CN108403483A - It is a kind of element face frost and its preparation process - Google Patents

Abstract

The invention discloses a kind of plain face frost and its preparation processes, belong to cosmetic technical field, which includes the component of following parts by weight：40 52 parts of pure water；23 parts of titanium dioxide；0.03 0.08 parts of triethoxy octyl silane；35 38 parts of moisturizer；4 6.5 parts of film forming agent；First 46 parts of emollient；Second 24 parts of emollient；1.08 1.52 parts of thickener/emulsifier；15 parts of glycine betaine；Palmityl tripeptides 1 are 0.5 2 parts；0.402 0.5825 parts of preservative；Moisturizer is made of yellow tang extract, niacinamide, panthenol, glycerine, butanediol；Film forming agent is made of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol 3；Thickener/emulsifier is made of sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, polysorbate80.Plain face frost in the present invention has the effect of preferable uniformly whitening, moisturizing, and skin can be made to keep water and oil balance.

Description

It is a kind of element face frost and its preparation process

Technical field

The present invention relates to cosmetic technical fields, more specifically, it relates to a kind of element face frost and its preparation process.

Background technology

Plain face frost is a new product between face cream and foundation cream, can play the role of skin whitening, bright color, and And the concept of bottom adornment and skin care is combined, i.e., have the effect of the effect of face cream simultaneously and makes bottom adornment.

The Chinese patent that application publication number is CN107468586A, data of publication of application is on December 15th, 2017 discloses one Kind water outlet moisturizing element face frost and preparation method thereof, the water outlet moisturizing element face frost is prepared by following raw material by weight percentage It forms：Emulsifier 3%~7%, thickening property elastomer 1%~5%, silicone oil 0.5%~3.5%, grease 5%~10%, titanium white Powder 5%~8%, oil phase thickeners 1%~5%, moisturizer 15%~25%, pH adjusting agent 0.9%~1.5%, preservative 0.1%~0.8%, active constituent 1%~3%, deionized water surplus.

Element face frost in the prior art has preferable whitening effect, however, silicone oil is used in the prior art, and it is long-term Silicone oil is contacted, skin can be made skin damage, or even carcinogenic risk is brought to human body by corrosion to a certain extent；Meanwhile The use of silicone oil and grease, and the dosage of grease is larger, it is more difficult to plain face frost in the prior art is smeared uniformly, and in certain journey Skin can be caused airtight on degree, to cause the unbalanced situation of skin water oil.

Invention content

In view of the deficienciess of the prior art, the purpose of the present invention one is to provide a kind of plain face frost, have preferable equal The effect of even whitening, moisturizing, and skin can be made to keep water and oil balance.

To achieve the above object one, the present invention provides following technical solutions：

A kind of element face frost, includes the component of following parts by weight：

40-52 parts of pure water；

2-3 parts of titanium dioxide；

0.03-0.08 parts of triethoxy octyl silane；

35-38 parts of moisturizer；

4-6.5 parts of film forming agent；

First 4-6 parts of emollient；

Second 2-4 parts of emollient；

1.08-1.52 parts of thickener/emulsifier；

1-5 parts of glycine betaine；

Palmityl tripeptides -1 are 0.5-2 parts；

0.402-0.5825 parts of preservative；

The grain size of the titanium dioxide is 30-45 μm；

The moisturizer is made of yellow tang extract, niacinamide, panthenol, glycerine, butanediol；

The film forming agent is made of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3；

The thickener/emulsifier is by sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, polysorbate- 80 compositions；First emollient includes blend, the poly- diformazan that dimethiconol and dimethyl silicone polymer are formed At least one of radical siloxane；

Second emollient includes at least one of Butyrospermum parkii fruit fat, double-PEG-18 methyl ethers dimethylsilanes.

Through the above technical solutions, the grain size of the titanium dioxide used in the application for 30-40 μm, has in skin surface Preferably fitting effect, the effect of to reach whitening sun protection, and contributes to bright color.In addition, titanium dioxide and three ethoxies Base octyl silane cooperates, and contributes to the effect for making the colour of skin obtain uniform whitening, and makes the colour of skin more naturally, using this After plain face frost in application, the effect of plain face can reach.

In the application, in the first emollient, dimethyl silicone polymer has the effect of preferably moisturizing the skin, and certain Hydrophobic effect is played in degree, it is clearly not glutinous greasy；And dimethiconol has the effect of preferable anti-foam, contacts skin After skin, can also be skin becomes soft.The blend that dimethiconol and dimethyl silicone polymer are formed, can reach more The effect of good skin care, is also less prone to generate glutinous soapy feeling.

In the application, in moisturizer, yellow tang extract has effects that good conditioning skin, wherein the seaweed contained Polysaccharide can enter inside skin, have the function that lasting moisturizing.Niacinamide has anti-inflammatory effect, in addition, helping to make this Shen Please in plain face frost there is preferable smooth effect can maintain the ceramide in skin and free fatty into after skin Level, and the water content of skin is maintained, once into skin corium microcirculation, keep skin water profit glossy.Panthenol is highly soluble in water, easily It is absorbed by the skin, can make skin that there is moisture-keeping function, and glycerine and butanediol are small molecule, penetrate into the effect of skin More preferably.In addition, the effect of panthenol, glycerine and butanediol all have bactericidal antiphlogistic, help to reduce in environment microorganism to skin The infringement of skin.Yellow tang extract, niacinamide, panthenol, glycerine, butanediol complex role under, help to improve to be formed The application in plain face frost moistening effect.

In film forming agent, Jojoba esters have preferable soft and moist effect and moisture-keeping function；Sunflower seed wax, Acacia decurrens flower Wax all has preferable soft and moist effect, and polyglycereol -3 has good moistening effect.Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3 mutual cooperation under, very thin layer protecting film can be formed in skin surface, make the sense of touch of skin It is soft and persistently smooth, moisture can be also effectively lockked, to the water and oil balance for making skin be maintained for a long time.

In second emollient, it is rich in unsaturated fatty acid in Butyrospermum parkii fruit fat, there is easily absorption and moisturizing effect is good Advantage can reinforce the moisture-retaining capacity of skin.Double-PEG-18 methyl ethers dimethylsilanes can also play the work of preferable moisturizing With may additionally facilitate the mutual dispersion of other components.

Moisturizer, film forming agent, the second emollient cooperate, and make the plain face frost to be formed that can be equably applied to face, And layer protecting film is formed in skin surface, the effect of the moisturizing to face is improved, makes natural dressing that can keep more long Time, additionally aid make skin keep water and oil balance, so that skin non-greasy is not also dried.

In thickener/emulsifier, sodium acrylate/sodium acryloyldimethyl taurate copolymers have preferable agglomeration resistance effect, Emulsification can not only be played, moreover it is possible to while achieving the effect that hydrophilic thickening.Isohexadecane helps to improve the plain face to be formed The texture that the silk of frost is slided, Polyoxyethylene Sorbitan Monooleate has preferable hydrophily, while also having preferable emulsification.And propylene Sour sodium/sodium acryloyldimethyl taurate copolymers, isohexadecane, Polyoxyethylene Sorbitan Monooleate cooperate, and help to improve this Shen Please in plain face frost thickening and emulsifying effectiveness, make plain face frost that there is preferable stable state, quality silk is slided soft, is less prone to It trickles serious phenomenon, while not easily causing the phenomenon that being difficult to smear.

Glycine betaine helps to control the water balance in living cells, prevents protein denaturation from helping to mitigate the stimulation of detergent Prevent protein denaturation from helping to mitigate the irritation of detergent.Palmityl tripeptides -1 cooperate with glycine betaine, can effectively promote Into I-type collagen synthesize, mitigate various wrinkles, compact skin and make skin have elasticity.

In addition, yellow tang extract extracts acquisition as follows：

Yellow tang is mixed according to volume ratio for 1: 10 with a concentration of 75% ethyl alcohol, impregnates and filtered for 24 hours through 80 mesh screens by step A, Obtain the first filtrate and filter residue；

The filter residue obtained in step A is extracted 1.5-2h using 40 times of deionized waters, obtains the second filtrate by step B；20 are used again Times deionized water extracts 1.5-2h to filter residue, obtains third filtrate；

Step C merges the second filtrate obtained in step B and third filtrate, then is filtered using cotton, forms merging filtrate；

The merging filtrate that step A the first filtrates obtained and step 3 obtain is uniformly mixed by step D, and spraying drying powder-forming obtains .

Further preferably：In the moisturizer, yellow tang extract, niacinamide, panthenol, glycerine, butanediol weight It is 5-6: 1: 0.75-1: 4-5: 7.5-8 to measure portion rate.

Through the above technical solutions, yellow tang extract, niacinamide within the scope of aforementioned proportion, panthenol, glycerine, fourth two Alcohol cooperates, and after usage, can help to further increase moistening effect well into skin inside, makes dry skin Skin is moistened.

Further preferably：In the film forming agent, Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3 Weight part ratio is 20.5-21.3: 10-10.8: 1: 1.

Through the above technical solutions, Jojoba esters, sunflower seed wax, Acacia decurrens floral wax within the scope of aforementioned proportion, poly- Glycerine -3 cooperates, and there is the plain face frost contributed in the application for making to be formed better film-formation result can make smearing first The skin of Yan Shuan of being always or usually as specified keeps natural dressing for a long time, and secondly, the film of formation has moisture-keeping function, and skin is made to keep water Oily equilibrium state.

Further preferably：It is sodium acrylate/sodium acryloyldimethyl taurate copolymers, different in the thickener/emulsifier Hexadecane, Polyoxyethylene Sorbitan Monooleate weight part ratio be 1: 1-3: 2-3.

Through the above technical solutions, sodium acrylate/sodium acryloyldimethyl taurate copolymers within the scope of aforementioned proportion, Isohexadecane, Polyoxyethylene Sorbitan Monooleate cooperate, and the plain face frost in the application can be made to have more stable state, used It is easier to be smeared but be less prone to serious phenomenon of trickling in the process.

Further preferably：First emollient is the dimethiconol that weight part ratio is 1: 2 and poly- two Blend that methylsiloxane is formed, dimethyl silicone polymer, in the blend, dimethiconol and poly dimethyl The weight part ratio of siloxanes is 6.5: 1.

Through the above technical solutions, the blending that the dimethiconol and dimethyl silicone polymer of aforementioned proportion are formed Object cooperates with dimethyl silicone polymer, helps to further increase the soothing effect of the plain face frost in the application, is using In the process, it is not easy to make skin phenomena such as dry, decortication occur, to keep plain face frost better with being bonded between skin.

Further preferably：Second emollient be weight part ratio be 1: 2-4 Butyrospermum parkii fruit fat, double-PEG- 18 methyl ether dimethylsilanes.

Through the above technical solutions, the Butyrospermum parkii fruit fat of aforementioned proportion, double-PEG-18 methyl ethers dimethylsilanes are mutual Cooperation helps further to mitigate the greasy feeling of grease or sticks greasy bar, while can also improve the moisturizing effect to skin.

Further preferably：The preservative by parts by weight be 0.15-0.25 parts methyl hydroxybenzoate, 0.15-0.20 parts Propylene glycol, 0.1-0.13 parts of Bis(hydroxymethyl)imidazolidinyl urea, 0.002-0.0025 parts of iodine propilolic alcohol butyl ammonia formic acid Ester forms.

Through the above technical solutions, propylene glycol, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate and hydroxyl Benzene methyl cooperates, and helps to improve the anti-corrosion effect of the plain face frost in the application, further decreases plain face frost by micro- life The probability of object pollution, to extend the shelf-life of plain face frost.

Further preferably：Further include the essence that parts by weight are 0.05-0.15 parts.

Through the above technical solutions, contributing to the experience sense for promoting user by and different types of essence can meet The requirement of different crowd.

The purpose of the present invention two is to provide a kind of preparation process of plain face frost, component therein is sufficiently mixed, shape is made At plain face frost have uniformly, the easy quality that tiles.

To achieve the above object two, the present invention provides following technical solutions：

A kind of preparation process of element face frost, includes the following steps：

Pure water, glycine betaine, moisturizer are mixed according to parts by weight, are warming up to 75-85 DEG C, are sufficiently mixed, obtained by step 1 First mixture；

Step 2, according to parts by weight, by titanium dioxide, triethoxy octyl silane, film forming agent, the first emollient, 0.3-0.6 Second emollient of part, the mixing of 0.1-0.25 parts of preservative, are warming up to 75-85 DEG C, are sufficiently mixed, obtain the second mixture；

The first mixture obtained in step 1 is uniformly mixed with the second mixture obtained in step 2, and presses by step 3 It according to parts by weight, adds thickener/emulsifier and is sufficiently mixed, obtain third mixture；

The third mixture obtained in step 3 is cooled to 40-50 DEG C, according to parts by weight, by palmityl tripeptides-by step 4 1, remaining preservative and remaining second emollient are added in the third mixture obtained into step 3, are sufficiently mixed, obtain Obtain plain face frost.

Through the above technical solutions, the second mixing obtained in the first mixture and step 2 of a kind of acquisition of step The temperature difference of object, the two is less, and in step 3, the two is mixed, and helps to improve the effect of mixing.When the first mixture After being mutually mixed with the second mixture, thickener/emulsifier is added, is helped to reduce after thickener/emulsifier is added required for stirring Energy consumption, but still itself and the first mixture and the second mixture can be stirred, obtain third mixture.In step In four, third mixture is cooled to 40-50 DEG C, adds palmityl tripeptides -1, remaining preservative and remaining second profit Skin agent the effect of helping fully to keep palmityl tripeptides -1, also can fully keep the effect in the second emollient,

Further preferably：In the step 4, the essence that parts by weight are 0.05-0.15 parts is added, is sufficiently mixed.

Through the above technical solutions, essence is added in step 4, the essence for making to be formed is contributed to keep more strong Fragrance, and the third mixture in step 4 has been thoroughly mixed, and after adding essence, mixed effect can be more preferably.

In conclusion the invention has the advantages that：

1. with the good screening flaw, U.S. fair-complexioned effect, and can make the colour of skin more naturally, to reach the effect of plain face after Fruit；

2. the compactness between skin of face is good, it is less prone to loose colour；

3. moisturizer, film forming agent, the second emollient cooperate, make the plain face frost to be formed that can be equably applied to face, and Layer protecting film is formed in skin surface, the effect of the moisturizing to face is improved, makes natural dressing that can keep more long Time, additionally aiding makes skin keep water and oil balance, and skin non-greasy is made also not dry；

4. palmityl tripeptides -1 cooperate with glycine betaine, I-type collagen synthesis can be effectively facilitated, mitigates various wrinkles, tightly It causes skin and makes skin that there is elasticity.

Specific implementation mode

With reference to embodiment, the present invention will be described in detail.

Embodiment 1：A kind of element face frost, included component and its corresponding parts by weight are as shown in table 1, and by as follows Step prepares：

Pure water, glycine betaine, moisturizer are mixed, are warming up to 85 DEG C, are sufficiently mixed, obtain the first mixture by step 1；

Step 2, by titanium dioxide, triethoxy octyl silane, film forming agent, the first emollient, 0.3 part of the second emollient, 0.15 part of preservative mixing, is warming up to 85 DEG C, is sufficiently mixed, obtain the second mixture；

The first mixture obtained in step 1 is uniformly mixed by step 3 with the second mixture obtained in step 2, then is added Enter thickener/emulsifier to be sufficiently mixed, obtains third mixture；

The third mixture obtained in step 3 is cooled to 45 DEG C by step 4, by palmityl tripeptides -1, remaining preservative and Remaining second emollient is added in the third mixture obtained into step 3, is sufficiently mixed, and obtains plain face frost.

Wherein, in step 1, in moisturizer, yellow tang extract, niacinamide, panthenol, glycerine, butanediol parts by weight Number is than being 5: 1: 0.75: 4: 7.5.

In step 2, the grain size of titanium dioxide is 30 μm；First emollient is the poly dimethyl silicon that weight part ratio is 1: 2 Blend, the dimethyl silicone polymer that oxygen alkanol and dimethyl silicone polymer are formed, wherein dimethiconol and poly- two In the blend that methylsiloxane is formed, the weight part ratio of dimethiconol and dimethyl silicone polymer is 6.5: 1； The preservative of addition is methyl hydroxybenzoate；In film forming agent, Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3 weight It is 21.3: 10: 1: 1 to measure portion rate；The Butyrospermum parkii fruit fat that the second emollient being added is 0.3 part.

In step 3, in thickener/emulsifier, sodium acrylate/sodium acryloyldimethyl taurate copolymers, is gathered isohexadecane The weight part ratio of sorbitol ester -80 is 1: 2: 3.

In step 4, remaining preservative is 0.15 part of propylene glycol, 0.10 part of Bis(hydroxymethyl)imidazolidinyl urea, 0.002 Part iodine propilolic alcohol butyl mephenesin Carbamate；Double-PEG-18 methyl ether dimethylsilanes that remaining second emollient is 1.7 parts.

Embodiment 2-4：A kind of element face frost, difference lies in included component and its corresponding parts by weight with embodiment 1 Number is as shown in table 1.In preparation process, essence is added into step 4, is sufficiently mixed.

Included component and its corresponding parts by weight in 1 embodiment 1-4 of table

Embodiment 5：A kind of element face frost, the difference from example 2 is that, in step 1, in moisturizer, yellow tang extraction Object, niacinamide, panthenol, glycerine, butanediol weight part ratio be 6: 1: 1: 5: 8.

Embodiment 6：A kind of element face frost, the difference from example 2 is that, in step 2, in film forming agent, Jojoba esters, Sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3 weight part ratio be 20.5: 10.8: 1: 1.

Embodiment 7：A kind of element face frost, the difference from example 2 is that, in step 3, in thickener/emulsifier, acrylic acid Sodium/sodium acryloyldimethyl taurate copolymers, isohexadecane, Polyoxyethylene Sorbitan Monooleate weight part ratio be 1: 3: 2.

Comparative example 1：It is a kind of element face frost, the difference from example 2 is that, use application publication number for CN107468586A, Data of publication of application is reality in a kind of water outlet moisturizing element face frost and preparation method thereof disclosed in the Chinese patent on December 15th, 2017 The preparation method for applying example 1 prepares.

Comparative example 2：A kind of element face frost, the difference from example 2 is that, do not include moisturizer.

Comparative example 3：A kind of element face frost, the difference from example 2 is that, do not include film forming agent.

Comparative example 4：A kind of element face frost, the difference from example 2 is that, do not include the second emollient.

Comparative example 5：A kind of element face frost, the difference from example 2 is that, do not include palmityl tripeptides -1.

Experiment one：Market survey is tested

Test specimen：The plain face frost in embodiment 1-7 is chosen as test sample 1-7, chooses comparative example 1-5 sample 1-5 as a contrast.

Test method：

1,120 areals are chosen, age bracket is 18-35 one full year of life, skin light yellow complexion, mixed type skin quality and the women with freckle White collar is equally divided into 12 groups, number group 1- groups 12 as subject.Every group of subject is handled using Cetaphil face cleaning milk face cleaning Afterwards, 2ml Cetaphils skin-moisturizing, skin breast is uniformly smeared, 1-7 groups subject uses test sample 1-7,8-12 groups tested respectively again Person uses control sample 1-5 respectively again, and the usage amount of test sample 1-7, control sample 1-5 are respectively 0.1ml, smears uniform.

Observation hide the flaw, whitening effect, if hide that flaw effect is good and whitening from then 8-9 points of marking, if screening flaw effect is preferable And whitening relatively certainly then is given a mark 6-7 points, if hiding, flaw effect is bad or whitening is not enough 1-5 points naturally；

It is pressed lightly on respectively using beautiful Bell's cotton pads and in the skin surface for being coated with sample, observes and whether glued in cotton pads With sample, the 8-9 that gives a mark if hardly adhering to points, 6-7 points if slight adhesion is given a mark；If adherency more at most 1-5 points of marking.

2, it allows after the daily face cleaning on daytime of above-mentioned subject and smears primary corresponding sample, persistently use 365 days, the 366th day When, observe the microgroove situation of every group of subject's skin of face and the situation of compacting of skin.

Test result：It is as shown in table 2 using the indices after test sample 1-7, control sample 1-5.

Table 2 uses the indices after test sample 1-7, control sample 1-5

Group number	Hide the flaw, whitening effect	Docile degree	Skin of face situation
				Group 1	9.1	8.8	Microgroove is desalinated, skin-tightening, high resilience
Group 2	9.2	9.1	Microgroove is desalinated, skin-tightening, high resilience
				Group 3	9.1	9.1	Microgroove is desalinated, skin-tightening, high resilience
Group 4	9.2	9.2	Microgroove is desalinated, skin-tightening, high resilience
				Group 5	9.0	8.9	Microgroove is desalinated, skin-tightening, high resilience
Group 6	9.1	9.2	Microgroove is desalinated, skin-tightening, high resilience
				Group 7	9.2	9.0	Microgroove is desalinated, skin-tightening, high resilience
Group 8	7.6	7.5	It has almost no change
				Group 9	4.3	3.5	It has almost no change
Group 10	4.1	3.8	It has almost no change
				Group 11	4.5	3.9	It has almost no change
Group 12	8.8	8.50	It has almost no change

As shown in Table 2, in group 1- groups 7, subject indicates that test sample 1-7 has the effect of preferably covering freckle, and reaches To white-skinned face function preferably and more naturally, be used for a long time also contribute to face tightening effect, make skin high resilience And desalinate microgroove.

And organize the subject in 8- groups 12 and then indicate, although effect of the control sample 1 with the relatively good screening flaw, natural whitening Fruit, but it is little to the help of skin compacted, desalinate wrinkle.Illustrate that a large amount of silicone oil contained in control sample 1 easily cause skin hardly possible It to absorb more nutrient, is not enough moistened so as to cause skin, microgroove is difficult to be desalinated, and skin quality is not enough compacted, and does not also have elasticity.

Control sample 2-4 is more inferior in terms of hiding the natural degree of flaw effect and whitening, and is applied on skin of face Occur not docile enough phenomenon afterwards, easily loses powder, and poor in the moisturizing effect to skin, main reason is that：Moisturizer, film forming Agent, the second emollient respective missing, easily lead to control sample 2-4 and be difficult to fully be absorbed by the skin, the part that is absorbed by the skin battalion Also more difficult long-time resides in skin surface to foster substance, to the microgroove for being difficult to smooth on skin, can not improve the relaxation of skin Sense.

Due to having lacked palmityl tripeptides -1 in control sample 5, it is difficult to form mating reaction with glycine betaine, finally be difficult to promote I-type collagen synthesizes, and therefore, it is difficult to mitigate various wrinkles, can not improve the relaxation sense of skin.

Experiment two：Moisturizing oil-control is tested

Test specimen：The plain face frost in embodiment 1-7 is chosen as test sample 1-7, chooses comparative example 1-4 sample 1-4 as a contrast.

Test method：Choose 120 areals, age bracket is 18-35 one full year of life, skin light yellow complexion, mixed type skin quality and length There is the women white collar of freckle as subject, is equally divided into 12 groups, number group 1- groups 12.Every group of subject is clean using Cetaphil After the processing of face milk face cleaning, moisture of skin test carried out respectively to every group of subject, after average treatment, at the beginning of recording every group of skin Beginning moisture value；

Every subject is allowed uniformly to smear 2ml Cetaphil skin-moisturizing, skin breasts in skin of face, 1-7 groups subject uses respectively again Test sample 1-7,8-12 groups subject uses control sample 1-4 respectively again, and the usage amount of test sample 1-7, control sample 1-4 are respectively 0.1ml smears uniformly, when smearing 3h, 6h, 12h, tests the skin moisture content that every group of subject mutually exists together respectively, average It after processing, carries out recording every group of skin moisture content respectively, and analyzes；And it when smearing 3h, 6h, 9h, is respectively adopted same Money oil-Absorbing Sheets press lightly in the areas T of every subject, observe the oil suction situation of oil-Absorbing Sheets, if at least six people is fuel-displaced seriously 5 scores are made, if at least six people is fuel-displaced more serious, makes 4 scores, 3 scores are made if at least six people is fuel-displaced generally, if at least six people Fuel-displaced relatively then to make 2 scores less, at least six people makes 1 score if not fuel-displaced, records and analyzes.

Test result：Moistening effect using skin after test sample 1-7, control sample 1-4 is as shown in table 3, uses test sample The oil-control effect of skin is as shown in table 4 after 1-7, control sample 1-4.

Table 3 uses the moistening effect of skin after test sample 1-7, control sample 1-4

As shown in Table 3, the initial moisture value difference of the skin of every group of subject is little, and uses the subject of test sample 1-7, After using 3h, 6h even 12h, skin moisture content is still higher by much than the initial moisture value of skin, illustrates test sample 1-7 has preferable assimilation effect, and can muchly keep skin wet.However, using the subject of control sample 1-4, For skin of face after fully absorbing corresponding sample, the rising of skin moisture content is more inferior compared to group 1- groups 12.And After 3h, there is decline by a relatively large margin in skin moisture content, and after 6h, the amplitude that skin moisture content reduces increases, in 9h Afterwards, the fall of skin moisture content further increases, and illustrates that the moistening effect of control sample 4-6 is not ideal enough, and moisturizing Persistence is poor.The main reason for above-mentioned condition occur is：Moisturizer, film forming agent, the second emollient to the moisturizing of skin with And oil-control has tremendous influence.

Table 4 uses the oil-control effect of skin after test sample 1-7, control sample 1-4

Group number	Fuel-displaced situation after 3h	Fuel-displaced situation after 6h	Fuel-displaced situation after 9h
				Group 1	1	1	2
Group 2	1	1	1
				Group 3	1	1	2
Group 4	1	1	2
				Group 5	1	1	1
Group 6	1	1	2
				Group 7	1	1	2
Group 8	2	3	5
				Group 9	3	4	5
Group 10	3	4	5
				Group 11	3	4	5

As shown in Table 4, preferable oil-control effect can be still kept after using 3h, 6h using the subject of test sample 1-7, After even 9h, fuel-displaced phenomenon is not obvious.However, using the subject of control sample 1-4, corresponding sample 3h is being used Afterwards, there is more apparent fuel-displaced phenomenon, after 6h and after 9h, fuel-displaced phenomenon is more serious.There is the original of above-mentioned phenomenon Because：The silicone oil that larger dosage is used in control sample 1 easily causes the blocking of skin, and it is serious to eventually lead to skin ingress of oil phenomenon The case where, with the extension of time, the phenomenon can be increasingly severe；In control sample 2-4, lacked respectively moisturizer, film forming agent, Second emollient to cause to be difficult to that skin is made fully to be moistened, and with the extension of time, causes water-dispersed in skin It loses, causes water oil uneven, skin ingress of oil phenomenon serious situation finally occur.

The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications It should be regarded as protection scope of the present invention.

Claims (10)

1. a kind of element face frost, which is characterized in that include the component of following parts by weight：

40-52 parts of pure water；

2-3 parts of titanium dioxide；

0.03-0.08 parts of triethoxy octyl silane；

35-38 parts of moisturizer；

4-6.5 parts of film forming agent；

First 4-6 parts of emollient；

Second 2-4 parts of emollient；

1.08-1.52 parts of thickener/emulsifier；

1-5 parts of glycine betaine；

Palmityl tripeptides -1 are 0.5-2 parts；

0.402-0.5825 parts of preservative；

The grain size of the titanium dioxide is 30-45 μm；

The moisturizer is made of yellow tang extract, niacinamide, panthenol, glycerine, butanediol；

The film forming agent is made of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3；

The thickener/emulsifier is by sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, polysorbate- 80 compositions；

First emollient includes blend, the poly dimethyl silicon that dimethiconol and dimethyl silicone polymer are formed At least one of oxygen alkane；

Second emollient includes at least one of Butyrospermum parkii fruit fat, double-PEG-18 methyl ethers dimethylsilanes.

2. a kind of plain face frost according to claim 1, which is characterized in that in the moisturizer, yellow tang extract, nicotinoyl Amine, panthenol, glycerine, butanediol weight part ratio be 5-6:1:0.75-1:4-5:7.5-8.

3. a kind of plain face frost according to claim 1, which is characterized in that in the film forming agent, Jojoba esters, sunflower Seed wax, Acacia decurrens floral wax, polyglycereol -3 weight part ratio be 20.5-21.3:10-10.8:1:1.

4. a kind of plain face frost according to claim 1, which is characterized in that in the thickener/emulsifier, sodium acrylate/propylene Acyl dimethyltaurine sodium copolymer, isohexadecane, Polyoxyethylene Sorbitan Monooleate weight part ratio be 1:1-3:2-3.

5. a kind of plain face frost according to claim 1, which is characterized in that it is 1 that first emollient, which is weight part ratio,: Blend that 2 dimethiconol and dimethyl silicone polymer are formed, dimethyl silicone polymer, in the blend, The weight part ratio of dimethiconol and dimethyl silicone polymer is 6.5:1.

6. a kind of plain face frost according to claim 1, which is characterized in that it is 1 that second emollient, which is weight part ratio,: The Butyrospermum parkii fruit fat of 2-4, double-PEG-18 methyl ethers dimethylsilanes.

7. a kind of plain face frost according to claim 1, which is characterized in that the preservative is 0.15- by parts by weight 0.25 part of methyl hydroxybenzoate, 0.15-0.20 parts of propylene glycol, 0.1-0.13 parts of pair（Methylol）Imidazolidinyl urea, 0.002- 0.0025 part of iodine propilolic alcohol butyl mephenesin Carbamate composition.

8. a kind of plain face frost according to claim 1, which is characterized in that further include parts by weight be 0.05-0.15 parts Essence.

9. a kind of preparation process of plain face frost described in any one of claim 1-7, which is characterized in that including walking as follows Suddenly：

Pure water, glycine betaine, moisturizer are mixed according to parts by weight, are warming up to 75-85 DEG C, are sufficiently mixed, obtained by step 1 First mixture；

Step 2, according to parts by weight, by titanium dioxide, triethoxy octyl silane, film forming agent, the first emollient, 0.3-0.6 Second emollient of part, the mixing of 0.1-0.25 parts of preservative, are warming up to 75-85 DEG C, are sufficiently mixed, obtain the second mixture；

The first mixture obtained in step 1 is uniformly mixed with the second mixture obtained in step 2, and presses by step 3 It according to parts by weight, adds thickener/emulsifier and is sufficiently mixed, obtain third mixture；

The third mixture obtained in step 3 is cooled to 40-50 DEG C, according to parts by weight, by palmityl tripeptides-by step 4 1, remaining preservative and remaining second emollient are added in the third mixture obtained into step 3, are sufficiently mixed, obtain Obtain plain face frost.

10. a kind of preparation process of plain face frost according to claim 9, which is characterized in that in the step 4, weight is added The essence that number is 0.05-0.15 parts is measured, is sufficiently mixed.