CN101744757A - Preservative-free moisturizing firming cosmetic containing natural and organic ingredients - Google Patents
Preservative-free moisturizing firming cosmetic containing natural and organic ingredients Download PDFInfo
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- CN101744757A CN101744757A CN200810219539A CN200810219539A CN101744757A CN 101744757 A CN101744757 A CN 101744757A CN 200810219539 A CN200810219539 A CN 200810219539A CN 200810219539 A CN200810219539 A CN 200810219539A CN 101744757 A CN101744757 A CN 101744757A
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Abstract
The invention relates to a group of cosmetic compositions which do not contain preservatives and have the effects of immediate firming, long-acting anti-wrinkle and moisturizing. The cosmetic compositions comprise a freshener, a moisturizer, a cream, an essence and a mask, wherein the moisturizer, the cream and the essence are emulsified products; and a surfactant is organic material coming from the natural plants. In the active ingredients, hydrolysis rhizobian gum and Arabic gum having the immediate firming effect, purified ingredients of natural polysaccharide extracted from oat grains, dipalmitoyl hydroxyproline having the long-acting anti-wrinkle effect, and xylitylglucoside, composition of anhydroxylitol and xylitol, trimethylglycine and sodium hyaluronate having the moisturizing effect are organic materials. The traditional preservatives are not contained in the product, and caprylyl glycine and caprylin substituting for the traditional preservatives come from the plants. The invention relates to an application of the organic materials and materials coming from the plants and a preparation method of the cosmetic.
Description
Technical field
The present invention relates to one group of cosmetic composition, comprise water preparation, emulsion, cream frost, essence and facial film with instant Firm, long-acting crease-resistant and moistening effect.Used surfactant is the Organic Ingredients in natural plants source in the above-mentioned cosmetics.In the active component, Herba bromi japonici wheat grain extract with instant Firm effect, hydrolysis root nodule bacteria glue and arabic gum compositions, dipalmitoyl hydroxyproline with long-acting anti-wrinkle effect, have xylitol glucoside, dehydration xylitol and the Xylitol compositions of moistening effect, trimethyl glycine and hyaluronate sodium are Organic Ingredients.Do not contain traditional antiseptic in the product, the succedaneum caprylyl glycine of employed traditional preservatives and caprylin are plant origin.Patent of the present invention relates to the application of these Organic Ingredientss and plant origin raw material and the manufacture method of above-mentioned cosmetics.
Background technology
Skin protection cosmetics has passed through a series of wind and rain baptism such as chemical industry epoch, animal component, biological preparation, and natural Organic Ingredients begins to apply in the cosmetics, and is subjected to people's favor gradually.
The notion of organic cosmetics activated feedstock is to extend from organic agriculture, prerequisite requires the contained plant component of its product must be derived from " organic plant " equally, promptly be not subjected to any noxious substance, under the environment of transgene component and heavy metal pollution, without chemosynthesis fertilizer, pesticide, insecticide, the crops of antibiotic and growth regulator plantation gained, and in subsequent product processing, do not add any artificial flavors, composition such as pigment and petroleum chemicals, antiseptic that is added and surfactant all must be subjected to strict restriction, and can not use zoopery in the manufacture process and utilize the lonizing radiation sterilization.The quick growth in contrast Organic food market, cosmetics market also will be experienced one and similarly change.Organic cosmetics can not cause any side effect to skin, and can in time repair impaired skin, make skin keep ultimate attainment perfection, meet people's healthy desire, and it is harmonious ecological to allow people initiatively incorporate.Therefore, organic cosmetics market potential is huge, and " organic " tide is irresistible.
Antiseptic in the cosmetics can suppress, kill microorganisms such as fungus and antibacterial, but life-time service also can bring potential hidden danger to skin health.In order to make healthy more personal care articles, people have begun one's study and have not added the cosmetics of antiseptic.So-called " no anticorrosion ", be meant and do not add the raw material that is listed in antiseptic in the corresponding standard (as the appendix VI of the 76/768/EEC of European Union) in the prescription, and using other raw materials with antisepsis, the raw material that substitutes protective system has cosmetology functions such as moisturizing, stuffing, perfuming usually.Before about 15 years, Dr.Straetmens company has released that (the INCI title: caprylyl glycol) be the raw material of the name of an article, this is to be used for one of multiple-effect cosmetic composition that substitutes antiseptic in the first batch with Dermosoft Octiol.Traditional preservatives substitutes composition and also has pentanediol, silver salt (citrate, silver coating TiO
2), lactoperoxidase/glucose oxidase, endecatylene acyl glycine, paraanisic acid, phenylpropanol, caprylyl glycol, glycerol caprylate etc.These unconventional antiseptic have been adopted in some cosmetics.As in CN1628632, promptly having announced a kind of skin care item that do not contain essence, pigment, mineral oil, antiseptic, use the pentanediol of Carboxymethyl Chitin to reach antiseptic effect.In the crease-resistant moisturiser that the responsive skin that EP1920756A1 announces is suitable for, the pentanediol of use 4% reaches antiseptic effect.Use among the WO03069994A1 to contain 1 of 5～10 carbon atoms, the 2-alkyl diol reaches antiseptic effect, as 2% 1,2-hexanediol and 1% ethohexadiol be composite to replace traditional antiseptic.Among the WO2007070795A2,, reach antiseptic effect with dihydroxylic alcohols such as ethohexadiol and multiple 'alpha '-hydroxy acids such as lactic acid, citric acid, mandelic acid, malic acid, tartaric acid, sorbic acid, the composite use of propanoic acid.Announced a kind of natural raw material---extracting method of licorice root extract and propolis extract that is used for food, medicine, cosmetics among the patent JP63145208A, but yet there are no the example that is used for cosmetics with antiseptic effect.Yet there are no the report that natural antiseptic succedaneum is used in cosmetic formulations.
As time goes on, a series of variation, most importantly natural aging and photoaging have also taken place in our skin unawares.With age growth, the barrier ability of skin reduces, and it is dry, coarse, responsive, lax that skin becomes, and produces wrinkle and crows-feet.The moisture of keratodermatitis can be kept skin health, and the various stimulations that defence is subjected to from the external world prevent skin aging and moist, beauty treatment skin.When horny layer moisture was not enough, skin can be dry, and was so long-term, can make chapped skin or edema, thereby skin is followed the string, coarse aging.Therefore, preserving moisture with defying age is to maintain the requisite content of skin.Modern female is more and more higher to the quality requirements of cosmetics, and they pay close attention to the demand of skin, and wishes that the daily nursing product can produce rapid visible effect, and the product with immediate effect more and more receives an acclaim.The cosmetics that now existing patent report has the effect of compacting as CN1606429A, have been reported the compact effect of alginic acid sugar to skin, yet there are no report but have the patent that the Organic Ingredients of immediate effect is applied in the cosmetics.Especially yet there are no and contain natural organic active raw material, have the report of the cosmetics of instant Firm, long-acting crease-resistant and moistening effect simultaneously.
In today that science and technology develops rapidly, whether the people of pursuit quality of the life are organic, healthy to the skin of oneself equally, environmental protection has been paid close attention to more.Therefore, the skin care item correlation technique should constantly be reformed, to satisfy these requirements of people.
Summary of the invention
In order to satisfy modern female to safe, healthy, the natural requirement of cosmetics with to the rapid visible demand of cosmetic result, the invention provides one group and have instant Firm and long-acting anti-wrinkle effect, can strengthen the cosmetic composition of skin moisture-keeping lock outlet capacity simultaneously.The product that contains instant Firm raw material is coated with and is used for skin, the very fast tension effect that can experience skin.Used this set product one month, the skin water content can increase, and the old and feeble situation of skin can improve, and wrinkle alleviates.Used two months, skin condition is further improved, and the lock outlet capacity strengthens, and skin is high resilience more.This series products comprises water preparation, emulsion, cream frost, essence, facial film.
The scheme that patent of the present invention solves its technical problem is: reach instant Firm, the long-acting crease-resistant and effect of preserving moisture by using effective natural organic active raw material; In the oil-in-water type products such as cream frost, emulsion, essence, used emulsifying agent is an Organic Ingredients; And do not add traditional antiseptic in the cosmetics, use the raw material of plant origin to reach antiseptic effect, these raw materials are not classified the antiseptic composition of cosmetics as in the appendix VI of the 76/768/EEC of European Union.
One of feature of the cosmetic composition that the present invention relates to is by xylitol glucoside, dehydration xylitol and Xylitol compositions, trimethyl glycine, oils and fats in hyaluronate sodium and the cosmetics is that skin keeps the skin wet, and prevents water loss, makes skin dynamic.By Herba bromi japonici wheat grain extract, hydrolysis root nodule bacteria glue and arabic gum reach the effect of instant Firm.By the content of dipalmitoyl hydroxyproline increase skin corium collagen fiber and elastin laminin, to defying age.Above-mentioned active component is Organic Ingredients.
The cosmetics that contain xylitol glucoside, dehydration xylitol and xylitol are coated with and are used for skin, can promote the hydration of epidermis, increase the epidermis water content, reduce the epidermis water loss, cooperate greasy moist moisture-keeping function in the cosmetics, use the epidermis hydration is increased, thereby embody quick-acting moistening effects.Can strengthen simultaneously the content of skin corium glycosaminoglycans (as hyaluronic acid and chondroitin sulfate), thereby the moisture that strengthens skin corium keeps, and promote the synthetic of ceramide, strengthen the barrier function of skin, reach long-acting effect of preserving moisture.Its consumption is recommended as 0.1～20%, and 0.5～10% is better, 1～6% the best.
Trimethyl glycine is a kind of natural, edible aminoacid fully.Has unique performance of preserving moisture and protecting cell membrane.In solution, can form very strong hydrogen bond, easy and water molecules, the hydrone of absorption is distributed in around it by stereochemical structure.But its fixing hydrone unlike other polyhydric alcohol wetting agent, when physical condition changed, it was easy to hydrone is discharged, and hydrone can be utilized by living cells.Trimethyl glycine also can strengthen skin elasticity, lipid regulating when increasing moisture of skin.Its consumption is recommended as 0.1～40%, and 0.5～20% is better, 2～12% the bests.
Hyaluronic acid has special water retention, is called as ideal nature moisturizing factor.Hyaluronic acid is one of main matrix composition of application on human skin epidermis and corium; its physiological function is to impel moisture to enter intercellular substance; and form protein gel with protein bound; cell is sticked together, and maintenance cell moisture is played in the cellular metabolism effect of bringing into normal play; the protection cell is not subjected to the infringement of pathogen; accelerate to recover skin histology, improve the wound healing regeneration capacity, effects such as enhancing immunity.Hyaluronic acid can also improve the skin growth condition, and for dermal collagen albumen and elastic fiber synthetic provides superior external environment condition, the effect of skin-protecting face nursing is played in the supply of reinforced nutrition matter.Hyaluronic acid can be regulated in varying environment after acting on the inner conditioning of skin automatically, keeps moisture of skin all the time 25～30%, keeps the moistening of skin, and is salubrious, makes more high resilience of skin.In cosmetics, use organic hyaluronate sodium in natural plants source, when keeping moisture of skin, also can play antidotal effect.Its consumption is recommended as 0.005～1.5%, and 0.01～0.5% is better, 0.02～0.2% the best.
For reaching the visible effect of compacting rapidly, can use a kind of purified components by the natural polysaccharide that extracts in the Herba bromi japonici wheat grain, it is 100% natural sugar by the linear polysaccharide molecular composition.This polysaccharide is stable by its intramolecularly and intermolecular hydrogen bonding, forms 3-D solid structure.A large amount of hydroxyls is arranged on its side chain, can combine, especially, make it that very strong adhesive capacity be arranged by the hydroxyl of self and the amino bonded of ceramide with cuticular intercellular lipid.This high-molecular weight sugar is very favourable to regulating the skin micro structure, and it is adsorbed in skin surface, forms viscoelasticity, adhesion, successive biofilm rapidly, realizes the effect of instant Firm.The consumption of this Herba bromi japonici wheat grain extract is recommended as 0.01～20%, and 0.05～10% is better, 0.1～5% the best.
Also have an a kind of compositions of being made up of hydrolysis root nodule bacteria glue and arabic gum, the cosmetics that contain this compositions are applied to also can produce the instant effect of compacting on the skin.Hydrolysis root nodule bacteria glue obtains by fermentation process, and the arabic gum extraction is from African branch with in doing.What this compositions caused is physical change, can promote skin, gives the skin-tightening effect, reduces little relief and wrinkle.Its consumption is recommended as 0.01～15%, and 0.05～10% is better, 0.1～6% the best.
With age growth, elastic fiber in the skin corium and collagen fiber reduce, and skin begins to wear out.Dipalmitoyl hydroxyproline is the Palmic acid of plant origin and combining of hydroxyproline; it can promote collagen fiber to shrink; remove free radical; and it is effective elastase inhibitor; can protect elastin laminin can not decomposed by enzyme; thereby the maintenance skin elasticity realizes the repair to skin corium.Be applied in the cosmetics, make it to have long-acting anti-wrinkle effect.Used 2 months, wrinkle can obviously improve.Its consumption is recommended as 0.01～15%, and 0.1～8% is better, 0.5～5% the best.
Another feature of the cosmetic composition that the present invention relates to is cream frost, emulsion, the used emulsifying agent 16 octadecyl glucosides of essence, the coco group glucoside is the Organic Ingredients in natural plants source, do not contain transgene component, and have the outstanding skin compatibility and excellent biodegradability, the good moisture preserving effect is provided simultaneously.Prepared cream frost and emulsion can form biplate layered liquid crystal structure, are similar to the structure of skin, can strengthen oils and fats protection barrier and prevent that moisture of skin runs off, and improves the stability of product simultaneously.Its consumption is recommended as 0.1～10%, and 0.3～7% is better, 0.5～4% the best.
The 3rd feature of the cosmetic composition that the present invention relates to is not contain artificial color, mineral oil or other petroleum-type products, spice, silicon ketone and traditional antiseptic; the caprylyl glycine of use plant origin and caprylin reach antiseptic effect as the succedaneum of traditional preservatives.Caprylin has stuffing, preserves moisture, deodorization.The decoyl glycine is the skin acidulant.These two kinds of chemical compounds are the film activity composition, can reduce surface tension, improve wettability, thereby strengthen the preservative efficacy of organic acid or other raw materials.And because the relation of structure, they can the permeation cell films and destroy the integrity of film, thereby cause the cells of microorganisms film to damage.Its consumption is recommended as 0.01～10%, and 0.1～6% is better, 0.5～3% the best.
Realize that by above-mentioned these methods people are to cosmetics safety, natural, healthy, organically requirement.Patent of the present invention relates to the application of these Organic Ingredientss and the manufacture method of above-mentioned cosmetics.
The specific embodiment
The application of above-mentioned raw materials in cosmetics embodies by the following example.
Embodiment 1 moisturizing firming water
With Herba bromi japonici wheat grain extract as instant Firm raw material, preparation moisturizing firming water, a wherein, b, c, d, the different models of the different corresponding Herba bromi japonici wheat grain extractive contents of numbering of e.Do not add traditional preservatives, reach antiseptic effect by adding the caprylyl glycine.Proportioning raw materials is as follows:
Among the embodiment 1, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol and Xylitol compositions, Herba bromi japonici wheat grain extract is an Organic Ingredients.
Technology: A group material prepares, and 90 ℃ of insulation 30min are cooled to below 35 ℃, adds B group material, stirs.
Verify instant Firm effect by smearing, method is: 20 volunteers (12 women, 8 male), respectively with above-mentioned a, b, c, d, e sample are applied to the back of the hand wrist place, and different samples are smeared more than the interval 8h, smear back 5min, 30min, 4h experience the effect of compacting respectively, and marking.5 are divided into best result, and expression has a very strong tension effect, and 4 are divided into stronger tension effect is arranged, and 3 are divided into tangible tension effect is arranged, and 2 are divided into some tension effects are arranged, and 1 is divided into no tension effect.Average and count final score, it is as follows to mark:
As seen, the aqua product that has added Herba bromi japonici wheat grain extract is applied on the skin, can experience the effect of compacting immediately, and sustainable several hrs.The moisturizing firming glassware for drinking water that contains 0.5～2% Herba bromi japonici wheat grain extract has instant preferably Firm effect, and the water preparation that contains 3% Herba bromi japonici wheat grain extract has the stronger effect of compacting, and the water preparation that contains 4% Herba bromi japonici wheat grain extract has the very strong effect of compacting.
The above-mentioned sample that contains 2% Herba bromi japonici wheat grain extract is carried out the test of microorganism challenge, and method is pressed examination criteria USP27＜51 〉, the result is as follows:
As seen, the succedaneum of employed traditional preservatives has the inhibitory or killing effect of extra-heavy to microorganism, can test by challenge.Product is not easy by microbial contamination when producing, preserving and using.
Embodiment 2 moisturizing firming water
Selecting hydrolysis root nodule bacteria glue and arabic gum for use is that instant Firm raw material is prepared moisturizing firming water, reaches antiseptic effect by adding the caprylyl glycine, and proportioning raw materials is as follows:
Among the embodiment 2, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol and Xylitol compositions, hydrolysis root nodule bacteria glue and arabic gum compositions are Organic Ingredients.
Technology is with embodiment 1.
Verify instant Firm effect by smearing, method is with embodiment 1, and it is as follows to mark:
As seen, contain 0.5～5% hydrolysis root nodule bacteria glue and arabic gum and add in the aqua product, be applied on the skin, can experience the effect of significantly compacting immediately, and sustainable several hrs, the moisturizing firming glassware for drinking water that contains 5% hydrolysis root nodule bacteria glue and arabic gum has very strong instant Firm effect.
Embodiment 3 moisturizing firming frosts
Select for use Herba bromi japonici wheat grain extract as instant Firm raw material, preparation moisturizing firming frost, a wherein, b, c, the difference of d model is Herba bromi japonici wheat grain extractive content difference, proportioning raw materials is as follows:
Among the embodiment 3,16 octadecyl glucosides, the coco group glucoside, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol and Xylitol compositions, dipalmitoyl hydroxyproline, Herba bromi japonici wheat grain extract is an Organic Ingredients.
Technology: A group material prepares, mix homogeneously, 90 ℃ of insulation 20min; B group material prepares, mix homogeneously, 80 ℃ of insulation 10min; B group material is added A group material, and homogenizing 5min stirs cooling, and 60 ℃ add C group material, stir cooling at a slow speed, and 35 ℃ add D group material, stir.
Estimate instant Firm effect by smearing test, method is: 28 volunteers (21 women, 7 male), respectively with above-mentioned a, b, c, d sample are applied to the back of the hand wrist place, and different samples are smeared more than the interval 8h, smear back 5min, 30min and 4h experience the effect of compacting respectively, and marking.5 are divided into best result, and expression has a strong tension effect, and 4 are divided into stronger tension effect is arranged, and 3 are divided into tangible tension effect is arranged, and 2 are divided into some tension effects are arranged, and 1 is divided into no tension effect.Average and count final score.
As seen, the cream frost product that contains Herba bromi japonici wheat grain extract is applied on the skin, can experience the effect of compacting immediately, and sustainable several hrs.The cream frost that contains 0.5～2% Herba bromi japonici wheat grain extract promptly has instant preferably Firm effect, and the cream frost that contains 3% Herba bromi japonici wheat grain extract has the strong effect of compacting immediately.
The moisturizing firming frost is applied to eye, to experience instant Firm effect.Method is: 38 volunteers (33 women, 5 male), and respectively with above-mentioned a, b, c, the d sample is applied near the eyes, and different samples are smeared more than the interval 24h, smear back 5min, and 30min, 4h experience the effect of compacting respectively, and marking.
As seen, the cream frost that adds Herba bromi japonici wheat grain extract is applied to eye, can experience the effect of very significantly compacting immediately, and the cream frost that contains 0.5% Herba bromi japonici wheat grain extract promptly has the obvious and lasting effect of compacting.
Preserve moisture and the anti-wrinkle effect assessment with the sample that contains 2% Herba bromi japonici wheat grain extract, method is: 27 female volunteers (30～45 years old age), sample is applied to face, and it is preserved moisture and anti-wrinkle effect to smear post-evaluation, and marking.5 are divided into best result, and the expression effect is very good, and 4 are divided into finely, and 3 are divided into positive effect is arranged, and 2 are divided into some effects are arranged, and 1 is divided into no tension effect.Average and count final score.The results are shown in following table:
As seen, the above-mentioned moisturizing firming frost that contains organic composition can reach well instant Firm, the long-acting crease-resistant and effect of preserving moisture.
The above-mentioned sample that contains 2% Herba bromi japonici wheat grain extract is carried out the test of microorganism challenge, and method is pressed examination criteria USP27＜51 〉, the result is as follows:
As seen, the succedaneum of employed traditional preservatives has the inhibitory or killing effect of extra-heavy to microorganism, can test by challenge.Product is not easy by microbial contamination when producing, preserving and using.
Embodiment 4 moisturizing firming frosts
Select for use hydrolysis root nodule bacteria glue and arabic gum as instant Firm raw material, preparation moisturizing firming frost, a wherein, b, c, d number test difference is that hydrolysis root nodule bacteria glue is different with arabic gum content, proportioning raw materials is as follows:
Among the embodiment 4,16 octadecyl glucosides, the coco group glucoside, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol and Xylitol compositions, dipalmitoyl hydroxyproline, hydrolysis root nodule bacteria glue and arabic gum are Organic Ingredients.
Technology is with embodiment 3.
Verify instant Firm effect by smearing, method is: 39 volunteers (31 women, 8 male), respectively with above-mentioned a, b, c, d sample are applied to the back of the hand wrist place, and different samples are smeared more than the interval 8h, smear back 5min, 30min, 4h experience the effect of compacting respectively, and marking.5 are divided into best result, and expression has a strong tension effect, and 4 are divided into stronger tension effect is arranged, and 3 are divided into tangible tension effect is arranged, and 2 are divided into some tension effects are arranged, and 1 is divided into no tension effect.Average and count final score.
As seen, the cream frost product that contains hydrolysis root nodule bacteria glue and arabic gum is applied on the skin, can experience the effect of compacting immediately, and sustainable several hrs.The cream frost that contains 0.5～2% hydrolysis root nodule bacteria glue and arabic gum promptly has instant preferably Firm effect, and the cream frost that contains 3% hydrolysis root nodule bacteria glue and arabic gum has the very strong effect of compacting.
The moisturizing firming frost is applied to eye, to experience its instant Firm effect.Method is: 20 volunteers (13 women, 7 male), and respectively with above-mentioned a, b, c, the d sample is applied near the eyes, and different samples are smeared more than the interval 24h, smear back 5min, and 30min, 4h experience the effect of compacting respectively, and marking.
As seen, the cream frost that adds hydrolysis root nodule bacteria glue and arabic gum is applied to eye, can experience the effect of very significantly compacting immediately, and the cream frost that contains 0.5% hydrolysis root nodule bacteria glue and arabic gum promptly has the obvious and lasting effect of compacting.
Preserve moisture and the anti-wrinkle effect assessment with the sample that contains 1% hydrolysis root nodule bacteria glue and arabic gum, method is: 20 female volunteers (30～45 years old age), above-mentioned sample is applied to face, and it is preserved moisture and anti-wrinkle effect to smear post-evaluation, and marking.5 are divided into best result, and the expression effect is very good, and 4 are divided into finely, and 3 are divided into positive effect is arranged, and 2 are divided into some effects are arranged, and 1 is divided into no tension effect.Average and count final score, the results are shown in following table:
As seen, the above-mentioned moisturizing firming frost that contains organic composition can reach well instant Firm, the long-acting crease-resistant and effect of preserving moisture.
The above-mentioned sample that contains 1% hydrolysis root nodule bacteria glue and arabic gum is carried out the test of microorganism challenge, and method is pressed examination criteria USP27＜51 〉, testing result is as follows:
As seen, the traditional preservatives succedaneum of employed plant origin has the inhibitory or killing effect of extra-heavy to microorganism, can test by challenge.Product is not easy by microbial contamination when producing, preserving and using.
Embodiment 5 moisturizing firming emulsions
Select for use 1% hydrolysis root nodule bacteria glue and arabic gum as instant Firm raw material, preparation moisturizing firming emulsion uses the caprylyl glycine to reach antiseptic effect, and proportioning raw materials is as follows:
Among the embodiment 5,16 octadecyl glucosides, the coco group glucoside, trimethyl glycine, hyaluronate sodium, the xylitol glucoside, the dehydration xylitol, xylitol, dipalmitoyl hydroxyproline, hydrolysis root nodule bacteria glue and arabic gum are Organic Ingredients.
Technology: A group material prepares, 90 ℃ of insulation 20min, and B group material prepares, and 80 ℃ of insulation 10min add A group material with B group material, and homogenizing 5min stirs cooling, adds C group material below 35 ℃, stirs.
Estimate its instant Firm, preserve moisture and anti-wrinkle effect by smearing test, method is: 26 female volunteers (30～45 years old), sample is applied to face, and estimate the effect of compacting that it uses back 30min; Use the effect of compacting of back 4h; Use the moistening effect of back 30min; Use the moistening effect of back 24h; Use the moistening effect of 1 month (every day, each was used once sooner or later) continuously; Use the anti-wrinkle effect of 1 month (every day, each was used once sooner or later) continuously; Use the anti-wrinkle effect of 2 months (every day, each was used once sooner or later) continuously.Give a mark according to result of use, 5 are divided into best result, and the expression effect is very good, and 4 are divided into finely, and 3 are divided into positive effect is arranged, and 2 are divided into some effects are arranged, and 1 is divided into no tension effect.Average and count final score, the results are shown in following table:
As seen, the above-mentioned moisturizing firming emulsion that contains organic composition can reach well instant Firm, long-acting crease-resistant and moistening effect.
Above-mentioned emulsion is carried out the test of microorganism challenge, and method is pressed examination criteria USP27＜51 〉, testing result is as follows:
As seen, the succedaneum of employed traditional preservatives has the inhibitory or killing effect of extra-heavy to microorganism, can test by challenge.Product is not easy by microbial contamination when producing, preserving and using.
Embodiment 6 essences
Select for use Herba bromi japonici wheat grain extract to prepare essence as instant Firm raw material, reach antiseptic effect by adding caprylin, proportioning raw materials is as follows:
Among the embodiment 6,16 octadecyl glucosides, the coco group glucoside, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol and Xylitol compositions, dipalmitoyl hydroxyproline, Herba bromi japonici wheat grain extract is an Organic Ingredients.
Technology: A group material prepares, mix homogeneously, 90 ℃ of insulation 20min; B group material prepares, mix homogeneously, 80 ℃ of insulation 10min; B group material is added A group material, and homogenizing 5min stirs cooling.35 ℃ add C group material, stir.
Estimate its instant Firm, preserve moisture and anti-wrinkle effect by smearing test, method is: 39 female volunteers (30～45 years old), sample is applied to face, and estimate the effect of compacting that it uses back 30min; Use the effect of compacting of back 4h; Use the moistening effect of back 30min; Use the moistening effect of back 24h; Use the moistening effect of 1 month (every day, each was used once sooner or later) continuously; Use the anti-wrinkle effect of 1 month (every day, each was used once sooner or later) continuously; Use the anti-wrinkle effect of 2 months (every day, each was used once sooner or later) continuously.Give a mark according to result of use, 5 are divided into best result, and the expression effect is very good, and 4 are divided into finely, and 3 are divided into positive effect is arranged, and 2 are divided into some effects are arranged, and 1 is divided into no tension effect.Average and count final score, the results are shown in following table:
As seen, the above-mentioned essence that contains organic composition can reach well instant Firm, the long-acting crease-resistant and effect of preserving moisture.
Above-mentioned essence is carried out the test of microorganism challenge, and method is by examination criteria USP27＜51〉carry out, the result is as follows:
As seen, the non-traditional antiseptic that uses microorganism is had the inhibitory or killing effect of extra-heavy, can test by challenge.Product is not easy by microbial contamination when producing, preserving and using.
Embodiment 7 moisturizing firming anti-wrinkle creams
Reduce the consumption of instant Firm raw material, make the cream frost have weak instant Firm effect,, strengthen anti-wrinkle effect by active components of plants and roe elite, coenzyme Q10, oligopeptide-1 (human epidermal cell growth factor) EGF are used, preparation moisturizing firming anti-wrinkle cream, proportioning raw materials is as follows:
Among the embodiment 7,16 octadecyl glucosides, the coco group glucoside, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol, Xylitol compositions, dipalmitoyl hydroxyproline, Herba bromi japonici wheat grain extract is an Organic Ingredients.
Technology is with embodiment 3.
Estimate its instant Firm by smearing test, preserve moisture and anti-wrinkle effect, method is: 21 female volunteers (30～45 years old), sample is applied to face, and estimate the effect of compacting that it uses back 30min; Use the effect of compacting of back 4h; Use the moistening effect of back 30min; Use the moistening effect of back 24h; Use the moistening effect of 1 month (every day, each was used once sooner or later) continuously; Use the anti-wrinkle effect of 1 month (every day, each was used once sooner or later) continuously; Use the anti-wrinkle effect of 2 months (every day, each was used once sooner or later) continuously.Give a mark according to result of use, 5 are divided into best result, and the expression effect is very good, and 4 are divided into finely, and 3 are divided into positive effect is arranged, and 2 are divided into some effects are arranged, and 1 is divided into no tension effect.Average and count final score, the results are shown in following table:
Above-mentioned sample is carried out patch test test its anaphylaxis skin, method is: select qualified speckle examination device for use, 0.025～0.03g sample is put into speckle examination device, speckle is tried device stick in the bent side of experimenter's forearm, make it to stick equably on skin with light pressure of palm, continue 72h.Removal is tried behind the thing speckle examination device 30min at interval, treats that the impression back that disappears observes dermoreaction.With reference to dermoreaction grade scale record reaction result in the cosmetics health standard (version in 2007).Negative control: white mineral oil.The experimenter is totally 150 people, male 56 people wherein, women 94 people.Result: this moisturizing firming anti-wrinkle cream is had irritated or other abnormal responses of 0 example.
As seen, above-mentioned moisturizing firming frost has the instant Firm effect that can experience with the composite a small amount of non-organic active raw material of organic active raw material, has good moisture preserving and anti-wrinkle effect simultaneously, and product is harmless non-stimulated to skin.
Above-mentioned moisturizing firming anti-wrinkle cream is carried out the test of microorganism challenge, and method is pressed examination criteria USP27＜51 〉, result of the test is as follows:
Experimental result: the non-traditional antiseptic that uses microorganism is had the inhibitory or killing effect of extra-heavy, can test by challenge.Product is not easy by microbial contamination when producing, preserving and using.
Embodiment 8 replenishing water and preserving moisture sleep facial film
The sleep facial film that preparation has the replenishing water and preserving moisture effect, proportioning raw materials is as follows:
Among the embodiment 8, trimethyl glycine, hyaluronate sodium, xylitol glucoside, dehydration xylitol and Xylitol compositions are Organic Ingredients.
Technology: A group material prepares, and 90 ℃ of insulation 20min are cooled to 60 ℃, adds B group material, stirs.Stirring is cooled to 35 ℃, adds C group material, and stirring gets final product.
Above-mentioned replenishing water and preserving moisture sleep facial film is carried out the moistening effect assessment, and method is: the female volunteers of 25 35～45 years old age brackets is not used any other skin care item after clean before sleeping every day, the facial film of will sleeping is applied to face, need not clean.After using 1 time, also mark respectively with its effect of use post-evaluation in 1 month.5 are divided into best result, and the expression effect is very good; 4 be divided into fine; 3 to be divided into effect obvious; 2 submeters are shown with some effects; 1 is divided into to no effect.It below is every average.The results are shown in following table:
As seen, above-mentioned sleep facial film can reach good replenishing water and preserving moisture effect.
The above, only be that the present invention contains organic principle and has the preferred embodiment of the no anticorrosion cosmetics and preparation method thereof of moisturizing firming effect, be not that technical scope of the present invention is imposed any restrictions, so every foundation technical spirit of the present invention all still belongs in the scope of technical solution of the present invention any trickle modification, equivalent variations and modification that above embodiment did.
Claims (4)
1. one group of cosmetic composition with instant Firm, long-acting crease-resistant and moistening effect.Comprise water preparation, emulsion, cream frost, essence and facial film.
2. the instant Firm effect in the described cosmetic composition of claim 1 is from hydrolysis root nodule bacteria glue and arabic gum compositions, by the purified components of the natural polysaccharide that extracts in the Herba bromi japonici wheat grain.The addition of hydrolysis root nodule bacteria glue and arabic gum compositions is 0.05～15%.The addition of Herba bromi japonici wheat grain extract is 0.05～20%.Long-acting anti-wrinkle effect is from dipalmitoyl hydroxyproline, and addition is 0.01～15%.Moistening effect is from compositions, trimethyl glycine and the hyaluronate sodium of xylitol glucoside, dehydration xylitol and xylitol.The addition of xylitol glucoside, dehydration xylitol and Xylitol compositions is 0.1～20%.The addition of trimethyl glycine is 0.1～40%.The addition of hyaluronate sodium is 0.005～1.5%.Above-mentioned active component is organic cosmetics activated feedstock.
3. emulsion, cream frost and the essence in the described cosmetic composition of claim 1 is the oil-in-water type product, employed emulsifying agent is the organic surface active agent in natural plants source, effective ingredient is 16 octadecyl glucosides and coco group glucoside, and addition is 0.1～10%.
4. all do not contain artificial color, mineral oil or other petroleum-type products, spice, silicon ketone and traditional antiseptic in the described cosmetic composition of claim 1.Use the caprylyl glycine and the caprylin of plant origin to replace traditional preservatives, addition is 0.01～10%
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