CN112675116A - Deep sea fish collagen silk formula and preparation method thereof - Google Patents

Deep sea fish collagen silk formula and preparation method thereof Download PDF

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Publication number
CN112675116A
CN112675116A CN202011610847.3A CN202011610847A CN112675116A CN 112675116 A CN112675116 A CN 112675116A CN 202011610847 A CN202011610847 A CN 202011610847A CN 112675116 A CN112675116 A CN 112675116A
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China
Prior art keywords
deep sea
collagen
fish collagen
skin
sea fish
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Pending
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CN202011610847.3A
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Chinese (zh)
Inventor
林立峰
李小翠
马嘉忆
张剑光
黎明诗
林立俊
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Guangzhou Danting Bath And Body Care Factory
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Guangzhou Danting Bath And Body Care Factory
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Priority to CN202011610847.3A priority Critical patent/CN112675116A/en
Publication of CN112675116A publication Critical patent/CN112675116A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a deep sea fish collagen silk formula and a preparation method thereof, wherein the deep sea fish collagen silk is prepared by mixing a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract, and the deep sea fish collagen silk is prepared by mixing the following components in parts by weight: 20-25 parts of deep sea fish collagen raw material, 2-6 parts of hydrolyzed collagen, 8-12 parts of seaweed extract, 2-4 parts of marine shellfish polypeptide and 1-3 parts of herbal extract. The formula and the preparation method of the deep sea fish collagen silk provided by the invention have the main advantages that the preparation process is simple, the raw material cost is low, the collagen content is high, the silk shape is convenient to carry and use, water dissolution is carried out according to the use requirement, the nutrition supplement is carried out on the skin, the effect range is wide, the penetration is strong, the absorption is convenient, the nutrition supplement is fully carried out, the laziness is avoided, the collagen molecular structure is prevented from being broken through manual subpackaging, the activity is kept, the skin is moistened and moisturized, and the skin is tender, smooth and compact.

Description

Deep sea fish collagen silk formula and preparation method thereof
Technical Field
The invention relates to collagen health care, in particular to a deep sea fish collagen silk formula and a preparation method thereof.
Background
The collagen accounts for 25-30% of human protein, is equivalent to 6% of the weight, has triple smooth and compact effects of supporting, repairing and protecting skin, and is loss of collagen which is one of main expression forms of human aging and is helpful for delaying skin aging.
Collagen skin care products used in the current market are mostly liquid, and still have defects in the using process, the collagen content is low, the molecular structure is inconvenient for skin absorption, and the collagen skin care products contain preservatives, are easy to lose activity, and have low absorption utilization rate, so that a formula of deep sea fish collagen silk and a preparation method thereof are provided.
Disclosure of Invention
The invention aims to solve the problems of low collagen content, easy inactivation and low absorption and utilization rate in the prior art, and provides a formula of deep sea fish collagen silk and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the formula of the deep sea fish collagen silk is prepared by mixing a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract according to the following weight ratio: 20-25 parts of deep sea fish collagen raw material, 2-6 parts of hydrolyzed collagen, 8-12 parts of seaweed extract, 2-4 parts of marine shellfish polypeptide and 1-3 parts of herbal extract.
Preferably, the deep sea fish collagen raw material is a mixture consisting of one or more of deep sea cod skin, cartilage and fish scales in any ratio.
Preferably, the seaweed extract comprises algal polysaccharides, phycobiliproteins, algal polypeptides and sodium alginate.
Preferably, the marine shellfish polypeptide comprises chitin and hyaluronic acid.
Preferably, the herbal extract is a mixture of one or more of vitamin C, vitamin E, hydrolyzed oat and snake venom peptide according to any ratio.
Preferably, the formula of the deep sea fish collagen silk and the preparation method thereof comprise the following steps:
s1: raw material treatment: sorting and removing impurities from raw materials of skin, cartilage and scale of deep sea cod entering a factory, and removing the raw materials with poor quality;
s2: rinsing: putting the processed raw materials of the skin, the cartilage and the fish scale of the deep sea cod into an automatic washing machine for rinsing;
s3: and (3) cooking: cooking the rinsed deep sea cod skin, cartilage and fish scales;
s4: and (3) drying: drying the rinsed deep sea cod skin, cartilage and fish scales to make the water content lower than 5%;
s5: crushing: crushing the dried skin, cartilage and fish scales of the deep sea cod to prepare a deep sea fish collagen raw material;
s6: emulsification: putting a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract into an emulsification tank in proportion, and fully emulsifying;
s7: freeze-drying: freeze-drying and concentrating the fully mixed and stirred deep-sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herbal extract;
s8: filamentation: filamentation is carried out on the freeze-dried deep sea fish collagen, so that the deep sea fish collagen is in a filamentous shape, and the deep sea fish collagen silk is prepared;
s9: subpackaging: and (4) manually subpackaging the prepared deep-sea fish collagen filaments, and performing vacuum sealing and storage after subpackaging.
Preferably, the rinsing temperature of the raw material of skin, cartilage and fish scale of the deep sea cod involved in the step of S2 is controlled to be 5 to 36 ℃.
Preferably, the cooking manner of the skin, the cartilage and the fish scales of the deep sea cod involved in the step S3 is that the rinsed raw materials of the skin, the cartilage and the fish scales of the deep sea cod and distilled water are put into a pot to be cooked by big fire, the ratio of the distilled water to the raw materials of the skin, the cartilage and the fish scales of the deep sea cod is 1:2, the raw materials of the skin, the cartilage and the fish scales of the deep sea cod are turned into small fire to be cooked when the water is heated to 100 ℃, and the raw materials of the skin, the cartilage and the fish scales of the deep sea cod are fished out of the pot to be cooled after.
Preferably, the pulverization involved in the step S5 is controlled to have a diameter of 0.03 to 0.01 mm.
Preferably, the emulsification tank involved in the step S6 is preheated before use, and the deep sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herb extract are stirred during emulsification to be sufficiently fused.
Compared with the prior art, the invention has the beneficial effects that: the formula and the preparation method of the deep sea fish collagen silk provided by the invention have the main advantages that the preparation process is simple, the raw material cost is low, the collagen content is high, the silk shape is convenient to carry and use, water dissolution is carried out according to the use requirement, the nutrition supplement is carried out on the skin, the effect range is wide, the penetration is strong, the absorption is convenient, the nutrition supplement is fully carried out, the laziness is avoided, the collagen molecular structure is prevented from being broken through manual subpackaging, the activity is kept, the skin is moistened and moisturized, and the skin is tender, smooth and compact.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1
The formula of the deep sea fish collagen silk is prepared by mixing a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract according to the following weight ratio: 20-25 parts of deep sea fish collagen raw material, 2-6 parts of hydrolyzed collagen, 8-12 parts of seaweed extract, 2-4 parts of marine shellfish polypeptide and 1-3 parts of herbal extract.
The deep-sea fish collagen raw material is processed from deep-sea cod skin.
The seaweed extract comprises algal polysaccharide, phycobiliprotein, algal polypeptide and sodium alginate.
The marine shellfish polypeptide comprises chitin and hyaluronic acid.
The herbal extract is a mixture of vitamin C and vitamin E.
The formula of the deep sea fish collagen silk and the preparation method thereof comprise the following steps:
s1: raw material treatment: sorting and removing impurities of deep sea cod skin raw materials entering a factory, and removing poor-quality raw materials;
s2: rinsing: putting the treated deep sea cod skin raw material into an automatic washing machine for rinsing;
s3: and (3) cooking: cooking the rinsed deep sea cod skin;
s4: and (3) drying: drying the rinsed deep sea cod skin to make the water content lower than 5%;
s5: crushing: crushing the dried deep sea cod skin to obtain a deep sea fish collagen raw material;
s6: emulsification: putting a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract into an emulsification tank in proportion, and fully emulsifying;
s7: freeze-drying: freeze-drying and concentrating the fully mixed and stirred deep-sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herbal extract;
s8: filamentation: filamentation is carried out on the freeze-dried deep sea fish collagen, so that the deep sea fish collagen is in a filamentous shape, and the deep sea fish collagen silk is prepared;
s9: subpackaging: and (4) manually subpackaging the prepared deep-sea fish collagen filaments, and performing vacuum sealing and storage after subpackaging.
The rinsing temperature of the deep sea cod skin raw material involved in the step S2 should be controlled at 26 ℃.
The deep sea cod skin cooking mode related to the step S3 is that the deep sea cod skin raw material and distilled water which are rinsed are placed into a pot to be cooked with big fire, the ratio of the distilled water to the deep sea cod skin raw material is 1:2, when the water is heated to 100 ℃, the deep sea cod skin raw material is turned into small fire to be cooked, and after 300min, the deep sea cod skin raw material is fished out of the pot to be cooled.
The pulverization involved in the step S5 should be controlled to have a diameter of 0.01 mm.
The emulsification tank involved in the step S6 is preheated before use, and the deep sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herb extract are stirred during emulsification to be fully fused.
Example 2
The formula of the deep sea fish collagen silk is prepared by mixing a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract according to the following weight ratio: 20-25 parts of deep sea fish collagen raw material, 2-6 parts of hydrolyzed collagen, 8-12 parts of seaweed extract, 2-4 parts of marine shellfish polypeptide and 1-3 parts of herbal extract.
The deep sea fish collagen raw material is a mixture consisting of deep sea cod skin, cartilage and fish scales.
The seaweed extract comprises algal polysaccharide, phycobiliprotein, algal polypeptide and sodium alginate.
The marine shellfish polypeptide comprises chitin and hyaluronic acid.
The herbal extract is a mixture of vitamin C, vitamin E, hydrolyzed oat, and snake venom like peptide.
The formula of the deep sea fish collagen silk and the preparation method thereof comprise the following steps:
s1: raw material treatment: sorting and removing impurities from raw materials of skin, cartilage and scale of deep sea cod entering a factory, and removing the raw materials with poor quality;
s2: rinsing: putting the processed raw materials of the skin, the cartilage and the fish scale of the deep sea cod into an automatic washing machine for rinsing;
s3: and (3) cooking: cooking the rinsed deep sea cod skin, cartilage and fish scales;
s4: and (3) drying: drying the rinsed deep sea cod skin, cartilage and fish scales to make the water content lower than 5%;
s5: crushing: crushing the dried skin, cartilage and fish scales of the deep sea cod to prepare a deep sea fish collagen raw material;
s6: emulsification: putting a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract into an emulsification tank in proportion, and fully emulsifying;
s7: freeze-drying: freeze-drying and concentrating the fully mixed and stirred deep-sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herbal extract;
s8: filamentation: filamentation is carried out on the freeze-dried deep sea fish collagen, so that the deep sea fish collagen is in a filamentous shape, and the deep sea fish collagen silk is prepared;
s9: subpackaging: and (4) manually subpackaging the prepared deep-sea fish collagen filaments, and performing vacuum sealing and storage after subpackaging.
The rinsing temperature of the raw material of skin, cartilage and fish scales of the deep sea cod involved in the step of S2 should be controlled at 15 ℃.
The cooking mode of the skin, the cartilage and the fish scales of the deep sea cod related in the step S3 is that the rinsed raw materials of the skin, the cartilage and the fish scales of the deep sea cod and distilled water are placed into a pot to be cooked by big fire, the ratio of the distilled water to the raw materials of the skin, the cartilage and the fish scales of the deep sea cod is 1:2, the raw materials of the skin, the cartilage and the fish scales of the deep sea cod are turned into small fire to be cooked when the water is heated to 100 ℃, and the raw materials of the skin, the cartilage and the fish scales of the deep sea cod are fished out of the pot.
The pulverization involved in the step S5 should be controlled to have a diameter of 0.03 mm.
The emulsification tank involved in the step S6 is preheated before use, and the deep sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herb extract are stirred during emulsification to be fully fused.
The formula and the preparation method of the deep sea fish collagen silk provided by the invention have the main advantages that the preparation process is simple, the raw material cost is low, the collagen content is high, the silk shape is convenient to carry and use, water dissolution is carried out according to the use requirement, the nutrition supplement is carried out on the skin, the effect range is wide, the penetration is strong, the absorption is convenient, the nutrition supplement is fully carried out, the laziness is avoided, the collagen molecular structure is prevented from being broken through manual subpackaging, the activity is kept, the skin is moistened and moisturized, and the skin is tender, smooth and compact.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (10)

1. The deep sea fish collagen silk formula is characterized in that: the deep sea fish collagen silk is prepared by mixing a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract, and the deep sea fish collagen silk is prepared by mixing the following components in parts by weight: 20-25 parts of deep sea fish collagen raw material, 2-6 parts of hydrolyzed collagen, 8-12 parts of seaweed extract, 2-4 parts of marine shellfish polypeptide and 1-3 parts of herbal extract.
2. The deep sea fish collagen silk formula according to claim 1, wherein: the deep sea fish collagen raw material is a mixture composed of one or more of deep sea cod skin, cartilage and fish scales according to any ratio.
3. The deep sea fish collagen silk formula according to claim 1, wherein: the seaweed extract comprises algal polysaccharide, phycobiliprotein, algal polypeptide and sodium alginate.
4. The deep sea fish collagen silk formula according to claim 1, wherein: the marine shellfish polypeptide comprises chitin and hyaluronic acid.
5. The deep sea fish collagen silk formula according to claim 1, wherein: the herbal extract is a mixture consisting of one or more of vitamin C, vitamin E, hydrolyzed oat and snake venom peptide according to any ratio.
6. The deep sea fish collagen silk formula and the preparation method thereof according to claim 1, wherein the deep sea fish collagen silk formula comprises the following components in percentage by weight: the method comprises the following steps:
s1: raw material treatment: sorting and removing impurities from raw materials of skin, cartilage and scale of deep sea cod entering a factory, and removing the raw materials with poor quality;
s2: rinsing: putting the processed raw materials of the skin, the cartilage and the fish scale of the deep sea cod into an automatic washing machine for rinsing;
s3: and (3) cooking: cooking the rinsed deep sea cod skin, cartilage and fish scales;
s4: and (3) drying: drying the rinsed deep sea cod skin, cartilage and fish scales to make the water content lower than 5%;
s5: crushing: crushing the dried skin, cartilage and fish scales of the deep sea cod to prepare a deep sea fish collagen raw material;
s6: emulsification: putting a deep sea fish collagen raw material, hydrolyzed collagen, a seaweed extract, marine shellfish polypeptide and a herbal extract into an emulsification tank in proportion, and fully emulsifying;
s7: freeze-drying: freeze-drying and concentrating the fully mixed and stirred deep-sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herbal extract;
s8: filamentation: filamentation is carried out on the freeze-dried deep sea fish collagen, so that the deep sea fish collagen is in a filamentous shape, and the deep sea fish collagen silk is prepared;
s9: subpackaging: and (4) manually subpackaging the prepared deep-sea fish collagen filaments, and performing vacuum sealing and storage after subpackaging.
7. The deep sea fish collagen silk formula and the preparation method thereof according to claim 6, characterized in that: the rinsing temperature of the raw materials of skin, cartilage and fish scale of the deep sea cod involved in the step of S2 should be controlled at 5-36 ℃.
8. The deep sea fish collagen silk formula and the preparation method thereof according to claim 6, characterized in that: the cooking mode of the skin, the cartilage and the fish scales of the deep sea cod related in the step S3 is that the rinsed raw materials of the skin, the cartilage and the fish scales of the deep sea cod and distilled water are placed into a pot to be cooked by big fire, the ratio of the distilled water to the raw materials of the skin, the cartilage and the fish scales of the deep sea cod is 1:2, the raw materials of the skin, the cartilage and the fish scales of the deep sea cod are turned into small fire to be cooked when the water is heated to 100 ℃, and the raw materials of the skin, the cartilage and the fish scales of the deep sea cod are fished out of the pot to be cooled.
9. The deep sea fish collagen silk formula and the preparation method thereof according to claim 6, characterized in that: the pulverization involved in the step S5 should be controlled to have a diameter of 0.03-0.01 mm.
10. The deep sea fish collagen silk formula and the preparation method thereof according to claim 6, characterized in that: the emulsification tank involved in the step S6 is preheated before use, and the deep sea fish collagen raw material, hydrolyzed collagen, seaweed extract, marine shellfish polypeptide and herb extract are stirred during emulsification to be fully fused.
CN202011610847.3A 2020-12-30 2020-12-30 Deep sea fish collagen silk formula and preparation method thereof Pending CN112675116A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178636A (en) * 2011-04-27 2011-09-14 中国科学院南海海洋研究所 Marine biological function cosmetic for minimizing pores
CN103932969A (en) * 2014-04-16 2014-07-23 法国奢蔻化妆品有限公司 Deep-sea fish skin collagen peptide cosmetic capable of delaying ageing, firming skin, brightening and moisturizing and preparation method thereof
CN104490732A (en) * 2014-12-10 2015-04-08 内蒙古天奇生物科技有限公司 Anti-aging scale collagen polypeptide facial mask and preparation method thereof
CN106387295A (en) * 2016-08-31 2017-02-15 万子霞 Extraction and shred drawing technology of cod collagen
CN107260602A (en) * 2017-06-20 2017-10-20 芜湖凌梦电子商务有限公司 A kind of preparation method of deep-sea cod collagen peptide moisturizing spraying
CN111557888A (en) * 2020-05-21 2020-08-21 林小红 Whitening mask rich in marine extract

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178636A (en) * 2011-04-27 2011-09-14 中国科学院南海海洋研究所 Marine biological function cosmetic for minimizing pores
CN103932969A (en) * 2014-04-16 2014-07-23 法国奢蔻化妆品有限公司 Deep-sea fish skin collagen peptide cosmetic capable of delaying ageing, firming skin, brightening and moisturizing and preparation method thereof
CN104490732A (en) * 2014-12-10 2015-04-08 内蒙古天奇生物科技有限公司 Anti-aging scale collagen polypeptide facial mask and preparation method thereof
CN106387295A (en) * 2016-08-31 2017-02-15 万子霞 Extraction and shred drawing technology of cod collagen
CN107260602A (en) * 2017-06-20 2017-10-20 芜湖凌梦电子商务有限公司 A kind of preparation method of deep-sea cod collagen peptide moisturizing spraying
CN111557888A (en) * 2020-05-21 2020-08-21 林小红 Whitening mask rich in marine extract

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