CN108143702A - A kind of efficient whitening and moisturizing facial mask liquid, facial mask and preparation method thereof - Google Patents
A kind of efficient whitening and moisturizing facial mask liquid, facial mask and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The present invention relates to cosmetics fields, and in particular to a kind of efficient whitening and moisturizing facial mask liquid, facial mask and preparation method thereof.A kind of efficient whitening and moisturizing facial mask liquid, in parts by weight, including at least following components：100 parts of deionized water, 6~13 parts of moisturizer, 3~9 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, including at least following components：16~23 parts of 36~42 parts of 3~7 parts of allantoin, Cer EOS~5 part, 35~44 parts of beta glucan, Europe gentian and grape seed extract, aurelia and rice extract.
Description
Technical field
The present invention relates to cosmetics fields, and in particular to a kind of efficient whitening and moisturizing facial mask liquid, facial mask and its
Preparation method.
Background technology
In personal nursing class daily chemical products, facial mask is a kind of preferable facial-care product being loved by consumers, people
The nursing of skin of face is especially paid attention to, pursue the maintenance of facial appearance.Mask product on the market has much at present, there is U.S.
Fine flour film, moisture saver mask, MASQUE APAISANT HYDRATANT etc., but the effect of many facial masks is not some chemical substances caused by natural component
It may be irritating to the skin, seriously can even cause skin of face allergy etc., it is commercially available to there are some mask products even also to relate to
And heavy metals exceeding standard.And consumer can collect whitening and moisturizing again for pure natural plant ingredients, especially pure natural plant ingredients
The facial mask of function has great demand.
The present invention is intended to provide a kind of facial mask liquid for making full use of pure natural animal and plant extracts, each component collaboration can be played
Calm, anti-inflammatory, neu- roimmunomodulation promotes skin regeneration, facial mask liquid of reasonable cost and facial mask.It is an object of the invention to
There is provided one kind directly act on skin sensitivity position, it is pure natural extract, have no toxic side effect, collect whitening, moisturizing, releive and other effects with
The mask product of the whole body is met people for skin care, mild antiallergic, safe and effective three kinds of demands, avoids being resisted using hormone
The quick injury come to skin tape.
Invention content
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of efficient whitening and moisturizing facial mask liquid,
In parts by weight, including at least following components：100 parts of deionized water, 6~13 parts of moisturizer, 3~9 parts of skin conditioning agent；With weight
Measure part meter, the skin conditioning agent, including at least following components：3~7 parts of allantoin, Cer EOS~5 part, beta glucan
16~23 parts of 36~42 parts of 35~44 parts, Europe gentian and grape seed extract, aurelia and rice extract.
As a kind of preferred technical solution of the present invention, in parts by weight, the moisturizer, including at least with the following group
Point：3 parts of small molecule polyol, 0.06~0.13 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.
As a kind of preferred technical solution of the present invention, the small molecule polyol is selected from 1,3-PD, glycerine, 1,
3- butanediols, 2- methyl-1,3-propanediols, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- hexylene glycols, dimerization the third three
Alcohol, dipropylene glycol, D-sorbite, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol any one or more of；Described is more
Carbohydrate moisturizer is selected from hyaluronic acid, chitin and its derivative, plant polyose, heparin any one or more of.
As a kind of preferred technical solution of the present invention, the small molecule polyol is glycerine, 2- methyl-1s, 3- the third two
The mixture of alcohol, dipropylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1~1.5：1.2
~2；The polysaccharide moisturizer is hyaluronic acid and the mass ratio of the mixture, wherein hyaluronic acid and trehalose of trehalose
It is 1：1~1.2.
As a kind of preferred technical solution of the present invention, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle molecule
It is the mixture of Sodium Hyaluronate, micromolecule hyaluronic acid sodium, wherein macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, small
The mass ratio of numerator sodium hyaluronate is 0.1：1：2.
As a kind of preferred technical solution of the present invention, the preparation method of the Europe gentian and grape seed extract,
Including at least following steps：
The Europe gentian and grape pip of freeze-drying are taken respectively, is crushed, and 60 mesh sieve are crossed, according to Europe gentian and grape pip matter
Amount is than being 35：1 uniformly mixing extracts 2~4h with the alcohol reflux that mass fraction is 75%, extracts 3~4 times, merge extracting solution,
Filtering, spray drying obtain the Europe gentian and grape seed extract.
As a kind of preferred technical solution of the present invention, the aurelia and rice extract are first by aurelia
It is digested with rice with amylase or protease, and adds in fermenting microbe and carry out the obtained substance that ferments.
As a kind of preferred technical solution of the present invention, auxiliary agent is further included in the efficient whitening and moisturizing facial mask liquid, institute
Mass fraction of the auxiliary agent stated in the efficient whitening and moisturizing facial mask liquid be less than 0.3%, the auxiliary agent be selected from thickener,
Chelating agent, solubilizer, pH adjusting agent any one or more of.
The second aspect of the invention provides the preparation method of the efficient MASQUE APAISANT HYDRATANT liquid, including at least following step
Suddenly：
Moisturizer is added in into the configuration pot for filling deionized water, 25~40Hz is stirred to being completely dissolved at 80 DEG C；Drop
Temperature adds in skin conditioning agent, 20~35Hz is stirred until homogeneous to 40 DEG C into configuration pot；Treat that temperature is down to room temperature, 200 mesh filter clothes
The efficient MASQUE APAISANT HYDRATANT liquid is obtained by filtration.
The third aspect of the invention provides a kind of facial mask, and the facial mask includes：As the mask matrix of carrier, with
And the efficient MASQUE APAISANT HYDRATANT liquid, the facial mask liquid is adsorbed in the mask matrix.
The above-mentioned of the application and other features, aspect and advantage is more readily understood with reference to following detailed description.
The main active of the present invention is all natural component extract, and primary raw material is all overseas imported product, not only
It is non-stimulated to skin, moreover it is possible to stimulate Skin Cell active, enhance the immunity protection function of skin itself, efficient repairing sheath skin screen
Barrier has both whitening, moisturizing, releives, multiple effects such as moisturizing, suitable for most skin quality.
Specific embodiment
The detailed description for preferred implementation method of the invention below of participating in the election of and including embodiment this hair can be more easily understood
Bright content.Unless otherwise defined, all technologies used herein and scientific terminology have common with fields of the present invention
The normally understood identical meaning of technical staff.When there is a conflict, the definition in this specification shall prevail.
As used herein term " by ... prepare " it is synonymous with "comprising".Term "comprising" used herein, " comprising ",
" having ", " containing " or its any other deformation, it is intended that cover including for non-exclusionism.For example, the combination comprising listed elements
Object, step, method, product or device are not necessarily limited to those elements, but can include not expressly listed other elements or
Such composition, step, method, product or the intrinsic element of device.
Conjunction " Consists of " excludes any element do not pointed out, step or component.If in claim, this
Phrase will make claim be closed, it be made not include the material in addition to the material of those descriptions, but relative normal
Except rule impurity.When being rather than immediately following after theme in the clause that phrase " Consists of " appears in claim main body,
It is only limited to the element described in the clause；Other elements are not excluded except the claim as a whole.
Equivalent, concentration or other values or parameter are excellent with range, preferred scope or a series of upper limit preferred values and lower limit
During the Range Representation that choosing value limits, this, which should be understood as, specifically discloses by any range limit or preferred value and any range
All ranges that any pairing of lower limit or preferred value is formed, regardless of whether the range separately discloses.For example, when open
During range " 1 to 5 ", described range should be interpreted as including range " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to
5 ", " 1 to 3 and 5 " etc..When numberical range is described herein, unless otherwise stated, otherwise range intention includes its end
Value and all integers and score in the range.
Singulative includes plural number and object is discussed, unless the context clearly dictates otherwise." optional " or it is " arbitrary
It is a kind of " refer to that the item described thereafter or event may or may not occur, and the description include situation that event occurs and
The situation that event does not occur.
Approximate term in specification and claims is used for modifying quantity, represents specific the present invention is not limited to this
Quantity further includes the modified part of the acceptable change without lead to related basic function close to the quantity.Phase
It answers, modifies a numerical value with " about ", " about " etc., mean that the present invention is not limited to the exact numericals.In some examples, it is approximate
Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, range limits can be with
It combines and/or exchanges, these ranges include all subranges contained therebetween if not stated otherwise.
In addition, indefinite article " one kind " before element of the present invention or component and "one" quantitative requirement to element or component
(i.e. occurrence number) unrestriction.Therefore "one" or " one kind " should be read as including one or at least one, and odd number
The element or component of form also include plural form, unless the apparent purport of the quantity refers to singulative.
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of efficient whitening and moisturizing facial mask liquid,
In parts by weight, including at least following components：100 parts of deionized water, 6~13 parts of moisturizer, 3~9 parts of skin conditioning agent；With weight
Measure part meter, the skin conditioning agent, including at least following components：3~7 parts of allantoin, Cer EOS~5 part, beta glucan
16~23 parts of 36~42 parts of 35~44 parts, Europe gentian and grape seed extract, aurelia and rice extract.
As a kind of preferred technical solution of the present invention, the efficient whitening and moisturizing facial mask liquid, in parts by weight, at least
Including following components：100 parts of deionized water, 8.6 parts of moisturizer, 5.5 parts of skin conditioning agent.
As a kind of preferred technical solution of the present invention, in parts by weight, the moisturizer, including at least with the following group
Point：3 parts of small molecule polyol, 0.06~0.13 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.
As a kind of preferred technical solution of the present invention, in parts by weight, the moisturizer, including at least with the following group
Point：3 parts of small molecule polyol, 0.11 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.
Small molecule polyol
Small molecule polyol refers to the alcohol containing two or more hydroxyls containing 2~9 carbon atoms.
As a kind of preferred technical solution of the present invention, the small molecule polyol is selected from 1,3-PD, glycerine, 1,
3- butanediols, 2- methyl-1,3-propanediols, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- hexylene glycols, dimerization the third three
Alcohol, dipropylene glycol, D-sorbite, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol any one or more of.
As a kind of preferred technical solution of the present invention, the small molecule polyol is selected from glycerine, 2- methyl-1s, 3- third
Glycol, dipropylene glycol any one or more of.
As a kind of preferred technical solution of the present invention, the small molecule polyol is glycerine, 2- methyl-1s, 3- the third two
The mixture of alcohol, dipropylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1~1.5：1.2
~2.
As a kind of preferred technical solution of the present invention, the small molecule polyol is glycerine, 2- methyl-1s, 3- the third two
The mixture of alcohol, dipropylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1.4：1.7.
Glycerine also known as glycerine, CAS：56-81-5, glycerine used in the present invention is Thailand's lotus flower board glycerine, purchased from upper
Hai Weigu Chemical Co., Ltd.s.
2- methyl-1s, 3-propanediol, CAS：2163-42-0, purchased from ALST CARE.
Dipropylene glycol, CAS：246-770-3, purchased from U.S. OXEA.
Polysaccharide moisturizer
Polysaccharide moisturizer refers to extracting to obtain the polysaccharose substance with performance of keeping humidity from animal or plant, tool
Have natural, nutrition, it is safe and non-stimulating, have no toxic side effect, with the characteristics such as the compatibility of skin is good.Therefore polysaccharide should as moisturizer
For in skin care item, meeting demand of the people to high-quality cosmetics, become the development trend of moisture-keeping cosmetics.Application at present
Polysaccharide moisturizer in cosmetics mainly has hyaluronic acid, chitin and its derivative, plant polyose extract, heparin
Deng.
As a kind of preferred technical solution of the present invention, the polysaccharide moisturizer be selected from hyaluronic acid, chitin and
Its derivative, plant polyose, heparin any one or more of.
The plant polyose is specifiable to have there is no other limitations：Tremella polysaccharides, trehalose, cactus polyoses, Huang
Astragalus polysaccharides, polysaccharides, sugarcane polysaccharide, Flos Lonicerae polysaccharide, Tea Polysaccharides etc..
As a kind of preferred technical solution of the present invention, the polysaccharide moisturizer is mixed for hyaluronic acid and trehalose
Object is closed, the wherein mass ratio of hyaluronic acid and trehalose is 1：1~1.2.
Hyaluronic acid
Hyaluronic acid (hyaluronic acid, HA) also known as Hyaluronic Acid, sodium hyaluronate, are by D- gluconic acids acid and N- acetyl
The branchiess glycosaminoglycan that aminoglucose disaccharide recurring unit is made up of β-(1 → 4) glycosidic bond and β-(1 → 3) glycosidic bond,
It is widely present in the cytoplasm of animal tissue and the folder film of certain bacteriums.Its relative molecular mass (Mr) is generally 1 × 105
~1 × 107D, the molar ratio of two kinds of monosaccharide is 1 in molecule：1.The common preparation methods of HA have animal tissue's extraction method and bacterium
Fermentation method.Commodity HA is generally its sodium salt, i.e. Sodium Hyaluronate (Sodium Hyaluronate, SH).
HA is widely present in the tissue of people and vertebrate, is one of several glutinous polysaccharide for forming extracellular matrix.By
Have that the macromolecules such as unique rheological properties, moisture retention, lubricity and thickening property stick the property of polysaccharide and it is natural in HA
Property, good biocompatibility and without anaphylaxis, therefore in cosmetic field, field of health care food, beauty treatment and medicine neck
Domain is extensively developed and applies.In addition to this, HA, which also has, eliminates the physiological activity such as free radical and adjusting cell function,
The generation of formation, blood vessel, the healing of wound, the maintenance of skin injury and prevention, tumour in the development of embryo, tissue and organ
Diffusion, control pain and inflammatory reaction etc. be respectively provided with very important physiological action.
One of important physiological function of HA is the water retention in skin histology.In higher concentration, length
Strand is just interweaved and reticulates, in addition oxygen key can be formed with hydrone containing a large amount of carboxyl and hydroxyl in molecule, so as to
Very strong water retention is played, HA can combine the water of 1000 times of its weight.Such a aqueous gelatinised matrix, makes skin
Smooth delicate and high resilience.The water retention property of HA and the concentration of HA and its Mr are proportionate, and to the permeability of water with
Its concentration and its Mr are negatively correlated.The aqueous solution painting of HA is touched in the surface of skin, it is possible to the ventilated membrane of one layer of moisturizing is formed,
Make skin lubrication glossy.Compared with other moisturizer, outstanding feature is that the relative humidity of external environment makees its moisturizing
Influence is smaller.Hygroscopic capacities of the HA in low relative humidity (33%) environment is highest, and in high relative humidity
(80%) hygroscopic capacity during environment is minimum instead.HA this unique moisturizing properties, positive adaptation is in different seasons, no
Under same environmental damp condition, such as time autumn and winter and summer, requirement of the skin to cosmetics moisture-keeping function.
Macromolecular hyaluronic acid (1800000~2200000D of molecular weight ranges) can skin surface formed one layer it is ventilative
Film moistens skin smooth, and can obstruct the intrusion of alien bacteria, dust, ultraviolet light, protects the skin from encroaching on；In point
Sub- hyaluronic acid (1000000~1800000D of molecular weight ranges) can be compacted skin, permanent moisturizing；Micromolecule hyaluronic acid
(400000~1000000D of molecular weight ranges) can penetrate into corium, have mild dilation capillary, increase blood circulation, improve
Intermediate supersession promotes skin-nourishing absorption, has the function of stronger wrinkle-chasing, can increase skin elasticity, delay skin aging.
It is to contain there are three types of the hyaluronic acid ingredient of different molecular weight as measurement standard, contain only single to weigh a good skin care item
The skin care item effect of molecular weight hyaluronic acid ingredient is limited, can not play the best skin-care effect of hyaluronic acid.
As a kind of preferred technical solution of the present invention, the hyaluronic acid is Sodium Hyaluronate, saturating selected from macromolecular
Bright matter acid sodium, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium any one or more of.
As a kind of preferred technical solution of the present invention, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle molecule
It is the mixture of Sodium Hyaluronate, micromolecule hyaluronic acid sodium, wherein macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, small
The mass ratio of numerator sodium hyaluronate is 0.1：1：2.
Macromolecular Sodium Hyaluronate of the present invention, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium are all purchased from
Japanese mound ratio.
Trehalose
Trehalose is also known as Radix Rhapontici seu Radix Echinopsis sugar, gill fungus sugar etc., is a kind of safe and reliable natural carbohydrate.Trehalose is by two grapes
The nonreducing sugar that glycan molecule is formed with 1,1- glycosidic bonds has 3 kinds of isomers i.e. trehalose (α, α), isotrehalose (β, β) and new
Trehalose (α, β), and there is non-specific protective effect to various bioactivators.Trehalose is many edible in nature
With being all widely present in animals and plants and microbial body, such as mushroom class edible in people's daily life, seaweeds, beans, shrimp, face
The trehalose for having content higher in packet, beer and yeast fermented food.
Trehalose has organism magical protective effect, it is in evils such as high temperature, high and cold, hyperosmosis and dry dehydrations
Unique protective film can be formed in cell surface under bad environmental condition, effectively protected protein matter molecule invariance inactivates, so as to
Sustain life the life process and biological characteristic of body.And such as other carbohydrates of sucrose, glucose in nature, do not have this
Function.This unique functional characteristic so that trehalose is in addition to that can be used as pharmaceutical grade protein, enzyme, vaccine and other biological system
Other than the excellent activity protective agent of product, cell activity, the important component of moisturizing class cosmetics are also to maintain, can more be used as prevents from eating
Product deterioration, the particular foodstuff dispensing for keeping food fresh flavor, promoting food quality.
Application of the trehalose on cosmetics is with excellent holding cell viability and large biological molecule activity based on it
Characteristic.Skin Cell, especially epidermal cell easily lose under the environment such as high temperature, high and cold, dry, intensive ultraviolet radiation
Moisture generation keratinization or even death come off and make skin damage.Trehalose can form one in cell surface in this case
The special protective film of layer, the mucus being precipitated from film not only moisten Skin Cell, also have and radiate external heat
Function, so as to keep the original nutrition of skin and moisture, avoid skin sunburn and melanin deposition, be effective against skin aging and show
As.Trehalose also has excellent hygroscopicity, can have both biological preservation with hyaluronic acid, glycine betaine synergy and intelligence is protected
Wet effect.Since trehalose can reduce the solidification point of water phase, with other components compatibilities using when can also play " stabilizer "
Effect.
It is former that the trehalose of the present invention is purchased from Japanese woods.
Amino acids moisturizer
The amino acids moisturizer refers to glycine betaine.Glycine betaine, also known as trimethylglycine, it is a kind of natural
, edible amino acid, be widely present in plant, such as beet, spinach, malt, mushroom and fruit, exist in very much
In animal body, such as the huge legendary turtle of lobster, octopus, squid and aquatic shellfish, shellfish or even the liver in human body
In also contain such substance.Glycine betaine is typically considered the intermediate product of life entity metabolism, it is also possible to as methyl
Supplier participates in synthetic methionine.Glycine betaine molecular formula C5H11NO2, structural formula isGlycine betaine has height
Bio-compatibility is highly soluble in water, dissolves in ethyl alcohol, very heat-resisting, acidproof and alkaline-resisting, and use scope is wide, it is easy to operate and
Safety and stability.Testing simultaneously proves that glycine betaine can be compatible with almost all of surfactant, forms the water phase of stable transparent
Solution and without consider its concentration used.
Carboxyl (COO-) in glycine betaine attracts the hydrogen atom in hydrone, and N atom pairs negative electrical charge generates attraction, with
The methyl of N atoms connection then generates repulsive force, and hydrone is distributed in beet base molecule under these interactions by stereo directional
Around.When a molecular water is combined by glycine betaine, it is also easy to be replaced by an other molecular water, that is to say, that hydrone exists
Nearby residence time is short compared with other moisturizer residence times for glycine betaine.Glycine betaine is that a kind of hydrone truly is taken
Band person, when physical condition changes, it is easy to hydrone being discharged into surrounding enviroment.Therefore, actually glycine betaine unlike
Hydrone is fixed other polyalcohol moisturizer (such as glycerine), it allows hydrone to be utilized completely by living cells, this work
Played the role of with effect to the moisture quantum balancing of Skin Cell good, the application for being also it in skin-protection product provides theory
It supports.
Modern research shows that glycine betaine mainly has the water holding capacity that can improve skin and hair rapidly, have only
Special moisturizing and protection cell film properties, while the solubility of active constituent in water can be increased, reduce surfactant or fruit
Acid is to the irritation of skin and the low-temperature stability of enhancing product etc..At present glycine betaine be widely used in skin-protection product,
It washes in the personal care products such as hair products and oral care product field.
The glycine betaine of the present invention is pharmaceutical grade glycine betaine, is purchased from same moral medicine company.
As a kind of preferred technical solution of the present invention, in parts by weight, the skin conditioning agent, including at least following
Component：41 parts of 5 parts of allantoin, Cer NP part, 40 parts of beta glucan, Europe gentian and grape seed extract, aurelia and
22 parts of rice extract.
Allantoin
Allantoin, molecular formula C4H6O3N4, CAS：97-59-6, alias Allantoin, Allantoin are
A kind of hydantoin derivatives.About 50,000 tons of the annual production capacity of allantoin, market are mainly medicine, change in the world at present
Cosmetic and agriculture three big fields.
Allantoin, sterling are a kind of nontoxic, tasteless and nonirritants, have promotion cell life without hypersensitive white crystal
It is long, accelerate the physiological functions such as wound healing, cutin-softening albumen, be the good consolidant and antiulcer agents of skin trauma.It can
As alleviating and treating xerodermia, scaling dermatopathy, skin ulcer, digestive tract ulcer and inflammation, to osteomyelitis, sugar
Urine disease, hepatic sclerosis, acne have good therapeutic effect.Since allantoin is a kind of amphoteric compound, can be formed with reference to many kinds of substance multiple
Salt, have be protected from light, sterilization and anticorrosion, analgesic, antioxidation, skin can be made to keep moisture content, moisten and soft, be cosmetology etc.
The additive of cosmetics is widely used in freckle cream, anti-acne toner, shampoo, perfumed soap, toothpaste, shaving lotion, conditioner, convergence
The additive of agent, anti-sweat deodorization lotion etc..The cosmetics of addition allantoin have protective tissue, it is hydrophilic, absorb water and prevent moisture
The effects that distributing；Add allantoin hair-cream, hair cream, shampoo, have protective effect to hair, can make hair not bifurcated, constantly
Hair；Skin, lip can be made soft for lipstick, the face cream of addition allantoin and high resilience, and has beautiful gloss.Allantoin promotes
Tissue growth, cell metabolism, cutin-softening layer albumen.
The allantoin of the present invention is purchased from dutch royal Royal DSM group.
Ceramide
Ceramide (Ceramide), also known as " molecule nail ", it can be close each cell as nail
" nail " is the very high maintenance ingredient of utilization rate in skin care item in recent years, in deep moisturizing face cream and antiallergic essence together
In can read its name.It is present in the outermost cytoplasm lipoid of human epidermal it is most important composition into
Point, this like cement and brick relationship, cell by ceramide can " viscous " together, just because of this, neural acyl
Amine has extraordinary permeability and skin-friendly.Ceramide is a kind of water-soluble lipid, it can active " catching " skin
In moisture, therefore, ceramide can quickly penetrate into skin epidermal cells and be combined with the moisture in cuticula, formed together
Water lock barrier makes skin inside as if being implanted into one layer " preservative film ", the state for making skin that water profit bullet be kept to slide for a long time.
The hyaluronic acid generated with skin itself is the same, and ceramide can also be reduced with the variation of age and environment,
And skin aging, drying, pruritus, skin problems a big chunk origin cause of formation such as allergic dermatitis is precisely due to ceramide
Lack.As one it is irreversible the fact, the secretory volume of ceramide can be reduced due to the increase at age eventually, cause cuticula
Water and nutrient can not be retained, gap, which occurs, in cytoplasm becomes loose, and skin is made to become to dry and is more susceptible to the shadow of internal and external environment
It rings and induces sensitive.But we still can make up the nutrient of skin deficiencies by using the skin care products containing ceramide,
Increase the bonding force of horn cell interstitial, remold " water lock net ", moisture evaporation and loss are prevented to greatest extent, so as to reach skin
The good effect of active moisturizing.
In view of environmental protection considers, the ceramide nowadays added in skin care item is changed to by original animal brain's extraction
Plant extract, such as rice, corn, wheat, konjaku, pineapple plant.
As a kind of preferred technical solution of the present invention, the ceramide is dihydrophytoceramide, purchased from U.S. Asia
Assorted orchid.
Beta glucan
The polysaccharide that the active structure of beta glucan is made of glucose unit, it can activated macrophage, it is thermophilic in
Property white blood cell etc., so as to improve leukin, the basic element of cell division and the content of distinct antibodies, stimulate the siberian crabapple of body comprehensively
System.Many experiments show that beta glucan can promote the generation of internal IgM antibody, to improve the immunocompetence of body fluid.In addition, β-
Glucan, which still has, removes free radical, radioresistance, dissolving cholesterol, prevents hyperlipidemia and resists filterable virus, fungi, bacterium
Deng caused by the effects that infection, therefore it is widely used in the industries such as medicine, food, cosmetics.Beta glucan can also stimulate Skin Cell
Activity enhances the immunity protection function of skin itself, and efficient repairing sheath skin reduces wrinkle of skin and generates, delay skin aging.Closely
Year is the study found that β -1,3- glucan can control cell point as the inhereditary material to play the role of a nucleus in vital movement
It splits and breaks up, adjust cell growth, have solely in treatment tumour, hepatitis, angiocarpy, diabetes and reducing blood lipid, anti-aging etc.
Special bioactivity.Countries in the world at present, especially in states such as Japan, the U.S., Russia, β -1,3- glucans are extensive
Applied to industries such as health care of food, beauty and skin cares.
The beta glucan of the present invention is the beta-1,3-dextran (trade name of cosmetics-stage：), CAS：1439905-
58-4。
Europe gentian and grape seed extract
Europe rough gentian is Chinese medicine name, is the drying root and rhizome of rough gentian plant Europe rough gentian Gentiana lutea L.；There is research
Show that Europe rough gentian root extract can inhibit arachidonic acid during inflammatory reaction to prostaglandin E2 and leukotriene C
Cascade reaction.Arachidonic acid is cell membrane to be released in allergic reaction or by environmental stimuli when, arachidonic acid metabolic
Inflammation cells, the expansion of blood vessel are caused to prostaglandin, the permeability raising of vascular wall additionally causes pain to show with what is generated heat
As Europe gentian can inhibit this inflammatory reaction process.In addition to this, Europe gentian can also effectively inhibit the generation of erythema and ultraviolet
The inflammation and pigmentation that line induces have extremely outstanding antiphlogistic effects, it is leniently calm, releive skin the effect of.
Grape seed extract is that isolated a kind of polyphenols is extracted from grape pip, mainly by procyanidine,
The polyphenols such as catechin, epicatechin, gallic acid, epicatechin, gallate form.Grape seed extract is so far
One of most efficient antioxidant of plant origin that the present finds, experiments have shown that, antioxidant effect is vitamin C and vitamin E
30~50 times.Grape seed extract is small to skin irritation simultaneously, and antiallergy, anti-irritant are good.
As a kind of preferred technical solution of the present invention, the preparation method of the Europe gentian and grape seed extract,
Including at least following steps：
The Europe gentian and grape pip of freeze-drying are taken respectively, is crushed, and 60 mesh sieve are crossed, according to Europe gentian and grape pip matter
Amount is than being 35：1 uniformly mixing extracts 2~4h with the alcohol reflux that mass fraction is 75%, extracts 3~4 times, merge extracting solution,
Filtering, spray drying obtain the Europe gentian and grape seed extract.
Aurelia and rice extract
Aurelia, Aurelia aurita (Linnaeus, 1758), be Yang Xu jellyfishes section aurelia subordinate one kind
Jellyfish.The medusoma of aurelia species cannot singly differentiate at all from appearance, it is necessary to be analyzed with gene to make.Hai Yueshui
Female medusoma is transparent, generally a diameter of 25~49 centimetres, there is 4 apparent horse-hof shape gonad.They can use tentacle
Prey is captured, such as medusoma, planktonic organism and mollusk.But the activity of tentacle is limited, they also can only drift with the tide.
Aurelia is distributed in 70 ° of north latitude to the marine site of 40 ° of south latitude, the Atlantic Ocean, the Pacific Ocean, the Indian Ocean.In general, they live
In offshore, them can be seen in river mouth and harbour.They inhabit the seawater in 6~31 DEG C of water temperature, are most suitable for 9~19 DEG C of water
Temperature.Aurelia likes the temperate zone ocean of waterflow stabilization.They generally occur in the marine site that salinity is less than 3~23ppt.
The main component of fresh aurelia is made of moisture, ash content, protein, carbohydrate, fat etc..It is existing
Research shows that rich in inorganic elements in aurelia, and trace element is complete, and the harmful metal elements content such as arsenic, mercury is very low,
This is in the two beneficial and positive effect of aspect of food nutrition and medicines and health protection.The total lipid content of aurelia accounts for it
The content of the 0.0031%~0.036% of fresh weight, wherein phosphatide accounts for the 1.3%~1.7% of total lipid, and phosphate ester accounts for total phospholipids
21.7%, lecithin accounts for 44.5%, and phosphatidyl-ethanolamine accounts for 18.6%, and cuorin accounts for 5.6%, and lipositol accounts for 2.6%, haemolysis
Phosphatidyl choline accounts for 5.0%.Unrighted acid is total lipid, polar lipid and neurostearic main component, is accounted for respectively
76.7%th, 83.0% and 67.6%.Saturated fatty acid accounts about the 43%~45% of total fatty acids in fresh aurelia, list
Unrighted acid accounts for 16%~23%, and polyunsaturated fatty acid accounts for 24%~32%.Saturated fatty acid is mainly palmitic acid
(C16：0) and stearic acid (C18：0).Main polyunsaturated fatty acid PUFA includes some special long-chain PUFA in aurelia,
6,9,12,15,18,21~24 carbon acids (THA, 24：6n-3) and rare 6,9,12,15,18~24 carbon 5 alkene acids
(24：5n-6) and eicosatetraenoic acid (AA, 3%~9%) etc..Protein content in aurelia contains compared with other compositions
Amount is higher, therefore is also development prospect The cream of the crop, clinical medicine, health products, functional food, cosmetics etc. can be used as to add
To develop and use.Collagen can be extracted for cosmetics from aurelia by having some researchs at present, in addition also had and learned
Person extracts a kind of polypeptide containing 40 residues with bacteriostatic activity from aurelia, it to gram-positive bacteria and
Gram-negative bacteria has inhibiting effect.
Rice (Rice) is paddy manufactured finished product after the processes such as cleaning, husking, husk rice, finished product arrangement.The embryo of paddy
Rice nutrition and the needed nutrient of more than 90% human body with containing nearly 64% in aleurone.The traditional Chinese medical science thinks that rice is sweet in flavor
It is mild-natured, there are tonifying middle-Jiao and Qi, strengthening spleen and nourishing stomach, the strong will of strengthening the essence and the five internal organs, promoting blood circulation, hearing-improing and eyesight improving and the five internal organs, promoting blood circulation, stop
Be tired of, quench the thirst, antidiarrheal the effect of, sing the praises of as " first of five cereals ", be the staple food crop of China, account for about plant cultivation grain area
A quarter.There is half population in the world using rice as staple food.
Rice enters spleen, stomach, lung channel, has the function of tonifying middle-Jiao and Qi, nourishing Yin and moistening lung, strengthening the spleen and stomach, relieving thirst and restlessness.Rice
Nutrition very abundant is one of main food of Chinese people.By taking polished rice as an example, in every hectogram polished rice, containing protein (albumen
Matter food) 6.7 grams, 0.9 gram of fat, 77.6 grams of carbohydrate, 0.3 gram of crude fibre, 7 milligrams of calcium (calcium food), 136 milli of phosphorus
Gram, 2.3 milligrams of iron (iron food), 0.16 milligram of vitamin B1,0.05 milligram of vitamin (vitamin food) B2,1 milli of niacin
Gram and 125 milligrams of methionine, 394 milligrams of valine, 610 milligrams of leucine, 251 milligrams of isoleucine, the milli of threonine 280
Gram, 94 milligrams of phenylalanine-3,4-quinone, 122 milligrams of tryptophan, a variety of nutriments such as 255 milligrams of lysine.Carbon hydrate in rice
If owner's starch, contained protein is mainly oryzenin, secondly oryzenin and globulin, the biology of protein
The composition of valency and amino acid is all higher than cereal crops such as wheat, barley, millet, corns, and digestibility 66.8%~
83.1% and grain protein in higher one kind.Contained linoleic acid content is higher in fat in rice, typically constitutes from complete
The 34% of portion's fat is 2~5 times more than rapeseed oil and tea oil difference.
Rice of the present invention is Jin Lilian Thailand perfume (or spice) brown rice, purchased from Guangzhou Tai Shi trade Co., Ltds.
As a kind of preferred technical solution of the present invention, the aurelia and rice extract are first by aurelia
It is digested with rice with amylase or protease, and adds in fermenting microbe and carry out the obtained substance that ferments.
As a kind of preferred technical solution of the present invention, the preparation method of the aurelia and rice extract, until
Include the following steps less：
A. rice is crushed with pulverizer, addition deionized water, the mass ratio of deionized water and rice is 1：4, it is mixed
It closes uniformly, then by its boiling 60min, then adds in deionized water thereto, the mass ratio of the deionized water and rice is
2：1, alpha-amylase, beta amylase are added in thereto, and the mass ratio of alpha-amylase, beta amylase and rice is 0.002：0.002：
1, it is digested at 55 DEG C 10 hours, then gradually improves after temperature carries out the boiling of 5min, be cooled to 50 DEG C and obtain rice enzymolysis
Liquid；
B. the acetic acid that fresh aurelia mass fraction is 3% is taken to handle, is washed, to smash to obtain aurelia tissue to pieces molten
Liquid adds in rice enzymolysis liquid thereto, and stirring is uniformly mixed it, and it is 6~8.5 to adjust pH, fresh aurelia and rice
Mass ratio is 20：3, under conditions of 30~60 DEG C, 800~1200 enzyme-activity units are added in every gram of fresh aurelia quality
For Standard entertion trypsase, 8~12 hours are kept the temperature, are then warming up to 140 DEG C, heat preservation 8s carries out enzyme deactivation, obtains sea
Month jellyfish and rice enzymolysis liquid；
C. the without fermented liquid that Solute mass fraction is 6% sucrose, Hai Yueshui are added in aurelia and rice enzymolysis liquid
Female and rice enzymolysis liquid and the volume ratio for the without fermented liquid that Solute mass fraction is 6% sucrose are 1000：1, then use
25MPa pressure carries out homogenization to mixed liquor, adds in bent rice trichoderma strain (Aspergillus oryzae), and the bent rice is mould
The mass ratio of bacterial strain and rice is 1：4, after being then sealed by fermentation 20~40 hours under the conditions of 20~25 DEG C, squeeze and filter will
Filtered fluid collects efflux and obtains aurelia and rice extract by activated-charcoal column.
The alpha-amylase is purchased from Jiangsu Cai Wei bio tech ltd, CAS：9000-90-2, model food
Grade, 1,000,000 u/g of enzyme activity.
The beta amylase is risen purchased from Zhengzhou up to food additives Co., Ltd, CAS：9000-91-3, model food
Grade, 700,000 u/g of enzyme activity.
The trypsase is purchased from Pangbo Bioengineering Co Ltd, Nanning, model PB20, enzyme activity 2500USP u/
mg。
The bent rice trichoderma strain (Aspergillus oryzae) is purchased from Nanjing Lin Nuo Trade Co., Ltd.s, model promise
Dimension letter alpha-amylase fungi BrewQ types.
The present invention is found surprisingly that during the experiment by the way that Europe gentian and grape pip be uniformly mixed to get
Extract has better whitening, effect of releiving, but the stability of Europe rough gentian and grape seed extract is poor, it is higher and compared with
Easily occur precipitating at low temperature and phenomena such as whitening, performance of releiving are decreased obviously.But it is added in the facial mask of the present invention
After aurelia and rice extract, the stability of Europe rough gentian and grape seed extract is remarkably reinforced, so as to further enhance
The long-acting whitening of the facial mask, effect of releiving, and aurelia and rice extraction have moisturizing, moisturizing, repair skin in itself
Skin barrier and other effects further expands the accommodation of the facial mask of the present invention.
The main active of the present invention is all natural component extract, and primary raw material is all overseas imported product, not only
It is non-stimulated to skin, moreover it is possible to stimulate Skin Cell active, enhance the immunity protection function of skin itself, efficient repairing sheath skin screen
Barrier has both whitening, moisturizing, releives, multiple effects such as moisturizing, suitable for most skin quality.
As a kind of preferred technical solution of the present invention, auxiliary agent is further included in the efficient whitening and moisturizing facial mask liquid, institute
Mass fraction of the auxiliary agent stated in the efficient whitening and moisturizing facial mask liquid be less than 0.3%, the auxiliary agent be selected from thickener,
Chelating agent, solubilizer, pH adjusting agent any one or more of.
As a kind of preferred technical solution of the present invention, the thickener is selected from carbomer, xanthans, natto gum, fiber
Element, Sodium Polyacrylate, polysorbate any one or more of.
As a kind of preferred technical solution of the present invention, the chelating agent is selected from disodium ethylene diamine tetraacetate, decoyl hydroxyl
Oxime acid, sodium phytate, hydroxy phenylpropionyl amine benzoic acid any one or more of.
As a kind of preferred technical solution of the present invention, the pH adjusting agent is selected from edetic acid(EDTA), natrium adetate, lemon
Acid, sodium citrate, sodium hydroxide, potassium hydroxide, triethanolamine any one or more of.
The second aspect of the invention provides the preparation method of the facial mask liquid, including at least following steps：
Moisturizer is added in into the configuration pot for filling deionized water, 25~40Hz is stirred to being completely dissolved at 80 DEG C；Drop
Temperature adds in skin conditioning agent, 20~35Hz is stirred until homogeneous to 40 DEG C into configuration pot；Treat that temperature is down to room temperature, 200 mesh filter clothes
The facial mask liquid is obtained by filtration.
The third aspect of the invention provides a kind of facial mask, and the facial mask includes：As the mask matrix of carrier, with
And the facial mask liquid, the facial mask liquid is adsorbed in the mask matrix.
The mask matrix is limited there is no other, it is specifiable have non-woven fabrics, pure cotton cloth/fruit-vegetable fibre, silica gel,
Crystal gel, plant fiber, biological fiber, silk, charcoal etc. made of agar etc..
The present invention is specifically described below by embodiment.It is necessarily pointed out that following embodiment is only used
In the invention will be further described, it is impossible to be interpreted as limiting the scope of the invention, professional and technical personnel in the field
Some the nonessential modifications and adaptations made according to the content of the invention described above, still fall within protection scope of the present invention.
It is if raw materials used to be all commercially available in addition, without other explanations.
Embodiment 1：
Embodiment 1 provides a kind of efficient whitening and moisturizing facial mask liquid, in parts by weight, including at least following components：Go from
Sub- 100 parts of water, 6 parts of moisturizer, 3 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, including at least with the following group
Point：36 parts of 3 parts of allantoin, Cer EOS part, 35 parts of beta glucan, Europe gentian and grape seed extract, aurelia and big
16 parts of rice extracts；In parts by weight, the moisturizer, including at least following components：3 parts of small molecule polyol, polysaccharide
0.06 part of moisturizer, 1 part of amino acids moisturizer；The small molecule polyol is glycerine, 2- methyl-1,3-propanediols, two
The mixture of propylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1：1.2；Described is more
Carbohydrate moisturizer is hyaluronic acid and the mixture of trehalose, and the wherein mass ratio of hyaluronic acid and trehalose is 1：1；Described
Hyaluronic acid is macromolecular Sodium Hyaluronate, the mixture of middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium, wherein big point
Sub- Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mass ratio be 0.1：1：2.
The Europe gentian and the preparation method of grape seed extract, including at least following steps：
The Europe gentian and grape pip of freeze-drying are taken respectively, is crushed, and 60 mesh sieve are crossed, according to Europe gentian and grape pip matter
Amount is than being 35：1 uniformly mixing extracts 3.5h with the alcohol reflux that mass fraction is 75%, extracts 4 times, merge extracting solution, mistake
Filter, spray drying obtain the Europe gentian and grape seed extract.
The aurelia and the preparation method of rice extract, including at least following steps：
A. rice is crushed with pulverizer, addition deionized water, the mass ratio of deionized water and rice is 1：4, it is mixed
It closes uniformly, then by its boiling 60min, then adds in deionized water thereto, the mass ratio of the deionized water and rice is
2：1, alpha-amylase, beta amylase are added in thereto, and the mass ratio of alpha-amylase, beta amylase and rice is 0.002：0.002：
1, it is digested at 55 DEG C 10 hours, then gradually improves after temperature carries out the boiling of 5min, be cooled to 50 DEG C and obtain rice enzymolysis
Liquid；
B. the acetic acid that fresh aurelia mass fraction is 3% is taken to handle, is washed, to smash to obtain aurelia tissue to pieces molten
Liquid adds in rice enzymolysis liquid thereto, and stirring is uniformly mixed it, and it is 6~8.5 to adjust pH, fresh aurelia and rice
Mass ratio is 20：3, under conditions of 45 DEG C, 1000 enzyme-activity units are added in using every gram of fresh aurelia quality and are added as standard
Enter trypsase, keep the temperature 10 hours, be then warming up to 140 DEG C, heat preservation 8s carries out enzyme deactivation, obtains aurelia and rice
Enzymolysis liquid；
C. the without fermented liquid that Solute mass fraction is 6% sucrose, Hai Yueshui are added in aurelia and rice enzymolysis liquid
Female and rice enzymolysis liquid and the volume ratio for the without fermented liquid that Solute mass fraction is 6% sucrose are 1000：1, then use
25MPa pressure carries out homogenization to mixed liquor, adds in bent rice trichoderma strain (Aspergillus oryzae), and the bent rice is mould
The mass ratio of bacterial strain and rice is 1：4, after being then sealed by fermentation 25 hours under the conditions of 20~25 DEG C, squeeze and filter will filter
Liquid collects efflux and obtains aurelia and rice extract by activated-charcoal column.
The preparation method of the efficient MASQUE APAISANT HYDRATANT liquid, including at least following steps：
Moisturizer is added in into the configuration pot for filling deionized water, 35Hz is stirred to being completely dissolved at 80 DEG C；It is cooled to
40 DEG C, skin conditioning agent is added in into configuration pot, 25Hz is stirred until homogeneous；Treat that temperature is down to room temperature, 200 mesh filter-cloth filterings obtain
The efficient MASQUE APAISANT HYDRATANT liquid.
Embodiment 2：
Embodiment 2 provides a kind of efficient whitening and moisturizing facial mask liquid, in parts by weight, including at least following components：Go from
Sub- 100 parts of water, 13 parts of moisturizer, 9 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, including at least with the following group
Point：42 parts of 7 parts of allantoin, 5 parts of ceramide, 44 parts of beta glucan, Europe gentian and grape seed extract, aurelia and big
23 parts of rice extracts；In parts by weight, the moisturizer, including at least following components：3 parts of small molecule polyol, polysaccharide
0.13 part of moisturizer, 1 part of amino acids moisturizer；The small molecule polyol is glycerine, 2- methyl-1,3-propanediols, two
The mixture of propylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1.5：2；Described is more
Carbohydrate moisturizer is hyaluronic acid and the mixture of trehalose, and the wherein mass ratio of hyaluronic acid and trehalose is 1：1.2.It is described
Hyaluronic acid for macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mixture, wherein greatly
Numerator sodium hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mass ratio be 0.1：1：2.
The preparation method is the same as that of Example 1 for the Europe gentian and grape seed extract.
The preparation method is the same as that of Example 1 for the aurelia and rice extract.
The preparation method is the same as that of Example 1 for the efficient MASQUE APAISANT HYDRATANT liquid.
Embodiment 3：
Embodiment 3 provides the efficient whitening and moisturizing facial mask liquid, in parts by weight, including at least following components：It goes
100 parts of ionized water, 8.6 parts of moisturizer, 5.5 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, includes at least
Following components：5 parts of allantoin, Cer NP part, 40 parts of beta glucan, Europe gentian and 41 parts of grape seed extract, Hai Yueshui
Female and 22 parts of rice extract.In parts by weight, the moisturizer, including at least following components：3 parts of small molecule polyol,
0.08 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.The small molecule polyol is glycerine, 2- methyl-1s, 3- the third two
The mixture of alcohol, dipropylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1.4：1.7.Institute
The polysaccharide moisturizer stated is hyaluronic acid and the mixture of trehalose, and the wherein mass ratio of hyaluronic acid and trehalose is 1：
1.05.The hyaluronic acid is the mixing of macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium
Object, wherein macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mass ratio be 0.1：1：2.
The preparation method is the same as that of Example 1 for the Europe gentian and grape seed extract.
The preparation method is the same as that of Example 1 for the aurelia and rice extract.
The preparation method is the same as that of Example 1 for the efficient MASQUE APAISANT HYDRATANT liquid.
Embodiment 4：
Embodiment 4 provides the efficient whitening and moisturizing facial mask liquid, in parts by weight, including at least following components：It goes
100 parts of ionized water, 8.6 parts of moisturizer, 5.5 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, includes at least
Following components：6 parts of allantoin, Cer NP part, 42 parts of beta glucan, Europe gentian and 39 parts of grape seed extract, Hai Yueshui
Female and 18 parts of rice extract.In parts by weight, the moisturizer, including at least following components：3 parts of small molecule polyol,
0.11 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.The small molecule polyol is glycerine, 2- methyl-1s, 3- the third two
The mixture of alcohol, dipropylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1.4：1.7.Institute
The polysaccharide moisturizer stated is hyaluronic acid and the mixture of trehalose, and the wherein mass ratio of hyaluronic acid and trehalose is 1：
1.05.The hyaluronic acid is the mixing of macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium
Object, wherein macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mass ratio be 0.1：1：2.
The preparation method is the same as that of Example 1 for the Europe gentian and grape seed extract.
The preparation method is the same as that of Example 1 for the aurelia and rice extract.
The preparation method is the same as that of Example 1 for the efficient MASQUE APAISANT HYDRATANT liquid.
Embodiment 5：
Embodiment 5 provides the efficient whitening and moisturizing facial mask liquid, in parts by weight, including at least following components：It goes
100 parts of ionized water, 8.6 parts of moisturizer, 5.5 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, includes at least
Following components：5 parts of allantoin, Cer NP part, 40 parts of beta glucan, Europe gentian and 41 parts of grape seed extract, Hai Yueshui
Female and 22 parts of rice extract.In parts by weight, the moisturizer, including at least following components：3 parts of small molecule polyol,
0.11 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.The small molecule polyol is glycerine, 2- methyl-1s, 3- the third two
The mixture of alcohol, dipropylene glycol, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio be 1：1.4：1.7.Institute
The polysaccharide moisturizer stated is hyaluronic acid and the mixture of trehalose, and the wherein mass ratio of hyaluronic acid and trehalose is 1：
1.05.The hyaluronic acid is the mixing of macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium
Object, wherein macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mass ratio be 0.1：1：2.
The preparation method is the same as that of Example 1 for the Europe gentian and grape seed extract.
The preparation method is the same as that of Example 1 for the aurelia and rice extract.
The preparation method is the same as that of Example 1 for the efficient MASQUE APAISANT HYDRATANT liquid.
Embodiment 6：
The specific embodiment of embodiment 6 is with embodiment 5, and the difference lies in the efficient whitening and moisturizing facial mask is also
Including auxiliary agent, mass fraction of the auxiliary agent in the efficient whitening and moisturizing facial mask liquid is 0.24%, the auxiliary agent
For chelating agent EDETATE SODIUM, thickener Carbomer981, pH adjusting agent triethanolamine, EDETATE SODIUM, carbomer and triethanolamine matter
Amount is than being 1：2：5.
EDETATE SODIUM, CAS：6381-92-6, purchased from same moral medicine company.
Carbomer981, purchased from Lubrizol Corp. of the U.S..
Triethanolamine, CAS：102-71-6, purchased from Shanghai Mike's woods biochemical technology Co., Ltd.
Comparative example 1：
The specific embodiment of comparative example 1 is with embodiment 6, and the difference lies in the efficient MASQUE APAISANT HYDRATANT liquid not
Including Europe gentian and grape seed extract.
Comparative example 2：
For the specific embodiment of comparative example 2 with embodiment 6, the difference lies in carry the Europe rough gentian and grape pip
Object is taken to be changed to Europe Radix Gentianae extract.
Comparative example 3：
For the specific embodiment of comparative example 3 with embodiment 6, the difference lies in carry the Europe rough gentian and grape pip
Object is taken to be changed to grape seed extract.
Comparative example 4：
The specific embodiment of comparative example 4 is with embodiment 6, and the difference lies in the efficient MASQUE APAISANT HYDRATANT liquid not
Including aurelia and rice extract.
Comparative example 5：
For the specific embodiment of comparative example 5 with embodiment 6, the difference lies in carry the aurelia and rice
Object is taken to be changed to aurelia extract.
Comparative example 6：
For the specific embodiment of comparative example 6 with embodiment 6, the difference lies in carry the aurelia and rice
Object is taken to be changed to rice extract.
Comparative example 7：
The specific embodiment of comparative example 7 is with embodiment 6, and the difference lies in during the Sodium Hyaluronate does not include
Numerator sodium hyaluronate
Performance evaluation：
Efficient whitening and moisturizing facial mask liquid is obtained using Examples 1 to 6 and comparative example 1~7 to produce facial mask.Facial mask can be with
Including the mask matrix as facial mask liquid carrier, these facial mask mechanism are immersed in the efficient whitening and moisturizing facial mask liquid,
Fully wetting post package.In the experimentation of the present invention, non-woven fabrics is selected as mask matrix.The user of the facial mask
Method is：The non-textile mulch of facial mask liquid will be impregnated on the face, then 20~25min removes facial mask.
1. stabilizing effect is evaluated
A. facial mask liquid is placed in (45 ± 2) DEG C electro-heating standing-temperature cultivator 30 days, its stability is observed after restoring room temperature；
B. facial mask is placed in the refrigerator of (- 5 ± 2) DEG C 30 days, its stability is observed after restoring room temperature.
Observation item：Facial mask liquid the transparency, precipitation, smell variation etc., if facial mask liquid still maintain it is transparent, without precipitation, nothing
Smell changes, then is recorded as stablizing, otherwise be recorded as unstable.Test result is as shown in table 1.
2. moisture retention effect assessment
Test philosophy：The biomaterial of cuticula, epidermis etc. is imitated using adhesive tape, facial mask is covered on adhesive tape, then
20min removes facial mask, simulates practical application situation.Sample is placed under conditions of constant humidity after a certain period of time, is weighed and is put front and rear matter
Amount is poor, and the loss of sample size is obtained, can calculate the effect of moisturizing ingredient moisturizing.Moisturizing rate calculation formula：Moisturizing rate=
(M2–M0)/(M1–M0) × 100%
In formula：M0：Empty belt quality/g；M1：Use belt quality quality/g after facial mask；M2：It is placed in drier several small
When after belt quality/g；Testing it, moisturizing rate, test result are as shown in table 1 in 0h and 8h when relative humidity is 60%.
3. whitening effect assessment
Tyrosinase activity is detected using biochemical-Enzymic method, the inhibiting rate of tyrosinase activity is commented by determination sample
The whitening effect of valency sample.
Table 1
As can be seen from Table 1, the efficient whitening mask stability in the present invention is good, has long-acting moisture retention, also with non-
Often good whitening effect.
4. skin test
The women that 600 ages are selected at random at 20~60 years old is tested, and is randomly divided into 6 groups, is 25 in room temperature
DEG C experimentation in, take several nonwoven cloth areas be 3cm2, stick the efficient whitening and moisturizing face of the embodiment of the present invention 1~6
In the left and right skin of face 20min in left hand the back of the hand portion and nose both sides, the present invention is sticked with skinanalysis apparatus test respectively for film liquid
Facial mask liquid and without using the melanin deposition situation of skin of face before and after facial mask liquid and skin water content, carried out again after 12h
Secondary test, comparative experimental data.
As a result, it has been found that：All testers occur without allergy and stimulation situation.Pass through the test result of skinanalysis apparatus
It can be found that applied the present invention facial mask liquid after, 98% people deposited position dermal melanin aggregate site melanin deposition
Situation is substantially reduced, and 100% people's skin water content significantly increases；After 12h, still there is the 90% deposited position of people institute
Dermal melanin aggregate site melanin deposition situation it is substantially reduced, 92% people's skin water content significantly increases.The present invention
Efficient whitening and moisturizing facial mask there is long-acting moisturizing, whitening effect, not sensitization non-stimulated to skin, suitable for each age
The crowd in stage.
Aforementioned example is merely illustrative, for explaining some features of the method for the invention.Appended right will
It asks and is intended to the range as wide as possible that requirement is contemplated that, and embodiments as presented herein is only according to all possible implementation
The explanation of the embodiment of the selection of the combination of example.Therefore, the purpose of applicant is that appended claim is not illustrated this hair
The exemplary selectional restriction of bright feature.Some numberical ranges used also include sub- model in the claims
It encloses, the variation in these ranges should be also construed in the conceived case by appended claim covering.
Claims (10)
1. a kind of efficient whitening and moisturizing facial mask liquid, which is characterized in that in parts by weight, including at least following components：Deionized water
100 parts, 6~13 parts of moisturizer, 3~9 parts of skin conditioning agent；In parts by weight, the skin conditioning agent, including at least following
Component：3~7 parts of allantoin, Cer EOS~5 part, 35~44 parts of beta glucan, Europe gentian and grape seed extract 36~
16~23 parts of 42 parts, aurelia and rice extract.
2. efficiently MASQUE APAISANT HYDRATANT liquid as described in claim 1, which is characterized in that in parts by weight, the moisturizer, at least
Including following components：3 parts of small molecule polyol, 0.06~0.13 part of polysaccharide moisturizer, 1 part of amino acids moisturizer.
3. efficiently MASQUE APAISANT HYDRATANT liquid as claimed in claim 2, which is characterized in that the small molecule polyol is selected from 1,3- third
Glycol, glycerine, 1,3 butylene glycol, 2- methyl-1,3-propanediols, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- oneself two
Any one of alcohol, two polyglycerols, dipropylene glycol, D-sorbite, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol are more
Kind；The polysaccharide moisturizer be selected from hyaluronic acid, chitin and its derivative, plant polyose, any one of heparin or
It is a variety of.
4. efficiently MASQUE APAISANT HYDRATANT liquid as claimed in claim 2, which is characterized in that the small molecule polyol is glycerine, 2-
Methyl-1,3-propanediol, dipropylene glycol mixture, wherein glycerine, 2- methyl-1s, 3-propanediol, dipropylene glycol mass ratio
It is 1：1~1.5：1.2~2；Mixture of the polysaccharide moisturizer for hyaluronic acid and trehalose, wherein hyaluronic acid and
The mass ratio of trehalose is 1：1~1.2.
5. efficiently MASQUE APAISANT HYDRATANT liquid as claimed in claim 4, which is characterized in that the hyaluronic acid is macromolecular hyalomitome
Sour sodium, middle numerator sodium hyaluronate, micromolecule hyaluronic acid sodium mixture, wherein macromolecular Sodium Hyaluronate, middle molecule be saturating
Bright matter acid sodium, micromolecule hyaluronic acid sodium mass ratio be 0.1：1：2.
6. efficiently MASQUE APAISANT HYDRATANT liquid as described in claim 1, which is characterized in that the Europe gentian and grape seed extract
Preparation method, including at least following steps：
The Europe gentian and grape pip of freeze-drying are taken respectively, is crushed, and 60 mesh sieve are crossed, according to Europe gentian and grape pip mass ratio
It is 35：1 uniformly mixing extracts 2~4h with the alcohol reflux that mass fraction is 75%, extracts 3~4 times, merge extracting solution, mistake
Filter, spray drying obtain the Europe gentian and grape seed extract.
7. efficiently MASQUE APAISANT HYDRATANT liquid as described in claim 1, which is characterized in that the aurelia and rice extract be
First aurelia and rice with amylase or protease are digested, and adds in fermenting microbe and carries out the obtained object that ferments
Matter.
8. efficiently MASQUE APAISANT HYDRATANT liquid as described in claim 1, which is characterized in that in the efficient whitening and moisturizing facial mask liquid also
Including auxiliary agent, mass fraction of the auxiliary agent in the efficient whitening and moisturizing facial mask liquid is less than 0.3%, the auxiliary agent
Selected from thickener, chelating agent, solubilizer, pH adjusting agent any one or more of.
9. such as the preparation method of the efficient MASQUE APAISANT HYDRATANT liquid of claim 1~8 any one of them, which is characterized in that include at least
Following steps：
Moisturizer is added in into the configuration pot for filling deionized water, 25~40Hz is stirred to being completely dissolved at 80 DEG C；It is cooled to
40 DEG C, skin conditioning agent is added in into configuration pot, 20~35Hz is stirred until homogeneous；Treat that temperature is down to room temperature, 200 mesh filter-cloth filterings
Obtain the efficient MASQUE APAISANT HYDRATANT liquid.
10. a kind of facial mask, which is characterized in that the facial mask includes：As the mask matrix of carrier and such as claim 1
~8 any one of them efficient MASQUE APAISANT HYDRATANT liquid is adsorbed with the facial mask liquid in the mask matrix.
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| CN109770275A (en) * | 2019-02-22 | 2019-05-21 | 水母娘娘海洋生物科技有限公司 | A kind of aurelia water and its preparation method and application |
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| CN110368330A (en) * | 2019-08-31 | 2019-10-25 | 苏格格 | A kind of moisturizing moisturizing cream |
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| CN110575405A (en) * | 2019-10-31 | 2019-12-17 | 广州市华晟健康产业有限公司 | method for preparing whitening cosmetic |
| CN110711168A (en) * | 2019-11-29 | 2020-01-21 | 桃源县兴隆米业科技开发有限公司 | Method for preparing amino acid skin care essence by using high essential amino acid rice saving |
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