CN106798702A - Moistening type lipstick and preparation method thereof - Google Patents
Moistening type lipstick and preparation method thereof Download PDFInfo
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- CN106798702A CN106798702A CN201710177795.7A CN201710177795A CN106798702A CN 106798702 A CN106798702 A CN 106798702A CN 201710177795 A CN201710177795 A CN 201710177795A CN 106798702 A CN106798702 A CN 106798702A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 38
- 230000000694 effects Effects 0.000 claims abstract description 21
- 239000003381 stabilizer Substances 0.000 claims abstract description 20
- 238000011049 filling Methods 0.000 claims abstract description 18
- 239000003921 oil Substances 0.000 claims description 40
- 235000019198 oils Nutrition 0.000 claims description 40
- 244000000626 Daucus carota Species 0.000 claims description 34
- 235000002767 Daucus carota Nutrition 0.000 claims description 34
- 241000196324 Embryophyta Species 0.000 claims description 30
- 241000220317 Rosa Species 0.000 claims description 30
- 235000013311 vegetables Nutrition 0.000 claims description 30
- 239000006210 lotion Substances 0.000 claims description 26
- 239000000203 mixture Substances 0.000 claims description 18
- -1 glycerine Adipate ester Chemical class 0.000 claims description 17
- 230000001954 sterilising effect Effects 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 14
- 238000004040 coloring Methods 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 12
- 239000008158 vegetable oil Substances 0.000 claims description 12
- 239000004034 viscosity adjusting agent Substances 0.000 claims description 12
- 150000002148 esters Chemical class 0.000 claims description 11
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 claims description 10
- 206010020649 Hyperkeratosis Diseases 0.000 claims description 10
- 235000015097 nutrients Nutrition 0.000 claims description 10
- 229920001577 copolymer Polymers 0.000 claims description 9
- 238000012216 screening Methods 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 6
- 235000017060 Arachis glabrata Nutrition 0.000 claims description 5
- 244000105624 Arachis hypogaea Species 0.000 claims description 5
- 235000010777 Arachis hypogaea Nutrition 0.000 claims description 5
- 235000018262 Arachis monticola Nutrition 0.000 claims description 5
- 230000004069 differentiation Effects 0.000 claims description 5
- 239000000835 fiber Substances 0.000 claims description 5
- 239000008172 hydrogenated vegetable oil Substances 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 238000002347 injection Methods 0.000 claims description 5
- 239000007924 injection Substances 0.000 claims description 5
- VAMFXQBUQXONLZ-UHFFFAOYSA-N n-alpha-eicosene Natural products CCCCCCCCCCCCCCCCCCC=C VAMFXQBUQXONLZ-UHFFFAOYSA-N 0.000 claims description 5
- 235000020232 peanut Nutrition 0.000 claims description 5
- 238000005070 sampling Methods 0.000 claims description 5
- 238000007493 shaping process Methods 0.000 claims description 5
- 238000004659 sterilization and disinfection Methods 0.000 claims description 5
- 235000020238 sunflower seed Nutrition 0.000 claims description 5
- 229920000305 Nylon 6,10 Polymers 0.000 claims description 4
- 235000004433 Simmondsia californica Nutrition 0.000 claims description 4
- NPAXBRSUVYCZGM-UHFFFAOYSA-N carbonic acid;propane-1,2-diol Chemical compound OC(O)=O.CC(O)CO NPAXBRSUVYCZGM-UHFFFAOYSA-N 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- CXMXRPHRNRROMY-UHFFFAOYSA-N n-Decanedioic acid Natural products OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims description 4
- 229920001083 polybutene Polymers 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 3
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims description 3
- 229910001887 tin oxide Inorganic materials 0.000 claims description 3
- BJRXGOFKVBOFCO-UHFFFAOYSA-N 2-hydroxypropyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(C)O BJRXGOFKVBOFCO-UHFFFAOYSA-N 0.000 claims description 2
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 claims description 2
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims description 2
- 101001031591 Mus musculus Heart- and neural crest derivatives-expressed protein 2 Proteins 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 claims description 2
- 239000007765 cera alba Substances 0.000 claims description 2
- 238000005520 cutting process Methods 0.000 claims description 2
- 239000008367 deionised water Substances 0.000 claims description 2
- 229910021641 deionized water Inorganic materials 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000008236 heating water Substances 0.000 claims description 2
- 239000000155 melt Substances 0.000 claims description 2
- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 claims description 2
- 229960001173 oxybenzone Drugs 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 229940042585 tocopherol acetate Drugs 0.000 claims description 2
- 101000905241 Mus musculus Heart- and neural crest derivatives-expressed protein 1 Proteins 0.000 claims 1
- 241000221096 Simmondsia chinensis Species 0.000 claims 1
- 125000002252 acyl group Chemical group 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 230000006698 induction Effects 0.000 claims 1
- 229940057874 phenyl trimethicone Drugs 0.000 claims 1
- 239000004575 stone Substances 0.000 claims 1
- LINXHFKHZLOLEI-UHFFFAOYSA-N trimethyl-[phenyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound C[Si](C)(C)O[Si](O[Si](C)(C)C)(O[Si](C)(C)C)C1=CC=CC=C1 LINXHFKHZLOLEI-UHFFFAOYSA-N 0.000 claims 1
- 239000003086 colorant Substances 0.000 abstract description 3
- 239000002537 cosmetic Substances 0.000 abstract description 2
- 210000000554 iris Anatomy 0.000 description 13
- 239000004150 EU approved colour Substances 0.000 description 12
- 229940006093 opthalmologic coloring agent diagnostic Drugs 0.000 description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 7
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 5
- 241000109329 Rosa xanthina Species 0.000 description 5
- 235000004789 Rosa xanthina Nutrition 0.000 description 5
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 4
- 235000011187 glycerol Nutrition 0.000 description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 4
- 241000221095 Simmondsia Species 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 238000002242 deionisation method Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 230000010412 perfusion Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229930003799 tocopherol Natural products 0.000 description 3
- 229960001295 tocopherol Drugs 0.000 description 3
- 239000011732 tocopherol Substances 0.000 description 3
- 235000010384 tocopherol Nutrition 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- ONNSSMGRFLULCC-UHFFFAOYSA-N icosan-9-ol Chemical class CCCCCCCCCCCC(O)CCCCCCCC ONNSSMGRFLULCC-UHFFFAOYSA-N 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 2
- 229930003427 Vitamin E Natural products 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Insects & Arthropods (AREA)
- Zoology (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of cosmetics, in particular to a moistening type lipstick and a preparation method thereof, wherein the moistening type lipstick comprises the following components: 52-80% of an oil phase component, 14-31% of a water phase component, 2-8% of a plant active matter, 1-3% of a stabilizer, 1-3% of a viscosity regulator and 1-3% of a colorant, and the lipstick has the advantages of good makeup effect and good moistening effect; the preparation method of the moistening type lipstick comprises the following steps: the preparation method comprises the steps of preparing the plant active matter, preparing the paste, and filling.
Description
Technical field
The present invention relates to cosmetic technical field, and in particular to a kind of moist type lipstick and preparation method thereof.
Background technology
Lipstick is a kind of solid lipstick, and current lipstick needs to have both the effect of lip care in addition to possessing makeups effect, also.It is existing
Have the makeups lipstick in technology be reach preferable landscaping effect and its be attached to lip persistence, it is necessary to add a certain amount ofization
Part is studied, but above-mentioned chemical analysis does not have magnetic lubricant nature usually, so that doing easily occurs in lip after user is finished lipstick
The problem of decortication is split, however, because the lip care composition for moistening has surface tension higher, the chemical analysis of makeups can be influenceed attached
The property, so that makeups effect can not be balanced preferably with the moisturizing effect of lipstick.Accordingly, it would be desirable to upgrading is optimized to lipstick,
With ensure lipstick makeups effect and its moist lip moist degree, and then improve lipstick quality.
The content of the invention
There is one of above-mentioned technical problem, the object of the invention for prior art to be that a kind of makeups effect of offer is good, grow
The good lipstick of profit effect.
There is above-mentioned technical problem for prior art, the two of the object of the invention is to provide a kind of system of moist type lipstick
Preparation Method, the method has the advantages that preparation process is simple, low cost.
One of to achieve the above object, there is provided following technical scheme：
A kind of moist type lipstick, including following component are provided
Oil phase components 52 ~ 80%
Water phase component 14 ~ 31%
Vegetable active thing 2 ~ 8%
Stabilizer 1 ~ 3%
Viscosity modifier 1 ~ 3%
Colouring agent 1% ~ 3%.
Preferably, the oil phase includes many acyl group adipate esters -2, octyl dodecanol of double-two glycerine, the poly- diformazan of stearyl
Siloxanes, cera alba, VP/ eicosene copolymers, hydrogenated vegetable oil, Jojoba esters, decanedioic acid ethylhexyl, phenyl gather
In trimethicone, propylene glycol isostearate, C20-24 alkyl dimethicones, PPG-51/SMDI copolymers
One or more mixture.
Preferably, the water mutually includes the one kind or two in deionized water, vitamin E, OXYBENZONE, tocopherol acetate
Plant the mixture of the above.
Preferably, the stabilizer is two hard ester dimethylammonium hectorites.
Preferably, viscosity modifier includes the mixed of one or more in polybutene, polyethylene, propylene glycol carbonate
Compound.
Preferably, the colouring agent includes CI77891, CI19140, CI77891, CI19140, CI15850 and tin oxide
In one or more mixture.
To achieve the above object two, there is provided following technical scheme：
A kind of preparation method of above-mentioned moist type lipstick, comprises the following steps：
The preparation of step one, vegetable active thing
1）Sampling：Win the plant with vital activity；
2）Sterilizing：It is explant by the plant sterilization, the histoorgan for then cutting the plant after sterilizing；
3）Culture：The explant of gained is placed in Fiber differentiation in N6 solid mediums, the callus of plant is obtained；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：The preferable cell mass Secondary Culture of form, so as to obtain the cell mass of loose particles shape；
c）Suspend culture：Shaking culture is carried out during the cell mass of loose particles shape is moved to the shaking flask equipped with nutrient solution, is swum
From cell；
d）Screening：Free plant cell is filtered, the cell mass of screening individual cells or peanut is used as competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, vegetable active thing is obtained, it is stand-by；
The preparation of step 2, lotion
1）The oil phase components of formula ratio are weighed, is heated with certain temperature, then lowered the temperature so that the oil phase components mixing is equal
It is even, it is obtained and melts uniform oil phase；
2）The water phase component of formula ratio is weighed, the water phase component is heated with certain temperature, then sequentially add vegetable active
Thing and colouring agent, and stir, the vegetable active thing and the colouring agent is sufficiently mixed in the water phase, it is obtained mixed
Compound；
3）By 2）Mixture is obtained and adds 1）In obtained oil phase, formula is then added while stirring in a certain temperature conditions
The stabilizer of amount and the colouring agent of formula ratio, are obtained the lotion of lipstick；
It is step 3, filling
By the pre- heat fusing of the lotion, the lotion that will be melted is with certain filling speed and with the horizontal the filling of certain angle
In angle injection lipstick mould, will then be filled with the lipstick mould of lotion addition refrigerator and cool down certain hour, the demoulding is obtained
To the lipstick of shaping.
Preferably, in the step one, the time of Fiber differentiation is 2 ~ 4 weeks, and the algebraically of Secondary Culture was 2 ~ 5 generations, described
Plant is one or more in iris, Carrot Roots, rose, and the vegetable oil is sunflower seed oil.
Preferably, in the step 2,1）In with 60 ~ 90 DEG C heating oil phase components, be then down to 30 ~ 40 DEG C；2）In with
30 ~ 40 DEG C of heating water phase components；3）In with 50 ~ 70 DEG C while stirring add formula ratio stabilizers and formula ratio
Toner.
Preferably, in the step 3, preheating temperature is 70 ~ 90 DEG C, and filling speed is 5 ~ 8ml/s, filling angle is 25 ~
40 °, the temperature of the refrigerator is -15 ~ -8 DEG C, and cool time is 6 ~ 20min.
Beneficial effects of the present invention：
（1）A kind of moist type lipstick of the invention, the lipstick by the oil phase of formula ratio, the water phase of formula ratio, formula ratio plant
Active matter, the viscosity modifier of formula ratio, the stabilizer of formula ratio, the colouring agent of formula ratio are prepared from.With prior art phase
Than, the lipstick can prepare the lipstick matrix with makeups effect, and vegetable active thing is then added in the formula of lipstick matrix,
The vegetable active thing is formed by vegetable active cell and the vegetable oil configuration of ecosystem, can not only give full play to competent cell
Activity, and the competent cell is stored in oil-soluble vegetable oil, substantially increases the oil soluble effect of vegetable active thing, and then
Enable that competent cell is preferably dispersed in the matrix of lipstick, mix so as to the makeups chemical analysis preferably with lipstick,
And then under the makeups effect for ensureing lipstick, the moist lip care effect of lipstick can be substantially increased.
（2）A kind of preparation method of moist type lipstick of the invention can prepare the plant containing local plants cell and live
Property thing, and can regulating and controlling temperature fusing oil phase, water phase, colouring agent, vegetable active, stabilizer and viscosity modifier and mix it
Obtain lotion, then regulate and control filling temperature and filling speed and angle, so as to prepare with makeups effect it is good, moisten shield
The good lipstick of lip effect, the preparation method has simple, low production cost and can be applied to the characteristics of mass producing.
Specific embodiment
Embodiment 1.
A kind of moist type lipstick in the present embodiment, first weighs following component：5.2kg oil phase components, 3.1kg water phase groups
Part, 0.8kg vegetable actives thing, 0.3kg stabilizers, 0.3kg viscosity modifiers, 0.3kg colouring agents；
Wherein, 5.2kg oil phases include:The many acyl group adipate esters -2 of double-two glycerine of 0.2kg, 1kg octyl dodecanols, 0.8kg are stearic
Base dimethione, 0.3kg cera albas, 0.5kgVP/ eicosene copolymers, 0.5kg hydrogenated vegetable oils, 0.6kg decanedioic acid
Ethylhexyl, 0.8kg phenyl trimethicones, 0.5kgC20-24 alkyl dimethicones；
Wherein, 3.1kg water mutually includes deionization 1.6kg water, 0.5kg vitamin Es, 0.5kg OXYBENZONEs, 0.5kg tocopherol second
Acid esters；
Wherein, 0.3kg stabilizers are two hard ester dimethylammonium hectorites；
Wherein, 0.3kg viscosity modifiers include 0.1kg polybutene, 0.1kg polyethylene, 0.1kg propylene glycol carbonates；
Wherein, 0.3kg colouring agents include 0.1kgCI77891,0.1kgCI19140,0.1kgCI77891；
Preparation method is as follows：
The preparation of step one, vegetable active thing
1）Sampling：Win the iris plant with vital activity, Carrot Roots plant, rose flowering plant；
2）Sterilizing：By iris plant, Carrot Roots plant, rose flowering plant sterilization, the iris after sterilizing is then cut respectively
Plant, Carrot Roots plant, rose flowering plant are explant；
3）Culture：The iris explant of gained, Carrot Roots explant, rose explant are placed in N6 solid mediums and lured
Culture 2 weeks is led, iris, Carrot Roots, the callus of rose three is obtained；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen in iris, Carrot Roots, the callus of rose three from gained；
b）Secondary Culture：, so that it is loose to obtain iris, Carrot Roots, rose in the form preferable generation of cell mass Secondary Culture 2
The cell mass of graininess three；
c）Suspend culture：During the cell mass of iris, Carrot Roots, rose loose particles shape is moved to the shaking flask equipped with nutrient solution
Shaking culture is carried out, free cell is obtained；
d）Screening：The plant cell of free iris, Carrot Roots, rose three is filtered, individual cells or peanut is screened
Cell mass as competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, it is preferable that vegetable oil is sunflower seed oil, is obtained
It is stand-by to iris active matter, Carrot Roots active matter, rose active matter.
The preparation of step 2, lotion
1）Claim 5.2kg oil phase components, heated with 60 DEG C of temperature, then temperature is down to 30 DEG C so that the oil phase components mixing is equal
It is even, the well mixed oil phase of each component is obtained；
2）Claim 3.1kg water phase components, institute's water phase component is heated with 30 DEG C of temperature, then sequentially add vegetable active thing and coloring
Agent, and stir, 0.8kg vegetable actives thing and 0.3kg colouring agents is sufficiently mixed in the water phase, mixture is obtained；
Wherein, 0.8kg vegetable actives thing includes 0.2kg irises active matter, 0.3kg Carrot Roots active matter, 0.3kg rose active matters；
3）By 2）Mixture is obtained and adds 1）In obtained oil phase, 0.3kg is then added while stirring under the conditions of temperature 50 C
Stabilizer and 0.3kg colouring agents, are obtained the lotion of lipstick；
It is step 3, filling
1）With rate of flooding it is 5ml/s by the lotion of fusing by the lotion with the fusing of 70 DEG C of preheating temperature, perfusion angle is
In 25 ° of injection lipstick moulds, will then be filled with the lipstick mould of lotion -15 DEG C of refrigerators of addition and cool down 6min, the demoulding is obtained
To the lipstick of shaping.
Embodiment 2.
A kind of moist type lipstick in the present embodiment, first weighs following component：8kg oil phase components, 1.4kg water phases component,
0.2kg vegetable actives thing, 0.1kg stabilizers, 0.1kg viscosity modifiers, 0.1kg colouring agents；
Wherein, 8kg oil phases include:The many acyl group adipate esters -2 of double-two glycerine of 1kg, 0.5kg octyl dodecanols, 1kg stearyls
Dimethione, 0.5kg cera albas, 0.8kgVP/ eicosene copolymers, 0.9kg hydrogenated vegetable oils, 0.3kg jojoba esters
Class, 0.5kg decanedioic acid ethylhexyl, 0.5kg phenyl trimethicones, 1kg propylene glycol isostearates,
1.2kgC20-24 alkyl dimethicones, 0.8kgPPG-51/SMDI copolymers；
Wherein, 1.4kg water mutually includes deionization 0.8kg water, 0.2kg vitamin Es, 0.2kg OXYBENZONEs, 0.2kg tocopherol second
Acid esters；
Wherein, 0.1kg stabilizers are two hard ester dimethylammonium hectorites；
Wherein, 0.1kg viscosity modifiers include 0.05kg polybutene, 0.05kg propylene glycol carbonates；
Wherein, 0.1kg colouring agents include 0.05CI19140,0.02CI15850 and 0.03 tin oxide.
Preparation method is as follows：
The preparation of step one, vegetable active thing
1）Sampling：Win the Carrot Roots plant with vital activity, rose flowering plant；
2）Sterilizing：By Carrot Roots plant, rose flowering plant sterilization, then cut respectively the Carrot Roots plant after sterilizing,
Rose flowering plant is explant；
3）Culture：The Carrot Roots explant of gained, rose explant are placed in Fiber differentiation 4 weeks in N6 solid mediums, are obtained
To Carrot Roots, the callus of both roses；
4）The preparation of competent cell：
a）Carrot Roots from gained, the selection preferable cell mass of body in the callus of both roses；
b）Secondary Culture：In the form preferable generation of cell mass Secondary Culture 5, thus obtain Carrot Roots, both roses it is loose
Granular cell mass；
c）Suspend culture：Shaken during the cell mass of Carrot Roots, rose loose particles shape is moved to the shaking flask equipped with nutrient solution
Bottle culture, obtains free cell；
d）Screening：Free Carrot Roots, rose plant cell are filtered, the cell mass of screening individual cells or peanut is made
It is competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, it is preferable that vegetable oil is sunflower seed oil, is obtained
It is stand-by to Carrot Roots active matter, rose active matter.
The preparation of step 2, lotion
1）Claim 8kg oil phase components, heated with 90 DEG C of temperature, then temperature is down to 40 DEG C so that the oil phase components are well mixed,
The well mixed oil phase of each component is obtained；
2）Claim 1.4kg water phase components, institute's water phase component is heated with 40 DEG C of temperature, then sequentially add vegetable active thing and coloring
Agent, and stir, 0.7kg vegetable actives thing and 0.1kg colouring agents is sufficiently mixed in the water phase, mixture is obtained；
Wherein, 0.7kg vegetable actives thing includes 0.3kg Carrot Roots active matter, 0.4kg rose active matters；
3）By 2）Mixture is obtained and adds 1）In obtained oil phase, 0.1kg is then added while stirring under the conditions of temperature 70 C
Stabilizer and 0.1kg colouring agents, are obtained the lotion of lipstick；
It is step 3, filling
With rate of flooding it is 8ml/s by the lotion of fusing by the lotion with the fusing of 90 DEG C of preheating temperature, perfusion angle is 40 °
In injection lipstick mould, will then be filled with the lipstick mould of lotion -8 DEG C of refrigerators of addition and cool down 20min, the demoulding is obtained
The lipstick of shaping.
The present embodiment 3.
A kind of moist type lipstick in the present embodiment, first weighs following component：6.9kg oil phase components, 2kg water phases component,
0.5kg vegetable actives thing, 0.2kg stabilizers, 0.2kg viscosity modifiers, 0.2kg colouring agents；
Wherein, 6.9kg oil phases include:The double many acyl group adipate esters -2 of-two glycerine of 1kg, 1kg stearyls dimethione,
0.9kg cera albas, 0.5kgVP/ eicosene copolymers, 0.9kg hydrogenated vegetable oils, 0.5kg Jojobas esters, 0.5kg phenyl
Poly- trimethicone, 0.3kg propylene glycol isostearates, 0.5kgC20-24 alkyl dimethicones, 0.8kgPPG-
51/SMDI copolymers.
Wherein, 2kg water mutually includes deionization 0.8kg water, 1kg OXYBENZONEs, 0.2kg tocopherol acetates.
Wherein, 0.2kg stabilizers are two hard ester dimethylammonium hectorites；
Wherein, 0.2kg viscosity modifiers are propylene glycol carbonates；
Wherein, 0.3kg colouring agents include 0.1kgCI77891,0.1kgCI19140,0.1kgCI19140；
Preparation method is as follows：
The preparation of step one, vegetable active thing
1）Sampling：Win the Carrot Roots plant with vital activity, rose flowering plant；
2）Sterilizing：By Carrot Roots plant, rose flowering plant sterilization, then cut respectively the Carrot Roots plant after sterilizing,
Rose flowering plant is explant；
3）Culture：The Carrot Roots explant of gained, rose explant are placed in Fiber differentiation 3 weeks in N6 solid mediums, are obtained
To Carrot Roots, rose callus；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen in Carrot Roots, rose callus from gained；
b）Secondary Culture：, so as to obtain Carrot Roots, rose loose particles shape in the form preferable generation of cell mass Secondary Culture 4
Cell mass；
c）Suspend culture：During the cell mass of Carrot Roots, the loose particles shape of both roses is moved to the shaking flask equipped with nutrient solution
Shaking culture is carried out, free cell is obtained；
d）Screening：The plant cell of free Carrot Roots, both roses is filtered, screening individual cells or peanut it is thin
Born of the same parents group is used as competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, it is preferable that vegetable oil is sunflower seed oil, is obtained
It is stand-by to Carrot Roots active matter, rose active matter.
The preparation of step 2, lotion
1）Claim 6.9kg oil phase components, heated with 80 DEG C of temperature, then temperature is down to 35 DEG C so that the oil phase components mixing is equal
It is even, the well mixed oil phase of each component is obtained；
2）Claim 2kg water phase components, institute's water phase component heated with 35 DEG C of temperature, then sequentially add vegetable active thing and colouring agent,
And stir, 0.5kg vegetable actives thing and 0.2kg colouring agents is sufficiently mixed in the water phase, mixture is obtained；Its
In, 0.5kg vegetable actives thing includes 0.3kg irises active matter, 0.2kg rose active matters；
3）By 2）Mixture is obtained and adds 1）In obtained oil phase, 0.2kg is then added while stirring under the conditions of temperature 60 C
Stabilizer and 0.2kg colouring agents, are obtained the lotion of lipstick；
It is step 3, filling
With rate of flooding it is 6ml/s by the lotion of fusing by the lotion with the fusing of 80 DEG C of preheating temperature, perfusion angle is 30 °
In injection lipstick mould, will then be filled with the lipstick mould of lotion -10 DEG C of refrigerators of addition and cool down 10min, the demoulding is obtained
The lipstick of shaping.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than the present invention is protected
The limitation of scope is protected, although being explained to the present invention with reference to preferred embodiment, one of ordinary skill in the art should
Work as understanding, technical scheme can be modified or equivalent, without deviating from the reality of technical solution of the present invention
Matter and scope.
Claims (10)
1. a kind of moist type lipstick, it is characterized in that：Including following component
Oil phase components 52 ~ 80%
Water phase component 14 ~ 31%
Vegetable active thing 2 ~ 8%
Stabilizer 1 ~ 3%
Viscosity modifier 1 ~ 3%
Colouring agent 1% ~ 3%.
2. a kind of moist type lipstick according to claim 1, it is characterized in that：The oil phase includes many acyl groups of double-two glycerine
Adipate ester -2, octyl dodecanol, stearyl dimethione, cera alba, VP/ eicosene copolymers, hydrogenated vegetable oil,
Jojoba esters, decanedioic acid ethylhexyl, phenyl trimethicone, propylene glycol isostearate, C20-24 alkyl gather
One or more mixture in dimethyl siloxane, PPG-51/SMDI copolymers.
3. a kind of moist type lipstick according to claim 1, it is characterized in that：The water mutually includes deionized water, micro-element
One or more mixture in E, OXYBENZONE, tocopherol acetate.
4. a kind of moist type lipstick according to claim 1, it is characterized in that：The stabilizer is that two hard ester dimethylammonium lithiums are covered
De- stone.
5. a kind of moist type lipstick according to claim 1, it is characterized in that：Viscosity modifier include polybutene, polyethylene,
One or more mixture in propylene glycol carbonate.
6. a kind of moist type lipstick according to claim 1, it is characterized in that：The colouring agent include CI77891,
One or more mixture in CI19140, CI77891, CI19140, CI15850 and tin oxide.
7. the preparation method of a kind of magnetic profit type lipstick as described in claim 1 to 6 any one, it is characterized in that：Including following
Step：
The preparation of step one, vegetable active thing
1）Sampling：Win the plant with vital activity；
2）Sterilizing：It is explant by the plant sterilization, the histoorgan for then cutting the plant after sterilizing；
3）Culture：The explant of gained is placed in Fiber differentiation in N6 solid mediums, the callus of plant is obtained；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：The preferable cell mass Secondary Culture of form, so as to obtain the cell mass of loose particles shape；
c）Suspend culture：Shaking culture is carried out during the cell mass of loose particles shape is moved to the shaking flask equipped with nutrient solution, is swum
From cell；
d）Screening：Free plant cell is filtered, the cell mass of screening individual cells or peanut is used as competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, vegetable active thing is obtained, it is stand-by；
The preparation of step 2, lotion
1）The oil phase components of formula ratio are weighed, is heated with certain temperature, then lowered the temperature so that the oil phase components mixing is equal
It is even, it is obtained and melts uniform oil phase；
2）The water phase component of formula ratio is weighed, the water phase component is heated with certain temperature, then sequentially add vegetable active
Thing and colouring agent, and stir, the vegetable active thing and the colouring agent is sufficiently mixed in the water phase, it is obtained mixed
Compound；
3）By 2）Mixture is obtained and adds 1）In obtained oil phase, formula is then added while stirring in a certain temperature conditions
The stabilizer of amount and the colouring agent of formula ratio, are obtained the lotion of lipstick；
It is step 3, filling
By the pre- heat fusing of the lotion, the lotion that will be melted is with certain filling speed and with the horizontal the filling of certain angle
In angle injection lipstick mould, will then be filled with the lipstick mould of lotion addition refrigerator and cool down certain hour, the demoulding is obtained
To the lipstick of shaping.
8. the preparation method of a kind of moist type lipstick according to claim 7, it is characterized in that：In the step one, induction
The time of culture is 2 ~ 4 weeks, and the algebraically of Secondary Culture was 2 ~ 5 generations, and the plant is the one kind in iris, Carrot Roots, rose
Or it is two or more, the vegetable oil is sunflower seed oil.
9. the preparation method of a kind of easily filling lipstick according to claim 7, it is characterized in that：In the step 2,1）
In with 60 ~ 90 DEG C heating oil phase components, be then down to 30 ~ 40 DEG C；2）In with 30 ~ 40 DEG C of heating water phase components；3）In with
The colouring agent of 50 ~ 70 DEG C of stabilizers for adding formula ratio while stirring and formula ratio.
10. the preparation method of a kind of easily filling lipstick according to claim 7, it is characterized in that：In the step 3, in advance
Hot temperature is 70 ~ 90 DEG C, and filling speed is 5 ~ 8ml/s, and filling angle is 25 ~ 40 °, and the temperature of the refrigerator is -15 ~ -8
DEG C, cool time is 6 ~ 20min.
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| CN108938497A (en) * | 2018-09-21 | 2018-12-07 | 娇时日化（杭州）股份有限公司 | A kind of bloom rich in extracted form natural plant moistens solid lip gloss and its production technology |
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