 female rabbit had mild irritation: mild erythema without edema |
| Example 3 | 4 has no irritation |
| Example 4 | 3 had no irritation, 1 female rabbit had mild irritation: mild erythema without edema |
As can be seen from table 3 above, the all-natural aqueous lip glaze of examples 1 to 4 has almost no irritation, and examples 2 and 4 have only mild erythema without edema, which indicates that the all-natural aqueous lip glaze provided by the present application has low irritation and high safety performance.
From the test results, the all-natural water-containing lip glaze of the embodiments 1 to 4 has good moistening and moisture-retaining effects, and good water locking effects, and both the irritation and the safety performance can meet the actual requirements, so that the all-natural water-containing lip glaze has innovativeness and novelty in the beauty and make-up market, and has strong product competitiveness.
In summary, in the application, the all-natural water-containing lip glaze takes 100% of all-natural materials (plant sources and mineral sources) as raw materials, and chemical synthetic or non-natural components in the traditional makeup product are replaced, so that the lip glaze is safer. Secondly, the raw materials of the all-natural water-containing lip glaze contain 20-48% of water phase components, so that the use effects of moisture retention, lightness and thinness of the all-natural water-containing lip glaze can be improved to the greatest extent, and the requirements of consumers on high moisture retention and lightness and thinness of the lip glaze are met. In addition, the plant components in the all-natural water-containing lip glaze can be degraded, and the lip glaze is environment-friendly.
While the invention has been described with reference to specific embodiments, the scope of the invention is not limited thereto, and those skilled in the art can easily conceive various equivalent modifications or substitutions within the technical scope of the invention. Therefore, the protection scope of the present application shall be subject to the protection scope of the claims.
Claims (10)
1. The all-natural water-containing lip glaze is characterized by comprising the following components in percentage by weight:
vegetable oil and fat: 30% -50%;
plant powder: 10% -25%;
plant emulsifier: 3% -15%;
water phase components: 20% -48%, wherein the water phase component comprises water, a plant humectant, an ion stabilizer, a pH regulator and a plant preservative;
natural thickeners: 0.1% -3%;
other auxiliary agents: 0.2 to 4 percent.
2. The all-natural aqueous lip glaze according to claim 1, wherein the aqueous phase component comprises, in weight percent:
water: 20% -30%;
plant humectant: 2% -5%;
an ionic stabilizer: 0.2 to 1.0 percent;
pH regulator: 0.3% -1.5%;
plant preservative: 0.1 to 8 percent.
3. The all-natural aqueous lip glaze according to claim 2, wherein the plant humectant is selected from one or more of glycerin, propylene glycol and 1, 3-butanediol;
the ionic stabilizer is selected from one or more of sodium chloride, magnesium chloride and calcium chloride;
the pH regulator is selected from one or more of citric acid, malic acid, tartaric acid and gallic acid;
the plant preservative is one or more selected from pentanediol, 1,2 hexanediol, glyceryl caprylate, anisic acid and cortex Magnolia officinalis extract.
4. The all natural aqueous lip glaze according to any one of claims 1 to 3, wherein the vegetable oil or fat is selected from one or more of jojoba oil, sunflower seed oil, castor oil, coconut oil, grape seed oil, shea butter, meadowfoam seed oil, macadamia nut oil, olive oil, palm oil, squalane, cocoa butter, jojoba fat, glycolipids, octyldodecanol, caprylic capric triglyceride, coco-caprylic capric triglyceride, oleic/linoleic/linolenic polyglycerin esters, and dioctyldodecanol dimer linoleate.
5. The all-natural water-containing lip glaze according to any one of claims 1 to 3, wherein the plant powder comprises plant toner and a filler;
wherein the plant toner is selected from one or more of tomato red, beet red, safflower red, purple sweet potato, elderberry red and radish red;
the filler is selected from corn starch and/or rice starch.
6. An all natural aqueous lip glaze according to any one of claims 1 to 3, wherein the vegetable emulsifier is selected from one or more of polyglyceryl-3 diisostearate, polyglyceryl 2-dipolyhydroxystearate, polyglyceryl-2 isostearate, polyglyceryl 4-isostearate, polyglyceryl 3-polyricinoleate, polyglyceryl 6-polyricinoleate, glyceryl stearate, sorbitan isostearate, sorbitan oleate and sucrose cocoate.
7. The all natural aqueous lip glaze according to any one of claims 1 to 3, wherein the natural thickener is selected from one or more of sunflower seed wax, candelilla wax, behenyl tribehenate, carnauba wax, cercis green flower wax, tara gum, dextrin palmitate, dextrin isostearate, disteardimonium hectorite, silica gel and bentonite.
8. The all natural aqueous lip glaze according to any one of claims 1 to 3, wherein the other auxiliary agents comprise a plant antioxidant and a plant essential oil;
the plant antioxidant is selected from one or more of tocopherol, tocopherol acetate, ascorbyl palmitate, tea polyphenol and rice bran oil;
the plant essential oil is one or more selected from lemon peel oil, citronellol, lavender oil, rosemary essential oil, palmarosa oil and geranium oil.
9. A process for the preparation of an all natural aqueous lip gloss according to any one of claims 1 to 8, characterized in that it comprises:
adding the uniformly mixed water phase component into a mixture containing the vegetable oil and fat, the vegetable powder, the vegetable emulsifier and the natural thickener at the temperature of 60-80 ℃, and reacting to obtain an emulsified mixture;
and cooling the mixture to below 40 ℃, adding the other auxiliary agents, and uniformly stirring to obtain the all-natural water-containing lip glaze.
10. The method for preparing the all-natural water-containing lip glaze according to claim 9, wherein the rotation speed during stirring is 4000-8000 rpm; preferably, the rotation speed during stirring is 4500-6500 rpm.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105250154A (en) * | 2014-07-11 | 2016-01-20 | 玫琳凯有限公司 | Cosmetic compositions |
| CN110638691A (en) * | 2019-11-14 | 2020-01-03 | 广州那比昂生物科技有限公司 | Paint light mirror color-holding lip glaze and preparation method thereof |
| CN110897907A (en) * | 2019-12-11 | 2020-03-24 | 花安堂生物科技集团有限公司 | Water-in-oil lip glaze without PEG emulsifier and preparation method thereof |
| CN113262178A (en) * | 2021-03-31 | 2021-08-17 | 科丝美诗(中国)化妆品有限公司 | Moistened satin gloss lip glaze and preparation method thereof |
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- 2022-06-08 CN CN202210639115.XA patent/CN114869807A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105250154A (en) * | 2014-07-11 | 2016-01-20 | 玫琳凯有限公司 | Cosmetic compositions |
| CN110638691A (en) * | 2019-11-14 | 2020-01-03 | 广州那比昂生物科技有限公司 | Paint light mirror color-holding lip glaze and preparation method thereof |
| CN110897907A (en) * | 2019-12-11 | 2020-03-24 | 花安堂生物科技集团有限公司 | Water-in-oil lip glaze without PEG emulsifier and preparation method thereof |
| CN113262178A (en) * | 2021-03-31 | 2021-08-17 | 科丝美诗(中国)化妆品有限公司 | Moistened satin gloss lip glaze and preparation method thereof |
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