CN103222935B - Armeniaca sibirica oil skin-moisturizing lotion and preparation method thereof - Google Patents

Armeniaca sibirica oil skin-moisturizing lotion and preparation method thereof Download PDF

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CN103222935B
CN103222935B CN201310153031.6A CN201310153031A CN103222935B CN 103222935 B CN103222935 B CN 103222935B CN 201310153031 A CN201310153031 A CN 201310153031A CN 103222935 B CN103222935 B CN 103222935B
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skin
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prunus armeniaca
moisturizing
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CN103222935A (en
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赵忠
王海泽
朱海兰
韦苑妮
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Northwest A&F University
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Abstract

The invention discloses an armeniaca sibirica oil skin-moisturizing lotion and a preparation method thereof. The lotion comprises the components of, by mass, 10-20% of detoxified armeniaca sibirica oil, 0.15-0.5% of hyaluronic acid, 2-5% of lubrajel, 2-4% of cetanol, 0.5-1.5% of an emulsifying agent, 1-2% of stearic acid, 0.1-0.5% of a fragrance, 0.2-0.5% of an antibacterial agent, and balance of deionized water. Armeniaca sibirica oil has high unsaturated fatty acid content and good permeation on skins. The effective components in the product can be rapidly absorbed by skin. Therefore, when the armeniaca sibirica oil skin-moisturizing lotion is applied on face, no greasy sensation is caused. With the lotion, a moisturizing and nourishing effect is substantial. The lotion is especially suitable for northern arid and semi-arid regions.

Description

A kind of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast and preparation method thereof
Technical field
The invention belongs to Prunus armeniaca L.var.ansu Maxim. oil development technique field, relate to a kind of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast and preparation method thereof.
Background technology
Prunus armeniaca L.var.ansu Maxim. (Armeniaca sibirica) belongs to Rosaceae Fructus Pruni and belongs to, and is a kind of wild natural hybrid species, originates in China and western part of Asia.Mainly being distributed in Muscovite Siberia, Mongolia and China's north latitude 35-degree northern area, is important economic forest and forests for water and soil conservation reproducting tree species.
Semen pruni armeniacae contains the oils and fats of 45% ~ 52%, wherein unsaturated fatty acid is more than 96%, and more than 95% is the unsaturated fatty acid such as linoleic acid, linolenic acid, protein content about 27% in Semen pruni armeniacae, wherein contained aminoacid collocation balance rationally, in addition, also contains 4.1% total sugar in Semen pruni armeniacae, the amygdalin of 3% and multiple mineral element and vitamin, Semen Armeniacae Amarum has cough-relieving, reduces phlegm, lung moistening, skin care, heat clearing away, relieving constipation effect.Modern medicine clinical investigation discloses, and Semen Armeniacae Amarum has blood fat reducing, and prevention of cardiac and atherosclerotic effect, have abundant nutritive value and health-care effect.
Summary of the invention
The object of the present invention is to provide a kind of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast and preparation method thereof, this Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast can moisten, skin care.
The present invention is achieved through the following technical solutions:
A kind of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 10 ~ 20%, hyaluronic acid 0.15 ~ 0.5%, reed fragrant plant glue 2 ~ 5%, hexadecanol 2 ~ 4%, emulsifying agent 0.5 ~ 1.5%, stearic acid 1 ~ 2%, essence 0.1 ~ 0.5% and antibacterial 0.2 ~ 0.5%, deionized water complements to 100%.
Further, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 ~ 13%, hyaluronic acid 0.15 ~ 0.25%, reed fragrant plant glue 4 ~ 5%, hexadecanol 3 ~ 4%, emulsifying agent 0.5 ~ 1.5%, stearic acid 1 ~ 2%, essence 0.1 ~ 0.5% and antibacterial 0.2 ~ 0.5%, it is 4.0 ~ 8.5 that deionized water complements to 100%, pH.
Further, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 ~ 13%, hyaluronic acid 0.15 ~ 0.25%, reed fragrant plant glue 5%, hexadecanol 2 ~ 4%, emulsifying agent 1.5%, stearic acid 2%, essence 0.1% and antibacterial 0.2%, it is 4.0 ~ 8.5 that deionized water complements to 100%, pH.
Described essence is the essence distributing Semen Armeniacae Amarum delicate fragrance.
Described essence is Semen Armeniacae Amarum quintessence oil.
Described emulsifying agent is Creagel Ez-7, and antibacterial is Glydant Plus_Liquid.
A preparation method for Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, comprises the following steps:
(1) by mass percentage, take the detoxification Prunus armeniaca L.var.ansu Maxim. oil of 10 ~ 20% respectively, the hyaluronic acid of 0.15 ~ 0.5%, the reed fragrant plant glue of 2 ~ 5%, the hexadecanol of 2 ~ 4%, the emulsifying agent of 0.5 ~ 1.5%, the stearic acid of 1 ~ 2%, the essence of 0.1 ~ 0.5%, the antibacterial of 0.2 ~ 0.5%, deionized water complements to 100%, for subsequent use;
(2) the detoxification Prunus armeniaca L.var.ansu Maxim. oil, stearic acid, the hexadecanol that step 1) are taken, be stirred well to and dissolve completely, obtain mixed material A at 80 ~ 90 DEG C;
(3) hyaluronic acid in step 1) being taken, reed fragrant plant glue, emulsifying agent and deionized water, be stirred well to and dissolve completely, obtain mixed material B at 80 ~ 85 DEG C;
(4) 80 ~ 90 DEG C, under stirring condition, mixed material A is added after carrying out emulsifying in mixed material B, to be emulsified completely after be cooled to 45 ~ 55 DEG C, add Semen Armeniacae Amarum quintessence oil fully to stir, and then add antibacterial stirring, stop stirring after naturally cooling to room temperature, obtain Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion.
At least emulsifying 30min in described step 4).
Described essence is Semen Armeniacae Amarum quintessence oil, and described emulsifying agent is Creagel Ez-7, and antibacterial is GlydantPlus_Liquid.
Described Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion is in the application preparing antipsoriatic medicine or skin care item.
Compared with prior art, the present invention has following useful technique effect:
Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast provided by the invention, contain detoxification Prunus armeniaca L.var.ansu Maxim. oil, because Prunus armeniaca L.var.ansu Maxim. oil unsaturated fatty acid content is high, strong to skin permeability, skin absorbs fast to effective ingredient in product, so Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast smears face without greasy feeling, smear rear moisturizing, moisturizing effect is obvious, be especially adapted to northern Arid&semi-arid area.
Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast provided by the invention, uniform and smooth, color is snow-white, is rich in gloss; Slightly Semen Armeniacae Amarum delicate fragrance, PH=4.0 ~ 8.5, to the stingless excitation of skin, meet national standard.And good stability:
Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin breast is after-5 ~-15 DEG C or 40 DEG C place 24h, or 2000r/min rotates 30min, recovers room temperature without oil-water separation phenomenon.
The preparation method of Prunus armeniaca L.var.ansu Maxim. provided by the invention oil skin-moisturizing, skin breast, due to have employed complex food safety requirements Prunus armeniaca L.var.ansu Maxim. oil, safety is high, environmental protection, and preparation method is simple, and production efficiency is high, is applicable to industrial-scale production.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail, and the explanation of the invention is not limited.
A kind of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 10 ~ 20%, hyaluronic acid (hyaluronic acid) 0.15 ~ 0.5%, reed fragrant plant glue 2 ~ 5%, hexadecanol 2 ~ 4%, emulsifying agent 0.5 ~ 1.5%, stearic acid 1 ~ 2%, essence 0.1 ~ 0.5% and antibacterial 0.2 ~ 0.5%, deionized water complements to 100%.
Further, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 ~ 13%, hyaluronic acid 0.15 ~ 0.25%, reed fragrant plant glue 4 ~ 5%, hexadecanol 3 ~ 4%, emulsifying agent 0.5 ~ 1.5%, stearic acid 1 ~ 2%, essence 0.1 ~ 0.5% and antibacterial 0.2 ~ 0.5%, it is 4.0 ~ 8.5 that deionized water complements to 100%, pH.
Further, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 ~ 13%, hyaluronic acid 0.15 ~ 0.25%, reed fragrant plant glue 5%, hexadecanol 2 ~ 4%, emulsifying agent 1.5%, stearic acid 2%, essence 0.1% and antibacterial 0.2%, it is 4.0 ~ 8.5 that deionized water complements to 100%, pH.
Described detoxification Prunus armeniaca L.var.ansu Maxim. oil, using Semen pruni armeniacae as raw material, is the standby detoxification Prunus armeniaca L.var.ansu Maxim. oil meeting food safety requirements of patent system of CN101589745 according to publication number, cyanide content lower than World Health Organization (WHO) to Cyanide in Drinking Water content requirement.
Concrete described emulsifying agent can be the celestial graceful Creagel Ez-7 of France, and antibacterial can be the Glydant Plus_Liquid of Switzerland's dragon sand.
Provide the embodiment of preparation 100kg Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion below, the proportioning of each component is as shown in table 1.
Table 1 Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion formulations (quality %)
Raw material Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 12 13 15 20
Stearic acid 2 2 2 1 1.5
Hexadecanol 2 3 4 2 2.5
Hyaluronic acid 0.15 0.2 0.25 0.2 0.25
Reed fragrant plant glue 5 4 5 2 3
Emulsifying agent 1.5 1.5 1.5 0.5 1
Antibacterial 0.2 0.3 0.2 0.4 0.5
Essence 0.1 0.2 0.15 0.2 0.5
Deionized water Surplus Surplus Surplus Surplus Surplus
Provide preparation embodiment below:
Embodiment 1
The preparation of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, comprises the following steps:
(1) detoxification Prunus armeniaca L.var.ansu Maxim. oil 11kg, hyaluronic acid 0.15kg is taken, reed fragrant plant glue 5kg, hexadecanol 2kg, emulsifying agent (the celestial graceful Creagel Ez-7 of France) 1.5kg, stearic acid 2kg, Semen Armeniacae Amarum quintessence oil 0.1kg, antibacterial (Switzerland Glydant Plus Liquid) 0.2kg, surplus is deionized water, for subsequent use;
(2) 11kg Prunus armeniaca L.var.ansu Maxim. oil, 2kg stearic acid and 2kg hexadecanol are placed in batch can, at 85 DEG C, are stirred to whole dissolving, obtain mixed material A;
(3) 0.15kg hyaluronic acid, 5kg reed fragrant plant glue, 1.5kg emulsifying agent and deionized water are placed in another material-compound tank, at 85 DEG C, are stirred to whole dissolving, obtain mixed material B;
(4) under the stirring condition of 85 DEG C, mixed material A is added in mixed material B and carries out emulsifying, after being cooled to 50 DEG C after 30min, adding 0.2kg antibacterial again after adding 0.1kg Semen Armeniacae Amarum quintessence oil, continue to be stirred to room temperature, obtain Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion.
Obtained emulsion, after-15 ~-5 DEG C and 40 DEG C place 24h, recovers room temperature without oil-water separation phenomenon.
Obtained emulsion 2000r/min rotates 30min, without oil-water separation phenomenon after leaving standstill.
Embodiment 2
The preparation of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, comprises the following steps:
(1) detoxification Prunus armeniaca L.var.ansu Maxim. oil 12kg, hyaluronic acid 0.2kg is taken, reed fragrant plant glue 5kg, hexadecanol 3kg, emulsifying agent (French Creagel Ez ~ 7) 1.5kg, stearic acid 2kg, Semen Armeniacae Amarum quintessence oil 0.1kg, antibacterial (Switzerland Glydant Plus Liquid) 0.2kg, surplus is deionized water, for subsequent use;
(2) 12kg Prunus armeniaca L.var.ansu Maxim. oil, 2kg stearic acid and 3kg hexadecanol are placed in batch can, at 85 DEG C, are stirred to whole dissolving, obtain mixed material A;
(3) 0.2kg hyaluronic acid, 5kg reed fragrant plant glue, 1.5kg emulsifying agent and deionized water are placed in another material-compound tank, at 85 DEG C, are stirred to whole dissolving, obtain mixed material B;
(4) under the stirring condition of 85 DEG C, mixed material A is added in mixed material B and carries out emulsifying, after being cooled to 50 DEG C after 30min, adding 0.2kg antibacterial again after adding 0.1kg Semen Armeniacae Amarum quintessence oil, continue to be stirred to room temperature, obtain Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion.
Embodiment 3
The preparation of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, comprises the following steps:
(1) detoxification Prunus armeniaca L.var.ansu Maxim. oil 13kg, hyaluronic acid 0.25kg is taken, reed fragrant plant glue 5kg, hexadecanol 4kg, emulsifying agent (French Creagel Ez ~ 7) 1.5kg, stearic acid 2kg, Semen Armeniacae Amarum quintessence oil 0.1kg, antibacterial (Switzerland Glydant Plus Liquid) 0.2kg, surplus is deionized water, for subsequent use;
(2) 13kg Prunus armeniaca L.var.ansu Maxim. oil, 2kg stearic acid and 4kg hexadecanol are placed in batch can, at 85 DEG C, are stirred to whole dissolving, obtain mixed material A;
(3) 0.25kg hyaluronic acid, 5kg reed fragrant plant glue, 1.5kg emulsifying agent and deionized water are placed in another material-compound tank, at 85 DEG C, are stirred to whole dissolving, obtain mixed material B;
(4) under the stirring condition of 85 DEG C, mixed material A is added in mixed material B and carries out emulsifying, after being cooled to 50 DEG C after 30min, after adding 0.1kg essence, add 0.2kg antibacterial again, continue to be stirred to room temperature, obtain Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion.
To sum up, the present invention is with detoxification Prunus armeniaca L.var.ansu Maxim. oil for primary raw material, and select the cosmetics adding ingredient be applicable to, make skin-moisturizing, skin emulsion according to a certain ratio, raw materials used green safety, preparation method is simple to operation, and production efficiency is high.
Provide the result of use of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion below:
Carried out 200 people at Yangling Shaanxi to try out, trial effect is good.This production is simple for process, reliable and stable, specifically as shown in table 2.
Table 2 product beta test effect
Especially, in above-mentioned crowd, find that Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion to have some improvement effect to psoriasis tool, so Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion is in the preparation that can be applicable to antipsoriatic medicine or skin care item.

Claims (10)

1. a Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, it is characterized in that, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 10 ~ 20%, hyaluronic acid 0.15 ~ 0.5%, reed fragrant plant glue 2 ~ 5%, hexadecanol 2 ~ 4%, Creagel Ez-7 0.5 ~ 1.5%, stearic acid 1 ~ 2%, essence 0.1 ~ 0.5% and antibacterial 0.2 ~ 0.5%, deionized water complements to 100%; Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion is after-5 ~-15 DEG C or 40 DEG C place 24h, or 2000r/min rotates 30min, recovers room temperature without oil-water separation phenomenon.
2. Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 1, it is characterized in that, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 ~ 13%, hyaluronic acid 0.15 ~ 0.25%, reed fragrant plant glue 4 ~ 5%, hexadecanol 3 ~ 4%, Creagel Ez-7 0.5 ~ 1.5%, stearic acid 1 ~ 2%, essence 0.1 ~ 0.5% and antibacterial 0.2 ~ 0.5%, it is 4.0 ~ 8.5 that deionized water complements to 100%, pH.
3. Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 1, it is characterized in that, in mass fraction, comprise following component: detoxification Prunus armeniaca L.var.ansu Maxim. oil 11 ~ 13%, hyaluronic acid 0.15 ~ 0.25%, reed fragrant plant glue 5%, hexadecanol 2 ~ 4%, Creagel Ez-7 1.5%, stearic acid 2%, essence 0.1% and antibacterial 0.2%, it is 4.0 ~ 8.5 that deionized water complements to 100%, pH.
4. Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 1, it is characterized in that, described essence is the essence distributing Semen Armeniacae Amarum delicate fragrance.
5. Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 1, it is characterized in that, described essence is Semen Armeniacae Amarum quintessence oil.
6. Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 1, it is characterized in that, antibacterial is Glydant Plus_Liquid.
7. a preparation method for Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion, is characterized in that, comprise the following steps:
1) by mass percentage, take the detoxification Prunus armeniaca L.var.ansu Maxim. oil of 10 ~ 20% respectively, the hyaluronic acid of 0.15 ~ 0.5%, the reed fragrant plant glue of 2 ~ 5%, the hexadecanol of 2 ~ 4%, the Creagel Ez-7 of 0.5 ~ 1.5%, the stearic acid of 1 ~ 2%, the essence of 0.1 ~ 0.5%, the antibacterial of 0.2 ~ 0.5%, deionized water complements to 100%, for subsequent use;
2) by step 1) the detoxification Prunus armeniaca L.var.ansu Maxim. oil, stearic acid, the hexadecanol that take, be stirred well at 80 ~ 90 DEG C and dissolve completely, obtain mixed material A;
3) by step 1) take in hyaluronic acid, reed fragrant plant glue, Creagel Ez-7 and deionized water, be stirred well at 80 ~ 85 DEG C and dissolve completely, obtain mixed material B;
4) 80 ~ 90 DEG C, under stirring condition, mixed material A is added after carrying out emulsifying in mixed material B, to be emulsified completely after be cooled to 45 ~ 55 DEG C, add Semen Armeniacae Amarum quintessence oil fully to stir, and then add antibacterial stirring, stop stirring after naturally cooling to room temperature, obtain Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion;
Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion is after-5 ~-15 DEG C or 40 DEG C place 24h, or 2000r/min rotates 30min, recovers room temperature without oil-water separation phenomenon.
8. the preparation method of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 7, is characterized in that, step 4) described in emulsifying at least emulsifying 30min.
9. the preparation method of Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion as claimed in claim 7, it is characterized in that, described essence is Semen Armeniacae Amarum quintessence oil, and antibacterial is Glydant Plus_Liquid.
10. Prunus armeniaca L.var.ansu Maxim. oil skin-moisturizing, skin emulsion according to claim 1 is in the application preparing antipsoriatic medicine or skin care item.
CN201310153031.6A 2013-04-27 2013-04-27 Armeniaca sibirica oil skin-moisturizing lotion and preparation method thereof Active CN103222935B (en)

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CN104707499B (en) * 2015-02-13 2016-11-23 西北农林科技大学 A kind of preparation method of nonionic Semen Armeniacae Amarum oil microemulsion
CN105919905A (en) * 2016-07-02 2016-09-07 国家林业局泡桐研究开发中心 Wild apricot eucommia ulmoides moisturizing and nourishing cream and preparation method thereof

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