CN109125138B - Moisturizing and high-gloss lipstick and preparation method thereof - Google Patents

Abstract

The invention discloses a moistening and high-gloss lipstick and a preparation method thereof, belonging to the technical field of cosmetics, and the lipstick comprises a thickening agent, a film-forming agent, a coloring agent, a skin-moistening agent and an effect additive, wherein the effect additive consists of an effect additive I and an effect additive II, the effect additive I is a mixture of wild soybean oil, a carrot root extract and beta-carotene, and the effect additive II is tocopherol; the mass percentage of the efficacy additive I and the efficacy additive II in the lipstick are respectively 0.1-5% and 0.1-0.5%; in addition, the preparation process of the lipstick is simple, and the prepared lipstick has good moistening and high-gloss effects.

Description

Moisturizing and high-gloss lipstick and preparation method thereof

Technical Field

The invention belongs to the technical field of cosmetics, and particularly relates to a moistening and high-gloss lipstick and a preparation method thereof.

Background

With the improvement of living standard, people have higher and higher requirements on life, especially the image of the people. Lipstick is a daily cosmetic, and is popular with women. At present, the lipstick sold in the market is various, including lipstick, alcohol stick, lip gloss, lip glaze and the like. However, the existing lipsticks have the following defects: has poor moistening and repairing effects.

Therefore, there is a need to design a new lipstick for improving moistening and repairing effects.

Disclosure of Invention

The invention aims to overcome the defects in the prior art and provide the moisturizing and high-gloss lipstick and the preparation method thereof.

In order to achieve the purpose, the invention adopts the technical scheme that: a moistening and high-gloss lipstick comprises a thickening agent, a film-forming agent, a coloring agent, an emollient and an effect additive, wherein the effect additive consists of an effect additive I and an effect additive II, the effect additive I is a mixture of wild soybean oil, carrot root extract and beta-carotene, and the effect additive II is tocopherol; the weight percentage of the efficacy additive I and the efficacy additive II in the lipstick are respectively 0.1-5% and 0.1-0.5%.

The carrot root extract can strengthen red blood cells, improve skin color, make skin more compact and elastic, become young and active, and lighten senile plaques; it is the first-aid of the premature aging skin. The wild soybean oil can be used as epidermal growth factor for regulating skin. The beta-carotene can absorb ultraviolet ray, and prevent skin aging and blackening. The efficacy additive is compounded by efficacy additive I and tocopherol, the mass percentage of the efficacy additive I and the tocopherol in the lipstick are respectively limited to 0.1-5% and 0.1-0.5%, and the efficacy additive I and the tocopherol have the efficacies of synergistically moistening and repairing lips: improving skin color, resisting aging, removing wrinkle, and promoting epidermal cell regeneration; has good repairing effect on symptoms such as dry lips, cracking and the like, and promotes wound scarring.

As an improvement of the technical scheme, the emollient is composed of octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerol cross-linked polymer, tridecyl alcohol trimellitate and sucrose acetate isobutyrate, and the mass percentage of the emollient in the lipstick is 65% -90%.

As a further improvement of the technical scheme, the mass ratio of the octyldodecanol, the isononyl isononanoate, the hydrogenated polyisobutene, the diisostearyl malate, the trimethylpentanediol/hexanediol/glycerin cross-linked polymer, the tridecyl alcohol trimellitate and the sucrose acetate isobutyrate is (5-30): 2-30): 5-30): 1-8): 5-50): 1-10.

The glycosyl of the sucrose acetate isobutyrate is plant-derived food-grade sucrose molecules, and the natural sucrose molecules are introduced to ensure that the sucrose acetate isobutyrate has very good biodegradation performance and can be absorbed by human bodies without stimulation to skin and eyes; sucrose acetate isobutyrate is close to sebum secreted by human skin in performance and has no irritation; the lipstick not only increases the skin luster, but also enhances the stability of the oil phase in the formula system and improves the water resistance of the lipstick. The emollient of lipstick of the invention is compounded by the above 7 compounds, the 7 compounds can synergistically moisten lips: the lips were moisturized.

As an improvement of the technical scheme, the thickening agent consists of microcrystalline wax, polyethylene and synthetic wax, and the mass percentage of the thickening agent in the lipstick is 3% -20%; the mass ratio of the microcrystalline wax to the polyethylene to the synthetic wax is (1-15): (2-15): 2-15).

As an improvement of the technical scheme, the colorant consists of calcium lake CI15850, red No. 6 sodium salt CI15850 and CI77499, and the mass percentage of the colorant in the lipstick is 4-20%; the mass ratio of the calcium lake CI15850 to the red No. 6 sodium salt CI15850 to the CI77499 is (0.1-15): (0.5-20): 0.1-20).

As an improvement of the technical scheme, the lipstick comprises 0.5-15% of the film forming agent by mass, and the film forming agent is a mixture of hydrogenated polycyclopentadiene, polyethylene, carnauba wax and vitamins.

The film forming agent is compounded by 4 compounds, the compound has the specific proportion of wax and resin, and can show the unique cooperativity of all components; it has high adhesion and staining properties, improves the water, rub and transfer resistance of the formulation, and imparts gloss and helps suspend the pigment.

As an improvement of the technical scheme, the lipstick consists of the following components in percentage by mass: 0.1-5% of efficacy additive I, 0.1-0.5% of efficacy additive II, 65-90% of emollient, 3-20% of thickening agent, 4-20% of colorant and 0.5-15% of film-forming agent;

the skin-moistening agent consists of octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerol cross-linked polymer, tridecyl alcohol trimellitate and sucrose acetate isobutyrate in a mass ratio of (5-30): 2-30: (5-30): 1-8): 5-50: (1-10);

the thickening agent consists of microcrystalline wax, polyethylene and synthetic wax in a mass ratio of (1-15) - (2-15);

the colorant comprises (by mass ratio) 0.1-15: 0.5-20: 0.1-20 calcium lake CI15850, red No. 6 sodium salt CI15850 and CI 77499;

the film forming agent is a mixture of hydrogenated polycyclopentadiene, polyethylene, carnauba wax and vitamins.

As a further improvement of the technical scheme, the lipstick consists of the following components in percentage by mass: 0.5% of effect additive I, 0.3% of effect additive II, 74.68% of emollient, 12.36% of thickening agent, 10.16% of colorant and 2% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 19.38:14:4.5:11:2.8:18:5, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 1.86:5.5:5, and the mass ratio of calcium lake CI15850, sodium salt Red No. 6 CI15850 and CI77499 in the colorant was 7.67:1.83: 0.66.

In addition, the invention also provides a preparation method of the lipstick, which comprises the following steps:

s1) adding microcrystalline wax, polyethylene, synthetic wax and film forming agent into a dissolving pot, and heating to 90-95 ℃ until the microcrystalline wax, the polyethylene, the synthetic wax and the film forming agent are completely melted;

s2) adding octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerol cross-linked polymer and tridecyl alcohol trimellitate into a dissolving pot, stirring until the mixture is uniformly dispersed, and cooling to 80 ℃ to obtain a mixture I;

s3) adding calcium lake CI15850, red 6 sodium salt CI15850 and CI77499 into the mixture I, uniformly mixing, and grinding until toner is completely dispersed to obtain a mixture II;

s4) heating the mixture II to 85-90 ℃, fully stirring and uniformly dispersing, and then cooling to 65 ℃;

s5) adding the efficacy additive I, sucrose acetate isobutyrate and tocopherol into the mixture II subjected to cooling treatment, uniformly stirring, taking out of the pot, and sealing for storage.

The invention has the beneficial effects that: the invention provides a moistening and high-gloss lipstick and a preparation method thereof, and the moistening and high-gloss lipstick has the following advantages:

1) the efficacy additive is compounded by efficacy additive I and tocopherol, and has the efficacy of synergistically moistening and repairing lips: improving skin color, resisting aging, removing wrinkle, and promoting epidermal cell regeneration; the product has good repairing effect on symptoms such as dry lips and cracks, and can promote wound scarring;

2) the emollient is compounded by the 7 compounds, and the 7 compounds can synergistically moisten lips: moisturizing the lips;

3) the sucrose acetate isobutyrate is added into the lipstick, so that the makeup holding effect of the lipstick can be greatly improved, and the pigment is prevented from migrating; in addition, the sucrose acetate isobutyrate has very high refractive index (1.45), can obviously improve the glossiness of the lipstick and endow the lipstick with gorgeous visual effect, and meanwhile, the hydrogenated polycyclopentadiene and the trimethylpentanediol/hexanediol/glycerin cross-linked polymer can be spread on the surface of lips, so that the moistening degree of the lipstick is improved, and the glossiness is better after use;

4) the preparation method of the lipstick is simple and easy to operate, and is suitable for popularization and production.

Detailed Description

To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.

In the following examples, the "film former (mixture of hydrogenated polycyclopentadiene, polyethylene, carnauba wax and vitamins)" is sold under the trade name Koboguard HRPC, the "calcium lake CI 15850" is sold under the trade name C19-7711, the "red 6 sodium salt CI 15850" is sold under the trade name C19-6619, the "CI 77499" is sold under the trade name C33-5198, the "efficacy additive i (mixture of wild soybean Oil, Carrot root extract and β -carotene)" is sold under the trade name Carrot Oil CLR, the "sucrose acetate isobutyrate" is sold under the trade name binetor SAAB, and the "efficacy additive ii tocopherol" is sold under the trade name DECANOX ts-50.

Example 1

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 0.5% of effect additive I, 0.3% of effect additive II, 74.68% of emollient, 12.36% of thickening agent, 10.16% of colorant and 2% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 19.38:14:4.5:11:2.8:18:5, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 1.86:5.5:5, and the mass ratio of calcium lake CI15850, sodium salt Red No. 6 CI15850 and CI77499 in the colorant was 7.67:1.83: 0.66.

In addition, the invention also provides a preparation method of the lipstick, which comprises the following steps:

s1) adding microcrystalline wax, polyethylene, synthetic wax and film forming agent into a dissolving pot, and heating to 90-95 ℃ until the microcrystalline wax, the polyethylene, the synthetic wax and the film forming agent are completely melted;

s2) adding octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerol cross-linked polymer and tridecyl alcohol trimellitate into a dissolving pot, stirring until the mixture is uniformly dispersed, and cooling to 80 ℃ to obtain a mixture I;

s3) adding calcium lake CI15850, No. 6 red sodium salt CI15850 and CI77499 into the mixture I, uniformly mixing, and grinding until the toner is completely dispersed to obtain a mixture II;

s4) heating the mixture II to 85-90 ℃, fully stirring and uniformly dispersing, and then cooling to 65 ℃;

s5) adding the efficacy additive I, sucrose acetate isobutyrate and tocopherol into the mixture II subjected to cooling treatment, uniformly stirring, taking out of the pot, and sealing for storage.

Example 2

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 0.1% of effect additive I, 0.5% of effect additive II, 65% of emollient, 3% of thickening agent, 20% of colorant and 11.4% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 5:5:7:19:1:26:1, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 1:2:15, and the mass ratio of calcium lake CI15850, Red No. 6 sodium salt CI15850 and CI77499 in the colorant was 15:0.5: 20.

In addition, the present invention also provides a method for preparing the lipstick, which can refer to example 1.

Example 3

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 5% of effect additive I, 0.4% of effect additive II, 79.1% of emollient, 11% of thickening agent, 4% of colorant and 0.5% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 21.38:30:2:5:8:5:7.5, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 6.8:10.5:2, and the mass ratio of calcium lake CI15850, sodium salt No. Red 158CI 50 and CI77499 in the colorant was 0.1:12.3: 0.1.

In addition, the present invention also provides a method for preparing the lipstick, which can refer to example 1.

Example 4

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 4% of effect additive I, 0.1% of effect additive II, 82% of emollient, 6% of thickening agent, 7% of colorant and 0.9% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 29.38:8:17:21:6.8:28:6.3, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 12.8:9.5:4, and the mass ratio of calcium lake CI15850, sodium salt Red No. 6 CI15850 and CI77499 in the colorant was 7.67:20: 20.

In addition, the present invention also provides a method for preparing the lipstick, which can refer to example 1.

Example 5

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 2% of effect additive I, 0.3% of effect additive II, 90% of emollient, 3% of thickening agent, 4% of colorant and 0.7% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 30:7:30:8:7:50:5, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 15:14.5:3.5, and the mass ratio of calcium lake CI15850, sodium Red No. 6 CI15850 and CI77499 in the colorant was 7.67:0.5: 10.

In addition, the present invention also provides a method for preparing the lipstick, which can refer to example 1.

Example 6

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 0.1% of effect additive I, 0.4% of effect additive II, 67% of emollient, 20% of thickening agent, 7% of colorant and 5.5% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 6.3:7:2:30:1:18:10, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 1.86:15:5, and the mass ratio of calcium lake CI15850, sodium Red No. 6 CI15850 and CI77499 in the colorant was 7.67:1.83: 0.66.

In addition, the present invention also provides a method for preparing the lipstick, which can refer to example 1.

Example 7

The implementation provides a moistening and high-gloss lipstick which comprises the following components in percentage by mass: 0.5% of effect additive I, 0.3% of effect additive II, 70% of emollient, 5% of thickening agent, 9.2% of colorant and 15% of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 29.8:5:4.5:11:2.8:18:3, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 12.86:5.5:5, and the mass ratio of calcium lake CI15850, sodium salt Red No. 6 CI15850 and CI77499 in the colorant was 12.8:1.83: 17.

In addition, the present invention also provides a method for preparing the lipstick, which can refer to example 1.

Comparative example 1

This comparative example provides a moisturizing and high gloss lipstick, which differs from example 1 in that: the functional additive is a functional additive I, and the mass percentage of the functional additive I in the lipstick is 0.8%.

In addition, reference is made to example 1 for a method of making the comparative lipstick.

Comparative example 2

This comparative example provides a moisturizing and high gloss lipstick, which differs from example 1 in that: the emollient consists of octyl dodecanol, isononyl isononanoate and hydrogenated polyisobutene in a mass ratio of 19.38:14:4.5, and the mass percentage of the emollient in the lipstick is 74.68%.

In addition, reference is made to example 1 for a method of making the comparative lipstick.

A study was conducted with the lipsticks prepared in examples 1-3 and comparative examples 1 and 2, 500 female volunteers were selected and randomly divided into 5 groups, and the volunteers were applied with the lipstick 1 time a day in the morning and the usage of the volunteers was recorded after 40 days as shown in Table 1.

TABLE 1

As shown in Table 1, compared with the lipstick prepared by the comparative example, the lipsticks prepared by the embodiments 1-3 of the invention have better moisturizing effect and repairing effect; in addition, the lipsticks prepared in other embodiments of the invention can also achieve the effect similar to the lipsticks prepared in embodiments 1-3; therefore, when the weight percentage of the effect additive I and the effect additive II in the lipstick are respectively 0.1-5% and 0.1-0.5%, the moistening effect and the repairing effect of the lipstick are better.

Finally, it should be noted that the above embodiments are intended to illustrate the technical solutions of the present invention and not to limit the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications and equivalent substitutions can be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (7)

1. The moistening and high-gloss lipstick is characterized by comprising a thickening agent, a film forming agent, a coloring agent, an emollient and an effect additive, wherein the effect additive consists of an effect additive I and an effect additive II, the effect additive I is a mixture of wild soybean oil, carrot root extract and beta-carotene, and the effect additive II is tocopherol; the mass percentage of the efficacy additive I and the efficacy additive II in the lipstick are respectively 0.1-5% and 0.1-0.5%; the emollient is composed of octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate; the mass ratio of the octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin cross-linked polymer, tridecanol trimellitate and sucrose acetate isobutyrate is (5-30): 2-30): 5-30): 1-8): 5-50): 1-10; the weight percentage of the emollient in the lipstick is 65% -90%.

2. The lipstick as claimed in claim 1, wherein the thickener is composed of microcrystalline wax, polyethylene and synthetic wax, and is present in the lipstick in an amount of 3% to 20% by mass; the mass ratio of the microcrystalline wax to the polyethylene to the synthetic wax is (1-15): (2-15): 2-15).

3. The lipstick as claimed in claim 1, wherein the colorant is composed of calcium lake CI15850, red No. 6 sodium salt CI15850 and CI77499, and the mass percentage of the colorant in the lipstick is 4% -20%; the mass ratio of the calcium lake CI15850 to the red No. 6 sodium salt CI15850 to the CI77499 is (0.1-15): (0.5-20): 0.1-20).

4. The lipstick according to claim 1, wherein the film forming agent is 0.5% to 15% by mass of the lipstick, and the film forming agent is a mixture of hydrogenated polycyclopentadiene, polyethylene, carnauba wax, and vitamins.

5. The lipstick according to claim 1, comprising the following components in percentage by mass: 0.1-5% of an efficacy additive I, 0.1-0.5% of an efficacy additive II, 65-90% of an emollient, 3-20% of a thickener, 4-20% of a colorant and 0.5-15% of a film-forming agent;

the skin-moistening agent consists of octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerol cross-linked polymer, tridecyl alcohol trimellitate and sucrose acetate isobutyrate in a mass ratio of (5-30): 2-30: (5-30): 1-8): 5-50: (1-10);

the thickening agent consists of microcrystalline wax, polyethylene and synthetic wax in a mass ratio of (1-15) - (2-15);

the colorant comprises (by mass ratio) 0.1-15: 0.5-20: 0.1-20 calcium lake CI15850, red No. 6 sodium salt CI15850 and CI 77499;

the film forming agent is a mixture of hydrogenated polycyclopentadiene, polyethylene, carnauba wax and vitamins.

6. The lipstick according to claim 5, comprising the following components in percentage by mass: 0.5 percent of efficacy additive I, 0.3 percent of efficacy additive II, 74.68 percent of emollient, 12.36 percent of thickening agent, 10.16 percent of colorant and 2 percent of film-forming agent;

the mass ratio of octyldodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerin crosspolymer, tridecyl trimellitate and sucrose acetate isobutyrate in the emollient was 19.38:14:4.5:11:2.8:18:5, the mass ratio of microcrystalline wax, polyethylene and synthetic wax in the thickener was 1.86:5.5:5, and the mass ratio of calcium lake CI15850, sodium salt Red No. 6 CI15850 and CI77499 in the colorant was 7.67:1.83: 0.66.

7. A method of preparing a lipstick as claimed in claim 5 or claim 6, comprising the steps of:

s1) adding microcrystalline wax, polyethylene, synthetic wax and film forming agent into a dissolving pot, and heating to 90-95 ℃ until the microcrystalline wax, the polyethylene, the synthetic wax and the film forming agent are completely melted;

s2) adding octyl dodecanol, isononyl isononanoate, hydrogenated polyisobutene, diisostearyl malate, trimethylpentanediol/hexanediol/glycerol cross-linked polymer and tridecyl alcohol trimellitate into a dissolving pot, stirring until the mixture is uniformly dispersed, and cooling to 80 ℃ to obtain a mixture I;

s3) adding calcium lake CI15850, red 6 sodium salt CI15850 and CI77499 into the mixture I, uniformly mixing, and grinding until toner is completely dispersed to obtain a mixture II;

s4) heating the mixture II to 85-90 ℃, fully stirring and uniformly dispersing, and then cooling to 65 ℃;

s5) adding the efficacy additive I, sucrose acetate isobutyrate and tocopherol into the mixture II subjected to cooling treatment, uniformly stirring, taking out of the pot, and sealing for storage.