CN104490732A - Anti-aging scale collagen polypeptide facial mask and preparation method thereof - Google Patents
Anti-aging scale collagen polypeptide facial mask and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a scale collagen polypeptide facial mask which consists of the following components: 1-20 parts by weight of scale collagen polypeptide powder, 0.5-3 parts by weight of a rhodiola rosea extract, 1-2 parts by weight of a seaweed extract, 3-6 parts by weight of glycerol, 1-4 parts by weight of olive oil, 1-3 parts by weight of pearl powder, 10-30 parts by weight of talcum powder, 10-30 parts by weight of a film-forming agent, 1-2 parts by weight of tween-80 and 0.10-1.2 parts by weight of an antiseptic. The facial mask disclosed by the invention has functions of nourishing skin and beautifying the face.
Description
Technical field
The present invention relates to daily use chemicals technical field, be specifically related to a kind of clean skin of face, make elasticity of skin compact, there is supplementary skin nutrition, the facial film of deferring senility.
Background technology
Collagen protein is protein component main in skin histology, account for 70% ~ 80% of skin dry weight, manufactured by the fibrocyte (Fibroblasts) in corium, collagen protein is a kind of white, transparent, branchiess fibril, itself is a kind of very firm protein, in youth, health, less by the skin of sun damages, it forms the slightly curved fiber of a branch of bundle, catch up with mutually the formation right-angle array of one deck and lower one deck, this makes skin obtain solid effect.But increase when the years, collagen protein not only quantity reduces, and arrangement also becomes irregular, and corium is thus thinning; Environmental factors more easily makes collagen protein dissolve disappearance. cause the aging of skin.Exactly because the loss of collagen protein causes supporting the collagen peptide bond of skin and elasticated net fracture, its spiral net-shaped structure is destroyed immediately, and skin histology is oxidized, atrophy, subside, and skin just there will be drying, wrinkle, the aging phenomenon such as lax nonelastic.Supplementing enough collagen protein can stimulate the fibroblast in skin corium to carry out the secretion of collagen protein voluntarily, make collagen protein voluntarily generting machanism and metabolic function recover normal, and then effective delaying skin is lax and aging.Zoopery shows, after smearing skin with the mastic containing collagen protein, epiderm skin and dermis can be improved effectively, and facilitate the synthesis of collagen in skin.Reality medical science is commonly used collagen protein and is improved looks, and collagen protein can directly act on the impaired collagen fiber of skin corium, makes it recover transverse flow fiber configuration rapidly.Hydrophilic group in the triple-helix structure of collagen protein uniqueness and collagen molecules, enhances skin constitutional hydrodynamic force, ensures the circulation of moisture in skin surface and deep layer, improves lymph circulation, and skin water is moistened fullly has vigor.But collagen molecules amount is large, directly adds in cosmetics and directly can not be absorbed by skin.
At present, what collagen protein production was extracted is mainly derived from three class materials: ossein, bathypelagic fish fish skin, fish scale.Wherein ossein is mainly from animals such as pig, cattle, sheep, raw material easily obtains, raw material source is stablized, but the ossein that animal bone is extracted contains comparatively fattiness, ossein purity is slightly low, beauty treatment performance is slightly poor, and due to religion and Animal diseases, the market share of animal bone collagen is more and more less.The bathypelagic fish fish skin being used for producing collagen protein is mainly skin deep-sea cod, and collagen protein of fish skin content is high, function admirable, but morrhua belongs to cold aqueous demersal fishes, live in less than 300 meters, sea, manually cannot cultivate, obtain difficulty comparatively large, technical requirement is high.The fish scale being used for producing collagen protein is mainly derived from tilapia, and present tilapia is the cultured freshwater fish that the emphasis scientific research of World Water industry is cultivated, and one of main source being described as animal protein.Relative to ossein, fish skin collagen, the advantage of scale collagen both; And by detecting, the hydroxyproline content of fish scale collagen is higher than other raw materials, and because collagen peptide in fish scale is similar to the structure of application on human skin collagen, compatible good, the collagen product prepared by fish scale, is more easily absorbed by the skin.
Radix Rhodiolae Latin name Rhodiola rosea, English name Roseroot is Crassulaceae renascent herb or shrub plant, grows the rare wild plant in the high and cold pollution-free area of height above sea level 800 ~ 2500 meters.For traditional medicine is commonly used in Asia, the applicating history of Radix Rhodiolae is long, and Radix Rhodiolae extract Main Ingredients and Appearance rhodioside and Radix Rhodiolae aglycon, have slow down aging, whitening, the function such as radioprotective, moistening skin and eliminating spot.Radix Rhodiolae is classified as in medicine top grade by Shennong's Herbal, takes Radix Rhodiolae and to make light of one's life by commiting suicide QI invigorating, always do not prolong life, and nontoxic many clothes, clothes of a specified duration are not hurted sb.'s feelings." modern practical book on Chinese herbal medicine " says that its effect has seven, namely " one, central inhibitory action.Two, antifatigue effect.Three, cardiotonic.Four, antiinflammatory action.Five, blood glucose rising effect is suppressed.Six, Hardy dwarfing.Seven, resisting microwave radiation effect ".
Sargassum extract (Sesmollient) is a kind of marine organisms product of pure natural.Containing algin acid in it, crude protein, multivitamin, enzyme and trace element.This type of nutrition, after skin absorbs, can reduce surperficial blood fat, promotes surface skin hemopoietic function, and also has fat-reducing, insulation, the function of thickening.Sargassum extract is had many uses, and adds in skin care item the smooth sensation that can increase product, in addition containing a large amount of anion, thus imparts that it is crease-resistant, antidotal performance.
Margarita powder is mainly with freshwater shellfish Margaritas that animal produces such as hydriopsis cumingii, cristaria plicata, pteria martensiis, the powder ground, in white or off-white color, physical method is adopted to manufacture, be characterized in not adding other material any, do not destroy any material, maintain all nutritional labelings of Margarita yet.Margarita powder is used for beauty treatment, can solve face oil and dead bark problem.Compendium of Material Medica is recorded: " Margarita salty in the mouth is sweet cold nontoxic, relieving palpitation point order.Painting face, makes us moist good color.Be coated with brothers, peeling skin hangnail, separates pox and treats poison.Confirm through modern science, the main nutrient composition such as serine, methionine, lysine, pearl protein aminoacid, alkaline phosphate and taurine contained in Margarita have unique improvement care effect to skin.
In cosmetics, directly add macromolecular natural collagen protein be difficult to be absorbed by the skin, when therefore collagen protein is used as skin protection raw material, all adopt the hydrolytic collagen peptide of molecular weight.Fish scale collagen peptide used in the present invention, is adopt enzyme directional enzymatic technology that the collagen protein orientation being difficult to directly absorb is cut into the small active peptides of applicable absorption of human body, enhances its water solublity and permeability.In facial film, collagen polypeptide combines with the active substance in Radix Rhodiolae extract, Sargassum extract, Margarita powder, supplement skin nutrition composition, increase skin elasticity, prevention and to anti-wrinkle, slow down aging.
Summary of the invention
The object of the present invention is to provide facial film of a kind of anti-skin of face aging and preparation method thereof, with scale collagen polypeptide, Radix Rhodiolae extract, Sargassum extract, Margarita powder is that main active combines.
Facial film of the present invention is made by the raw material of following weight:
A kind of scale collagen polypeptide facial film, containing following composition: scale collagen polypeptide 1 ~ 20 weight portion, Radix Rhodiolae extract 0.5 ~ 3 weight portion, Sargassum extract 1 ~ 2 weight portion, glycerol 3 ~ 6 weight portion, olive oil 1 ~ 4 weight portion, Margarita powder 1 ~ 3 weight portion, Pulvis Talci 10 ~ 30 weight portion, film former 10 ~ 30 weight portion, Tween 80 1 ~ 2 weight portion, antiseptic 0.10 ~ 1.2 weight portion.
Described film former, described film former is made up of carboxymethyl cellulose and polyvidone, and carboxymethyl cellulose is 3 ~ 5: 5 ~ 7 with povidone weight ratio.
Described antiseptic, is made up of methyl parahydroxybenzoate and propyl p-hydroxybenzoate, and methyl parahydroxybenzoate and propyl p-hydroxybenzoate weight ratio are 4: 1.
Described scale collagen polypeptide, makes by following preparation method: get fish scale, and clear water is cleaned, oven drying at low temperature, pulverizes, adds 1% hydrochloric acid solution 10 times amount, soak 12 hours, frequently stir, and changes hydrochloric acid solution, continues immersion 12 hours, filters; Clear water rinsing for several times, adds in 10 times amount saturated limewaters, soaks 12 hours, frequently stir, and changes saturated limewater, continues immersion 12 hours, filters; Wash by purified water again after filtering residue tap water, add 15 ~ 20 times amount purified water, control ph 6.5 ~ 7.5, temperature adds papain at 45 ~ 55 DEG C, this enzyme and filtering residue ratio are 0.5 ~ 3.0kg: 100kg, mixing speed 100 ~ 300r/min, 0.5 ~ 1.5 hour time, is incubated 3 ~ 8 hours, boil 30min, inactivator; Control ph 1.0 ~ 3.0, temperature adds pepsin at 55 ~ 70 DEG C, this enzyme and filtering residue ratio are 0.1 ~ 3.0kg: 100kg, mixing speed 100 ~ 300r/min, are incubated 1 ~ 3 hour, boil 30min, inactivator; Filter, filtrate spraying dry, to obtain final product.
Described Radix Rhodiolae extract, be outsourcing product, also can prepare, its preparation method is: by the Radix Rhodiolae raw material pulverizing of drying, crosses 10 mesh sieves, adds 80% ethanol water 6 times amount, stirs immersion 30 minutes, is heated to 90 DEG C, and 2h is extracted in insulation, filters, and collects filtrate.Filtering residue adds 80% ethanol water 4 times amount and stirs immersion 30 minutes, is heated to 90 DEG C, and 1.5h is extracted in insulation, filters, and collects filtrate.Merge extracted twice liquid, be evaporated to without alcohol taste, obtain extractum.Get extractum, add resin, detect without rhodioside in stirring and adsorbing to waste liquid, collect resin, a large amount of clear water rinsing, get the dress of the resin after rinsing post, clear water rinsing is to going out saliva without color, and pH value, in neutral, closes bottom valve, add the ethanol of 90%, soak 30min, add 90% ethanol, opening bottom valve coutroi velocity is 2L/min, collect eluent, when amount of alcohol is amount of resin 1.5 times, stop eluting.Getting eluent is evaporated to without alcohol taste, and spraying dry, to obtain final product.
Described Sargassum extract, is outsourcing product, also can be made up of following method: get Sargassum, clean water three times, removes salt and other impurity; Dry.Pulverize, cross 20 mesh sieves, freezing at-20 DEG C, with 95% ethanol for solvent, at 45 DEG C, melt mechanical shaking extraction 2h, extract 3 times, merge extractive liquid, 3500r/min centrifugalize 10min, collect supernatant; Rotary evaporator concentrates, and is dried to constant weight, obtains final product at 50 DEG C.
Described Margarita powder, is made up of following method: get mussel pearl, and clear water is cleaned, and dries, and pulverizer is pulverized, and crosses 80-120 mesh sieve and obtains Margarita powder.
The present invention also discloses a kind of preparation method of defying age scale collagen peptide facial mask, it is characterized in that with scale collagen polypeptide, Radix Rhodiolae extract, Sargassum extract, Margarita powder etc. are function raw material, with film former, Pulvis Talci, glycerol, olive oil and Tween 80 for auxiliary material, in raw material, each component is all with mass ratio range, comprises following processing step:
(1) get film former (carboxymethyl cellulose 3 ~ 5 parts, polyvidone 5 ~ 7 parts) 10 ~ 30 parts, with dissolve with ethanol, stir.
(2) get Margarita powder 1 ~ 3 part, Pulvis Talci 10 ~ 30 parts, glycerol 3 ~ 6 parts is placed in container, adds deionized water 60 ~ 90 parts, is heated to 70 ~ 90 DEG C, stirring and evenly mixing.
(3) maintain (2) Buwen's degree, (1) step gains are added wherein, stirs.
(4) by (3) step gains, temperature controls at 45 ~ 55 DEG C, is sequentially added into Tween 80 1 ~ 2 part while stirring, 1 ~ 4 part, olive oil, and scale collagen polypeptide 1 ~ 20 part, stirs
(5) control temperature is down to 40 DEG C, and add Radix Rhodiolae extract 0.5 ~ 3 part, Sargassum extract 1 ~ 2 part, antiseptic 0.10 ~ 1.2 part, mix homogeneously, cools and get final product.
The using method of facial film of the present invention is: before using facial film, first deeply clean facial, again facial film is coated on face, after 15 ~ 25 minutes, facial film active substance is absorbed by the skin, and moisture evaporates, thin film is formed gradually at face, this thin film is peeled off from face, the dirt on skin of face, scurf also stick on thin film in company with and be eliminated, face seems clean, smooth.
Product beneficial effect of the present invention is as follows:
(1) main active of the present invention is natural animal-plant and extracts acquisition, and have no side effect, raw material easily obtains, and extraction process is simple, all has commercially available prod, moderate.
(2) fish scale collagen peptide of the present invention, safety is high, and disease contamination risk is low; Content of peptides is high, and molecular weight is little, soluble in water, can effectively directly be absorbed by skin, deep layer nourishes rough skin.
(3) fish scale collagen peptide used in the present invention, raw material, from the garbage of processing of aquatic products, improves the added value of aquaculture, reduces environmental pollution and the wasting of resources simultaneously.
(4) raw material scale collagen Gly-His-Lys of the present invention, Radix Rhodiolae extract, Sargassum extract, Margarita powder are used in combination, formula rationally, there is the effect of Synergistic, strengthen anti aging effect effect, Radix Rhodiolae has aromatic odor, improve product odour simultaneously, without the need to adding essence, increase Product Safety.
Detailed description of the invention
Below by specific embodiment, the present invention is described in further detail.
Embodiment 1
The preparation of scale collagen polypeptide:
Get fish scale, clear water is cleaned, oven drying at low temperature, pulverizes, adds 1% hydrochloric acid solution 10 times amount, soak 12 hours, frequently stir, and changes hydrochloric acid solution, continues immersion 12 hours, filters; Clear water rinsing for several times, adds in 10 times amount saturated limewaters, soaks 12 hours, frequently stir, and changes saturated limewater, continues immersion 12 hours, filters; Again with purified water washing after filtering residue tap water, get filtering residue 10kg, add 20 times amount purified water, control ph 6.9, temperature adds papain 0.1kg at 50 DEG C,, mixing speed 130r/min, 1.5 hours time, be incubated 6 hours, boil 30min, inactivator; Control ph 2.0, temperature adds pepsin 0.05kg at 65 DEG C, speed 130r/min stirs 1 hour, is incubated 3 hours, boils 30min, inactivator; Filter, filtrate spraying dry, to obtain final product.
By the scale collagen polypeptide that above technique is obtained, after sampling, analytical test, content of peptides is 96.65%, and products obtained therefrom be pale powder, soluble in water, dissolve abnormal smells from the patient afterwards pure and fresh, not there is fishy smell.
Embodiment 2
Following component is all with mass ratio range:
(1) get carboxymethyl cellulose 12 parts, polyvidone 18 parts, with dissolve with ethanol, stirs.
(2) get Margarita powder 2 parts, Pulvis Talci 30 parts, glycerol 6 parts is placed in container, adds deionized water 90 parts, is heated to 75 DEG C, stirring and evenly mixing.
(3) maintain (2) Buwen's degree, (1) step gains are added wherein, stirs.
(4) by (3) step gains, temperature controls at 45 DEG C, is sequentially added into 1 part of Tween 80 while stirring, 2 parts, olive oil, and fish scale collagen peptide 2 parts, stirs
(5) control temperature is down to 40 DEG C, adds Radix Rhodiolae extract 1 part, Sargassum extract 1 part, antiseptic 0.15 part, mix homogeneously, and cooling, obtains scale collagen polypeptide facial film.
Embodiment 3
(1) get carboxymethyl cellulose 6 parts, polyvidone 14 parts, with dissolve with ethanol, stirs.
(2) get Margarita powder 3 parts, Pulvis Talci 20 parts, glycerol 4 parts is placed in container, adds deionized water 75 parts, is heated to 70 DEG C, stirring and evenly mixing.
(3) maintain (2) Buwen's degree, (1) step gains are added wherein, stirs.
(4) by (3) step gains, temperature controls at 50 DEG C, is sequentially added into 1.5 parts of Tween 80s while stirring, 3 parts, olive oil, and fish scale collagen peptide 4 parts, stirs
(5) control temperature is down to 40 DEG C, adds Radix Rhodiolae extract 0.5 part, Sargassum extract 1 part, antiseptic 0.2 part, mix homogeneously, and cooling, obtains scale collagen polypeptide facial film.
Embodiment 4
(1) get carboxymethyl cellulose 5 parts, polyvidone 5 parts, with dissolve with ethanol, stirs.
(2) get Margarita powder 1 part, Pulvis Talci 10 parts, glycerol 3 parts is placed in container, adds deionized water 60 parts, is heated to 80 DEG C, stirring and evenly mixing.
(3) maintain (2) Buwen's degree, (1) step gains are added wherein, stirs.
(4) by (3) step gains, temperature controls at 50 DEG C, is sequentially added into 2 parts of Tween 80s while stirring, 4 parts, olive oil, and fish scale collagen peptide 2 parts, stirs
(5) control temperature is down to 40 DEG C, adds Radix Rhodiolae extract 1 part, Sargassum extract 1.5 parts, antiseptic 0.2 part, mix homogeneously, and cooling, obtains scale collagen polypeptide facial film.
Test example 1
Below by human body service test, facial film curative effect provided by the invention is described:
(1) physical data
Select healthy, without dermatosis and allergies, experimenter 75 example of non-sensitive skin.Wherein man 4 example, female 71 example, 28 ~ 61 years old age, average 49 years old.
(2) using method
After the clean skin of experimenter, the facial film obtained by embodiment 2 carries out left side half face flush coat, first three sky, and every day uses once just before going to bed, after this every three days, uses just before going to bed once, uses one month continuously; Right side half face only does general duty nursing.
(3) evaluation methodology
Use the 4th weekend, feel with experimenter and compare marking on the left of oneself face with right side.Marking index is 5: skin elasticity, moisture of skin, wrinkle (being mainly forehead, upper palpebra inferior, paropia, all positions of mouth), skin smoothness, skin colourity.Each individual event significantly improves+2 points, improves+1 point, unchanged or variation+0 point, full marks 10 points.
(4) evaluation criterion
Efficacy determination is divided into significantly effectively, effectively, minor effect and invalid four kinds:
Significantly effectively: score >=8 point;
Effective: 3 points of < score < 8 points;
Minor effect: 0 point of < score≤3 point;
Invalid: score≤0.
Total effective rate=significantly effectively+effectively+minor effect,
Obvious effective rate=significantly effectively+effectively.
(5) experimental result
In 75 examples using this facial film, significantly effective 18 examples, effective 29 examples, minor effect 24 example, invalid 4 examples, total effective rate 95.7%, obvious effective rate is 62.7%, and details sees the following form
Claims (7)
1. a scale collagen polypeptide facial film, containing following composition: scale collagen polypeptide 1 ~ 20 weight portion, Radix Rhodiolae extract 0.5 ~ 3 weight portion, Sargassum extract 1 ~ 2 weight portion, glycerol 3 ~ 6 weight portion, olive oil 1 ~ 4 weight portion, Margarita powder 1 ~ 3 weight portion, Pulvis Talci 10 ~ 30 weight portion, film former 10 ~ 30 weight portion, Tween 80 1 ~ 2 weight portion, antiseptic 0.10 ~ 1.2 weight portion.
2. scale collagen polypeptide facial film according to claim 1, is characterized in that, described film former is made up of carboxymethyl cellulose and polyvidone, and carboxymethyl cellulose is 3 ~ 5: 5 ~ 7 with povidone weight ratio.
3. scale collagen polypeptide facial film according to claim 1, is characterized in that, described antiseptic is made up of methyl parahydroxybenzoate and propyl p-hydroxybenzoate, and methyl parahydroxybenzoate and propyl p-hydroxybenzoate weight ratio are 4: 1.
4., according to the preparation method of the arbitrary described scale collagen polypeptide facial film of claim 1-3, comprise the following steps:
(1) get film former, with dissolve with ethanol, stir.
(2) get Margarita powder, Pulvis Talci, glycerol is placed in container, adds deionized water, is heated to 70 ~ 90 DEG C, stirring and evenly mixing.
(3) maintain (2) Buwen's degree, (1) step gains are added wherein, stirs.
(4) by (3) step gains, temperature controls, at 45 ~ 55 DEG C, to be sequentially added into Tween 80 while stirring, olive oil, scale collagen polypeptide, to stir
(5) control temperature is down to 40 DEG C, adds Radix Rhodiolae extract, Sargassum extract, antiseptic, mix homogeneously, cools and get final product.
5. the preparation method of scale collagen polypeptide facial film according to claim 4, it is characterized in that, described scale collagen polypeptide is prepared by the following method: get fish scale, and clear water is cleaned, oven drying at low temperature, pulverize, add 1% hydrochloric acid solution 10 times amount, soak 12 hours, frequently stir, change hydrochloric acid solution, continue immersion 12 hours, filter; Clear water rinsing for several times, adds 10 times amount saturated limewaters, soaks 12 hours, frequently stir, and changes saturated limewater, continues immersion 12 hours, filters; Wash by purified water again after filtering residue tap water, get filtering residue, add 15 ~ 20 times amount purified water, control ph 6.5 ~ 7.5, temperature at 45 ~ 55 DEG C, add papain, this enzyme and filtering residue ratio are 0.5 ~ 3.0kg: 100kg, mixing speed 100 ~ 300r/min, 0.5 ~ 1.5 hour time, is incubated 3 ~ 8 hours, boil 30min, inactivator; Control ph 1.0 ~ 3.0, temperature adds pepsin at 55 ~ 70 DEG C, this enzyme and filtering residue ratio are 0.1 ~ 3.0kg: 100kg, mixing speed 100 ~ 300r/min, are incubated 1 ~ 3 hour, boil 30min, inactivator; Filter, filtrate spraying dry, to obtain final product.
6. the preparation method of scale collagen polypeptide facial film according to claim 4, it is characterized in that, described Radix Rhodiolae extract is prepared by the following method: by the Radix Rhodiolae raw material pulverizing of drying, cross 10 mesh sieves, add 80% ethanol water 6 times amount, stir immersion 30 minutes, be heated to 90 DEG C, reflux, extract, 2h, filters, and collects filtrate; Filtering residue adds 80% ethanol water 4 times amount and stirs immersion 30 minutes, is heated to 90 DEG C, reflux, extract, 1.5h, filters, and collects filtrate; Merge extracted twice liquid, be evaporated to without alcohol taste, obtain extractum.Get extractum, add resin, detect without rhodioside in stirring and adsorbing to waste liquid, collect resin, a large amount of clear water rinsing, get the dress of the resin after rinsing post, open bottom valve, clear water rinsing is to going out saliva without color, pH value in neutral, closedown bottom valve, add the ethanol of 90%, soak 30min, add 90% ethanol, opening bottom valve coutroi velocity is 2L/min, collect eluent, when amount of alcohol is amount of resin 1.5 times, stop eluting; Getting eluent is evaporated to without alcohol taste, and spraying dry, to obtain final product.
7. the preparation method of scale collagen polypeptide facial film according to claim 4, is characterized in that, described Sargassum extract is prepared by the following method: get Sargassum, clean water three times, removes salt and other impurity, dries, pulverize, cross 20 mesh sieves, freezing at-20 DEG C, with 95% ethanol for solvent, melt mechanical shaking extraction 2h at 45 DEG C, extract 3 times, merge extractive liquid, 3500r/min centrifugalize 10min, collects supernatant; Rotary evaporator concentrates, and 50 DEG C are dried to constant weight, obtain final product.
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| CN107157865A (en) * | 2017-07-25 | 2017-09-15 | 四川吉晟生物医药有限公司 | A kind of anti-wrinkle combined containing gadol extract and active peptides repairs cosmetics |
| CN107174559A (en) * | 2017-05-25 | 2017-09-19 | 杭州千岛湖蓝色天使实业有限公司 | A kind of anti-fog haze facial mask |
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| CN107174559A (en) * | 2017-05-25 | 2017-09-19 | 杭州千岛湖蓝色天使实业有限公司 | A kind of anti-fog haze facial mask |
| CN107157797A (en) * | 2017-06-20 | 2017-09-15 | 青岛金典生化器材有限公司 | A kind of preparation technology of Application of Collagen from Fish Scales facial mask |
| CN107233227A (en) * | 2017-06-20 | 2017-10-10 | 青岛金典生化器材有限公司 | A kind of theanine is modified the preparation method of fish scale protein facial mask |
| CN107260572A (en) * | 2017-06-20 | 2017-10-20 | 青岛金典生化器材有限公司 | A kind of antibacterial fish scale protein facial mask and preparation method thereof |
| CN107157865A (en) * | 2017-07-25 | 2017-09-15 | 四川吉晟生物医药有限公司 | A kind of anti-wrinkle combined containing gadol extract and active peptides repairs cosmetics |
| CN112675116A (en) * | 2020-12-30 | 2021-04-20 | 广州丹葶日用品实业有限公司 | Deep sea fish collagen silk formula and preparation method thereof |
| CN112724245A (en) * | 2021-02-04 | 2021-04-30 | 海南华研胶原科技股份有限公司 | Method for extracting micromolecular collagen peptide by fish scale enzymolysis |
| CN113332221A (en) * | 2021-07-23 | 2021-09-03 | 衢州市衢江区廿里镇养和残疾人之家 | Anti-aging composition, preparation method and facial mask prepared from anti-aging composition |
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| CN104490732B (en) | 2017-12-26 |
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Address after: 024000 the Inner Mongolia Autonomous Region Chifeng City Hongshan high tech Industrial Park (West Water Town of Hongmiao village) Co-patentee after: INNER MONGOLIA TIANQI ZHONGMENG PHARMACEUTICAL Co.,Ltd. Patentee after: INNER MONGOLIA TIANQI BIOTECHNOLOGY Co.,Ltd. Co-patentee after: INNER MONGOLIA TIANQI MONGOLIAN MEDICINE GROUP Co.,Ltd. Address before: 024000 the Inner Mongolia Autonomous Region Chifeng City Hongshan high tech Industrial Park (West Water Town of Hongmiao village) Co-patentee before: INNER MONGOLIA TIANQI ZHONGMENG PHARMACEUTICAL Co.,Ltd. Patentee before: INNER MONGOLIA TIANQI BIOTECHNOLOGY Co.,Ltd. Co-patentee before: INNER MONGOLIA TIANQI PHARMACEUTICAL GROUP Co.,Ltd. Address after: 024000 the Inner Mongolia Autonomous Region Chifeng City Hongshan high tech Industrial Park (West Water Town of Hongmiao village) Co-patentee after: INNER MONGOLIA TIANQI ZHONGMENG PHARMACEUTICAL Co.,Ltd. Patentee after: INNER MONGOLIA TIANQI BIOTECHNOLOGY Co.,Ltd. Co-patentee after: INNER MONGOLIA TIANQI PHARMACEUTICAL GROUP Co.,Ltd. Address before: 024000 the Inner Mongolia Autonomous Region Chifeng City Hongshan high tech Industrial Park (West Water Town of Hongmiao village) Co-patentee before: INNER MONGOLIA TIANQI ZHONGMENG PHARMACEUTICAL Co.,Ltd. Patentee before: INNER MONGOLIA TIANQI BIOTECHNOLOGY Co.,Ltd. Co-patentee before: INNER MONGOLIA TIANQI PHARMACEUTICAL INVESTMENT (Group) Co.,Ltd. |