CN106176321A - A kind of lipstick rich in moisture and preparation method thereof - Google Patents
A kind of lipstick rich in moisture and preparation method thereof Download PDFInfo
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- CN106176321A CN106176321A CN201610778728.6A CN201610778728A CN106176321A CN 106176321 A CN106176321 A CN 106176321A CN 201610778728 A CN201610778728 A CN 201610778728A CN 106176321 A CN106176321 A CN 106176321A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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Abstract
The invention discloses a kind of lipstick rich in moisture, including the following component of weight percentage: emulsifying agent 1 10%;Water phase components 1 25%;Oil phase component 65 98%.This lipstick also can be added as needed on pigment, pearlizing ingredients and water-soluble active ingredient.The invention also discloses the preparation method of above-mentioned lipstick.Using the lipstick that the present invention makes, mastic is soft and smooth, and gloss is bright, and bright in colour charming, natural running water content can effectively desalinate cheilogramma, and deep layer moistens lip, prevents lip water loss, makes lips lasting water profit glossy.Be suitable for the different colour of skin, the crowd of all ages and classes uses.
Description
Technical field
The present invention relates to a kind of lipstick, be specifically related to a kind of lipstick rich in moisture and preparation method thereof, belong to individual's lip
Portion's nursing product technical field.
Background technology
Lip gloss or lipstick typically use pure oiliness formula, and common lipstick is typically without moisture.But it is a large amount of to skin
Or lip has the composition of protectiveness and is water solublity, therefore it is difficult to be added in traditional lipstick.Occur having at present
The lip gloss of certain water content or lipstick, but its water content is the lowest, and prior art with the addition of moisture
Lipstick product can not keep stable solid shape during storage and use, it is impossible to meets the lipstick forming high moisture content
The needs of product.
Summary of the invention
Low for lipstick water content present in prior art, it is difficult to add the problem of water-soluble active ingredient, the present invention
The first purpose be to provide a kind of lipstick rich in moisture and preparation method thereof.Its higher moisture can bring consumer not
The same skinfeel of smearing, more comfortable, more soft and smooth, Geng Shuirun.
Second object of the present invention is to provide for the preparation method of a kind of lipstick rich in moisture.
First purpose realizing the present invention can reach by adopting the following technical scheme that:
A kind of lipstick rich in moisture, it is characterised in that include the following component of weight percentage:
Emulsifying agent 1-10%;
Water phase components 1-25%;
Oil phase component 65-98%.
As preferably, described emulsifying agent is polyglyceryl fatty acid ester, polysiloxane-modified thing, polyoxyethylene sorbitan
One or more mixture in fatty acid ester and fatty acid ester.Lose it is furthermore preferred that described emulsifying agent is polyoxyethylene
Water sorbitan oleate, cetyl PEG/PPG-10/1 polydimethylsiloxane, linolenic acid polyglycereol esters, polyglycereol three are different firmly
One or more mixture in fat acid ester.
As preferably, described water phase components be Jojoba wax class (with) Acacia decurrens floral wax (with) Semen Helianthi wax (with) poly-sweet
Oil-3And water, Jojoba wax class (with) Acacia decurrens floral wax (with) Semen Helianthi wax (with) polyglycereol-3 and water
Weight ratio be 1:10-2:5.It is furthermore preferred that described water phase components also includes the mixed of one or more of C1-C4 alcohol apoplexy due to endogenous wind
Compound, most preferably glycerol, propylene glycol, butanediol;It is furthermore preferred that water-soluble bioactive can be added in water phase components
Point, plant extract or water solublity polysaccharide, most preferably hyaluronate sodium, HANSHENGJIAO, xanthan gum or glucosan.
As preferably, the eutectic temperature scope of described oil phase component is between 30-60 DEG C, and oil-phase component includes: octanoic acid/last of the ten Heavenly stems
Acid glycerol three ester, polyisobutylene, polyethylene, octyl dodecanol, double isooctadecanol malic acid, Cera Flava, microwax, shea butter,
Brazil wax, Castor oil, C10-C30 acid cholesterol/lanosterol mixed ester, candelilla wax, Jojoba oil, dimerization season penta
One or more mixture of tetrol hexahydroxystearic acid ester/six stearate/six rosinate.
As preferably, described lipstick is also added with the water resistant film former that consumption accounts for the 0.01%-0.5% of formula total amount.More
Preferably, described preservative is ANTARON V-216.
As preferably, described lipstick is also added with the pigment that consumption accounts for the 0.1%-20% of formula total amount, and pigment includes: logical
The inorganic pigment often used and organic pigment, e.g., CI 19140, CI 15985, CI 15850, CI 45410, CI 16035, CI
42090 etc..During use, these pigment compositions are ground uniformly with oil phase.
As preferably, described lipstick is also added with the pearlizing ingredients that consumption accounts for the 0.1%-15% of formula total amount.Pearly-lustre becomes
It is divided into normally used pearling agent, such as Muscovitum etc..
As preferably, described lipstick is also added with the essence that consumption accounts for the 0.01%-0.5% of formula total amount.
As preferably, described lipstick is also added with the preservative that consumption accounts for the 0.01%-0.5% of formula total amount.More preferably
, described preservative is phenoxyethanol.
As preferably, described lipstick is also added with the tocopherol acetas that consumption accounts for the 0.01%-0.5% of formula total amount.
Realize second object of the present invention to reach by adopting the following technical scheme that:
The preparation method of a kind of lipstick rich in moisture, it is characterised in that comprise the steps:
1) raw material is got out according to formulation ratio;
2) each component in oil phase is mixed with water resistant film former, be heated to 80-85 DEG C while stirring, be dissolved to clarification thoroughly
Bright, obtain the first mixture;
3) take part the first mixture to add in grinder, gradually add pigment, mix with remaining first after grinding uniformly
Compound mixes, and is heated to 80-85 DEG C while stirring, is allowed to mix homogeneously, obtains the second mixture;
4) each component in aqueous phase is mixed, be heated to 80-85 DEG C while stirring, be allowed to dissolve completely, obtain the 3rd and mix
Compound;
5) being joined in the second mixture by emulsifying agent, temperature is maintained at 70-85 DEG C, is stirred continuously and is allowed to mix homogeneously,
Obtain the 4th mixture;
6) joining in the 4th mixture by the 3rd mixture, temperature is maintained at 70-85 DEG C, is stirred continuously and is allowed to mixing all
Even, obtain the 5th mixture;
7) treat that the temperature of the 5th mixture is down to 64-66 DEG C, add preservative and tocopherol acetas, stir,
To the 6th mixture;
8) by the 6th mixture injection molding at 65-85 DEG C, it is cooled to room temperature or cools down 5-10 minute at-5 DEG C to-15 DEG C
Aftershaping, the demoulding obtains product.
The beneficial effects of the present invention is:
Lipstick rich in moisture of the present invention complies fully with the quality standard of general lipstick, the temperature of-15 DEG C to 52 DEG C
Deposit in the range of degree 3 months, still can keep the shape that its solid-state is bar-shaped, there is no perspiration, cracking, pore, bubble, surface detail
With the bad phenomenon such as crooked, and to its apply certain external mechanical power smear time, its shape invariance, room temperature also can be kept to smear
Functional, soft, it is easy to smear.
Detailed description of the invention
In order to make technical scheme and advantage become apparent from understanding, the present invention is the most furtherly
Bright, but declare specific embodiment described in the invention at this and be only intended to illustrate, it is not intended to limit the present invention.This
Employed in invention, raw material is all commercially available.
Embodiment 1:
A kind of lipstick rich in moisture, including the following component of weight percentage, is specifically shown in Table 1.
Table 1
The preparation method of a kind of lipstick rich in moisture, comprises the steps:
1) raw material is got out according to formulation ratio;
2) each component in oil phase is mixed with water resistant film former, be heated to 80-85 DEG C while stirring, be dissolved to clarification thoroughly
Bright, obtain the first mixture;
3) take part the first mixture to add in grinder, gradually add pigment, mix with remaining first after grinding uniformly
Compound mixes, and is heated to 80-85 DEG C while stirring, is allowed to mix homogeneously, obtains the second mixture;
4) each component in aqueous phase is mixed, be heated to 80-85 DEG C while stirring, be allowed to dissolve completely, obtain the 3rd and mix
Compound;
5) being joined in the second mixture by emulsifying agent, temperature is maintained at 70-85 DEG C, is stirred continuously and is allowed to mix homogeneously,
Obtain the 4th mixture;
6) joining in the 4th mixture by the 3rd mixture, temperature is maintained at 70-85 DEG C, is stirred continuously and is allowed to mixing all
Even, obtain the 5th mixture;
7) treat that the temperature of the 5th mixture is down to 64-66 DEG C, add preservative and tocopherol acetas, stir,
To the 6th mixture;
8) by the 6th mixture injection molding at 65-85 DEG C, it is cooled to room temperature or cools down 5-10 minute at-5 DEG C to-15 DEG C
Aftershaping, the demoulding obtains product.
Embodiment 2:
A kind of lipstick rich in moisture, including the following component of weight percentage, is specifically shown in Table 2.
Table 2
The described preparation method rich in the lipstick of moisture is same as in Example 1.
Embodiment 3:
A kind of lipstick rich in moisture, including the following component of weight percentage, is specifically shown in Table 3.
Table 3
The described preparation method rich in the lipstick of moisture is same as in Example 1.
Testing example:
Compare test and appraisal with like product degree of moistening: 50 volunteers of random choose, select public praise on the market the most several
Brand lipstick, including brand 1, brand 2, brand 3, embodiment 2 running water lipstick.Volunteer is allowed to smear 4 lipsticks respectively, and to it
Carrying out moistening the scoring of degree, 5 are divided into the most moist, and 4 are divided into moist, and 3 are divided into general moistening, and 2 are divided into the most moist, and 1 is divided into not
Moisten.Evaluating result such as table 4 below.
Table 4
According to appraisal result it can be seen that the moist degree of embodiment 2 running water lipstick the highest, meansigma methods reaches 4.73,
Relatively for the lipstick of other full oil phases, can preferably moisten lip skin, reach water profit gloss.
Formulation Design Principle: lip gloss or lipstick typically use pure oiliness formula, and common lipstick is typically without moisture.But
It is that a large amount of composition to skin or lip with protectiveness is water solublity, is therefore difficult to be added in traditional lipstick.
Acticire (Jojoba wax class (with) Acacia decurrens floral wax (with) Semen Helianthi wax (with) polyglycereol-3) it is a kind of texture type moisturizing
Agent, can allow water be dispersed stably in oils and fats, increases the performance of keeping humidity of lipstick.The proportioning of Acticire and water is largely
Determine the moisture-keeping efficacy of lipstick, in order to determine optimal ratio range, compare experiment.
Method of testing: use Jojoba wax class (with) Acacia decurrens floral wax (with) Semen Helianthi wax (with) polyglycereol-3
(Acticire) press different proportion with other water phase components to compound, with lip after skin moisture loss tester test use lipstick
Water loss situation, evaluate the performance of keeping humidity of lipstick with this.Concrete outcome is shown in Table 5.
Table 5
By test result it can be seen that the proportioning of Acticire and water performance of keeping humidity between 1:10-2:5 is good, lipstick
Water content is high, and aqueous phase can be stably dispersed in lipstick, and mastic is soft and smooth, and can keep stable solid shape.
For a person skilled in the art, can technical scheme as described above and design, make other each
Plant corresponding change and deformation, and all these changes and deforms the protection model that all should belong to the claims in the present invention
Within enclosing.
Claims (10)
1. the lipstick rich in moisture, it is characterised in that include the following component of weight percentage:
Emulsifying agent 1-10%;
Water phase components 1-25%;
Oil phase component 65-98%.
Lipstick rich in moisture the most according to claim 1, it is characterised in that described emulsifying agent is polyglycerol fatty acid
One or more mixed in ester, polysiloxane-modified thing, polyoxyethylene sorbitan fatty acid ester and fatty acid ester
Compound.
Lipstick rich in moisture the most according to claim 1, it is characterised in that described water phase components is Jojoba wax class
(with) Acacia decurrens floral wax (with) Semen Helianthi wax (with) polyglycereol-3 and water, Jojoba wax class (with) Acacia decurrens floral wax (with) to day
Certain herbaceous plants with big flowers seed wax (with) weight ratio of polyglycereol-3 and water is 1:10-2:5.
Lipstick rich in moisture the most according to claim 1, it is characterised in that the eutectic temperature scope of described oil phase component
Between 30-60 DEG C, oil-phase component includes: caprylic/capric triglyceride, polyisobutylene, polyethylene, octyl dodecanol, double different
Stearyl alcohol malic acid, Cera Flava, microwax, shea butter, Brazil wax, Castor oil, C10-C30 acid cholesterol/Pilus Caprae seu Ovis steroid
Alcohol mixed ester, candelilla wax, Jojoba oil, dipentaerythritol hexahydroxystearic acid ester/six stearate/six rosinate one
Kind or two or more mixture.
Lipstick rich in moisture the most according to claim 3, it is characterised in that described lipstick has been also added with consumption and has accounted for formula
The water resistant film former of the 0.01%-0.5% of total amount.
Lipstick rich in moisture the most according to claim 5, it is characterised in that described lipstick has been also added with consumption and has accounted for formula
The pigment of the 0.1%-20% of total amount.
Lipstick rich in moisture the most according to claim 6, it is characterised in that described lipstick has been also added with consumption and has accounted for formula
The preservative of the 0.01%-0.5% of total amount;Described lipstick is also added with the fertility that consumption accounts for the 0.01%-0.5% of formula total amount
Phenol acetas.
Lipstick rich in moisture the most according to claim 1, it is characterised in that described lipstick has been also added with consumption and has accounted for formula
The pearlizing ingredients of the 0.1%-15% of total amount.
Lipstick rich in moisture the most according to claim 1, it is characterised in that described lipstick has been also added with consumption and has accounted for formula
The essence of the 0.01%-0.5% of total amount.
10. the preparation method of the lipstick rich in moisture according to claim 7, it is characterised in that include walking as follows
Rapid:
1) raw material is got out according to formulation ratio;
2) each component in oil phase is mixed with water resistant film former, is heated to 80-85 DEG C while stirring, is dissolved to clear,
Obtain the first mixture;
3) take part the first mixture to add in grinder, gradually add pigment, with remaining first mixture after grinding uniformly
Mixing, is heated to 80-85 DEG C while stirring, is allowed to mix homogeneously, obtain the second mixture;
4) each component in aqueous phase is mixed, be heated to 80-85 DEG C while stirring, be allowed to dissolve completely, obtain the 3rd mixture;
5) being joined in the second mixture by emulsifying agent, temperature is maintained at 70-85 DEG C, is stirred continuously and is allowed to mix homogeneously, obtains
4th mixture;
6) joining in the 4th mixture by the 3rd mixture, temperature is maintained at 70-85 DEG C, is stirred continuously and is allowed to mix homogeneously,
Obtain the 5th mixture;
7) treat that the temperature of the 5th mixture is down to 64-66 DEG C, add preservative and tocopherol acetas, stir, obtain the
Six mixture;
8) by the 6th mixture injection molding at 65-85 DEG C, become after being cooled to room temperature or cooling down 5-10 minute at-5 DEG C to-15 DEG C
Type, the demoulding obtains product.
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Cited By (11)
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CN106798702A (en) * | 2017-03-23 | 2017-06-06 | 广州翰江生物科技有限公司 | A kind of moist type lipstick and preparation method thereof |
CN106821951A (en) * | 2017-03-23 | 2017-06-13 | 广州翰江生物科技有限公司 | A kind of easily filling lipstick and preparation method thereof |
CN106924082A (en) * | 2017-05-08 | 2017-07-07 | 共聚生化科技(昆山)有限公司 | The moist lip gloss of high-moisture |
CN107184431A (en) * | 2017-05-11 | 2017-09-22 | 娇时日化(杭州)股份有限公司 | Moisturizing emulsion and moisturizing eye shadow applied to moisturizing eye shadow |
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CN110354006A (en) * | 2019-08-09 | 2019-10-22 | 东晟源研究院(广州)有限公司 | Solve the problems, such as the water outlet lipstick Recipe and preparation method that lipstick lotion is sweated |
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Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106821951A (en) * | 2017-03-23 | 2017-06-13 | 广州翰江生物科技有限公司 | A kind of easily filling lipstick and preparation method thereof |
CN106798702A (en) * | 2017-03-23 | 2017-06-06 | 广州翰江生物科技有限公司 | A kind of moist type lipstick and preparation method thereof |
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