CN102133169B - Cosmetic for protecting eye and preparation method thereof - Google Patents
Cosmetic for protecting eye and preparation method thereof Download PDFInfo
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- CN102133169B CN102133169B CN2011100698486A CN201110069848A CN102133169B CN 102133169 B CN102133169 B CN 102133169B CN 2011100698486 A CN2011100698486 A CN 2011100698486A CN 201110069848 A CN201110069848 A CN 201110069848A CN 102133169 B CN102133169 B CN 102133169B
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- 238000002360 preparation method Methods 0.000 title abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
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Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses cosmetic for protecting eyes. The cosmetic for protecting the eyes consists of the following components in percentage by weight: phase A consisting of hydrolyzed pearl, ethylene diamine tetraacetic acid, hyaluronic acid, imidazolidinyl urea and water, phase B consisting of glycerin, lubrajel, and marine algae extract, phase C consisting of carbomer resin, pouch removing toning essence, elastin, collagen, lecithin and the water and phase D consisting of witch hazel extract and triethanolamine. The invention also discloses a preparation method for the cosmetic for protecting the eyes. The formula of the cosmetic for protecting the eyes has no oil components, is rich in seawater pearl extract, the pouch removing toning essence, anti-wrinkle moisturizing factors, the hyaluronic acid and the like, and is prepared by using an advanced biological technology; the cosmetic for protecting the eyes can be easily absorbed by skin, and by using the cosmetic, the eye skin has no burden; the extracted top-level components and basic components are combined completely; and the cosmetic for protecting the eyes is all natural, has no perfume and pigment and reduces tension of the skin and the skin returns to nature.
Description
Technical field
The present invention relates to the cosmetics technical field, especially a kind of eye protection applies some make up, and preparation method thereof.
Background technology
Along with the quickening of modernized rhythm of life, add the pollution of living environment, and the popularizing gradually of computer applications, cause much human excess eye-using to occur, as the problems such as big eye pouch, black eye, crows-feet, fat granule occur of not having enough sleep.To the above-mentioned facial bad phenomenon that occurs, people generally more goes to select cosmetics to change, and the one, utilize the trophism of cosmetics itself, promotion eye part skin blood circulation recovers its vigor, reaches the minimizing eye wrinkle-removing; The 2nd, adopt cosmetics that the defective of eye is covered, change the look tired of user, reach a kind of energetic image to others; The 3rd, cosmetics itself are easy to carry, can use at any time; Other also has cosmetics can reach cleaning or revises effect such as human scent.Therefore cosmetics become requisite the articles for daily use in people's life gradually.
The cosmetics brand of circulation is more in the market, and especially external brand is occupied on market than great share, and like Estee Lauder, Lancome, SK-II etc., but their price Gao Mao is not that the Ms that likes to be beautiful of general wage-earners can afford to consume.Though there is advantage in the home brands cosmetics on price, on performance, also can't contend with foreign brand name, there are some defectives simultaneously: or overnutrition, or collocation is not good, or, fail to satisfy mass consumption person's demand because of price reasons.
Summary of the invention
The present invention is directed to deficiency, propose a kind of eye protection and apply some make up, the nutritional labeling collocation rationally improves the eye bad phenomenon.
In order to realize the foregoing invention purpose, the present invention provides following technical scheme: a kind of eye protection applies some make up, and is made up of following components in weight percentage:
A phase:
B phase:
C phase:
D phase: Radix Hamamelidis Mollis extracting solution 3%～10%
Triethanolamine 0.3%～1%.
Compared with prior art, eye protection of the present invention does not have oil ingredient in applying some make up and filling a prescription, and is rich in sea water pearls and skims the cream off milk, and goes the eye pouch convergence plain, crease-resistant NMF, and hyaluronic acid or the like adopts advanced biotechnology formulated.Accurately grasp the anti-maximum temperature requirement of each active component, avoid high temperature active influence.The high polymer dissolving is abundant, in order to avoid influence product appearance and effect.Formulation stability is good, and performance is good.Have the following advantages: be easy to skin and absorb, eye skin zero is born, and refines the complete combination of top component and basic components, and pure natural does not add essence, pigment, is the skin decompression, back to nature.
The eye protection that the present invention adopts a plurality of combination of compositions to form applies some make up, and wherein Margarita has the arresting convulsion of calming the nerves, and the heat clearing away YIN nourishing makes eye bright, and aspects such as slow down aging, freckle removing and whitening, supplement calcium all have unique effect.Modern study shows the main component of Margarita: calcium carbonate, Organic substance, water, and inorganic microelement.Be rich in peptide matters in the liquid of Margarita after hydrolysis, its composition of peptide matters is less than 50 amino acid whose low molecular weight proteins, is undertaking important regulatory function in vivo, therefore is called as biologically active peptide (also being Functional Polypeptides).The nutritive value Functional Polypeptides of Functional Polypeptides is best at the assimilation effect of intestinal, and the human body internal protein in fact major part be that form with polypeptide absorbs.After deliberation, Functional Polypeptides has its unique effect aspect beauty treatment, thereby like the situation of osseocolla polypeptide collagen synthetic low effect improvement skin that has clear improvement that ageing-related; Collagen polypeptide is rich in the hydrophilic NMF, can conserve moisture of skin, makes skin have good affinity and elasticity.
To imidazolidinyl urea is the antiseptic in a kind of cosmetics, is mainly used in the breeding that suppresses microorganism.Action principle is a slow release formaldehyde, to removing from office blue formula positive bacteria, the blue formula negative bacterium of leather, comprises that pseudomonas has fungistatic effect, and yeast, mycete are suppressed selectively.But this side chain low-molecular-weight ester can improve the coating of product and a kind of slick aftereffect sensation is arranged, and can significantly reduce product because of adding thick and heavy greasy feeling and the viscosity that UV absorbent and pigment cause.
Hyaluronic acid has special water retention; It is the best material of finding at present of occurring in nature moisture retention; (Natural moisturizing factor, NMF) for example: the water-soluble fluid power of 2% pure hyaluronic acid keeps 98% moisture securely to be called as ideal nature moisturizing factor.Hyaluronic acid is a kind of multi-functional substrate, and hyaluronic acid (hyaluronic acid) HA is distributed widely in the partes corporis humani position.Wherein skin also contains a large amount of hyaluronic acids.Ripe and the ageing process of human skin also changes along with hyaluronic content and metabolism; It can improve the skin-nourishing metabolism; Making that skin is tender, smooth, wrinkle removing, increase elasticity, prevent aging, is again the good transdermal absorption enhancer when preserving moisture.Be used with other nutritional labelings, can play the better effect that promotes alimentation.
The main component of reed fragrant plant glue (Lubrajel) is the polymethyl acid glyceride, is a kind of water-soluble not dry lubricant, and performance of keeping humidity is excellent, is widely used in particularly eye-care cosmetics of gel cosmetic products.Improve the skin sense and the lubricity of product.Good water solubility is transparent moisturizing substrate.Have dual moisture-keeping efficacy, be easy to during massage and skin absorbs, microcirculation improvement promotes cellular metabolism, adjustment skin pH value, effectively lipid regulating secretion, pore refining.Because of the polymethyl acid glyceride forms unique cagelike structure, make reed fragrant plant glue have the strong point of water-soluble skin isostearyl glyceryl pentaerythrityl ether and glossy skin isostearyl glyceryl pentaerythrityl ether concurrently, have the lock outlet capacity, be a kind of wettability equilibrium agent.
Go that main component includes 20 sour octadecanol esters, 20 acid-16-methyl-15,16-alkene Heptadecyl alcohol ester, Palmic acid, cupreol, oleanolic acid and daucosterol in the eye pouch convergence element.
Main one-tenth includes tannin, kaempferol, Quercetin in the Sargassum extract.
Main one-tenth includes close glycoprotein, polysaccharide, vitamin in the Radix Hamamelidis Mollis extracting solution.
Each component in the effect of being played during eye protection of the present invention applies some make up respectively shown in following table 1,2,3 and 4:
Table 1 is the A effect of each component mutually
| Material name | Effect |
| Hydrolyzed pearl | Preserve moisture, whiten, crease-resistant |
| Disodiumedetate | Chelating agent |
| Water | Solvent |
| Hyaluronic acid | Wetting agent |
| To imidazolidinyl urea | Antiseptic |
Table 2 is the B effect of each component mutually
| Material name | Effect |
| Glycerol | Wetting agent |
| Reed fragrant plant glue | Wetting agent |
| Sargassum extract | Preserve moisture, crease-resistant |
| Water | Solvent |
Table 3 is the C effect of each component mutually
| Material name | Effect |
| Carbomer | Thickening |
| Go the eye pouch convergence plain | Remove eye pouch |
| Elastin laminin | Repair thin tail stricture of vagina |
| Collagen protein | Crease-resistant |
| Lecithin | Crease-resistant |
| Water | Solvent |
Table 4 is the D effect of each component mutually
| Material name | Effect |
| The Radix Hamamelidis Mollis extracting solution | Crease-resistant, releive |
| Triethanolamine | Thickening, pH regulator |
The method for preparing that the present invention also provides above-mentioned eye protection to apply some make up may further comprise the steps:
1., by weight ratio with hydrolyzed pearl, disodiumedetate, to imidazolidinyl urea and water mixing, be heated with stirring to 45 ℃～65 ℃ dissolvings; Filter cleaner is cooled to 35 ℃～45 ℃ and adds hyaluronic acid, stirs, and makes the A phase;
2., by weight ratio with glycerol, reed fragrant plant glue, Sargassum extract and water mixing, be heated with stirring to 45 ℃～65 ℃ dissolvings, filter cleaner, the B phase;
3., by weight ratio will remove eye pouch convergence element, elastin laminin, collagen protein, lecithin and water mixing, be heated with stirring to 45 ℃～65 ℃ dissolvings; Filter cleaner is cooled to 35 ℃～45 ℃ and adds carbomer, and stirring and dissolving is even, gets the C phase;
4., with step 1. with the A that 2. prepares respectively mutually with B mutually, add the C phase that 3. step prepares, stir, leave standstill;
5., with the Radix Hamamelidis Mollis extracting solution of D in mutually add step 4. in the homomixture, stir, leave standstill froth breaking; Add the triethanol ammonium of D in mutually again, stir.
Preferably, step is the method for distilling of middle Margarita hydrolysate 1., may further comprise the steps:
(1), get Margarita freshwater mussel internal organs, break into meat slurry; Meat slurry is 1～2 part by weight, in the meat slurry, adds 2～4 parts of volume ratios and be 1～2: 2～4 CHCl
3: CH
3The OH mix reagent stirred 0.5～2 hour; Add 1～2 part of CHCl again
3, stirred 1～2 hour, add 1～2 part of distilled water, stirred 1～2 hour; Sucking filtration must be filtrated, and standing demix is collected CHCl
3Layer; CHCl
3Layer is under 30 ℃～40 ℃, and evacuation is removed CHCl
3With CH
3OH gets the internal organs extract;
(2), sucking filtration gained filtering residue adds the water layer in the standing demix, the isopyknic concentrated hydrochloric acid of adding behind the mixing, stirring in the step (); Treat to add alkali adjusting pH value to 6.5～7.5, standing demix after the concentrated hydrochloric acid volatilization; Add the papain of supernatant cumulative volume 0.8%～1.2%, stir, 58 ℃～65 ℃ following hydrolysis 15～30 hours; Sucking filtration is collected filtrating, with the internal organs extract mixing of step (), gets the Margarita hydrolysate.
Preferably, the nitrogen content of said hydrolyzed pearl >=2.4%.
Preferably, the step 2. method for preparing of middle Sargassum extract is with the Sargassum pulping, adds 60%～75% ethanol extraction, filters and collects filtrating, and is concentrated.
The present invention adopts pure natural Margarita freshwater mussel to carry out biological enzymolysis to react and extract the Margarita hydrolysate; Extract the effective ingredient in the pure natural Margarita freshwater mussel in two steps: the internal organs extract that step () is extracted is a docosahexenoic acid; Step (two) obtains the docosahexenoic acid mixing of hydrolysate and step () through enzymolysis, promptly gets the Margarita hydrolysate; With eye protection component that each phase the comprised stirring and evenly mixing respectively that applies some make up, in certain sequence with each phase mix homogeneously, each material can be dissolved more fully more then; Shorten the production time; Whole process operation is easy, can in the required separately temperature of each component, dissolve, and effective ingredient is discharged reach capacity; Help production operation, production process is better smooth and easy.
The specific embodiment
Describe the present invention below in conjunction with specific embodiment, the description of this part only is exemplary and explanatory, should any restriction not arranged to protection scope of the present invention.
Need to prove that the manufacturer of the employed material of following embodiment is as shown in the table respectively:
Embodiment 1
The method for preparing that eye protection applies some make up may further comprise the steps:
1, gets Margarita freshwater mussel internal organs, break into the meat slurry; The meat slurry is 1 part by weight, and 4 parts of volume ratios of adding are 1: 4 CHCl in the meat slurry
3: CH
3The OH mix reagent stirred 0.5 hour; Add 2 parts of CHCl again
3, stirred 1 hour, add 2 parts of distilled water, stirred 1 hour; Sucking filtration must be filtrated, and standing demix is collected CHCl
3Layer; CHCl
3Layer is under 40 ℃, and evacuation is removed CHCl
3With CH
3OH gets the internal organs extract;
2, sucking filtration gained filtering residue adds the water layer in the standing demix in the step 1, adds isopyknic concentrated hydrochloric acid behind the mixing, stirs; Treat to add alkali adjusting pH value to 6.5, standing demix after the concentrated hydrochloric acid volatilization; Add the papain of supernatant cumulative volume 1.2%, stir, 58 ℃ of following hydrolysis 30 hours; Sucking filtration is collected filtrating, with the internal organs extract mixing of step 1, gets hydrolyzed pearl;
3, get step 2 hydrolyzed pearl, disodiumedetate, to imidazolidinyl urea and water mixing, be heated with stirring to 65 ℃; Filter cleaner is cooled to 35 ℃ and adds hyaluronic acid, stirs, and makes the A phase; Wherein Margarita hydrolysate, disodiumedetate, imidazolidinyl urea and water are respectively 2%, 0.5%, 0.1%, 0.5%, 10% at the shared weight content of output aggregate;
4, with glycerol, reed fragrant plant glue, Sargassum extract and water mixing, be heated with stirring to 45 ℃, filter cleaner gets the B phase; Wherein glycerol, reed fragrant plant glue, Sargassum extract and water are respectively 10%, 2%, 5%, 10% at the shared weight content of output aggregate;
5, will remove eye pouch convergence element, elastin laminin, collagen protein, lecithin and water mixing, be heated with stirring to 65 ℃; Filter cleaner is cooled to 35 ℃ and adds carbomer, stirs, and gets the C phase; Wherein carbomer, go eye pouch convergence element, elastin laminin, collagen protein, lecithin and water to be respectively 1%, 0.2%, 0.5%, 0.2%, 0.5%, 40% at the shared weight content of output aggregate;
6, the A that step 3 and 4 is prepared respectively mutually with B mutually, add the C phase of step 5 preparation, stir, leave standstill;
7, with in the homomixture in the Radix Hamamelidis Mollis extracting solution adding step 6, stir, leave standstill froth breaking; Add the triacetic acid ammonium again, stir, promptly get eye protection and apply some make up; Wherein Radix Hamamelidis Mollis extracting solution and triacetic acid ammonium are respectively 10% and 0.3% at the shared weight content of output aggregate.
Embodiment 2
The method for preparing that eye protection applies some make up may further comprise the steps:
1, gets Margarita freshwater mussel internal organs, break into the meat slurry; The meat slurry is 2 parts by weight, and 2 parts of volume ratios of adding are 1: 1 CHCl in the meat slurry
3: CH
3The OH mix reagent stirred 2 hours; Add 1 part of CHCl again
3, stirred 2 hours, add 1 part of distilled water, stirred 2 hours; Sucking filtration must be filtrated, and standing demix is collected CHCl
3Layer; CHCl
3Layer is under 30 ℃, and evacuation is removed CHCl
3With CH
3OH gets the internal organs extract;
2, sucking filtration gained filtering residue adds the water layer in the standing demix in the step 1, adds isopyknic concentrated hydrochloric acid behind the mixing, stirs; Treat to add alkali adjusting pH value to 7.5, standing demix after the concentrated hydrochloric acid volatilization; Add the papain of supernatant cumulative volume 0.8%, stir, 65 ℃ of following hydrolysis 15 hours; Sucking filtration is collected filtrating, with the internal organs extract mixing of step 1, gets hydrolyzed pearl;
3, get step 2 hydrolyzed pearl, disodiumedetate, to imidazolidinyl urea and water mixing, be heated with stirring to 45 ℃; Filter cleaner is cooled to 45 ℃ and adds hyaluronic acid, stirs, and makes the A phase; Wherein Margarita hydrolysate, disodiumedetate, imidazolidinyl urea and water are respectively 5%, 0.1%, 0.5%, 0.2%, 20% at the shared weight content of output aggregate;
4, with glycerol, reed fragrant plant glue, Sargassum extract and water mixing, be heated with stirring to 65 ℃, filter cleaner gets the B phase; Wherein glycerol, reed fragrant plant glue, Sargassum extract and water are respectively 3%, 8%, 2%, 20% at the shared weight content of output aggregate;
5, will remove eye pouch convergence element, elastin laminin, collagen protein, lecithin and water mixing, be heated with stirring to 45 ℃; Filter cleaner is cooled to 35 ℃ and adds carbomer, stirs, and gets the C phase; Wherein carbomer, go eye pouch convergence element, elastin laminin, collagen protein, lecithin and water to be respectively 0.2%, 1%, 0.2%, 0.5%, 0.2%, 50% at the shared weight content of output aggregate;
6, the A that step 3 and 4 is prepared respectively mutually with B mutually, add the C phase of step 5 preparation, stir, leave standstill;
7, with in the homomixture in the Radix Hamamelidis Mollis extracting solution adding step 6, stir, leave standstill froth breaking; Add the triacetic acid ammonium again, stir, promptly get eye protection and apply some make up; Wherein Radix Hamamelidis Mollis extracting solution and triacetic acid ammonium are respectively 3% and 1% at the shared weight content of output aggregate.
Embodiment 3
The method for preparing that eye protection applies some make up may further comprise the steps:
1, gets Margarita freshwater mussel internal organs, break into the meat slurry; The meat slurry is 1.5 parts by weight, and 3 parts of volume ratios of adding are 1.5: 2.5 CHCl in the meat slurry
3: CH
3The OH mix reagent stirred 1 hour; Add 1.5 parts of CHCl again
3, stirred 1.2 hours, add 1.6 parts of distilled water, stirred 1.5 hours; Sucking filtration must be filtrated, and standing demix is collected CHCl
3Layer; CHCl
3Layer is under 35 ℃, and evacuation is removed CHCl
3With CH
3OH gets the internal organs extract;
2, sucking filtration gained filtering residue adds the water layer in the standing demix in the step 1, adds isopyknic concentrated hydrochloric acid behind the mixing, stirs; Treat to add alkali adjusting pH value to 7, standing demix after the concentrated hydrochloric acid volatilization; Add the papain of supernatant cumulative volume 1.0%, stir, 62 ℃ of following hydrolysis 20 hours; Sucking filtration is collected filtrating, with the internal organs extract mixing of step 1, gets hydrolyzed pearl;
3, get step 2 hydrolyzed pearl, disodiumedetate, to imidazolidinyl urea and water mixing, be heated with stirring to 53 ℃; Filter cleaner is cooled to 38 ℃ and adds hyaluronic acid, stirs, and makes the A phase; Wherein Margarita hydrolysate, disodiumedetate, imidazolidinyl urea and water are respectively 4%, 0.2%, 0.3%, 0.4%, 13% at the shared weight content of output aggregate;
4, with glycerol, reed fragrant plant glue, Sargassum extract and water mixing, be heated with stirring to 56 ℃, filter cleaner gets the B phase; Wherein glycerol, reed fragrant plant glue, Sargassum extract and water are respectively 6%, 4%, 3%, 17% at the shared weight content of output aggregate;
5, will remove eye pouch convergence element, elastin laminin, collagen protein, lecithin and water mixing, be heated with stirring to 50 ℃; Filter cleaner is cooled to 42 ℃ and adds carbomer, stirs, and gets the C phase; Wherein carbomer, go eye pouch convergence element, elastin laminin, collagen protein, lecithin and water to be respectively 0.6%, 0.4%, 0.3%, 0.4%, 0.3%, 43% at the shared weight content of output aggregate;
6, the A that step 3 and 4 is prepared respectively mutually with B mutually, add the C phase of step 5 preparation, stir, leave standstill;
7, with in the homomixture in the Radix Hamamelidis Mollis extracting solution adding step 6, stir, leave standstill froth breaking; Add the triacetic acid ammonium again, stir, promptly get eye protection and apply some make up; Wherein Radix Hamamelidis Mollis extracting solution and triacetic acid ammonium are respectively 8% and 0.6% at the shared weight content of output aggregate.
Embodiment 4
The method for preparing that eye protection applies some make up may further comprise the steps:
1, gets Margarita freshwater mussel internal organs, break into the meat slurry; The meat slurry is 1.8 parts by weight, and 3.5 parts of volume ratios of adding are 2: 3 CHCl in the meat slurry
3: CH
3The OH mix reagent stirred 1.5 hours; Add 1.6 parts of CHCl again
3, stirred 1.2 hours, add 1.7 parts of distilled water, stirred 1.5 hours; Sucking filtration must be filtrated, and standing demix is collected CHCl
3Layer; CHCl
3Layer is under 34 ℃, and evacuation is removed CHCl
3With CH
3OH gets the internal organs extract;
2, sucking filtration gained filtering residue adds the water layer in the standing demix in the step 1, adds isopyknic concentrated hydrochloric acid behind the mixing, stirs; Treat to add alkali adjusting pH value to 7.5, standing demix after the concentrated hydrochloric acid volatilization; Add the papain of supernatant cumulative volume 1.1%, stir, 60 ℃ of following hydrolysis 22 hours; Sucking filtration is collected filtrating, with the internal organs extract mixing of step 1, gets hydrolyzed pearl;
3, get step 2 hydrolyzed pearl, disodiumedetate, to imidazolidinyl urea and water mixing, be heated with stirring to 55 ℃; Filter cleaner is cooled to 41 ℃ and adds hyaluronic acid, stirs, and makes the A phase; Wherein Margarita hydrolysate, disodiumedetate, imidazolidinyl urea and water are respectively 4%, 0.2%, 0.4%, 0.3%, 14% at the shared weight content of output aggregate;
4, with glycerol, reed fragrant plant glue, Sargassum extract and water mixing, be heated with stirring to 56 ℃, filter cleaner gets the B phase; Wherein glycerol, reed fragrant plant glue, Sargassum extract and water are respectively 5%, 6%, 3%, 14% at the shared weight content of output aggregate;
5, will remove eye pouch convergence element, elastin laminin, collagen protein, lecithin and water mixing, be heated with stirring to 53 ℃; Filter cleaner is cooled to 37 ℃ and adds carbomer, stirs, and gets the C phase; Wherein carbomer, go eye pouch convergence element, elastin laminin, collagen protein, lecithin and water to be respectively 0.7%, 0.5%, 0.3%, 0.3%, 0.4%, 48% at the shared weight content of output aggregate;
6, the A that step 3 and 4 is prepared respectively mutually with B mutually, add the C phase of step 5 preparation, stir, leave standstill;
7, with in the homomixture in the Radix Hamamelidis Mollis extracting solution adding step 6, stir, leave standstill froth breaking; Add the triacetic acid ammonium again, stir, promptly get eye protection and apply some make up; Wherein Radix Hamamelidis Mollis extracting solution and triacetic acid ammonium are respectively 6% and 0.5% at the shared weight content of output aggregate.
Adopt the prepared product of the foregoing description, select 20～50 years old Ms of different skin matter to use, compare operating position such as following each table with the result of use of commercially available eye cream product.
Method for using: after clean, dip in nameless abdomen and to get an amount of product, press palpebra inferior and canthus skin gently for several times, softly be massaged into absorption then from inside to outside.
Test Example 1, be 20～30 ℃ in the weather mass dryness fraction, relative humidity is 60～90%, and 80 Mries dry skin are divided into two groups: one group is used embodiment 1 product; Another group is divided equally five kinds of commercially available eye creams of use; Through 2 months effects relatively, the result sees the following form 1.
Table 1, dry skin
Test Example 2, be 20～30 ℃ in the weather mass dryness fraction, relative humidity is 60～90%, and 80 Mries neutral skin are divided into two groups: one group is used embodiment 2 products; Another group is divided equally five kinds of commercially available eye creams of use; Through 2 months effects relatively, the result sees the following form 2.
Table 2 neutral skin
Test Example 3, be 20～30 ℃ in the weather mass dryness fraction, relative humidity is 60～90%, and 80 Mries mixed skin are divided into two groups: one group is used embodiment 3 products; Another group is divided equally five kinds of commercially available eye creams of use; Through 2 months effects relatively, the result sees the following form 3.
Table 3, mixed skin
Test Example 4, be 20～30 ℃ in the weather mass dryness fraction, relative humidity is 60～90%, and 80 Mries oily skin are divided into two groups: one group is used embodiment 4 products; Another group is divided equally five kinds of commercially available eye creams of use; Through 2 months effects relatively, the result sees the following form 4.
Table 4, oily skin
To sum up four forms are said, and product of the present invention obviously is better than commercially available brand eye cream to the eye problem effective percentage of all kinds of skin matter, reach 91.3% at effective percentage aspect moist the preserving moisture; Reach 80% at effective percentage aspect the desalination microgroove, reach 71.3% at effective percentage aspect the black eye of dispelling; Reach 70% at effective percentage aspect the eye pouch of dispelling; Reach 96.3% at effective percentage aspect the fat granule of dispelling.
Therefore explain that product of the present invention has following effect:
1, effectively prevents and improve eye microgroove, crows-feet; Prevent that the eye skin is lax sagging; Effectively alleviate black eye, eye pouch etc.
2, effectively replenish skin loss collagen, keep collagen fiber and elastic fibers vigor, alleviate the eye skin ageing.
3, can prevent fibrous tissue sclerosis and aging for skin replenishes and the pinning adequate water, make skin around the eyes jade-like stone profit, full, dynamic.
4, the fatigue of effectively releiving is shone eye life.
It below only is preferred implementation of the present invention; Should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention; Can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. an eye protection applies some make up, and is made up of following components in weight percentage:
2. one kind prepares the method that the said eye protection of claim 1 applies some make up, and may further comprise the steps:
1., by weight ratio with hydrolyzed pearl, disodiumedetate, to imidazolidinyl urea and water mixing, be heated with stirring to 45 ℃～65 ℃; Filter cleaner is cooled to 35 ℃～45 ℃ and adds hyaluronic acid, and stirring and dissolving is even, makes the A phase;
2., by weight ratio with glycerol, reed fragrant plant glue, Sargassum extract and water mixing, be heated with stirring to 45 ℃～65 ℃ dissolvings, filter cleaner, the B phase;
3., by weight ratio will remove eye pouch convergence element, elastin laminin, collagen protein, lecithin and water mixing, be heated with stirring to 45 ℃～65 ℃ dissolvings; Filter cleaner is cooled to 35 ℃～45 ℃ and adds carbomer, and stirring and dissolving is even, gets the C phase;
4., with step 1. with the A that 2. prepares respectively mutually with B mutually, add the C phase that 3. step prepares, stir, leave standstill;
5., with the Radix Hamamelidis Mollis extracting solution of D in mutually add step 4. in the homomixture, stir, leave standstill froth breaking; Add the triethanol ammonium of D in mutually again, stir.
3. method as claimed in claim 2 is characterized in that: step is the method for distilling of middle hydrolyzed pearl 1., may further comprise the steps:
(1), get Margarita freshwater mussel internal organs, break into meat slurry; Meat slurry is 1～2 part by weight, in the meat slurry, adds 2～4 parts of volume ratios and be 1～2: 2～4 CHCl
3: CH
3The OH mix reagent stirred 0.5～2 hour; Add 1～2 part of CHCl again
3, stirred 1～2 hour, add 1～2 part of distilled water, stirred 1～2 hour; Sucking filtration must be filtrated, and standing demix reclaims CHCl
3Layer; CHCl
3Layer is under 30 ℃～40 ℃, and evacuation is removed CHCl
3With CH
3OH gets the internal organs extract;
(2), sucking filtration gained filtering residue adds the water layer in the standing demix, the isopyknic concentrated hydrochloric acid of adding behind the mixing, stirring in the step (); Treat to add alkali adjusting pH value to 6.5～7.5, standing demix after the concentrated hydrochloric acid volatilization; Add the papain of supernatant cumulative volume 0.8%～1.2%, stir, 58 ℃～65 ℃ following hydrolysis 15～30 hours; Sucking filtration is collected filtrating, with the internal organs extract mixing of step (), gets the Margarita hydrolysate.
4. like claim 2 or 3 described methods, it is characterized in that: the nitrogen content of said hydrolyzed pearl >=2.4%.
5. method as claimed in claim 2 is characterized in that: the step 2. method for preparing of middle Sargassum extract is with the Sargassum pulping, adds 60%～75% ethanol extraction, filters to collect and filtrates, and is concentrated.
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| DE102011078260A1 (en) * | 2011-06-29 | 2013-01-03 | Beiersdorf Ag | Cosmetic product e.g. cloth from a composition comprising either an inorganic compound or an extract with inorganic compound, or pearl hydrolyzate and a nonwoven comprising fibers of cotton and/or bamboo |
| CN103006524A (en) * | 2012-11-28 | 2013-04-03 | 西安泰科迈医药科技有限公司 | Anti-wrinkle anti-aging eye cream for pregnant women and preparation method thereof |
| CN103222935B (en) * | 2013-04-27 | 2015-07-15 | 西北农林科技大学 | Armeniaca sibirica oil skin-moisturizing lotion and preparation method thereof |
| CN104207959B (en) * | 2013-06-05 | 2018-06-26 | 陈慧敏 | A kind of eye compacts Essence |
| CN103655336B (en) * | 2013-12-11 | 2015-04-29 | 诺斯贝尔(中山)无纺日化有限公司 | Collagen eye massaging gel |
| CN105662911A (en) * | 2016-03-02 | 2016-06-15 | 佛山市万盈化妆品有限公司 | Ocular region roll-on essence containing bone collagen |
| CN105662912A (en) * | 2016-03-02 | 2016-06-15 | 佛山市万盈化妆品有限公司 | Preparation method of ossein-containing eye roll-on essence |
| CN114504550B (en) * | 2022-04-18 | 2022-08-19 | 中山大学中山眼科中心 | Eye gel containing metronidazole and preparation method thereof |
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|---|---|---|---|---|
| CN101288640A (en) * | 2008-05-23 | 2008-10-22 | 海南京润珍珠生物技术股份有限公司 | Anti-acne essence added with pearl hydrolysate liposome |
| CN101313887A (en) * | 2008-05-23 | 2008-12-03 | 海南京润珍珠生物技术股份有限公司 | Whitening scream with additive pearl hydrolysate liposome |
| CN101697956A (en) * | 2009-10-19 | 2010-04-28 | 海南京润珍珠生物技术股份有限公司 | Anti-acne jelly with pearl hydrolyzate liposome |
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|---|---|
| CN102133169A (en) | 2011-07-27 |
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