CN106821951A - Easily-filled lipstick and preparation method thereof - Google Patents
Easily-filled lipstick and preparation method thereof Download PDFInfo
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- CN106821951A CN106821951A CN201710178394.3A CN201710178394A CN106821951A CN 106821951 A CN106821951 A CN 106821951A CN 201710178394 A CN201710178394 A CN 201710178394A CN 106821951 A CN106821951 A CN 106821951A
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- lipstick
- preparation
- oil
- plant
- lotion
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- 238000002360 preparation method Methods 0.000 title claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000003381 stabilizer Substances 0.000 claims abstract description 16
- 230000000694 effects Effects 0.000 claims abstract description 7
- 239000003921 oil Substances 0.000 claims description 38
- 235000019198 oils Nutrition 0.000 claims description 38
- 244000000626 Daucus carota Species 0.000 claims description 33
- 235000002767 Daucus carota Nutrition 0.000 claims description 33
- 239000006210 lotion Substances 0.000 claims description 33
- 235000013311 vegetables Nutrition 0.000 claims description 29
- 241000196324 Embryophyta Species 0.000 claims description 26
- 235000011201 Ginkgo Nutrition 0.000 claims description 23
- 235000008100 Ginkgo biloba Nutrition 0.000 claims description 23
- 239000000203 mixture Substances 0.000 claims description 23
- 238000002844 melting Methods 0.000 claims description 20
- 230000008018 melting Effects 0.000 claims description 20
- 239000003795 chemical substances by application Substances 0.000 claims description 19
- 230000001954 sterilising effect Effects 0.000 claims description 18
- 238000004040 coloring Methods 0.000 claims description 15
- 239000004034 viscosity adjusting agent Substances 0.000 claims description 13
- 206010020649 Hyperkeratosis Diseases 0.000 claims description 10
- -1 Polyethylene Polymers 0.000 claims description 10
- 125000005456 glyceride group Chemical group 0.000 claims description 10
- 235000015097 nutrients Nutrition 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000004659 sterilization and disinfection Methods 0.000 claims description 8
- BANXPJUEBPWEOT-UHFFFAOYSA-N 2-methyl-Pentadecane Chemical compound CCCCCCCCCCCCCC(C)C BANXPJUEBPWEOT-UHFFFAOYSA-N 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 238000012216 screening Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000000835 fiber Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 claims description 5
- 235000019482 Palm oil Nutrition 0.000 claims description 5
- 239000004952 Polyamide Substances 0.000 claims description 5
- 239000004698 Polyethylene Substances 0.000 claims description 5
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 229920006037 cross link polymer Polymers 0.000 claims description 5
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 5
- 235000019866 hydrogenated palm kernel oil Nutrition 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 239000000155 melt Substances 0.000 claims description 5
- 239000002540 palm oil Substances 0.000 claims description 5
- 229920002647 polyamide Polymers 0.000 claims description 5
- 229920000573 polyethylene Polymers 0.000 claims description 5
- 238000005070 sampling Methods 0.000 claims description 5
- 229920005573 silicon-containing polymer Polymers 0.000 claims description 5
- 235000020238 sunflower seed Nutrition 0.000 claims description 5
- 235000017060 Arachis glabrata Nutrition 0.000 claims description 4
- 244000105624 Arachis hypogaea Species 0.000 claims description 4
- 235000010777 Arachis hypogaea Nutrition 0.000 claims description 4
- 235000018262 Arachis monticola Nutrition 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 230000004069 differentiation Effects 0.000 claims description 4
- 235000020232 peanut Nutrition 0.000 claims description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
- 239000008158 vegetable oil Substances 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- DMBUODUULYCPAK-UHFFFAOYSA-N 1,3-bis(docosanoyloxy)propan-2-yl docosanoate Chemical compound CCCCCCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCCCCCC DMBUODUULYCPAK-UHFFFAOYSA-N 0.000 claims description 2
- 229940043268 2,2,4,4,6,8,8-heptamethylnonane Drugs 0.000 claims description 2
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims description 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 2
- 241000220317 Rosa Species 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 238000005520 cutting process Methods 0.000 claims description 2
- PDYOTPOJFZAOIS-UHFFFAOYSA-N decanoic acid;2,2-dimethylpropane-1,3-diol;octanoic acid Chemical compound OCC(C)(C)CO.CCCCCCCC(O)=O.CCCCCCCCCC(O)=O PDYOTPOJFZAOIS-UHFFFAOYSA-N 0.000 claims description 2
- KUVMKLCGXIYSNH-UHFFFAOYSA-N isopentadecane Natural products CCCCCCCCCCCCC(C)C KUVMKLCGXIYSNH-UHFFFAOYSA-N 0.000 claims description 2
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 2
- 239000002304 perfume Substances 0.000 claims description 2
- 230000010412 perfusion Effects 0.000 claims description 2
- 229940042585 tocopherol acetate Drugs 0.000 claims description 2
- 229940098780 tribehenin Drugs 0.000 claims description 2
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims description 2
- 244000194101 Ginkgo biloba Species 0.000 claims 1
- 101000905241 Mus musculus Heart- and neural crest derivatives-expressed protein 1 Proteins 0.000 claims 1
- SOAINXKLHJAHCP-UHFFFAOYSA-N [Li+].C(CCCCCCCCCCCCCCCCC)[N+](C)(C)CCCCCCCCCCCCCCCCCC Chemical group [Li+].C(CCCCCCCCCCCCCCCCC)[N+](C)(C)CCCCCCCCCCCCCCCCCC SOAINXKLHJAHCP-UHFFFAOYSA-N 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims 1
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims 1
- 229910052901 montmorillonite Inorganic materials 0.000 claims 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 239000002537 cosmetic Substances 0.000 abstract description 3
- 239000013543 active substance Substances 0.000 abstract 1
- 239000003086 colorant Substances 0.000 abstract 1
- 244000181025 Rosa gallica Species 0.000 description 32
- 235000011696 French rose Nutrition 0.000 description 29
- 241000218628 Ginkgo Species 0.000 description 22
- 239000000243 solution Substances 0.000 description 13
- 239000004150 EU approved colour Substances 0.000 description 6
- 229940006093 opthalmologic coloring agent diagnostic Drugs 0.000 description 6
- 229940008099 dimethicone Drugs 0.000 description 4
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 4
- 239000004205 dimethyl polysiloxane Substances 0.000 description 4
- OGQYPPBGSLZBEG-UHFFFAOYSA-N dimethyl(dioctadecyl)azanium Chemical group CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC OGQYPPBGSLZBEG-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 3
- 239000007844 bleaching agent Substances 0.000 description 3
- NPAXBRSUVYCZGM-UHFFFAOYSA-N carbonic acid;propane-1,2-diol Chemical compound OC(O)=O.CC(O)CO NPAXBRSUVYCZGM-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 3
- ONNSSMGRFLULCC-UHFFFAOYSA-N icosan-9-ol Chemical class CCCCCCCCCCCC(O)CCCCCCCC ONNSSMGRFLULCC-UHFFFAOYSA-N 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000002347 injection Methods 0.000 description 3
- 239000007924 injection Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000419 plant extract Substances 0.000 description 3
- 239000008223 sterile water Substances 0.000 description 3
- 239000006228 supernatant Substances 0.000 description 3
- 230000009182 swimming Effects 0.000 description 3
- 230000001360 synchronised effect Effects 0.000 description 3
- 229960001295 tocopherol Drugs 0.000 description 3
- 229930003799 tocopherol Natural products 0.000 description 3
- 235000010384 tocopherol Nutrition 0.000 description 3
- 239000011732 tocopherol Substances 0.000 description 3
- 244000088415 Raphanus sativus Species 0.000 description 2
- 235000006140 Raphanus sativus var sativus Nutrition 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical class OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- WFXHUBZUIFLWCV-UHFFFAOYSA-N (2,2-dimethyl-3-octanoyloxypropyl) octanoate Chemical compound CCCCCCCC(=O)OCC(C)(C)COC(=O)CCCCCCC WFXHUBZUIFLWCV-UHFFFAOYSA-N 0.000 description 1
- 244000020518 Carthamus tinctorius Species 0.000 description 1
- 235000003255 Carthamus tinctorius Nutrition 0.000 description 1
- 244000170916 Paeonia officinalis Species 0.000 description 1
- 235000006484 Paeonia officinalis Nutrition 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004113 cell culture Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 description 1
- 229910000271 hectorite Inorganic materials 0.000 description 1
- 210000000554 iris Anatomy 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Tropical Medicine & Parasitology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of cosmetics, in particular to an easily-filled lipstick and a preparation method thereof, wherein the lipstick consists of 35-80% of an oil phase component, 6-25% of a water phase component, 0.5-10% of a plant active substance, 5-15% of a stabilizer, 2-5% of a viscosity regulator and 3-10% of a colorant, and the lipstick in the formula is not easy to generate bubbles at high temperature, is easy to fill and has the advantage of good skin care effect; the preparation method of the lipstick comprises the following steps: the preparation method comprises the steps of preparing the plant active matter, preparing the paste, and filling.
Description
Technical field
The present invention relates to cosmetic technical field, and in particular to a kind of easily filling lipstick and preparation method thereof.
Background technology
Lipstick is a kind of lipstick of solid, and with era development, for women, lipstick is from indispensable cosmetics
Develop into life in essential product, accordingly, it would be desirable to continue to optimize upgrading lipstick preparation technology, with improve lipstick performance and then
Meet the demand of people.In the prior art, lipstick is mainly and is made up of chemical composition and skin care component, and chemical composition is lipstick
Basic ingredient, and skin care ingredient is then used to improve the performance of lipstick, at present, common skin care ingredient is that plant is added in lipstick
Extract, however, plant extracts is a kind of water-soluble substances concentrated obtained by plant liquid, and water-soluble substances is filled in lotion
During dress, easily by high-temperature heating and then generation bubble, so that the lotion of lipstick produces stomata, for the product of bubble is reduced or avoided
It is raw, filling speed and filling temperature need to be strictly controlled when lipstick is filling, filling difficulty is so considerably increased, it is unfavorable for
Mass production lipstick.
The content of the invention
There is one of above-mentioned technical problem, the object of the invention for prior art is to provide be not easy to produce under a kind of high temperature
Anger is steeped and then is easy to filling lipstick, and the lipstick has the advantages that skin effect is good.
There is above-mentioned technical problem for prior art, the two of the object of the invention is to provide a kind of easily filling lipstick
Preparation method, the characteristics of the method has operation simple, low production cost.
One of to achieve the above object, the present invention provides following technical scheme：
A kind of easily filling lipstick and preparation method thereof, including following component are provided：
Oil phase components 35 ~ 80%
Water phase component 6 ~ 25%
Vegetable active thing 0.5 ~ 10%
Stabilizer 5 ~ 15%
Viscosity modifier 2 ~ 5%
Colouring agent 3 ~ 10%.
Preferably, the oil phase components include isohexadecane, polyethylene, hydrogenated palm kernel oil glyceride type, hydrogenated palm
Oil glyceride class, dimethyl silicone polymer, Dimethicone Crosspolymer, Aden perfume base malonic acid ethylhexyl,
Two or more mixture in caprylic/capric triglyceride.
Preferably, the water phase component include octyl dodecanol, tribehenin essence, neopentyl glycol dicaprylate/dicaprate,
Any two or more mixture in octyl dodecanol, tocopherol acetate.
Preferably, the stabilizer is distearyl dimethylammonium hectorite.
Preferably, the viscosity modifier includes one or two the mixture in propylene glycol carbonate, polyamide fibre -12.
Preferably, the colouring agent includes the one kind in CI77891, CI19140, CI15850, CI73360, CI45410
Or two or more mixtures.
To achieve the above object two, the present invention provides following technical scheme：
A kind of preparation method of above-mentioned easily filling lipstick is provided, is comprised the following steps：
The preparation of step one, vegetable active thing
1）Sampling：Win the plant with vital activity；
2）Sterilizing：It is explant by the plant sterilization, the histoorgan for then cutting the plant after sterilizing；
3）Culture：The explant of gained is placed in Fiber differentiation in N6 solid mediums, the callus of plant is obtained；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：The preferable cell mass Secondary Culture of form, so as to obtain the cell mass of loose particles shape；
c）Suspend culture：Shaking culture is carried out during the cell mass of loose particles shape is moved to the shaking flask equipped with nutrient solution, is swum
From cell；
d）Screening：Free plant cell is filtered, the cell mass of screening individual cells or peanut is used as competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, vegetable active thing is obtained, it is stand-by.
The preparation of step 2, lotion
1）The oil phase components of formula ratio are put into the first blender, are heated with certain temperature, then lowered the temperature so that oil phase melts
Solution is uniform, and the oil phase for melting is obtained；
2）The water phase component of formula ratio, the vegetable active thing of formula ratio, the colouring agent of formula ratio are put into the second blender, and
Stirring, is then heated with certain temperature, continues to stir so that water phase, vegetable active thing and colouring agent are well mixed, and is obtained mixed
Compound；
3）By 2）In obtained mixture add 1）In obtained melting oil phase components in, and add formula ratio stabilizer and
The viscosity modifier of formula ratio, makes each material be well mixed at a certain temperature, obtains lotion；
It is step 3, filling
1）By the pre- thermal melting of lotion obtained by step 2, the lotion of melting is injected in lipstick mould with certain angle that pours into；
2）After the completion of tank note, the lipstick mould that will be equipped with lotion is put into cooling certain hour in refrigerator, and the demoulding is molded
Lipstick.
Preferably, in the step one, the time of Fiber differentiation is 2 ~ 4 weeks, and the algebraically of Secondary Culture was 2 ~ 5 generations, described
Plant is one or more during Carrot Roots, ginkgo leaf, safron, french rose are spent, and the vegetable oil is sunflower seed
Oil.
Preferably, in the step 2, then first blender is down to 70 ~ 80 DEG C with 80 ~ 100 DEG C of heating, described
Second blender is well mixed with 25 ~ 30 DEG C of heating, each material at 70 ~ 90 DEG C.
Preferably, in the step 3, preheating temperature is 70 ~ 90 DEG C, and perfusion angle is 25 ~ 40 °, the temperature of the refrigerator
Degree is -10 ~ -2 DEG C, and cool time is 8 ~ 15min.
Beneficial effects of the present invention：
（1）A kind of easily filling lipstick of the invention, with the oil phase of formula ratio, the water phase of formula ratio, formula ratio vegetable active
Thing, the stabilizer of formula ratio, the viscosity modifier of formula ratio, the colouring agent of formula ratio prepare lipstick；Compared with prior art,
The lipstick prepares lipstick matrix using the component of formula ratio, and the vegetable active thing containing competent cell is used in basic components
Used as the plant component of skin care, the competent cell is the plant component of ecosystem and is stored in oil soluble sexual element, be instead of existing
There are the water solubility properties of plant extracts, so as to effectively prevent because filling temperature higher causes water soluble plant extract to steam
Send out and produce bubble so that the uneven problem of lotion dispersion, filling at high temperature beneficial to lotion, and then simplifies filling lipstick
Operation, improve the preparation efficiency of lipstick；Further, since the oil soluble performance of vegetable active thing, can preferably with the base of lipstick
Plinth component is well mixed, and can substantially increase component of the vegetable active thing in lipstick, and then effectively increase the skin care of lipstick
Effect.
（2）A kind of preparation method of easily filling lipstick of the invention, the method is first prepared by the way of cell culture
Go out vegetable active thing, the lotion of lipstick, last filling formation lipstick are then mixed to prepare at a certain temperature.With prior art phase
Than the preparation method of vegetable active thing is ripe and easy to operate, can effectively increase the yield of vegetable active thing；Also, lipstick
Lotion only needs heating to be obtained by mixing, and production process is simple, additionally, during filling lotion, because lotion uses oil-soluble plant
Composition, without strictly controlling filling temperature and filling speed, you can Quick-filling, substantially increases the filling efficiency of lipstick.
（3）A kind of easily filling lipstick of offer that the present invention is provided and preparation method thereof, with preparation method it is simple, produce
Low cost simultaneously can be applied to the characteristics of mass producing.
Specific embodiment
Embodiment 1.
Easily filling lipstick and preparation method in the present embodiment, first weigh 7.5kg oil phases, 0.6kg water phase, 0.25kg steady
Determine agent, 0.2kg viscosity modifiers, 0.3kg colouring agents.
Wherein, 7.5kg oil phases include 1.8kg isohexadecanes, 1.0kg polyethylene, 1.5kg hydrogenated palm kernel oil glycerides
Class, 1.5kg hydrogenated palm oil glycerides class, 1.6kg dimethyl silicone polymers, 1.1kg Dimethicone Crosspolymers；
Wherein, 0.6kg water mutually include 0.2kg octyl dodecanols, 0.05kg tribehenins essence, 0.05kg neopentyl glycols dicaprylate/
Dicaprate, 0.3kg tocopherol acetates；
Wherein, 0.25kg stabilizers are distearyl dimethylammonium hectorites；
Wherein, 0.2kg viscosity modifiers are 0.1kg propylene glycol carbonates, the mixture of 0.1kg polyamide fibres -12；
Wherein, 0.3kg colouring agents are the mixtures of 0.1kgCI77891,0.1kg CI19140,0.1kg CI15850；
Preparation method, comprises the following steps：
The preparation of step one, vegetable active thing
1）Sampling：Win the Carrot Roots with vital activity, ginkgo leaf, safron, french rose flowering plant；
2）Sterilizing：By Carrot Roots, ginkgo leaf, safron, french rose flower difference sterilization, the Hu after sterilizing is then cut
Radish root, ginkgo leaf, safron, french rose flower are explant；
Wherein, the step of sterilization includes first cleaning plant with alcohol, and then plant is soaked in the supernatant of saturation bleaching powder
In liquid, then through sterile water wash.
3）Culture：The Carrot Roots of gained, ginkgo leaf, safron, french rose flower are placed in N6 solid mediums and induced
Culture 3 weeks, obtains Carrot Roots, ginkgo leaf, safron, the callus of french rose flower；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：Carrot Roots, ginkgo leaf, safron, the preferable cell mass difference Secondary Culture of french rose floral shape
4 generations, so as to obtain the cell mass of loose particles shape；
c）Suspend culture：The cell mass of loose particles shape is spent to move to respectively Carrot Roots, ginkgo leaf, safron, french rose right
Shaking culture is carried out in the shaking flask equipped with nutrient solution answered, free cell is obtained；
d）Screening：Carrot Roots, ginkgo leaf, safron, french rose synchronized swimming from plant cell filter respectively, screen it is single
The cell mass of cell or peanut is used as competent cell；
5) clean：The Carrot Roots of gained, ginkgo leaf, safron, french rose flower competent cell are placed on gauze, Ran Houyong
Clear water is rinsed, so that the impurity in removing nutrient solution, obtains clean competent cell；
6) disperse：The clean competent cell of gained is scattered in sunflower seed oil, carrot active matter, ginkgo leaf is obtained and is lived
Property thing, safron active matter, french rose flower active matter, it is stand-by.
The preparation of step 2, lotion
1）7.5kg oil phases are put into the first blender, are heated with 80 DEG C of temperature, be then cooled to 70 DEG C so that oil phase melts
Solution is uniform, the oil phase of melting；
2）The colouring agent of the water phase of 0.6kg, the vegetable active thing of 0.9kg, 0.3kg is put into the second blender, and is stirred, so
25 DEG C of temperature heating afterwards, continue to stir so that water phase, vegetable active thing and colouring agent are well mixed, and mixture is obtained；
Wherein, the vegetable active thing of 0.9kg includes 0.2kg carrots active matter, 0.2kg safron active matter, the white irises of 0.3kg
Active matter, 0.2kg Chinese herbaceous peony active matters；
3）By 2）During obtained mixture adds the oil phase for melting, and add the stabilizer of 0.25kg and the viscosity of 0.2kg to adjust
Section agent, makes each material be well mixed at a temperature of 70 DEG C, obtains lotion；
It is step 3, filling
1）By the lotion obtained by step 2 with 70 DEG C of pre- thermal meltings, the lotion of melting is poured into being 25 ° with horizontal line angle
In angle injection lipstick mould；
2）After the completion of tank note, the lipstick mould that will be equipped with lotion is put into cooling 8min in -10 DEG C of refrigerator, and the demoulding is obtained into
The lipstick of type.
Embodiment 2.
A kind of easily filling lipstick in the present embodiment, first weigh 8kg oil phases, 0.6kg water phase, 0.5kg stabilizers,
0.2kg viscosity modifiers, 0.3kg colouring agents.
Wherein, 8kg oil phases include 0.8kg isohexadecanes, 1.0kg polyethylene, 1.5kg hydrogenated palm kernel oils glyceride type,
1.5kg hydrogenated palm oil glycerides class, 0.6kg dimethyl silicone polymers, 1.6kg Dimethicone Crosspolymers, 1 Asia
Cloves propylmalonic acid ethylhexyl；
Wherein, 0.6kg water mutually include 0.2kg octyl dodecanols, 0.05kg tribehenins essence, 0.05kg neopentyl glycols dicaprylate/
Dicaprate, 0.1 octyl dodecanol, 0.2kg tocopherol acetates；
Wherein, 0.5kg stabilizers are distearyl dimethylammonium hectorites；
Wherein, 0.2kg viscosity modifiers are 0.2kg polyamide fibres -12；
Wherein, 0.3kg colouring agents are the mixtures of 0.1kgCI77891,0.1kg CI15850,0.1CI73360；
Preparation method, comprises the following steps
The preparation of step one, vegetable active thing
1）Sampling：Win the Carrot Roots with vital activity, safron, french rose flowering plant；
2）Sterilizing：By Carrot Roots, safron, french rose flower respectively sterilization, then cut sterilizing after Carrot Roots, kind
Safflower, french rose flower are explant；
Wherein, the step of sterilization includes first cleaning plant with alcohol, and then plant is soaked in the supernatant of saturation bleaching powder
In liquid, then through sterile water wash.
3）Culture：The Carrot Roots of gained, safron, french rose flower are placed in Fiber differentiation 2 in N6 solid mediums
In week, obtain Carrot Roots, safron, the callus of french rose flower；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：Carrot Roots, safron, the preferable cell mass of french rose floral shape are distinguished the generation of Secondary Culture 5, from
And obtain the cell mass of loose particles shape；
c）Suspend culture：The cell mass of Carrot Roots, safron, french rose flower loose particles shape is moved to corresponding dress respectively
Having in the shaking flask of nutrient solution carries out Shaking culture, obtains free cell；
d）Screening：Carrot Roots, safron, french rose synchronized swimming from plant cell filter respectively, screen individual cells or small
The cell mass of number is used as competent cell；
5) clean：The Carrot Roots of gained, safron, french rose flower competent cell are placed on gauze, are then rushed with clear water
Wash, so that the impurity in removing nutrient solution, obtains clean competent cell；
6) disperse：The clean competent cell of gained is scattered in sunflower seed oil, carrot active matter, safron is obtained and is lived
Property thing, french rose flower active matter, it is stand-by.
The preparation of step 2, lotion
1）8kg oil phases are put into the first blender, are heated with 100 DEG C of temperature, be then cooled to 80 DEG C so that oil phase melts
Uniformly, the oil phase of melting；
2）The colouring agent of the water phase of 0.6kg, the vegetable active thing of 0.4kg, 0.3kg is put into the second blender, and is stirred, so
30 DEG C of temperature heating afterwards, continue to stir so that water phase, vegetable active thing and colouring agent are well mixed, and mixture is obtained；
Wherein, the vegetable active thing of 0.4kg includes 0.15kg carrots active matter, 0.1kg safron active matter, 0.15kg France
Rose active matter；
3）By 2）During obtained mixture adds the oil phase for melting, and add the stabilizer of 0.25kg and the viscosity of 0.2kg to adjust
Section agent, makes each material be well mixed at a temperature of 90 DEG C, obtains lotion；
It is step 3, filling
1）By the lotion obtained by step 2 with 90 DEG C of pre- thermal meltings, the lotion of melting is poured into being 40 ° with horizontal line angle
In angle injection lipstick mould；
2）After the completion of tank note, the lipstick mould that will be equipped with lotion is put into cooling 15min in -2 DEG C of refrigerator, and the demoulding is obtained into
The lipstick of type.
The present embodiment 3.
Easily filling lipstick in the present embodiment, first weighs 3.5kg oil phases, 2.5kg water phase, 1.5kg stabilizers, 0.5kg
Viscosity modifier, 1kg colouring agents.
Wherein, 3.5kg oil phases include 0.9kg isohexadecanes, 0.9kg polyethylene, 0.8kg hydrogenated palm kernel oil glycerides
Class, 0.5kg hydrogenated palm oil glycerides class, 0.4kg Dimethicone Crosspolymers；
Wherein, 2.5kg water mutually includes 0.5kg octyl dodecanols, 0.4kg tribehenins essence, 0.5kg neopentyl glycol dicaprylate/bis-
Decylate, 0.8 octyl dodecanol, 0.3kg tocopherol acetates；
Wherein, 1.5kg stabilizers are distearyl dimethylammonium hectorites；
Wherein, 0.5kg viscosity modifiers are 0.25kg propylene glycol carbonates, the mixture of 0.25kg polyamide fibres -12；
Wherein, 1kg colouring agents be 0.2kgCI77891,0.2kgCI19140,0.2kg CI15850,0.2kg CI73360,
The mixture of 0.2kgCI45410；
Preparation method, comprises the following steps
The preparation of step one, vegetable active thing
1）Sampling：Win the Carrot Roots with vital activity, ginkgo leaf, safron, french rose flowering plant；
2）Sterilizing：By Carrot Roots, ginkgo leaf, safron, french rose flower difference sterilization, the Hu after sterilizing is then cut
Radish root, ginkgo leaf, safron, french rose flower are explant；
Wherein, the step of sterilization includes first cleaning plant with alcohol, and then plant is soaked in the supernatant of saturation bleaching powder
In liquid, then through sterile water wash.
3）Culture：The Carrot Roots of gained, ginkgo leaf, safron, french rose flower are placed in N6 solid mediums and induced
Culture 2 weeks, obtains Carrot Roots, ginkgo leaf, safron, the callus of french rose flower；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：Carrot Roots, ginkgo leaf, safron, the preferable cell mass difference Secondary Culture of french rose floral shape
4 generations, so as to obtain the cell mass of loose particles shape；
c）Suspend culture：The cell mass of loose particles shape is spent to move to respectively Carrot Roots, ginkgo leaf, safron, french rose right
Shaking culture is carried out in the shaking flask equipped with nutrient solution answered, free cell is obtained；
d）Screening：Carrot Roots, ginkgo leaf, safron, french rose synchronized swimming from plant cell filter respectively, screen it is single
The cell mass of cell or peanut is used as competent cell；
5) clean：The Carrot Roots of gained, ginkgo leaf, safron, french rose flower competent cell are placed on gauze, Ran Houyong
Clear water is rinsed, so that the impurity in removing nutrient solution, obtains clean competent cell；
6) disperse：The clean competent cell of gained is scattered in sunflower seed oil, carrot active matter, ginkgo leaf is obtained and is lived
Property thing, safron active matter, french rose flower active matter, it is stand-by.
The preparation of step 2, lotion
1）3.5kg oil phases are put into the first blender, are heated with 90 DEG C of temperature, be then cooled to 75 DEG C so that oil phase melts
Solution is uniform, the oil phase of melting；
2）The colouring agent of the water phase of 2.5kg, the vegetable active thing of 1kg, 1kg is put into the second blender, and is stirred, then 28
The heating of DEG C temperature, continues to stir so that water phase, vegetable active thing and colouring agent are well mixed, and mixture is obtained；
Wherein, the vegetable active thing of 1kg includes 0.2kg Carrot Roots active matter, 0.2kg ginkgo leaves active matter, 0.2kg safron
Active matter, 0.2kg french roses flower active matter；
3）By 2）During obtained mixture adds the oil phase for melting, and add the stabilizer of 1.5kg and the viscosity of 0.5kg to adjust
Agent, makes each material be well mixed at a temperature of 85 DEG C, obtains lotion；
It is step 3, filling
1）By the lotion obtained by step 2 with 85 DEG C of pre- thermal meltings, the lotion of melting is poured into being 30 ° with horizontal line angle
In angle injection lipstick mould；
2）After the completion of tank note, the lipstick mould that will be equipped with lotion is put into cooling 10min in -5 DEG C of refrigerator, and the demoulding is obtained into
The lipstick of type.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than the present invention is protected
The limitation of scope is protected, although being explained to the present invention with reference to preferred embodiment, one of ordinary skill in the art should
Work as understanding, technical scheme can be modified or equivalent, without deviating from the reality of technical solution of the present invention
Matter and scope.
Claims (10)
1. a kind of easily filling lipstick, it is characterized in that：Including following component：
Oil phase components 35 ~ 80%
Water phase component 6 ~ 25%
Vegetable active thing 0.5 ~ 10%
Stabilizer 5 ~ 15%
Viscosity modifier 2 ~ 5%
Colouring agent 3 ~ 10%.
2. a kind of easily filling lipstick according to claim 1, it is characterized in that：The oil phase components include isohexadecane,
Polyethylene, hydrogenated palm kernel oil glyceride type, hydrogenated palm oil glycerides class, dimethyl silicone polymer, dimethyl silicone polymer
Two or more mixture in cross-linked polymer, Aden perfume base malonic acid ethylhexyl, caprylic/capric triglyceride.
3. a kind of easily filling lipstick according to claim 1, it is characterized in that：The water phase component includes octyl group 12
It is any two or more in alcohol, tribehenin essence, neopentyl glycol dicaprylate/dicaprate, octyl dodecanol, tocopherol acetate
Mixture.
4. a kind of easily filling lipstick according to claim 1, it is characterized in that：The stabilizer is distearyl dimethylammonium lithium
Montmorillonite.
5. a kind of easily filling lipstick according to claim 1, it is characterized in that：The viscosity modifier includes carbonic acid the third two
Alcohol ester and/or polyamide fibre -12.
6. a kind of easily filling lipstick according to claim 1, it is characterized in that：The colouring agent include CI77891,
One or more mixture in CI19140, CI15850, CI73360, CI45410.
7. using a kind of preparation method of the easily filling lipstick described in claim 1 to 6 any one, it is characterized in that：Including
Following steps：
The preparation of step one, vegetable active thing
1）Sampling：Win the plant with vital activity；
2）Sterilizing：It is explant by the plant sterilization, the histoorgan for then cutting the plant after sterilizing；
3）Culture：The explant of gained is placed in Fiber differentiation in N6 solid mediums, the callus of plant is obtained；
4）The preparation of competent cell：
a）The preferable cell mass of body is chosen from the callus of gained；
b）Secondary Culture：The preferable cell mass Secondary Culture of form, so as to obtain the cell mass of loose particles shape；
c）Suspend culture：Shaking culture is carried out during the cell mass of loose particles shape is moved to the shaking flask equipped with nutrient solution, is swum
From cell；
d）Screening：Free plant cell is filtered, the cell mass of screening individual cells or peanut is used as competent cell；
5) clean：The competent cell of gained is placed on gauze, is then rinsed with clear water, so that the impurity in removing nutrient solution,
Obtain clean competent cell；
6) disperse：The clean competent cell of gained is scattered in vegetable oil, vegetable active thing is obtained, it is stand-by；
The preparation of step 2, lotion
1）The oil phase components of formula ratio are put into the first blender, are heated with certain temperature, then lowered the temperature so that oil phase melts
Solution is uniform, and the oil phase for melting is obtained；
2）The water phase component of formula ratio, the vegetable active thing of formula ratio, the colouring agent of formula ratio are put into the second blender, and
Stirring, is then heated with certain temperature, continues to stir so that water phase, vegetable active thing and colouring agent are well mixed, and is obtained mixed
Compound；
3）By 2）In obtained mixture add 1）In obtained melting oil phase components in, and add formula ratio stabilizer and
The viscosity modifier of formula ratio, makes each material be well mixed at a certain temperature, obtains lotion；
It is step 3, filling
1）By the pre- thermal melting of lotion obtained by step 2, the lotion of melting is injected in lipstick mould with certain angle that pours into；
2）After the completion of tank note, the lipstick mould that will be equipped with lotion is put into cooling certain hour in refrigerator, and the demoulding is molded
Lipstick.
8. the preparation method of a kind of easily filling lipstick according to claim 7, it is characterized in that：In the step one, lure
The time for leading culture is 2 ~ 4 weeks, and the algebraically of Secondary Culture was 2 ~ 5 generations, and the plant is Carrot Roots, ginkgo leaf, safron, method
One or more in state rose, the vegetable oil is sunflower seed oil.
9. the preparation method of a kind of easily filling lipstick according to claim 7, it is characterized in that：In the step 2, institute
The first blender is stated with 80 ~ 100 DEG C of heating, 70 ~ 80 DEG C are then down to, second blender is described each with 25 ~ 30 DEG C of heating
Material is well mixed at 70 ~ 90 DEG C.
10. the preparation method of a kind of easily filling lipstick according to claim 7, it is characterized in that：In the step 3, in advance
Hot temperature is 70 ~ 90 DEG C, and perfusion angle is 25 ~ 40 °, and the temperature of the refrigerator is -10 ~ -2 DEG C, cool time is 8 ~
15min。
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