CN104490732B - A kind of anti-aging scale collagen polypeptide facial mask and preparation method thereof - Google Patents
A kind of anti-aging scale collagen polypeptide facial mask and preparation method thereof Download PDFInfo
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- CN104490732B CN104490732B CN201410775834.XA CN201410775834A CN104490732B CN 104490732 B CN104490732 B CN 104490732B CN 201410775834 A CN201410775834 A CN 201410775834A CN 104490732 B CN104490732 B CN 104490732B
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Abstract
The invention discloses a kind of scale collagen polypeptide facial mask, contain following component：The parts by weight of scale collagen polypeptide powder 1~20, the parts by weight of gadol extract 0.5~3, the parts by weight of marine algae extract 1~2, the parts by weight of glycerine 3~6, the parts by weight of olive oil 1~4, the parts by weight of pearl powder 1~3, the parts by weight of talcum powder 10~30, the parts by weight of film forming agent 10~30, the parts by weight of Tween 80 1~2, the parts by weight of preservative 0.10~1.2.Gained facial mask has the function that nourishes rough skin, beautifying face and moistering lotion.
Description
Technical field
The present invention relates to daily use chemicals technical field, and in particular to one kind cleaning skin of face, makes elasticity of skin compact, has and mend
Fill skin nutrition, the facial mask of deferring senility.
Background technology
Collagen is protein component main in skin histology, the 70%~80% of skin dry weight is accounted for, by corium
Fibrocyte (Fibroblasts) manufacture, collagen is a kind of white, transparent, branchiess fibrillation, is a kind of in itself
Very firm protein, in youth, health, less in by the skin of sun damages, it forms the slightly curved fiber of a branch of beam, mutually
With last layer and next layer of formation right-angle array, this makes skin obtain solid effect.But when the years increase, collagen is not
But quantity reduce, and arrangement also become irregular, corium thus it is thinning；Environmental factor is easier to make collagen dissolving disappear
Losing causes the aging of skin.Exactly because the loss of collagen causes the collagen peptide bond for supporting skin and elasticated net fracture, its
Spiral net-shaped structure is destroyed immediately, and skin histology is oxidized, atrophy, collapsed, and dryings, wrinkle, loose nothing just occurs in skin
The aging phenomenons such as elasticity.Supplementing enough collagens can stimulate the fibroblast in skin corium voluntarily to carry out collagen
Secretion so that voluntarily generting machanism and metabolic function recover normal to collagen, so effectively the relaxation of delaying skin with it is old
Change.Zoopery shows that after smearing skin with the lotion containing collagen, epiderm skin and dermis can effectively change
It is kind, and promote the synthesis of collagen in skin.Real medical science often carries out beauty with collagen, and collagen can directly act on
The impaired collagenous fibres of skin corium, make it recover transverse flow fiber configuration rapidly.Collagen unique triple-helix structure and glue
Hydrophilic group in former protein molecular, enhances skin primary hydrodynamic force, ensures that moisture in the circulation of skin surface and deep layer, changes
Kind Lymphatic Circulation, make skin water profit full vibrant.But collagen molecules amount is big, being directly added into cosmetics can not be by skin
Directly absorb.
At present, what collagen production was extracted is mainly derived from three class materials：Ossein, deep-sea fish fish-skin, fish scale.Wherein
Ossein easily obtains essentially from the animals such as pig, ox, sheep, raw material, and raw material source is stable, but the ossein of Animal Bone extraction contains
Compared with fattiness, ossein purity is slightly lower, and beauty performance is slightly worse, and due to religion and Animal diseases, animal ossein
The market share it is less and less.It is mainly skin deep-sea cod for producing the deep-sea fish fish-skin of collagen, fish skin collagen
Protein content is high, function admirable, but cod belongs to cold aqueous demersal fishes, lives in below 300 meters of sea, can not manually enter
Row cultivation, acquisition difficulty is larger, and technical requirements are high.Tilapia mossambica, present sieve are mainly derived from for producing the fish scale of collagen
Non- fish is the cultured freshwater fish of the emphasis scientific research culture of world's aquatic products industry, and be described as animal protein main source it
One.Relative to ossein, fish skin collagen, scale collagen has the advantage of the two concurrently；And pass through detection, the hydroxyl of fish scale collagen
Proline content is higher than other raw materials, and because collagen peptide is similar to the structure of application on human skin collagen in fish scale, compatibility is good, by
Collagen product prepared by fish scale, it is easier to be absorbed by the skin.
Rhodiola root Latin name Rhodiola rosea, English name Roseroot, are Crassulaceae renascent herb or filling
Wood plant, it is grown in the rare wild plant of the high and cold contamination-freely band of 800~2500 meters of height above sea level.Traditional medicine is often used for Asia
Material, the applicating history of rhodiola root is long, gadol extract Main Ingredients and Appearance rhodioside and rhodiola root aglycon, has and delays to decline
The function such as always, whitening, radioresistance, moistening skin and eliminating spot.《Sheng Nong's herbal classic》Rhodiola root is classified as top grade in medicine, rhodiola root is taken and makes light of one's life by commiting suicide
QI invigorating, not old macrobiosis, nontoxic more clothes, long term usage are not hurted sb.'s feelings.《Modern practical book on Chinese herbal medicine》Say that its effect has seven, i.e., " one, CNS inhibition make
With.2nd, antifatigue effect.3rd, cardiotonic.4th, antiinflammatory action.5th, blood glucose rise effect is suppressed.6th, Hardy dwarfing.
7th, resisting microwave radiation acts on ".
Marine algae extract (Sesmollient) is a kind of pure natural marine organisms product.Contain phycocolloid acid, thick egg in it
In vain, multivitamin, enzyme and trace element.Such nutrition can reduce surface blood fat after skin absorbs, and promote surface skin and make
Blood function, and also have and lose weight, insulation, the function of thickening.Marine algae extract has many uses, and production can be increased by adding in skin care item
The smooth sensation of product, crease-resistant so as to impart its additionally containing substantial amounts of anion, the performance of anti-aging.
Pearl powder mainly produces pearl with the freshwater shellfish animal such as hydriopsis cumingii, cristaria plicata, pteria martensii, grinds
The powder formed, white or off-white color, using physical method manufacture, it is characterized in being added without any other material,
Any material is not destroyed, maintains all nutritional ingredients of pearl.Pearl powder is used for beauty, can solve the problems, such as face oil and dead skin.
《Compendium of Materia Medica》Record：" salty sweet nontoxic, the relieving palpitation point mesh of trembling with fear of pearl taste.Painting face, make us moist good color.Brothers are applied, go skin inverse
Set out, solution acne treats poison.Confirmed through modern science, contained serine in pearl, methionine, lysine, pearl protein amino acid,
The main nutrient composition such as alkaline phosphate and taurine has the improvement care effect of uniqueness to skin.
The natural collagen protein that macromolecular is directly added into cosmetics is difficult to be absorbed by the skin, therefore collagen is used as
Molecular weight less hydrolytic collagen peptide is used during skin care raw material.Fish scale collagen peptide used in the present invention, it is to use biology enzyme
Directional enzymatic technology cuts into the collagen orientation for being difficult to directly absorb the small active peptides of suitable absorption of human body, enhancing
Its water-soluble and permeability.Collagen polypeptide and the active material in gadol extract, marine algae extract, pearl powder in facial mask
It is combined, supplements skin nutrition composition, increase skin elasticity, prevents and to anti-wrinkle, anti-aging.
The content of the invention
It is more with scale collagen it is an object of the invention to provide a kind of facial mask of anti-skin of face aging and preparation method thereof
Peptide, gadol extract, marine algae extract, pearl powder are that main active ingredient combinations form.
Facial mask of the present invention is as made by the raw material of following weight：
A kind of scale collagen polypeptide facial mask, contains following component：The parts by weight of scale collagen polypeptide 1~20, rhodiola root extraction
The parts by weight of thing 0.5~3, the parts by weight of marine algae extract 1~2, the parts by weight of glycerine 3~6, the parts by weight of olive oil 1~4, pearl powder 1~
3 parts by weight, the parts by weight of talcum powder 10~30, the parts by weight of film forming agent 10~30, the parts by weight of Tween 80 1~2, preservative 0.10~
1.2 parts by weight.
Described film forming agent, described film forming agent are made up of carboxymethyl cellulose and PVP, and carboxymethyl cellulose is with gathering
It is 3~5: 5~7 to tie up ketone weight ratio.
Described preservative, is made up of methyl p-hydroxybenzoate and propylparaben, P-hydroxybenzoic acid first
Ester is 4: 1 with propylparaben weight ratio.
The scale collagen polypeptide, it is made by following preparation methods：Fish scale is taken, clear water is cleaned, low temperature drying, is crushed, is added
Enter 1% hydrochloric acid solution, 10 times of amounts, soak 12 hours, stir frequently, change hydrochloric acid solution, continue immersion 12 hours, filtering；Clear water
Rinsing for several times, adds in 10 times of amount saturated limewaters, soaks 12 hours, stir frequently, change saturated limewater, continue immersion 12
Hour, filtering；Filter residue with again with purifying water washing, adding 15~20 times of amount purified waters after originally water washing, control ph 6.5~
7.5th, temperature adds papain at 45~55 DEG C, and the enzyme and filter residue ratio are 0.5~3.0kg: 100kg, mixing speed
100~300r/min, 0.5~1.5 hour time, 3~8 hours are incubated, boils 30min, inactivator；Control ph 1.0~
3.0th, temperature adds pepsin at 55~70 DEG C, and the enzyme and filter residue ratio are 0.1~3.0kg: 100kg, mixing speed 100
~300r/min, 1~3 hour is incubated, boils 30min, inactivator；Filtering, filtrate spray drying, is produced.
The gadol extract, it is outsourcing product, can also prepares, its preparation method is：By dry rhodiola root raw material
Crush, cross 10 mesh sieves, add 80% ethanol water, 6 times of amounts, stirring immersion 30 minutes, be heated to 90 DEG C, insulation extraction 2h, mistake
Filter, collect filtrate.Filter residue adds the amount stirring immersion 30 minutes of 4 times of 80% ethanol water, is heated to 90 DEG C, insulation extraction
1.5h, filtering, collect filtrate.Merge extract solution twice, be concentrated under reduced pressure into no alcohol taste, obtain medicinal extract.Medicinal extract is taken, resin is added, stirs
Mix to be adsorbed in waste liquid and detected without rhodioside, collect resin, a large amount of clear water rinsings, take the resin dress post after rinsing, clear water drift
Saliva is washed till out to close bottom valve in neutrality without color, pH value, add 90% ethanol, soak 30min, add 90% ethanol, beat
It is 2L/min to open bottom valve coutroi velocity, collects eluent, when amount of alcohol is 1.5 times of amount of resin, terminates elution.Eluent is taken to subtract
Pressure is concentrated into no alcohol taste, is spray-dried, produces.
The marine algae extract, it is outsourcing product, can be also made up of following methods：Marine alga is taken, clear water cleans three times, removes
Salt and other impurities；Dry.Crush, cross 20 mesh sieves, freezed at -20 DEG C, using 95% ethanol as solvent, melt vibration at 45 DEG C
2h is extracted, is extracted 3 times, merges extract solution, 3500r/min centrifuges 10min, collects supernatant；Rotary evaporator concentrates, and 50
Dry to constant weight, produce at DEG C.
The pearl powder, it is made up of following methods：Fresh water pearl is taken, clear water is cleaned, and drying, pulverizer crushes, and crosses 80-
120 mesh sieves obtain pearl powder.
Invention additionally discloses a kind of preparation method of anti-aging scale collagen peptide facial mask, it is characterized in that more with scale collagen
Peptide, gadol extract, marine algae extract, pearl powder etc. are function raw material, with film forming agent, talcum powder, glycerine, olive oil and are told
Temperature 80 is auxiliary material, and each component comprises the following steps that with weight ratio meter in raw material：
(1) 10~30 parts of film forming agent (3~5 parts of carboxymethyl cellulose, 5~7 parts of PVP) is taken, is dissolved with ethanol, is stirred
Uniformly.
(2) 1~3 part of pearl powder, 10~30 parts of talcum powder are taken, 3~6 parts of glycerine is placed in container, adds deionized water 60
~90 parts, 70~90 DEG C are heated to, is stirred and evenly mixed.
(3) (2) step temperature is maintained, (1) step gains are added thereto, stirred.
(4) by (3) step gains, temperature control is sequentially added into 1~2 part of Tween 80 while stirring at 45~55 DEG C,
1~4 part of olive oil, 1~20 part of scale collagen polypeptide, stirs
(5) control temperature is down to 40 DEG C, adds 0.5~3 part of gadol extract, 1~2 part of marine algae extract, preservative
0.10~1.2 part, it is well mixed, cools down and produce.
The application method of facial mask of the present invention is：Before facial mask, first deeply cleaning is facial, then facial mask is coated on into face
Portion, after 15~25 minutes, facial mask active material is absorbed by the skin, moisture evaporation, and thin film is gradually formed in face, and this is thin
Film is peeled off from face, and the dirt, scurf on skin of face are also adhered on film in company with and be eliminated, face seem totally, light
It is sliding.
The product beneficial effect of the present invention is as follows：
(1) main active of the invention is that natural animal-plant extraction obtains, and is had no toxic side effect, and raw material easily obtains,
Extraction process is simple, is commercially available product, moderate.
(2) fish scale collagen peptide of the invention, safe, disease contamination risk is low；Content of peptides is high, and molecular weight is small, easily
Water is dissolved in, effectively can directly be absorbed by skin, deep layer nourishes rough skin.
(3) fish scale collagen peptide used in the present invention, discarded object of the raw material from processing of aquatic products, aquaculture is improved
Added value, while reduce environmental pollution and the wasting of resources.
(4) raw material scale collagen Gly-His-Lys of the present invention, gadol extract, marine algae extract, pearl powder are used in mixed way, formula
Rationally, there is Synergistic, strengthen anti aging effect effect, rhodiola root has aromatic odor, while improves product gas
Taste, without adding essence, increase Product Safety.
Embodiment
Below by specific embodiment, the present invention is described in further detail.
Embodiment 1
The preparation of scale collagen polypeptide：
Fish scale is taken, clear water is cleaned, low temperature drying, is crushed, and is added 1% hydrochloric acid solution, 10 times of amounts, is soaked 12 hours, stir frequently
Mix, change hydrochloric acid solution, continue immersion 12 hours, filtering；Clear water rinses for several times, adds in 10 times of amount saturated limewaters, immersion
12 hours, stir frequently, change saturated limewater, continue immersion 12 hours, filtering；Filter residue uses purifying again after using originally water washing
Water washing, filter residue 10kg is taken, add 20 times of amount purified waters, control ph adds papain in 6.9, temperature at 50 DEG C
0.1kg, mixing speed 130r/min, 1.5 hours time, 6 hours are incubated, boils 30min, inactivator；Control ph 2.0,
Temperature adds pepsin 0.05kg at 65 DEG C, and speed 130r/min is stirred 1 hour, is incubated 3 hours, is boiled 30min, is inactivated
Enzyme；Filtering, filtrate spray drying, is produced.
The scale collagen polypeptide as made from process above, after sampled, analysis test, content of peptides 96.65%, and institute
Product be in pale powder, be easily soluble in water, after dissolving smell it is pure and fresh, without fishy smell.
Embodiment 2
Following each component is with weight ratio meter：
(1) 12 parts of carboxymethyl cellulose is taken, 18 parts of PVP, is dissolved, stirred with ethanol.
(2) 2 parts of pearl powder, 30 parts of talcum powder are taken, 6 parts of glycerine is placed in container, is added 90 parts of deionized water, is heated to 75
DEG C, stir and evenly mix.
(3) (2) step temperature is maintained, (1) step gains are added thereto, stirred.
(4) by (3) step gains, temperature control is sequentially added into 1 part of Tween 80, olive oil 2 while stirring at 45 DEG C
Part, 2 parts of fish scale collagen peptide, stir
(5) control temperature is down to 40 DEG C, adds 1 part of gadol extract, 1 part of marine algae extract, 0.15 part of preservative, mixes
Close uniformly, cooling, obtain scale collagen polypeptide facial mask.
Embodiment 3
(1) 6 parts of carboxymethyl cellulose is taken, 14 parts of PVP, is dissolved, stirred with ethanol.
(2) 3 parts of pearl powder, 20 parts of talcum powder are taken, 4 parts of glycerine is placed in container, is added 75 parts of deionized water, is heated to 70
DEG C, stir and evenly mix.
(3) (2) step temperature is maintained, (1) step gains are added thereto, stirred.
(4) by (3) step gains, temperature control is sequentially added into 1.5 parts of Tween 80s, olive while stirring at 50 DEG C
3 parts of oil, 4 parts of fish scale collagen peptide, stirs
(5) control temperature is down to 40 DEG C, adds 0.5 part of gadol extract, 1 part of marine algae extract, 0.2 part of preservative,
It is well mixed, cooling, obtain scale collagen polypeptide facial mask.
Embodiment 4
(1) 5 parts of carboxymethyl cellulose is taken, 5 parts of PVP, is dissolved, stirred with ethanol.
(2) 1 part of pearl powder, 10 parts of talcum powder are taken, 3 parts of glycerine is placed in container, is added 60 parts of deionized water, is heated to 80
DEG C, stir and evenly mix.
(3) (2) step temperature is maintained, (1) step gains are added thereto, stirred.
(4) by (3) step gains, temperature control is sequentially added into 2 parts of Tween 80s, olive oil 4 while stirring at 50 DEG C
Part, 2 parts of fish scale collagen peptide, stir
(5) control temperature is down to 40 DEG C, adds 1 part of gadol extract, 1.5 parts of marine algae extract, 0.2 part of preservative,
It is well mixed, cooling, obtain scale collagen polypeptide facial mask.
Test example 1
Facial mask curative effect provided by the invention is illustrated using experiment below by human body：
(1) general information
Select health, no skin disease and allergies, the experimenter of non-sensitive skin 75.Wherein man 4, female 71
Example, it is 28~61 years old age, average 49 years old.
(2) application method
After experimenter's clean skin, the facial mask made from embodiment 2 carries out half face surface application of left side, first three day, uses just before going to bed daily
Once, hereafter every three days, just before going to bed using once, it is used continuously one month；The face of right side half only does general duty nursing.
(3) evaluation method
In using for the 4th weekend, felt with subject to being given a mark on the left of oneself face compared with right side.Marking refers to
It is designated as 5：Skin elasticity, moisture of skin, wrinkle (predominantly forehead, upper palpebra inferior, paropia, mouth week position), skin smooth
Degree, skin colourity.Each individual event significantly improves+2 points, improves+1 point, unchanged or+0 point of variation, full marks 10 divide.
(4) evaluation criterion
Efficacy determination be divided into significantly effectively, effectively, minor effect and invalid four kinds：
Significantly effectively：Score >=8 point；
Effectively：3 points of ＜ scores ＜ 8 divide；
Minor effect：0 point of ＜ score≤3 point；
It is invalid：Score≤0.
Total effective rate=significantly effectively+effectively+minor effect,
Obvious effective rate=significantly effectively+effectively.
(5) experimental result
In 75 using this facial mask, significantly effective 18, effective 29, minor effect 24, invalid 4, total effective rate
95.7%, obvious effective rate 62.7%, details see the table below
Claims (6)
1. a kind of scale collagen polypeptide facial mask, contains following component：The parts by weight of scale collagen polypeptide 1~20, gadol extract
0.5~3 parts by weight, the parts by weight of marine algae extract 1~2, the parts by weight of glycerine 3~6, the parts by weight of olive oil 1~4, pearl powder 1~3
Parts by weight, the parts by weight of talcum powder 10~30, the parts by weight of film forming agent 10~30, the parts by weight of Tween 80 1~2, preservative 0.10~
1.2 parts by weight；Described scale collagen polypeptide is prepared as follows：Fish scale is taken, clear water is cleaned, low temperature drying, is crushed, and is added
1% 10 times of hydrochloric acid solution is measured, and is soaked 12 hours, is stirred frequently, changes hydrochloric acid solution, continues immersion 12 hours, filtering；Clear water floats
Wash for several times, add 10 times of amount saturated limewaters, soak 12 hours, stir frequently, change saturated limewater, it is small to continue immersion 12
When, filtering；Filter residue adds 15~20 times of amount purified waters, control ph exists with, again with water washing is purified, filter residue is taken after originally water washing
6.5~7.5, temperature adds papain at 45~55 DEG C, and the enzyme and filter residue ratio are 0.5~3.0kg: 100kg, stirring
100~300r/min of speed, 0.5~1.5 hour time, 3~8 hours are incubated, boils 30min, inactivator；Control ph exists
1.0~3.0, temperature adds pepsin at 55~70 DEG C, and the enzyme and filter residue ratio are 0.1~3.0kg: 100kg, stirring speed
100~300r/min is spent, 1~3 hour is incubated, boils 30min, inactivator；Filtering, filtrate spray drying, is produced.
2. scale collagen polypeptide facial mask according to claim 1, it is characterised in that described film forming agent is by carboxymethyl cellulose
Element and PVP composition, carboxymethyl cellulose are 3~5: 5~7 with povidone weight ratio.
3. scale collagen polypeptide facial mask according to claim 1, it is characterised in that described preservative is by para hydroxybenzene first
Sour methyl esters and propylparaben composition, methyl p-hydroxybenzoate are 4: 1 with propylparaben weight ratio.
4. according to the preparation method of any scale collagen polypeptide facial masks of claim 1-3, comprise the following steps：
(1) film forming agent is taken, is dissolved with ethanol, is stirred；
(2) pearl powder, talcum powder are taken, glycerine is placed in container, is added deionized water, is heated to 70~90 DEG C, stirs and evenly mixs；
(3) (2) step temperature is maintained, (1) step gains are added thereto, stirred；
(4) (3) step gains, temperature control are sequentially added into Tween 80, olive oil, fish while stirring at 45~55 DEG C
Squama collagen polypeptide, stirs；
(5) control temperature is down to 40 DEG C, adds gadol extract, marine algae extract, preservative, is well mixed, cools down and produce.
5. the preparation method of scale collagen polypeptide facial mask according to claim 4, it is characterised in that described rhodiola root carries
Thing is taken to be prepared as follows：Dry rhodiola root raw material is crushed, crosses 10 mesh sieves, 80% ethanol water, 6 times of amounts is added, stirs
Immersion 30 minutes is mixed, 90 DEG C, refluxing extraction 2h is heated to, filtering, collects filtrate；Filter residue adds 80% ethanol water, 4 times of amounts
Stirring immersion 30 minutes, 90 DEG C, refluxing extraction 1.5h are heated to, filtering, collects filtrate；Merge extract solution twice, be concentrated under reduced pressure
To without alcohol taste, medicinal extract is obtained；Medicinal extract is taken, adds resin, stirring and adsorbing detects into waste liquid without rhodioside, collects resin, largely
Clear water is rinsed, and takes the resin dress post after rinsing, opens bottom valve, and clear water is rinsed to saliva is gone out without color, pH value in neutrality, closes bottom
Valve, 90% ethanol is added, soak 30min, add 90% ethanol, it is 2L/min to open bottom valve coutroi velocity, collects eluent,
When amount of alcohol is 1.5 times of amount of resin, elution is terminated；Take eluent to be concentrated under reduced pressure into no alcohol taste, be spray-dried, produce.
6. the preparation method of scale collagen polypeptide facial mask according to claim 4, it is characterised in that described marine alga extraction
Thing is prepared as follows：Marine alga is taken, clear water cleans three times, removes desalination and other impurity, dry, and crushes, and crosses 20 mesh sieves, in-
Freezed at 20 DEG C, using 95% ethanol as solvent, melt mechanical shaking extraction 2h at 45 DEG C, extract 3 times, merge extract solution, 3500r/min
10min is centrifuged, collects supernatant；Rotary evaporator concentrates, and 50 DEG C of dryings produce to constant weight.
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| CN107174559A (en) * | 2017-05-25 | 2017-09-19 | 杭州千岛湖蓝色天使实业有限公司 | A kind of anti-fog haze facial mask |
| CN107233227A (en) * | 2017-06-20 | 2017-10-10 | 青岛金典生化器材有限公司 | A kind of theanine is modified the preparation method of fish scale protein facial mask |
| CN107260572A (en) * | 2017-06-20 | 2017-10-20 | 青岛金典生化器材有限公司 | A kind of antibacterial fish scale protein facial mask and preparation method thereof |
| CN107157797A (en) * | 2017-06-20 | 2017-09-15 | 青岛金典生化器材有限公司 | A kind of preparation technology of Application of Collagen from Fish Scales facial mask |
| CN107157865A (en) * | 2017-07-25 | 2017-09-15 | 四川吉晟生物医药有限公司 | A kind of anti-wrinkle combined containing gadol extract and active peptides repairs cosmetics |
| CN112675116A (en) * | 2020-12-30 | 2021-04-20 | 广州丹葶日用品实业有限公司 | Deep sea fish collagen silk formula and preparation method thereof |
| CN112724245A (en) * | 2021-02-04 | 2021-04-30 | 海南华研胶原科技股份有限公司 | Method for extracting micromolecular collagen peptide by fish scale enzymolysis |
| CN113332221A (en) * | 2021-07-23 | 2021-09-03 | 衢州市衢江区廿里镇养和残疾人之家 | Anti-aging composition, preparation method and facial mask prepared from anti-aging composition |
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